Embodiments disclosed herein relate to the field of processes for recovering bitumen from oil sand and, more particularly, to a fluidized froth holding tank for improved froth handling.
Oil sands extracted from deposits, such as those found in Alberta, Canada, comprise water-wet sands that are held together by a matrix of viscous heavy oil or “bitumen”. Bitumen recovery processes can involve extracting the oil sands from mines, slurry conditioning the oil sands, such as with hot water, for transport to extraction and froth treatment. The bitumen, water, sand, silt and clay matrix is transported for further processing via a primary separation process and downstream froth treatment processes such as froth separation units (FSUs). FSU's, are commonly used in which bitumen-rich froth and solvent are fed to the FSU, whereby mineral and non-mineral solids separate (via gravity) from the solvent diluted bitumen. Solvent is later recovered in various solvent recovery processes.
Such processes are subject to the vagaries of large scale materials processing resulting in the occasional need for surge between the various stages. In one instance, it is known to provide surge capacity between the primary separation and froth treatment stages using an intermediate froth storage or holding tank. The tank receives bitumen froth and ultimately discharges the entire contents for transport to the FSU or other downstream processing, however, during continuous or surge operation, free solids can settle to the bottom. The tank has a discharge located at the bottom and solids tend build up as a sloped bed on the bottom forming a semi-stable bed surface at an angle of repose angled from a low point, at the tank discharge, to one or more high points spaced from the tank discharge.
Main issues arising with solids build up include: accumulation reduces tank holding capacity with dead volume lost to solids and commensurate loss of operating capacity, accumulation at a high side of the bed places inordinate loading on the tank side walls, and periodic sloughing of solids from the bed surface can overwhelm and block the discharge (e.g. outflow/pump suction line), which is typically mitigated by maintaining a liquid level above the solids build up and this itself contributes to additional operating capacity loss.
Prior solutions include an acceptance of lost storage volume by designing larger tanks and with the use of reinforced construction to resist the increased pressure on tank walls from the dead load including reinforced floor and foundation.
Build up and sloughing issues have been addressed using tanks having conical-shaped bottoms to both urge solids to the discharge with minimal to no accumulation and to keep the solids flowing to avoid periodic sloughing. The lower conical walls of such tanks are typically angled to avoid solids build up. Further, mechanical aids such as rotating rakes can be used to guide solids towards the discharge, however the costs of operating and maintaining rakes capable of guiding highly viscous media is extremely high. Conical vessels significantly add to the height, supporting structure and capital cost.
There is interest in providing an improved, generally flat bottomed froth holding tank for storing bitumen froth that is reliable, low cost and maintains the capacity to effectively store froth over extended periods of time.
In accordance with the present description, apparatus and methodology for settling solids management in a froth surge or holding tank is provided. Generally, a flat bottomed tank is provided with arrays of fluidization nozzles for maintaining one of or a combination of characteristics including maintaining any solids in a stable, generally fluidized state for eventual discharge. Where solids do settle, if any, a series of low elevation, conical-sloped beds or sub-beds are formed, thereby minimizing the height of solids accumulation against the tank side walls. Settled solids are discouraged from settling adjacent side walls, or in some embodiments even to substantially eliminate the settling of solids at all, thereby resulting in the ability to store froth for longer periods of time (e.g. for a minimum of four hours, and upwards of approximately fifteen to twenty hours).
It is understood herein that the term solids includes that which settles in a typical tank environment, including mineral, or combinations of mineral, bitumen and trapped water as is known in the oilsands of northern Alberta, Canada. Oilsands are also referred to in the art as oil-sands, oil sands and tar sands and tarsands.
In embodiments described herein, froth holding tanks have a chamber formed within a vessel having a substantially flat bottom wall and cylindrical side walls. The bottom wall can be slightly sloped to a discharge outlet that can aid in maintenance, including cleaning, but does not significantly impact structural height and related considerations. Slight sloping of the bottom wall can include a minimal slope below a normal angle of repose of settled solids without embodiments described herein would suffer the same accumulation disadvantages as flat bottom tanks.
