Air management system for the manufacture of nonwoven webs and laminates

Information

  • Patent Grant
  • 6499982
  • Patent Number
    6,499,982
  • Date Filed
    Thursday, December 28, 2000
    23 years ago
  • Date Issued
    Tuesday, December 31, 2002
    21 years ago
Abstract
An air handler for collecting air discharged from a melt spinning apparatus. The air handler includes an outer housing having walls defining a first interior space. One of the walls has an intake opening for receiving the discharge air. Another wall has an exhaust opening for discharging the air. The intake opening is in fluid communication with the first interior space. An inner housing is positioned within the first interior space and has walls defining a second interior space. At least one of the walls of the inner housing has an opening. The first interior space communicates with the second interior space through the opening. The second interior space is in fluid communication with the exhaust opening.
Description




FIELD OF THE INVENTION




The present invention generally relates to apparatus and methods for managing air flow during the manufacture of nonwoven webs and laminates.




BACKGROUND OF THE INVENTION




Meltblowing and spunbond processes are commonly employed to manufacture nonwoven webs and laminates. With meltblowing, a molten thermoplastic is extruded from a die tip to form a row of filaments or fibers. Converging sheets or jets of hot air impinge upon the fibers as they are extruded from the die tip to stretch or draw the fibers, thereby reducing the diameter of the fibers. The fibers are then deposited in a random manner onto a moving collector belt to form a nonwoven web.




With spunbond processes, continuous fibers are extruded through a spinneret. Air is directed at the extruded fibers to separate and orient them. The fibers are collected onto a moving collector belt. At a downstream location, the fibers are consolidated by passing the layer of fibers through compacting roller, for instance. The spunbond process frequently utilizes quenching air to cool the extruded before they contact the collector belt.




Large volumes of air are used during both the meltblown and spunbond process. Moreover, much of the air is heated and moving at very high velocities, sometimes approaching the speed of sound. Without properly collecting and disposing of the process air, the air would likely disturb personnel working around the manufacturing apparatus and other nearby equipment. Further, the heated air would likely heat the surrounding area in which the nonwoven is being produced. Consequently, attention must be paid to collecting and disposing of this process air.




Managing the process air is also important to producing a homogeneous nonwoven web across the width of the web. The homogeniety of the final nonwoven web depends greatly on the air flow around the fibers as they are deposited onto the collector belt. For instance, if the air flow velocity is not uniform in the cross-machine direction, the fibers will not be deposited onto the collector belt uniformly, yielding a non-homogeneous nonwoven web.




Various air management systems have been used to collect and dispose of the process air. One particular air management system uses a collecting duct situated below a perforated collector belt to collect and dispose of the process air. An air moving device, such as a fan or vacuum pump, is connected to the collecting duct to actively draw the air into the collecting duct. The collecting duct is comprised of a plurality of a smaller air passageways arranged side-by-side in a rectangular grid. The grid includes a central row of air passageways extending across the machine width and upstream and downstream air passageways flanking either side of the central row. The central row of air passageways is disposed directly below the extrusion die in what is commonly referred to as the forming zone. Each air passageway includes an inlet and an outlet with a 90 degree elbow in between. An air moving device is operatively connected to each outlet to draw the process air into the individual inlets.




As mentioned above, the air flow velocity of the process air around the collector belt should be uniform, especially in the machine direction at the forming zone, to form a homogeneous nonwoven web. Achieving a uniform air flow velocity, however, has proven challenging. In the collecting duct described above, moveable dampers are associated with each outlet of the air passageways. To achieve uniform air flow velocity with this collecting duct, an technician must manually manipulate each damper until the air flow velocity is sufficiently uniform. In some instances, the technician may be unable to achieve a uniform air flow velocity no matter how much time and effort is spent adjusting the dampers. Moreover, the dampers must be readjusted each time a different fiber material or process air flow rate is used. Thus, the operator must readjust the dampers virtually every time the process is started or an operating condition is changed. The readjustment process takes a great deal of time and may ultimately yield a nonuniform air flow velocity regardless of how the moveable dampers are adjusted.




What is needed, therefore, is an air management system that can collect and dispose of the process air so as to produce a uniform air flow velocity at the collector belt, especially around the forming zone. The air management system should be designed such that dampers and other manual controls are not necessary, even over a wide range of process air flow rates.




