1. Technical Field
This disclosure relates to an airflow classifier to perform a classification operation on a particulate material, and to a particulate material preparing apparatus to prepare a particulate material having a desired particle size using the airflow classifier.
2. Discussion of the Related Art
There are particulate material preparing apparatuses including a pulverization and coarse particle classification device and a fine particle classification device. Conventional pulverization and coarse particle classification devices typically include two sets of one pulverizer and one classifier connected with the pulverizer, or a combination of one pulverizer and two classifiers. Specific examples of the pulverizer include jet mills in which a particulate raw material is fed into jet airflow spouted from a jet nozzle so that particles of the raw material collide against each other or a collision material (such as collision plates and walls), resulting in pulverization of the raw material; and mechanical pulverizers in which a particulate raw material is fed to a gap between a rotor having convexes and concaves on the surface thereof and a stator also having convexes and concaves so that the raw material is collided against the rotor and stator by swirling airflow caused by the rotor and stator. After the raw material is pulverized by one or two of such pulverizers, the pulverized material is classified with a combination of two coarse particle classifiers. The particulate material from which coarse particles are removed (i.e., relatively fine particles) are then subjected to fine particle classification using a fine particle classification device in which two classifiers are typically connected.
As illustrated on the left side of
In the coarse particle classification process, the particulate material fed to the classifier 85 is the pulverized raw material (i.e., the particulate material in the process of pulverization), and therefore the particulate material circulating in the circuit has a broad particle diameter distribution. When a product (particulate materials such as toner) having a desired particle diameter distribution is obtained from the particulate material, the yield of the product is very low, and the apparatus has to be operated with a heavy load because the amount of the particulate material returned to the pulverizer is large.
The fine particles collected by the cyclone 87 are subjected to a fine particle classification process. Specifically, the fine particles are then fed to a fine particle classifier 88 to be further classified, and particles having particle diameters in a desired particle diameter range are collected as a product in a product container 89.
The fine particles thus obtained in the fine particle classification process are collected by a cyclone 91 through a passage 90, and then fed to a fine particle classifier 94 through a passage 92 to be further classified. In this case, the relatively large particles are returned to the classifier 88 through a passage 93 while relatively fine particles are fed to a cyclone 96 through a passage 95 to be collected, and the collected fine particles are then fed to a container 97. A one-step or two-step classifier can be used for each of the fine particle classifiers 88 and 94 with consideration of the processing ability thereof.
In this system, a mixture of particles of the raw material and particles in process of pulverization, whose particle diameters fall in a wide particle diameter range, is circulated between a pulverizer and a classifier, and therefore the mixture has a very broad particle diameter distribution. Therefore, in order to prepare a product having a particle diameter in a desired particle diameter range, the system has to be operated with a heavy load. Accordingly, the resultant product tends to include a large amount of undesired coarse particles deteriorating image qualities. Meanwhile, relatively coarse particles returned to the pulverizer to be pulverized again include a large amount of relatively fine particles, which need not be further pulverized. Since such relatively fine particles are also pulverized by the pulverizer, the amount of finer particles included in the resultant pulverized particles increases, and in addition a problem in that the finer particles aggregate is also caused. Therefore, when the thus pulverized particles are classified in the following classification process to obtain a product, the yield of the product is low.
Since a toner prepared by such a conventional particulate material preparing apparatus includes large amounts of coarse particles and fine particles, the particles of the toner have a wide range of charge quantities, resulting in variation of the image density of images produced by the toner. In addition, excessively pulverized toner particles cause a background development problem in that the background area of an image is soiled with the toner particles, and coarse toner particles, which are not sufficiently pulverized, cause an insufficient transfer problem in that the toner particles are not transferred to an image area of an image bearing member, resulting in formation of an image having omissions. In addition, since a heavy load is applied on the classifiers of the particulate material preparing apparatus as mentioned above, the apparatus has low classification efficiency while having low pulverization energy efficiency in the pulverization process.
