The invention relates to flow rate sensing, microflow sensors, and energy conversion.
Flow sensing has many important applications, including industry, transportation vehicles, and medicine. Flow sensors should ideally have the following desirable characteristics:
Over the years, flow sensor technologies have been developed by both academic researchers and industries. Micro electro mechanical systems (MEMS) flow sensors have been developed based on heat transfer principles, on thermal time of flight principles, and on momentum transfer principles. Some advanced flow sensors have attempted mimic flow sensors found on fish (lateral line) and spiders (leg hairs).
An artificial haircell microsensor (AHC) and a method of fabricating it on an SOI wafer are described by N. Chen et al. in “Design and Characterization of Artificial Haircell Sensor for Flow Sensing With Ultrahigh Velocity and Angular Sensitivity”, Vol. 16, No. 5, October 2007, and comprises a cylindrical, substantially rigid cilium made of SU-8 epoxy located at a distal end of a paddle-shaped silicon cantilever beam. Doped silicon piezoresistive strain gages are located at the base of the cantilever.
Applicant's U.S. Pat. Nos. 7,357,035 and 7,516,671 describe a sensor chip having a flexible polymer-based substrate and one or more micro-fabricated rectangular-cross section haircell sensors disposed vertically on the substrate together with one or more other sensors, such as a temperature sensor, thermal conductivity sensor, and contact force and hardness sensor.
The present invention provides in one embodiment an array of a plurality of passive and/or active sensors each having an artificial cilium on a cantilever wherein the sensors are systematically configured and arranged relative to one another in the array to achieve both large dynamic range and low detection limit. In an illustrative embodiment, a one- or two-dimensional array of haircell sensors is provided wherein one or more sensor parameters systematically change from one sensor to the next in the array to achieve both large dynamic range and low detection limit. The sensor parameters can include the height (h) of the artificial cilium, the diameter (d) of the artificial cilium, the cantilever length (l), the cantilever width (w), the cantilever thickness (t) and/or relative cantilever orientations to this end.
An active flow sensor pursuant to the invention can include a piezoelectric element as an active actuator and/or active energy harvesting element in flow sensing applications. The piezoelectric element can convert electric potential (or field) to mechanical stress and displacement. Conversely, the piezoelectric element can turn mechanical stress and strain into charge accumulation and electric potential. As such, the sensor of this embodiment can perform a number of unique functions, including:
The piezoelectric element can be located on the cantilever or on the artificial cilium, or on any part of the sensor structure as long as favorable electrical-mechanical conversion can be achieved and the fabrication process is feasible.
Furthermore, it is possible to chemically functionalize parts of the sensor, such as the artificial cilium using chemically functional materials such that the sensor's mass will change upon binding with species in the fluid. As a result, the sensor will be made capable of chemical and biological sensing.
Embodiments of the invention can provide a multi-modal flow sensor that comprises one or more flow sensors each with an artificial cilium on a cantilever, one or more pressure sensors, one or more temperature sensors, etc. For example, using the same microfabrication process as used to fabricate the sensor with the cilium on the cantilever, it is possible to fabricate a sensor chip that also contains one or more diaphragm pressure sensors, hot film anemometers, hot wire anemometers, thermal-transfer based flow shear stress sensors, temperature sensors, and time-of-flight flow velocity sensors. These multi-modal sensors present a comprehensive view of the flow field of interest.
Advantages of the present invention will become more apparent from the following detailed description taken with the following drawings.
a through 16h illustrates a microfabrication process for making a passive haircell sensor with a piezoresistive element.
In one illustrative embodiment of the present invention, an array of a plurality of passive and/or active artificial haircell (ACH) sensors is provided wherein the sensors are systematically configured and arranged relative to one another in the array to achieve both large dynamic range and low detection limit. For purposes of illustration,
Such passive haircell sensors, as well as active haircell sensors described below, exhibit a number of important technical and operational advantages:
The passive AHC device shown schematically in
where E is the Young's modulus of silicon, w the cantilever width, and t the cantilever thickness.
When used as a flow sensor, flow passing through the cilium introduces a bending moment (M) due to frictional and pressure drag. The sensitivity analysis is presented in the next section.
The moment exerted on the cilium, M, is estimated using the local drag coefficient approach references [4, 5]. The cilia are cylindrical in shape and are modeled as right cylinders of uniform cross-section and finite length. The flow characteristic in this case is assumed to be nearly two dimensional. Applicant also assumes the case of steady-state flow for the analysis. Further, the direction of the flow is perpendicular to the longitudinal axis of the cilium.