SUMMARY OF THE INVENTION




The present invention provides a melt spinning system and, more particularly, a melt spinning and air management system that overcomes the drawbacks and disadvantages of prior air management systems. The air management system of the invention includes at least one air handler for collecting air discharged from a melt spinning apparatus. In accordance with a general objective of the invention, the air handler produces a uniform air flow velocity in at least the cross-machine direction as the air enters the air handler. This is accomplished without the typical adjustable baffles and dampers required in the past. The air handler generally includes an outer housing having walls defining a first interior space. One of the walls has an intake opening for receiving the discharge air from the melt spinning apparatus. Another wall has an exhaust opening for discharging the air collected by the air handler. The intake opening is in fluid communication with the first interior space. An inner housing is positioned within the first interior space and has walls defining a second interior space. At least one of the walls of the inner housing has an opening. The first interior space communicates with the second interior space through the opening. The second interior space is in fluid communication with the exhaust opening.




In one aspect of the invention, the opening between the first interior space and the second interior space is an elongate slot and preferably includes a center portion having a wider dimension than the end portions thereof. The intake opening is positioned at the top of the outer housing, and the slot in the inner housing is disposed proximate to the bottom of the outer housing. The outer housing can further include a filter member for filtering particulates from the air discharged by the melt spinning apparatus.




The invention further provides an air management system including three air handlers. One air handler is positioned directly below the melt spinning apparatus in a forming zone. Another air handler is positioned upstream of the forming zone, and the other air handler is positioned downstream of the forming zone. The widths of the intake opening of the upstream and downstream air handlers in the machine direction are respectively greater than the width of the intake opening of the air handler positioned below the forming zone. The upstream and downstream air handlers collect air which spills over, i.e., not collected, from the air handler below the forming zone.




Various additional advantages and features of the invention will become more readily apparent to those of ordinary skill in the art upon review of the following detailed description taken in conjunction with the accompanying drawings.











DETAILED DESCRIPTION OF DRAWINGS





FIG. 1

is a schematic plan view of a two-station production line incorporating the air management system of the invention;





FIG. 2

is a perspective view of the two-station production line of

FIG. 1

with the collector belt removed for clarity;





FIG. 3

is a perspective view of the air management system of

FIG. 1

;





FIG. 4

is a partially disassembled perspective view of the forming zone air handler of

FIG. 3

;





FIG. 5

is a cross sectional view of the forming zone air handler in

FIG. 4

taken along lines


5





5


;





FIG. 6

is a plan view of the forming zone air handler bottom in

FIG. 4

taken along lines


6





6


;





FIG. 7

is a partially disassembled perspective view of one of the spillover air handlers of

FIG. 3

;





FIG. 8

is a perspective view of another embodiment of the air management system of the invention; and





FIG. 9

is cross sectional perspective view of the air management system in

FIG. 8

taken along lines


9





9


.











DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENT




With reference to

FIG. 1

, a two-station production line


10


is schematically illustrated. The production line


10


incorporates an air management system


12


of the invention at both an upstream station


14


and a downstream station


16


. While the air management system


12


has been illustrated in conjunction with the two-station production line


10


, the air management system


12


is generally applicable to other production lines having a single station or a plurality of stations. In a single station production line, the nonwoven web can be manufactured using any one of a number of process, such as a meltblowing process or a spunbond process.




In a multiple-station production line, a plurality of nonwoven webs can be manufactured to form a multiply laminate. Any combination of meltblowing and spunbonding processes may be used to manufacture the laminate. For instance, the laminate may include only nonwoven meltblown webs or only nonwoven spunbond webs. However, the laminate may include any combination of meltblown webs and spunbond webs.




The two-station production line


10


in

FIG. 1

is shown forming a two-ply laminate


18


with a meltblown layer or web


20


on the bottom and a spunbond layer or web


22


on the top. The two-ply laminate


18


is consolidated downstream using compacting rolls, for example. The upstream station


14


includes a melt spinning assembly


24


with a metblowing die


26


and the downstream station


16


includes a melt spinning assembly


28


with a spunbond die


30


.




