The present disclosure relates to extraction of resins from plant materials.
Many plants concentrate resin in glandular structures called trichomes on the outside of leaves. These can be mechanically separated from the plant matter to collect the resin without the use of solvents. Various devices are known in the art for mechanically separating resins from plant materials.
For example, U.S. Pat. No. 6,158,591 to Delp discloses a method and apparatus for extracting plant resins wherein a washing chamber is filled with cold water, plant material, and ice, then an agitator (e.g. an electric mixer with stirring whisks) is used to mix the contents of the chamber to separate the resins. The resins are allowed to settle and then collected by a filter. However, the apparatus and method disclosed by Delp are not suited for high throughput resin extraction.
The inventors have determined a need for improved apparatus and methods for resin extraction.
One aspect of the present disclosure provides an apparatus for extracting resin from plant material. The apparatus comprises an agitation tank having an open top and an outlet at a bottom thereof, a strainer basket installed within the agitation tank, the strainer basket comprising walls constructed from a mesh material selected based on a type of plant material to be processed, and, an agitator comprising a motor which turns a shaft and two impellers mounted on the shaft.
The two impellers may comprise an upper impeller which urges material downwardly and a lower impeller which urges material upwardly. Alternately, the two impellers may both urge material upwardly, or both urge material downwardly. In some embodiments, the agitator may comprise an impeller configured to lacerate material.
The walls of the strainer basket may have openings with a diameter in a range of 200-230 microns. The strainer basket may comprise a plurality of baffles extending inwardly from a sidewall of the strainer basket. A side gap may separate each baffle from the sidewall, and a bottom gap may separate each baffle from a bottom wall of the strainer basket. The baffles may comprise rounded baffles each having an oval-shaped cross-section.
The strainer basket may be removeable from the agitation tank, and may comprise a plurality of mounting tabs extending outwardly from an upper rim of the strainer basket for suspending the strainer basket within the agitation tank. The strainer basket may comprise a plurality of draining tabs extending outwardly from a middle portion of the strainer basket for suspending the strainer basket partially out of the agitation tank.
Another aspect of the present disclosure provides a process for extracting resin from plant material. The process comprises placing a quantity of plant material within a strainer basket comprising walls constructed from a mesh material, submersing the strainer basket in a tank filled with chilled water at a temperature in the range of 0-10 Celsius, agitating the plant material and chilled water within the strainer basket to separate trichomes from the plant material, and, removing a mixture of water and trichomes from an outlet at the bottom of the tank. The process may further comprise providing the mixture of water and trichomes to a separator apparatus to separate the mixture into water a final product containing the trichomes and recycling the separated water back to the tank.
Another aspect of the present disclosure provides a system for extracting resin from plant material. The system comprises an agitation apparatus for receiving plant material and chilled water, the agitation apparatus configured to agitate the plant material to separate trichomes from the plant material to produce a mixture of water and trichomes, and a separator apparatus connected to receive the mixture of water and trichomes from the agitation apparatus, the vibratory separator apparatus configured to separate water from the mixture to produce a final product containing the trichomes. The separator apparatus may comprise a vibratory separator apparatus, or may comprise a flow path with a plurality of in-line screens.
The agitation apparatus may comprise an agitation tank having an open top and an outlet at a bottom thereof, a strainer basket installed within the agitation tank, the strainer basket comprising walls constructed from a mesh material selected based on a type of plant material to be processed, and, an agitator comprising a motor which turns a shaft and two impellers mounted on the shaft.
The agitation apparatus may comprise a passageway having an inlet and an outlet and a plurality of abrupt changes in direction between the inlet and the outlet. The agitation apparatus may further comprise an agitation chamber, with the passageway being contained within the agitation chamber. One or more vibratory transducers may be coupled to the agitation chamber. The system may comprise a filter between the outlet of the passageway and the vibratory separator apparatus to filter plant material from the mixture of water and trichomes. The vibratory separator apparatus may be configured to separate plant material from the mixture of water and trichomes.
Further aspects of the present disclosure and details of example embodiments are set forth below.
The following figures set forth embodiments in which like reference numerals denote like parts. Embodiments are illustrated by way of example and not by way of limitation in the accompanying figures.