The cylindrical cilium is divided into N segments with unit length Δh. Applicant assumes the linear density of local drag force, FD
where ui is the local flow velocity at the ith segment of the cilium, CD(ui) the local drag coefficient, ρ the fluid density and d the diameter of the cilium.
The procedure for estimating CD is discussed here. The local drag coefficient CD(ui) is dependant on the local Reynolds number. For Re(ui)<10, the magnitude of CD(ui) is determined by logarithmically interpolating the experimental drag coefficient versus Reynolds number data [5], according to
ln CD(ui)≈−0.67 ln Re(ui)+2.51 (3)
Otherwise, the drag coefficient is determined by graphically interpolating the experimental data in reference [6].
The Reynolds number is dependent on the local flow velocity, ui. The local Reynolds number is related to the local flow velocity by
In order to estimate the magnitude of ui, the flow velocity profile along the length of the cilium shank is determined first. In micro scale, the formation of boundary layer has significant effect on the flow velocity profile along the cilium. Depending on the applications, the haircell elements are often entirely immersed in the boundary layer, although occasionally the immersion may be partial. The boundary layer thickness (δ) is calculated based on flow velocity and distance from the leading edge of the aerodynamic structure, on which the AHC sensors are mounted, according to
where ρ is the viscosity, x the distance from the leading edge and U the steady state mean stream inflow velocity.
If a section of the cilium is completely immersed in the boundary layer, the local velocity is determined by the velocity profile along the cilium, reference [6]. If a section lies outside of the boundary layer, the local flow velocity, ui, is taken as the mean stream velocity, U.
Integrating local drag force over the length of the cilium, h, will give us an estimate of moment acting at the base of the cilium. This is done by numerical integration over the N segments of the cilium,
Here, M is also equal to the moment loaded on the distal end of the cantilever.
These equations only serve as an estimate of the moment loading of the cantilever. One source of error in the analysis comes from the drag coefficients. Cylinders of finite length have smaller drag coefficient comparing to cylinders of infinite length, reference [7]. Further, applicant has assumed the simplest case where the cilium is fixed on the substrate in the flow. In fact, the cantilevers may be deflected slightly, causing the effective height of the cilium to change at high flow velocity.
The ACH sensor devices are fabricated on SOI wafers with a 2-μm-thick epitaxial silicon layer on top, 2-μm-thick oxide, and 300-μm-thick handle wafer. SU-8 epoxy is chosen for its ability to form rigid high aspect ratio structures. The piezoresistive strain gauges are achieved by ion implantation. The ion implantation is performed on very lightly doped, <100>-oriented, n-type device layer of the SOI wafer. The wafer is selectively doped to p-type with boron to take advantage of the higher gauge factor of p-type silicon, reference [8]. To optimize the performance of the stain gauge, applicant chooses the ion implantation parameters so that the doping depth is approximately ⅓ of the total beam thickness and the doping concentration is on the order of 1×1020 cm−3, reference [9]. The ion implantation was performed at 60 KeV energy for a dose of 2×1015 cm−2.
The SOI wafer is first oxidized and patterned for ion implantation [
The paddle-like cantilevers are then defined by front side DRIE (see
For pre-exposure bake, the samples are ramped up to 105° C. at 150° C./hr ramp rate and soaked at 105° C. After a total bake time of 13 hours the samples are then ambient cooled to room temperature. The photolithography is done using a Karl Suss contact aligner at 365 nm. A high-wavelength-pass optical filter with cutoff wavelength of 300 nm is used during exposure to eliminate the “T-topping” effect of the SU-8 structures, which has been observed by others as well, reference [10]. The exposure dose is 3000 mJ/cm2. For a light intensity of 10 mW/cm2, the exposure time is 5 min. For post-exposure bake, the samples are again ramped up to 105° C. at 150° C./hr ramp rate and kept at 105° C. for half an hour. The samples are then ramped down to room temperature at a controlled rate of 15° C./hr.
After the post-exposure bake, the wafer is to be diced up using a dicing saw. The wafer is first flip-bonded to the dicing saw adhesive tape with the backside of the SOI wafer facing up. It is then diced up with the dicing depth carefully calibrated so that the SOI wafer is diced through but the SU-8 thick film is still holding up in one piece. No cracking or debonding from the substrate is observed in the SU-8 thick film during dicing. Subsequently, the pre-exposed SU-8 epoxy is developed. The development is performed using designated SU-8 developer with IPA as the end point indicator. Upon the development of SU-8 thick film, the dies (typically 3×5 mm in size in the current run) are mechanically released from each other into individual sensor units by breaking along the diced groves. Developing the SU-8 after the physical dicing is critical to ensure 100% process yield. If the development is done prior to the dicing, the cooling fluid jet may damage the cilia and/or the paddle.