Froth is delivered to the tank through at least one froth feed inlet or nozzle located at or near the bottom wall and directed generally upwardly into the chamber for suspending solids thereabove in a fluidized state within the chamber. Froth is removed from the tank through at least one outlet located at or near the bottom wall. In embodiments, around each feed inlet is formed a sub-bed in the form of an inverted cone or a funnel. A plurality of feed inlets produces a plurality of sub-beds, each of which has a low height and when arranged as set forth herein, obviates side wall loading and sloughing risk. Simplistically, a bed of settled solids that would normally build up at side walls to a maximum bed height that exceeds design criteria is interrupted by a feed nozzle for fluidizing the solids settling thereat and forming a sub-bed. The sub-bed resets the build-up of settled solids to a new bed height about the periphery of the funnel. A sub-bed that is sufficiently spaced from a side wall could also build up to a maximum bed height that exceeds design criteria. Accordingly, froth is introduced at spaced locations between the outlet and the side walls as necessary to form a series of sub-beds as necessary to maintain the maximum bed height at an elevation equal to or below a design threshold height. The threshold height can be equal to or less than the height that imposes a maximum loading on the side walls; the maximum loading typically including a factor of safety. The desired bed height may range from approximately 0 (substantially no settling of solids) to a pre-determined maximum threshold height of the bed contacting the side walls.
In further embodiments, internal annular elements within chamber provide additional side wall relief by directing solids radially inwardly away from the walls.
Further, conical skirts about one or more of the feed inlet (and possibly the outlet), having conical slopes at or about the angle of repose, can minimize or eliminate bed formation, all of the active settling solids being engaged by the feed inlets (and outlets, where applicable) for fluidization.
A methodology for holding froth produced from extracted oil sands between froth processing stages is provided, wherein the froth contains at least bitumen and solids, the method comprising: introducing the froth into a tank, fluidizing the settling solids in the froth such that the solids remain suspended in the froth or distribute to form a bed of solids having a maximum height of less than a maximum threshold height.
The above-mentioned and other features of the present apparatus and methodology will be best understood by reference to the following description of the embodiments.
As will be appreciated by those of skill in the art, embodiments of holding tanks taught herein are suitable for extended storage of froth streams produced as a result of an oil sands extraction process. The froth typically comprises a bitumen-to-solids ratio of about 4:1. Solids in the froth are largely fine solids, typically having a size less than about 44 microns. Froth is therefore significantly different than initial oil sands slurries in the extraction process which have a bitumen-to-solids ratio of about 1:8 in which the solids include both coarse and fine solids. Holding tanks according to embodiments taught herein are generally unsuitable for use for storage of oil sand slurries and particularly for extended periods of time.
An improved fluidized froth holding tank is provided having regard to
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Tank 10 can include at least one entry inlet 18 for introducing froth into the chamber 12. The froth may be introduced via entry 18 positioned substantially at or near the bottom of tank 10, through the bottom wall 16, through side wall 14 or through an elevated entry inlet 18a, with or without an anti-syphon system in order to avoid backflow.
Froth is discharged or removed from the tank 10 via outlet 22. Outlet 22 is positioned substantially at or near bottom wall 16, and may be located adjacent a side wall 14 per
In one embodiment, the froth is pumped into chamber 12 through one or more feed inlets or nozzles 20 positioned low in the chamber 12 such as adjacent the bottom wall 16. Each feed inlet 20 can direct a flow of froth upwardly into the chamber 12 to engage solids settling therein. For example, froth flow rate via inlets 20 may be sufficient to maintain an approximate feed vertical component velocity of at least 0.5 m/s at the inlets 20. In one embodiment, secondary feed inlet nozzles 20a may be oriented horizontally, or substantially parallel with the bottom wall 16, such as to direct settling or settled solids towards vertically-oriented inlets 20. As shown in
The size, location and capacity of the feed inlets 20 is configured to maintain and distribute suspended solids in a stable, generally fluidized state pending recovery from outlet 22.