The following describes an improved process and apparatus to separate glandular trichomes containing plant resins from plant material using cold water. Current and existing methods for extracting plant resins mechanically using ice and water do not scale well for large commercial ventures and are often inefficient. The agitation mechanisms used (forward/reverse washing machines, or hand drills) are inefficient and reduce overall yield. The separation of water and resin is laborious and the overall processes are not of a pharmaceutical standard, especially important when separating resin material for medical purposes. The present disclosure is directed to improved systems and processes for extraction or resin, and certain embodiments use an agitator tank with an interior mesh basket, to facilitate the easy replacement of spent material in the extraction chamber with new material. Certain embodiments provide an agitation apparatus comprising a baffle and two impeller systems within the interior mesh basket to cause a full rotation of plant material within the tank, which rubs against the mesh basket, speeding the removal of trichomes from plant matter. Systems according to the present disclosure can significantly improve yields and processing times over currently available methods. As described below, in an example system, after agitation, water containing resin passes through a vibratory sifting apparatus with suitably sized mesh screens (dependent on the plant material/trichome size) to remove resin from water and unwanted debris, and the resin is collected from the vibratory sifting apparatus. Water from the vibratory sifting apparatus is collected in a catchment tank and can be pumped back into the agitator to collect resin in batches or a continuous process.
For simplicity and clarity of illustration, reference numerals may be repeated among the figures to indicate corresponding or analogous elements. Numerous details are set forth to provide an understanding of the examples described herein. The examples may be practiced without these details. In other instances, well-known methods, procedures, and components are not described in detail to avoid obscuring the examples described. The description is not to be considered as limited to the scope of the examples described herein.
As illustrated in
In some embodiments, the agitation apparatus 100 may comprise an impeller in the form of a blade impeller 139 mounted on the shaft 136. The blade impeller 139 comprises upwardly and downwardly extending teeth 139A and 139B for lacerating the material within the basket. In some embodiments, the blade impeller is mounted on the bottom of the shaft 136, in addition to the impellers 137, 138, as shown in
The agitation apparatus 100 shown in
In some embodiments, the agitation apparatus 100 may include alternate or additional agitation means than the impeller-based agitator 130 shown in
In some embodiments, jets of a liquid or gas can be injected into the tank 110 of the agitation apparatus 100. Bubbles from a gas or flow streams from a liquid, such as water, will move plant material and cause the breaking of terpenes. In some embodiments, small pieces of solid material may be added to the plant material within the strainer basket 120 to facilitate agitation when mixed by an impeller. These materials would mimic the agitation caused by ice cubes in the mixture, but would not melt and allow a longer and greater and fuller agitation inside the tank versus using ice.
An example tank 110 is shown in
An example strainer basket 120 is shown in
Another example strainer basket 160 is shown in
In some embodiments, the bottom of the basket 120/160 comprises a hinged door to facilitate emptying of the product.
The wedge wires 162 comprise metal wires with a triangular cross section, and having a gap g between adjacent wires 162 as shown in
In some embodiments, water (and the resin contained therein) may be removed from the outlet 116 at the bottom of the tank 110, and drained into a gravity filter to separate water from resin as known in the art. Alternatively, in some embodiments, such as the example shown in
The system 400 comprises an agitation apparatus 410 (which may, for example, comprise the example apparatus 100 discussed above, or variations thereof). The outlet 412 of the agitation apparatus 410 is connected to a first pump 414. The agitation apparatus 410 and pump 414 are respectively controlled by Variable Frequency Drives (VFD) 411 and 415 connected to a power supply 401 to control their speed. The output 416 from the first pump 414 is directed to empty into the top of a vibratory separator apparatus 420 which is powered through an on/off switch 421 connected to the power supply 401. Product outlets 422 from the vibratory separator apparatus 420 are connected to a collection vessel 424 for collecting final product (resin/trichomes). The vibratory separator apparatus 420 may, for example, comprise a plurality of screens with openings of successively smaller diameters (e.g., a first screen with opening diameters in the range of 190-170 microns for catching debris, then a series of screens with opening diameters in the range of 170-30 microns (e.g. three screens with opening diameters of 120 microns, 70 microns, 40 microns) for catching resin). A water outlet 426 from the vibratory separator apparatus 420 is connected to a water catchment tank 428. The water catchment tank 428 collects the water removed from resin and has an outlet which leads into a second pump 430 controlled by another VFD 431 to recycle water back into the agitation apparatus 410 during cycling, or into the drain to dispose of water at the end of a cycle.