Recent image forming apparatuses typically form digital images using toner and are required to produce high quality images. Therefore, toner used for such image forming apparatuses is also required to have a sharp particle diameter distribution while minimizing the amounts of coarse and fine particles. Since conventional pulverizers consume much energy for a fine pulverization process, the pulverizers are not economically preferable for producing such toner. In addition, since jet air pulverizers produce toner including coarse particles in a relatively large amount of from 1% to 15% by weight, it is necessary to remove such coarse particles, resulting in deterioration of production efficiency. Alternatively, it is necessary to further perform a pulverization operation. In this case, the energy consumption is increased. Further, since the above-mentioned conventional pulverization/classification apparatuses have insufficient pulverization properties such as pulverization processing ability and energy consumption, the toner produced by the apparatuses has broad particle diameter distribution and broad charge quantity distribution, and therefore it is difficult for the toner to produce high quality images.
In attempting to efficiently produce a particulate material having a sharp particle diameter distribution while minimizing the amount of fine particles and coarse particles, airflow classifiers including a dispersing chamber and a classification chamber have been proposed. However, it is necessary for such airflow classifiers to improve the coarse particle classification accuracy.
Because of these reasons, the inventor recognized that there is a need for a particulate material preparing apparatus which can produce a particulate material having a desired particle diameter distribution (such as volume average particle diameter of not greater than 5 μm) while minimizing the amount of fine particles and coarse particles.
As an aspect of this disclosure, an airflow classifier is provided which includes a dispersing chamber to disperse a powdery raw material with high pressure air; a classifying chamber which is located below the dispersing chamber and which includes a center core and a separator core having an opening at a center thereof on upper and lower sides of the classifying chamber, respectively, to subject the powdery raw material, which is fed from the dispersing chamber, to centrifugal classification to separate the powdery raw material into relatively coarse particles and relatively fine particles; a fine particle feeding pipe connected with a lower portion of the opening of the separator core to feed the fine particles; a shield ring covering an upper portion of the opening of the separator core to prevent the coarse particles from entering into the opening; and a louver pipe which is located above the shield ring and in which plural blades are circularly arranged on an edge of the opening of the separator core at predetermined intervals to prevent the coarse particles from entering into the opening.
As another aspect of this disclosure, a particulate material preparing apparatus is provided which includes a pulverization and coarse particle classification device including at least one pulverizer selected from the group consisting of mechanical pulverizers and airflow pulverizers to pulverize a raw material; and at least one classifier, which is the airflow classifier mentioned above and which is connected with the pulverizer to classify the pulverized raw material into relatively coarse particles and relatively fine particles. The particulate material preparing apparatus can further include a fine particle classification device to classify the relatively fine particles into relatively coarse particles and relatively fine particles.
The aforementioned and other aspects, features and advantages will become apparent upon consideration of the following description of the preferred embodiments taken in conjunction with the accompanying drawings.
The airflow classifier of this disclosure will be described by reference to drawings.
a) is a schematic cross-sectional view illustrating an example of the airflow classifier of this disclosure, and
Referring to
In the dispersing chamber 1, a louver ring 1Q having plural blades 1q circularly arranged at regular intervals, a space 1b, which is located along the peripheral surface of the louver ring 1Q and which serves as a flow path, along which the high pressure air and the powdery material fed from the feed opening 1a are fed, are provided as illustrated in
By providing the louver ring 1Q in the dispersing chamber 1, the mixture of high pressure air and the powdery material (i.e., powder fluid) fed from the feed opening 1a circulates around the entire peripheral surface of the louver ring 1Q while passing through the space 1b, and is fed into an inner portion 1c of the dispersing chamber 1 through spaces formed between the blades 1q. Thus, the powder fluid is uniformly fed into the inside of the louver ring 1Q (i.e., the inner portion 1c of the dispersing chamber 1), and thereby dispersing of the powdery material in the dispersing chamber 1 can be further improved.
The center core 5 has a fine particle exit 5a at the center thereof, and a second fine particle feeding pipe 5b extending from the fine particle exit 5a to the opening 7 of the separator core 8. Therefore, the powdery material fed into the inside of the dispersing chamber 1 through the louver ring 1Q forms swirling flow in the dispersing chamber 1 while being accelerated by suction of the second fine particle feeding pipe 5b, resulting in improvement of the dispersibility of the powdery material. At the same time, the finely pulverized material included in the powdery material are fed as fine particles through the fine particle exit 5a, the fine particle feeding pipe 5b, the opening 7 of the separator core 8, and a first fine particle feeding pipe 13 connected with the lower side of the opening 7.