The one or more feed inlets 20 are located intermediate the outlet 22 and the side walls 14, each feed inlet 20 fluidizing solids settling thereabout and forming a bed 23 of solids about its respective feed inlet 20, each bed 23 that reaches the side walls 14 having a maximum height of less than a threshold height. If a bed reaches a height greater than the threshold height at or before reaching the side walls, then a successive feed inlet is located between the previous or first feed inlet and the side walls 14.
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Feed inlets 20 or array 21 of feed inlets 20 can be spaced areally so that at least the sub-beds of settling solids formed adjacent the side walls 14 have an elevation below a design loading threshold. The spacing of the feed inlets 20 and resulting sub-beds in the array 21 is such that many adjacent sub-beds about may intersect at the threshold elevation.
The size, location and position of the feed inlets 20 and arrangement thereof can vary depending upon the size and capacity of tank 10 and upon the characteristics of the froth. It is desired that the size, location and position of the feed inlets 20 are configured to fluidize relatively large solids (e.g. maximum approximate size of 250 microns and average diameter of 20-22 microns), in fluid having relatively low viscosity (e.g. >100 cP), by providing sufficient spacing and discharge velocity of the inlets 20.
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Simply, where the one or more feed inlets 20 are arranged as first array 21a, and where beds 23 about the array 21a would reach the side wall 14 having a maximum height greater than the threshold height, then the beds 23 need to be interrupted with additional and successive feed inlets (e.g. arranged as feed array 21b). This, one or more successive feed inlets 20 can be located between the first array 21a and the side wall 14 for fluidizing the settling solids in the froth about one or more successive feed inlets 20 such that settling solids about each of the one or more successive feed inlets 20 form one or more successive beds 23 of solids, each successive bed 23 reaching the side wall 14 having a maximum height less than the threshold height.
As further shown in
The sub-bed 23 height, from the second or successive feed inlets array 21b, results in bed heights less than or about the threshold or design height H1.
Tank 10 may further be configured to comprise one or more directing elements for urging or guiding of settling solids in a manner to optimize fluidization thereof.
In one embodiment, having regard to
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In yet another embodiment, having regard to
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A methodology for storing or handling bitumen froth produced from extracted oil sands between bitumen processing stages is provided, the method comprising introducing the bitumen froth into the tank 10, and suspending or distributing settling solids in the bitumen froth in a fluidized bed within the tank 10 until such time as the bitumen froth is removed from the tank 10.
The present disclosure provides a detailed description of various elements required to operate a fluidized froth holding tank, but many other known elements such as valves, pumps and other tanks interconnected to tank 10, and required to operate the present apparatus and method, have not been described herein.
Example embodiments of the present invention are described in the following Examples, which are set forth to aid in the understanding of the present tank 10, and should not be construed to limit in any way the scope of the invention as defined in the claims which follow thereafter.
With reference to
As such, using Stock's law, the settling velocity of the particles is shown in Table 1:
A total of four inlets, each inlet having an internal diameter (ID) of 6 or 8 inches, were used, the size of which being selected to achieve the desired velocity. As shown in Table 2, the desired discharge velocity of each inlet was significantly higher than the settling velocity for the largest mineral particles, thereby optimizing mixing and fluidization of the fluids in the tank.
With reference to
A total of 13 inlets were used, having an ID of 3 or 4 inches, the size of which being selected to achieve the desired velocity. As shown in Table 3, the desired discharge velocity of each inlet was significantly higher than the settling velocity for the largest mineral particles, thereby optimizing mixing and fluidization of the fluids in the tank.
Although a few embodiments have been shown and described, it will be appreciated by those skilled in the art that various changes and modifications might be made without departing from the scope of the invention. The terms and expressions used have been used as terms of description and not of limitation, and there is no intention in the use of such terms and expressions of excluding equivalents of the features shown and described or portions thereof, it being recognized that the invention is defined and limited only by the claims that follow.