To form the meltblown web


20


, the meltblowing die


26


extrudes a plurality of thermoplastic filaments or fibers


32


onto a collector such as a belt


34


. It will be appreciated that the collector


34


may be any other substrate, such as a substrate used as a component in the manufacture of a product. Converging sheets or jets of hot air, indicated by arrows


36


, from the meltblowing die


26


impinge upon the fibers


32


as they are extruded to stretch or draw the fibers


32


. The fibers


32


are then deposited in a random manner onto the collector moving belt


34


from right to left to form the meltblown web


20


. The collector belt


34


is perforated to permit the air to flow through the collector belt


34


and into the air management system


12


.




Similarly, to form the spunbond web


22


, the spunbond die


30


extrudes a plurality of thermoplastic filaments or fibers


38


onto the meltblown web


20


being transported by the moving collector belt


34


. Hot air, indicated by arrows


40


, from the spunbond die


30


impinges upon the fibers


38


to impart rotation to the fibers


38


. Additionally, air ducts


42


direct quenching air onto the extruded fibers


38


to cool the fibers


38


before they reach the meltblown web


20


. As with the upstream station


14


, the air at downstream station


16


passes through the nonwoven web


20


and the collector belt


34


and into the air management system


12


.




Several cubic feet of air per minute per inch of die length flow through each station


14


,


16


during the manufacture of the meltblown and spunbond webs


20


,


22


. The air management system


12


of the invention efficiency collects and disposes of the air from through the stations


14


,


16


. More importantly and as will be discussed in greater detail below, the air management system


12


collects the air such that the air has a substantially uniform flow velocity at least in the cross-machine direction as the air passes through the collector belt


34


. Ideally, the fibers


32


,


38


are deposited on the collector belt


34


in a random fashion to form the meltblown and spunbond webs


20


,


22


which are homogeneous. If the air flow velocity through the collector belt


34


is nonuniform, the resultant web will likely not be homogeneous.




With reference to

FIG. 2

, transport structure


50


of the two-station production line


10


of

FIG. 1

is shown. While the two-station production line


10


includes two air management systems


12


, the following description will focus on the air management system


12


associated with the upstream station


14


. Nevertheless, the description will be equally applicable to the air management system associated with downstream station


16


.




With further reference to

FIGS. 2 and 3

, air management system


12


includes three discrete air handlers


52


,


54


,


56


disposed directly below the collector belt


34


. Air handlers


52


,


54


,


56


include intake openings


58


,


60


,


62


and oppositely disposed exhaust openings


64


,


66


,


68


. Individual exhaust conduits


70


,


72


,


74


are connected respectively to exhaust openings


64


,


66


,


68


. Exhaust conduit


70


, which is representative of exhaust conduits


72


,


74


, is comprised of a series of individual components: first elbows


76


, second elbows


78


, elongated portion


80


, down portion


82


, and third elbow


84


. A series of parallel guide vanes


86


extend through down portion


82


and third elbow


84


. In operation, a variable speed fan (not shown) or any other suitable air moving device is connected to third elbow


84


to draw the air through the air management system


12


.




With continued reference to

FIGS. 2 and 3

, air handler


54


is located directly below the forming zone, i.e., the location where the fibers contact the collector belt


34


. As such, air handler


54


collects and disposes of the largest portion of air used during the extrusion process. Upstream air handler


56


and downstream air handler


52


collect spill over air which air handle


54


does not collect.




With reference now to

FIGS. 4-6

, forming zone air handler


54


includes an outer housing


94


which includes intake opening


60


and oppositely disposed exhaust openings


66


. Intake opening


60


includes a perforated cover


96


with a series of apertures through which the air flows. Depending of the manufacturing parameters, air handler


54


may be operated without using the perforated cover


96


at all. Air handler


54


further includes an inner housing or box


98


which is suspended from the outer housing


94


by means of spacing members


100


which include a plurality of openings


101


therein. Two filter members


102


,


104


are selectively removable from air handler


54


so that they may be periodically cleaned. The filter members


102


,


104


slide along stationary rail members


106


,


108


. Each of these filter members


102


,


104


are perforated with a series of apertures through which the air flows.




The inner box


98


has a bottom panel


110


that includes an opening such as slot


112


with ends


114


,


116


and a center portion


118


. As illustrated in

FIG. 6

, slot


112


extends substantially across the width, i.e., the cross-machine direction, of the inner box


98


. The slot


112


is narrow at ends


114


,


116


and widens at center portion


118


. The slot


112


could be formed from one or more openings of various shapes, such as round, elongate, rectangular, etc.