A pinnate secondary air entrance 9 (i.e., a classification louver), through which air is fed to form secondary airflow (semi-free vortex flow), is provided on the peripheral wall of the classification chamber 2 to disperse the powdery material in the classification chamber while accelerating the powdery material. Therefore, fine particles in the classification chamber 2 are guided to the opening 7 of the separator core 8 by the airflow, and fed through the first fine particle feeding pipe 13 by suction of a blower. In addition, when coarse particles (having a particle diameter of not less than about 8 μm) are swirled on the separator core 8, the coarse particles are fed to a circular coarse particle exit 6, which is located between the separator core 8 and the secondary air entrance 9 and which is located around the lower edge of the separator core 8, by the centrifugal force of the airflow, and the coarse particles passing the circular coarse particle exit 6 then fall into the lower hopper 3 by gravity. The coarse particles in the hopper 3 are returned to the supply tube 81 through the pipe 83.
As illustrated in
In addition, a shield ring 2FR is provided on the upper end of the opening 7 to block or bounce coarse particles moving up to the shield ring along the upper surface of the separator core 8 so that the coarse particles are not fed into the opening 7. The shield ring 2FR is made of an electroconductive material, and is fixed to the separator core 8 similarly to the louver pipe 2F.
As illustrated in
In this regard, the following relationship is preferably satisfied:
H/5≦T≦3H/5,
wherein T represents the height of the shield ring 2FR, and H represents the height of the louver pipe 2F.
As illustrated in
In this regard, the flange 2FRa preferably has a width D of from R/20 to 5R/20, wherein R represents the diameter of the shield ring 2FR as illustrated in
Referring back to
As illustrated in
Next, the particulate material preparing apparatus of this disclosure will be described.
The particulate material preparing apparatus has a configuration similar to that illustrated in
Since the functions of the airflow classifiers BZ1 and BZ2 are the same as each other and the functions of the pulverizers FZ1 and FZ2 illustrated in
Referring to
Thus, the fine particles obtained by the classification operation of the first classifier BZ1 is further classified by the second classifier BZ2, and therefore the resultant fine particles have a sharp particle diameter distribution. In addition, by serially connecting two or more combinations of a classifier and a pulverizer, a product having a relatively small average particle diameter can be produced with minimal change of the device and/or the production capacity can be increased.
In this system, the powdery material fed to the classifier includes not only the raw material but also the pulverized material, namely, particles having a variety of particle diameters are circulated in a closed circuit including the pulverizer and the classifier.
The pulverizer used for the pulverization and coarse particle classification device is a mechanical or airflow pulverizer. Specific examples of the pulverizer include jet air pulverizers in which high pressure air emitted from a jet nozzle catches a raw material therein so that the particles of the raw material strike each other or a collision wall, plate or the like, resulting in pulverization of the raw material. Specific examples of the commercial pulverizers include I type mill from Nippon Pneumatic Mfg. Co., Ltd.
Having generally described this invention, further understanding can be obtained by reference to certain specific examples which are provided herein for the purpose of illustration only and are not intended to be limiting. In the descriptions in the following examples, the numbers represent weight ratios in parts, unless otherwise specified.
The following toner components were mixed.
The mixture was subjected to melt kneading using a roll mill, and then cooled to solidify the kneaded toner component mixture. The kneaded toner component mixture was then crushed by a hammer mill. The crushed toner component mixture was then pulverized and classified by a particulate material preparing apparatus using the pulverization and coarse particle classification device illustrated in
In this regard, the specifications of the pulverization and coarse particle classification device used are as follows.
(1) First and second classifiers BZ1 and BZ2: The airflow classifier illustrated in
(2) Height T of shield ring 2FR: 0.8H/5 (mm) (H represents the height (mm) of the louver pipe 2F)
(3) Inner diameter A of air discharging pipe 15: B/3 (B represents the inner diameter (mm) of the fine particle exit 5a)
(4) Length UL of portion of air discharging pipe 15 within dispersing chamber 1: 3.5DL/5 (DL represents the height (mm) of the dispersing chamber 1)
As a result of analysis of the particle diameter properties of the toner using a particle analyzer MULTISIZER from Beckman Coulter Inc., it was confirmed that the toner of Example 1 has a weight average particle diameter of 5.0 μm, and includes fine particles having a particle diameter of not greater than 4 μm in an amount of 90% by quantity while including coarse particles having a particle diameter of not less than 8 μm in an amount of 1.5% by volume. The yield of the toner was 97%.