The sensor devices are released in BOE to free the cilium-on-cantilever structures [
The SU-8 properties are very sensitive to processing parameters and ambient environment, reference [11]; hence calibration is needed for different lab settings. Once the processing recipe is established, it is very repeatable and able to achieve high device yield.
Finally, the entire sensor can be chemically treated or encapsulated to prevent electric leakage, or adverse chemical reactions. One possible option is to encapsulate the structure with a conformal coverage of Parylene thin film.
The cilia are made in a monolithically integrated process, eliminating the needs of low-yield and low-efficiency manually assembly. The signal processing electronics also can be integrated with the sensor monolithically wherein the pre-fabricated electronics reside in the epitaxial silicon layer on the SOI wafer.
As mentioned above, practice of the present invention envisions an array of a plurality of passive and/or active artificial sensors wherein the sensors are systematically configured and arranged relative to one another in the array to achieve both large dynamic range and low detection limit. The passive haircell sensors are described in detail above and in references 1, 2, and 3.
The active sensors can be provided pursuant to another embodiment of the invention as an active haircell sensor. In particular, referring to
The piezoelectric element of the active haircell sensor can function as an active actuator and/or active energy harvesting element in flow sensing applications. For example, the piezoelectric element can convert electric potential (or field) to mechanical stress and displacement to oscillate or vibrate in a manner to interact with the fluid environment. Conversely, the piezoelectric element can turn mechanical stress and strain into charge accumulation and electric potential for energy harvesting. As such, the active haircell sensor can perform a number of unique functions, including:
When functioning as an active energy harvesting element, the signal output of the piezoelectric element can be rectified to a DC signal and sent to a storage capacitor of a controller for later use of the stored energy. When functioning as an active actuator to oscillate or vibrate in a fluid environment, the input of the piezoelectric element can be connected to a suitable computer controlled oscillator to provide DC oscillating voltage signals to the piezoelectric element.
In still another embodiment of the invention, the individual haircell sensor for use in the array can include both a active piezoelectric element (14) and a passive position-sensing piezoresistive element (16) as shown in
A one- or two-dimensional array of the passive and/or active haircell sensors typically is provided wherein one or more haircell parameters systematically change from one sensor to the next in the array to achieve both large dynamic range and low detection limit. The haircell parameters of interest can include the height (h) of the artificial cilium, the diameter (d) of the artificial cilium, the cantilever length (l), the cantilever width (w), the cantilever thickness (t) and/or relative cantilever orientations to this end.
Referring to
Practice of a further embodiment of the invention provides a multi-modal flow sensor that comprises one or more the above-described passive and/or active haircell sensors, one or more pressure sensors, one or more temperature sensors, etc. For example, using the same MEMS microfabrication process as used to fabricate the haircell sensor, it is possible to fabricate a sensor chip that also contains one or more diaphragm pressure sensors, hot film anemometers, hot wire anemometers, thermal-transfer based flow shear stress sensors, temperature sensors, and time-of-flight flow velocity sensors.
Referring to
Such multi-modal flow sensor chip as shown in
The invention envisions in the practice of the embodiments described above treatment of haircell sensor in a manner to chemically functionalize parts of the haircell sensor. For purposes of illustration and not limitation, the artificial cilium can be treated with a chemical functional binding material such that a species in the fluid will bind with the chemically functionalized cilium and change the sensor's mass upon such binding. As a result, the sensor will be made capable of chemical and biological sensing.
Although the invention has been described in detail in connection with certain embodiments thereof, those skilled in the art will appreciate that changes and modification can be made therein within the scope of the invention as set forth in the appended claims.
This application claims benefits and priority of U.S. provisional application Ser. No. 61/335,951 filed Jan. 14, 2010, the disclosure of which is incorporated herein by reference.
This invention was made with government support under Grant No.: FA9550-05-1-0459 (UIUC) NU Subcontract: 2005-02899-08 awarded by AFOSR (Air Force Office of Scientific Research). The Government has certain rights in the invention.
| Number | Date | Country | |
|---|---|---|---|
| 61335951 | Jan 2010 | US |