The shape of slot


112


influences the air flow velocity in the cross machine direction at the intake opening


60


. If the shape of the slot


112


is not properly contoured the air flow velocities at the intake opening


60


may vary greatly in the cross machine direction. The particular shape shown in

FIG. 6

was determined through an iterative process using a computational fluid dynamics (CFD) model which incorporated the geometry of the air handler


54


. A series of slot shapes were evaluated at intake air flow velocities ranging between 500 to 2500 feet per minute. After the CFD model analyzed a particular slot shape, the air flow velocity profile in the cross machine direction was checked. Ultimately, the goal was to choose a shape for the slot


112


which provided a substantially uniform air flow velocity in the cross machine direction at intake opening


60


. Initially, a rectangular slot


112


was evaluated, yielding air flow velocities in the cross machine direction at the intake opening


60


which varied by as much as twenty percent. With the rectangular slot


112


, the air flow velocities near the ends of the intake opening


60


were greater than the air flow velocities approaching the center of the intake opening


60


. To address this uneven air flow velocity profile, the width of ends


114


,


116


was reduced relative to the width of the center portion


118


. After approximately five iterations, the shape of slot


118


is

FIG. 6

was chosen. That slot shape yields air flow velocities in the cross machine direction at the intake opening


60


which varied by ±5.0%.




With specific reference to

FIG. 5

, air enters through perforated cover


96


and passes through perforated filter members


102


,


104


as illustrated by arrows


120


. The air passes through the gap between the inner box


98


and the outer housing


94


as illustrated by arrows


122


. The air then enters the interior of inner box


98


through slot


112


as illustrated by arrows


124


. Finally, the air exits the inner box


98


through exhaust opening


66


as illustrated by arrows


126


and then travels through exhaust conduit


72


. The openings


101


in spacing members


100


allow the air to move in the cross-machine direction to minimize transverse pressure gradients.




Generally, air handlers


52


,


56


have a similar construction and air flow path as air handler


54


. However, as

FIG. 3

illustrates, air handlers


52


,


56


have much wider, i.e, in the machine direction, intake openings


58


,


62


than intake opening


60


of air handler


54


. The width of the these intake openings


58


,


62


may vary depending on the particular manufacturing parameters. The following discussion of air handler


52


is equally applicable to air handler


56


. Thus, with specific reference to

FIG. 7

, air handler


52


includes an outer housing


136


which includes intake opening


58


and exhaust openings


64


. Intake opening


58


includes a perforated cover


137


with a series of apertures through which the air flows. Depending on the manufacturing parameters, air handler


52


may be operated without using perforated cover


137


at all. Air handler


52


further includes an inner housing or box


138


which is suspended from the outer housing


136


by means of spacing members


140


which include a plurality of openings


142


therein. Unlike air handler


54


, air handlers


52


,


56


do not include filter members


102


,


104


.




The inner box


138


includes a bottom panel


144


with a slot


146


which is configured similarly to slot


112


. Slot


146


includes ends


148


,


150


and center portion


152


. Like slot


112


, the width at center portion


152


is greater than the width at ends


148


,


150


.




As mentioned above, the air flow path through air handler


52


is similar to the air flow path in air handler


54


. Specifically, air enters through perforated cover


137


as illustrated by arrows


154


and passes through the gap between the inner box


138


and the outer housing


136


as illustrated by arrows


156


. The air then enters the interior of inner box


138


through slot


146


as illustrated by arrow


158


. Finally, the air exits the inner box


138


through exhaust opening


64


as illustrated by arrow


160


and then travels through exhaust conduit


70


. The openings


142


in spacing members


140


allow the air to move in the cross-machine direction to minimize transverse pressure gradients.




Another embodiment of the air management system of the invention is shown generally as


170


in

FIGS. 8 and 9

. As described above, air management system


12


includes three separate and discrete air handlers


52


,


54


,


56


. In contrast, air management system


170


includes air handlers


172


,


174


,


176


which share common walls to form a unitary device. Air handler


174


is placed under the forming zone of the production line to collect the majority of the process air and air handlers


172


,


176


collect spill over air which air handler


174


does not collect. Each air handler


172


,


174


,


176


includes an intake opening


178


,


180


,


182


over which a single perforated cover


184


is placed. A plurality of individual perforated covers may be used in place of the single perforated cover


184


. Each air handler


172


,


174


,


176


further includes exhaust openings


186


,


188


,


190


oppositely disposed on either end of the respective air handlers


172


,


174


,


176


. Separate exhaust conduits (not shown) similar to exhaust conduits


70


,


72


,


74


connect to exhaust openings


186


,


188


,


190


to pull the air out of the air handlers


172


,


174


,


176


. Air handler


174


may include a filter member having a perforated surface through which the incoming air flows.