The procedure for preparation and evaluation of the toner in Example 1 was repeated except that the shield ring 2FR was not used.
As a result, it was confirmed that the toner of Comparative Example 1 has a weight average particle diameter of 5.1 μm, and includes fine particles having a particle diameter of not greater than 4 μm in an amount of 92% by quantity while including coarse particles having a particle diameter of not less than 8 μm in an amount of 2.5% by volume. The yield of the toner was 80%.
The procedure for preparation and evaluation of the toner in Example 1 was repeated except that the height (T) of the shield ring 2FR was changed to 2H/5.
As a result, it was confirmed that the toner of Example 2 has a weight average particle diameter of 5.0 μm, and includes fine particles having a particle diameter of not greater than 4 μm in an amount of 90% by quantity while including coarse particles having a particle diameter of not less than 8 μm in an amount of 1.0% by volume. The yield of the toner was 97%.
The procedure for preparation and evaluation of the toner in Example 2 was repeated except that the shield ring was replaced with the shield ring 2FR illustrated in
As a result, it was confirmed that the toner of Example 3 has a weight average particle diameter of 4.9 μm, and includes fine particles having a particle diameter of not greater than 4 μm in an amount of 88% by quantity while including coarse particles having a particle diameter of not less than 8 μm in an amount of 0.9% by volume. The yield of the toner was 97%.
The procedure for preparation and evaluation of the toner in Example 3 was repeated except that the width D of the flange 2FRa was changed to 3R/20 (R represents the diameter of the shield ring).
As a result, it was confirmed that the toner of Example 4 has a weight average particle diameter of 4.9 μm, and includes fine particles having a particle diameter of not greater than 4 μm in an amount of 85% by quantity while including coarse particles having a particle diameter of not less than 8 μm in an amount of 0.8% by volume. The yield of the toner was 98%.
The procedure for preparation and evaluation of the toner in Example 4 was repeated except that the inner diameter A of the air discharging pipe 15 was changed to 3B/2.
As a result, it was confirmed that the toner of Example 5 has a weight average particle diameter of 4.8 μm, and includes fine particles having a particle diameter of not greater than 4 μm in an amount of 85% by quantity while including coarse particles having a particle diameter of not less than 8 μm in an amount of 0.6% by volume. The yield of the toner was 98%.
The procedure for preparation and evaluation of the toner in Example 5 was repeated except that the length UL of the air discharging pipe 15 in the dispersing chamber 1 was changed to 2DL/5.
As a result, it was confirmed that the toner of Example 6 has a weight average particle diameter of 4.8 μm, and includes fine particles having a particle diameter of not greater than 4 μm in an amount of 85% by quantity while including coarse particles having a particle diameter of not less than 8 μm in an amount of 0.4% by volume. The yield of the toner was 98%.
In addition, it was confirmed that each of the toners prepared in Examples 1-6 has a sharp particle diameter distribution and a good charge quantity stability, and images formed by using these toners have good image qualities without defective images such as background development and omissions caused by defective image transferring.
As mentioned above, the airflow classifier of this disclosure has a shield ring and a louver pipe, and therefore inclusion of excessively coarse particles in the product can be prevented. Therefore, the airflow classifier has better classification accuracy than conventional classifiers.
In addition, since the particulate material preparing apparatus of this disclosure is equipped with the airflow classifier, a particulate material consisting essentially of fine particles having a sharp particle diameter distribution can be prepared. Since coarse particles obtained in a classification process are pulverized again by a pulverizer to be used for the product, material saving and energy saving can be made. The particulate material preparing apparatus of this disclosure is preferably used for preparing toner.
Additional modifications and variations of the present invention are possible in light of the above teachings. It is therefore to be understood that within the scope of the appended claims the invention may be practiced other than as specifically described herein.
This document claims priority and contains subject matter related to Japanese Patent Application No. 2010-101934, filed on Apr. 27, 2010, the entire contents of which are herein incorporated by reference.
Number | Date | Country | Kind |
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2010-101934 | Apr 2010 | JP | national |