In some embodiments, one or more of the VFDs 411/415/431 and switch 421 can be coupled to be controlled by a suitably programmed computer system, or could be replaced entirely by a dedicated controller configured to run the system 400. All of the running of the various parts (agitation, pumps, separator) can be programmed to run according to pre-set cycles, such that no human operation is required during a resin extraction cycle and every step is automated resulting in higher yields and less labour costs.
An example extraction process will now be described with reference to the system 400 of
For a batch wise process the agitation cycle runs for a set time (usually 10-30 minutes) and then turned off. After the agitation cycle, the first pump 414 and vibratory separator apparatus 420 are turned on and water containing plant resin is drained from the agitation apparatus 100/410 into the separator apparatus 420. Once all water has drained into the catchment tank 428 and final product has been collected in the collection vessel 424, the separator apparatus 420 is turned off and water from the catchment tank 428 is pumped by the second pump 430 back into the agitator tank to repeat the cycle. This can be repeated over multiple cycles to extract all resin possible.
For a continuous water flow process, some water is added to the catchment tank 428, and then the vibratory separator apparatus 420 and both pumps 411 and 420 run simultaneously with the agitation apparatus 410. Using the VFDs 415/431, the flow of each pump 414/430 is set to be equal such that the levels of water in the agitation tank 110 and catchment tank 428 stay the same and resin is being constantly extracted in the agitation apparatus 410 and collected in the separator apparatus 420. The cycle is allowed to run for a time appropriate for the plant material being processed, usually 30-90 minutes. Once a cycle is complete the strainer basket 120 can be removed from the agitation tank 110 and spend plant material removed and replaced with new plant material for another cycle. Using multiple interior baskets already filled with plant material and ice lowers downtime and allows greater extraction throughput.
In some embodiments, instead of plant material being put into a basket in an agitation tank and removed after each batch, plant material can flow through an agitation apparatus configured to serve as a continuous reaction cell. In some embodiments, plant material in cold water flows through a passageway wherein resin is continuously separated from the plant material. Agitation is applied as plant material flows through the passageway, and trichomes are separated from plant material. Plant material is then extruded from the machine as more enters in a continuous process. Such embodiments may be well suited for large production facilities which have a constant supply of plant material to process.
An example agitation apparatus 500 configured for continuous processing of plant material is shown in
In some embodiments, the outlet 506 of the agitation apparatus 500 may be connected to provide the mixture of water and trichomes, along with processed plant material (from which trichomes have been removed), directly to a vibratory separator apparatus such as apparatus 420 of
In some embodiments, a filter may be provided downstream of the agitation apparatus 500 to remove processed plant material (from which trichomes have been removed) from the mixture of water and trichomes.
The present disclosure may be embodied in other specific forms without departing from its spirit or essential characteristics. The described embodiments are to be considered in all respects only as illustrative and not restrictive.
Moreover, the scope of the present application is not intended to be limited to the particular embodiments of the process, machine, manufacture, composition of matter, means, methods and steps described in the specification. As one of ordinary skill in the art will readily appreciate from the disclosure of the present invention, processes, machines, manufacture, compositions of matter, means, methods, or steps, presently existing or later to be developed, that perform substantially the same function or achieve substantially the same result as the corresponding embodiments described herein may be utilized. Accordingly, the appended claims are intended to include within their scope such processes, machines, manufacture, compositions of matter, means, methods, or steps.
As can be understood, the examples described above and illustrated are intended to be examples.
This application claims the benefit of priority of U.S. Provisional Patent Application No. 62/561,535, which was filed on Sep. 21, 2017, and U.S. Provisional Patent Application No. 62/580,102, which was filed on Nov. 1, 2017, both of which are hereby incorporated herein by reference in their entireties.
Filing Document | Filing Date | Country | Kind |
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PCT/CA2018/051197 | 9/21/2018 | WO | 00 |
Number | Date | Country | |
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62561535 | Sep 2017 | US | |
62580102 | Nov 2017 | US |