Air handlers


172


,


174


,


176


include inner boxes


192


,


194


,


196


and sidewalks


198


,


200


,


202


,


204


. Spacing members


206


,


208


,


210


hold inner boxes


192


,


194


,


196


away from sidewalks


198


,


200


,


202


,


204


. Inner boxes


192


,


194


,


196


include bottom panels


212


,


214


,


216


having slots


218


,


220


,


222


. The airflow path through air handlers


172


,


174


,


176


is similar to the air flow path in air handlers


52


,


54


,


56


. The air flow path through air handler


174


is represented by arrows


224


.




While the present invention has been illustrated by a description of various preferred embodiments and while these embodiments have been described in considerable detail in order to describe the best mode of practicing the invention, it is not the intention of applicants to restrict or in any way limit the scope of the appended claims to such detail. Additional advantages and modifications within the spirit and scope of the invention will readily appear to those skilled in the art. The invention itself should only be defined by the appended claims, wherein we claim:



Claims
  • 1. An air handler for positioning below a melt spinning apparatus configured to discharge filaments of material onto a collector moving in a machine direction and collecting air discharged from the melt spinning apparatus, said air handler comprising:an outer housing having walls defining a first interior space, one of said walls having an intake opening for receiving the discharged air and an exhaust opening for discharging the air, said intake opening in fluid communication with said first interior space; and an inner housing positioned within said first interior space and having walls defining a second interior space, at least one of said walls of said inner housing having an elongate intake having a length extending in a cross-machine direction, said first interior space communicating with said second interior space through said elongate intake, said second interior space in fluid communication with said exhaust opening.
  • 2. The air handler of claim 1, wherein said elongate intake is a slot.
  • 3. The air handler of claim 2, wherein said slot includes a center portion with a first width and oppositely disposed end portions each with a second width, said first width being greater than said second width.
  • 4. The air handler of claim 1, wherein said outer housing includes a top and a bottom, one of said walls of said outer housing being a top wall and including said intake opening, one of said walls of said outer housing being a bottom wall and said elongate intake of said inner housing positioned proximate to said bottom wall of said outer housing.
  • 5. The air handler of claim 1, wherein said outer housing further includes a filter member for filtering particulates from the air discharged from the melt spinning apparatus.
  • 6. An air handler positioning below a melt spinning apparatus configured to discharge filaments of material onto a collector moving in a machine direction and collecting air discharged from the melt spinning apparatus, said air handler comprising:an outer housing having walls defining a first interior space, one of said walls forming the top of said outer housing and including an intake opening for receiving the discharged air, one of said walls forming a side of said outer housing and including an exhaust opening, one of said walls forming the bottom of said outer housing, said intake opening being in fluid communication with said first interior space; an inner housing positioned within said first interior space and having walls defining a second interior space, one of said walls of said inner housing forming the bottom of the inner housing and including an intake slot, said bottom wall being proximate to the bottom of the outer housing, said first interior space communicating with said second interior space through said intake slot, said second interior space in fluid communication with said exhaust opening.
  • 7. The air handler of claim 6, wherein said intake slot is elongate and has a length extending in a cross-machine direction of the melt spinning apparatus.
  • 8. The air handler of claim 7, wherein said elongate intake slot includes a center portion with a first width and oppositely disposed end portions each with a second width, said first width being greater than said second width.
  • 9. The air handler of claim 6, wherein said outer housing further including a filter member for filtering particulates from the air discharged by the melt spinning apparatus.
  • 10. An air handler for positioning below a melt spinning apparatus configured to discharge filaments of material onto a collector moving in a machine direction and collecting air discharged from the melt spinning apparatus, said air handler comprising:an outer housing having first and second side walls, first and second end walls, a bottom wall and a top cover, said walls and said top cover defining a first interior space, said top cover having an intake opening for receiving the discharged air, said intake opening being in fluid communication with said first interior space; an inner housing positioned within said first interior space and having first and second side walls and top and bottom walls, said walls defining a second interior space having a rectangular cross section, said walls having first and second ends abutting said first and second end walls of said outer housing and conforming to said exhaust openings therein, said bottom wall of said inner housing being proximate to the bottom of the outer housing and including an intake slot aligned along the longitudinal axis of the inner housing, said intake slot having a center portion with a first width and oppositely disposed end portions each with a second width, said first width being greater than said second width, said first interior space communicating with said second interior space through said intake slot, said second interior space in fluid communication with said exhaust openings.
  • 11. The air handier of claim 10, wherein said outer housing further including a filter member for filtering particulates from the air discharged by the melt spinning apparatus.
  • 12. An air management system for collecting air discharged from a melt spinning apparatus configured to discharge filaments of material onto a collector moving in a machine direction, the air management system includes first, second, and third air handlers, the second air handler positioned directly below the melt spinning apparatus in a forming zone, the first air handler being positioned upstream of the second air handler and the forming zone, the third air handler being positioned downstream of the second air handler and the forming zone, each air handler comprising:an outer housing having walls defining a first interior space, one of said walls having an intake opening for receiving the air and an exhaust opening for discharging the air, said intake opening in fluid communication with said first interior space; and an inner housing positioned within said first interior space and having walls defining a second interior space, at least one of said walls of said inner housing having an elongate intake, said first interior space communicating with said second interior space through said elongate intake, said second interior space in fluid communication with said exhaust opening.
  • 13. The air management system of claim 12, wherein said elongate intake is an elongate slot having a length extending in a cross-machine direction of the melt spinning apparatus.
  • 14. The air management system of claim 13, wherein said elongate slot includes a center portion with a first width and oppositely disposed end portions each with a second width, said first width being greater than said second width.
  • 15. The air management system of claim 12, wherein each outer housing includes a top and a bottom, one of said walls of each outer housing being a top wall and including said intake opening, one of said walls of each outer housing being a bottom wall and each elongate intake of each inner housing positioned proximate to said bottom wall of each outer housing.
  • 16. The air management system of claim 12, wherein each outer housing further includes a filter member for filtering particulates from the air discharged by the melt spinning apparatus.
  • 17. The air management system of claim 12, wherein said intake opening of said first and third air handlers has a width in said machine direction, said intake opening of said second air handler has a width in said machine direction, said width of said intake opening of said first and third air handlers being greater than the width of said intake opening of said second air handler.
  • 18. The air management system of claim 12, wherein each air handler is separate and distinct from the other air handlers.
  • 19. A system for manufacturing nonwoven webs comprising:a melt spinning apparatus adapted to discharge filaments of material, said melt spinning apparatus including at least one discharge orifice, said discharge orifice adapted to discharge a stream of pressurized air onto the filaments; a collector belt positioned below said melt spinning apparatus for receiving the filaments and moving in a machine direction; and an air handler positioned below said collector belt and including an outer housing having walls defining a first interior space, one of said walls having an intake opening for receiving the discharge air and an exhaust opening for discharging the air, said intake opening in fluid communication with said first interior space; and an inner housing positioned within said first interior space and having walls defining a second interior space, at least one of said walls of said inner housing having an elongate intake, said first interior space communicating with said second interior space through said elongate intake, said second interior space in fluid communication with said exhaust opening.
  • 20. The system of claim 19, wherein said elongate intake is an elongate slot having a length extending in a cross-machine direction of the melt spinning apparatus.
  • 21. The system of claim 20, wherein said elongate slot includes a center portion with a first width and oppositely disposed end portions each with a second width, said first width being greater than said second width.
  • 22. The system of claim 19, wherein said outer housing includes a top and a bottom, one of said walls of said outer housing being a top wall and including said intake opening, one of said walls of said outer housing being a bottom wall and said elongate intake opening of said inner housing positioned proximate to said bottom wall of said outer housing.
  • 23. The system of claim 19, wherein said outer housing further including a filter member for filtering particulates from the air discharged from the melt spinning apparatus.
US Referenced Citations (5)
Number Name Date Kind
2933152 Carpenter et al. Apr 1960 A
3748693 Jespersen Jul 1973 A
4432714 Forry et al. Feb 1984 A
4526733 Lau Jul 1985 A
5984990 McDonald Nov 1999 A