The following generally relates to cleaning inner surfaces of tubing.
In the field of heater exchangers and chemical reactors, tubing is often used. For example, in cracking furnaces and heater exchangers, there are parallel tubes connected to each other at their ends using bends, such as U-bends or other types of bends, to form a continuous tube. Fluid typically flows through the piping while the chamber or environment around the piping is heated to heat the fluid flowing within the piping.
In a tubular reactor for cracking, a furnace houses banks of tubes that are connected to each other to form one or more continuous tubes for fluid to flow through. The tubes may form a serpentine configuration. Furnace guns or heat generators, for example, surround the banks of tubes.
The straight parallel portions of the tubing are typically positioned close together to reduce the amount of space being used within the furnace or the heat exchanger. There may be dozens to hundreds of straight portions of tubes. The inner diameter of the tubes typically range from under one inch to several inches.
The cracking process results in deposits, scales, product or by-product build-up, and material in general to collect on the inner surfaces of the tubes. This reduces the flow of fluid within the tubes, as well as the efficiency of the cracking process.
Cleaning the tubes in the furnace is costly, typically requires a lot of manual labour and large machinery, and typically requires an extended amount of time during which the cracking furnace is shut down.
To clean the surfaces of an object, ultrasonic acoustic waves acting on a fluid in contact with the surface can provide enough energy to remove unwanted product build-up. This fluid undergoes cavitation through the use of ultrasonic transducers. The forces caused by cavitation combined with cleaning chemicals present in the fluid work to dislodge the layers of built-up deposits.
U.S. Pat. No. 4,120,699 describes multiple transducers are placed around a jacket that contains therein a tube bank, and which is immersed in fluid. The transducers are not directly mounted to a given tube within the bundle.
U.S. Pat. No. 6,290,778 describes a heat exchanger cleaning device for tube-in-shell heat exchangers. An ultrasonic transducer probe array, which is positioned at the end of a cable, is inserted inside a fluid filled shell and swept along the interior tubes producing acoustic waves causing cavitation of the fluid for cleaning. This requires access to the interior of a tube, which can have many bends, such as U-bends, that may cause the probe to become lodged.
U.S. Pat. Nos. 7,500,402 and 3,987,674 each describe an ultrasonic transducer measuring device that are to be positioned on a pipe. The transducer energy and operation settings are used for sensing, and not for cleaning.
U.S. Pat. No. 4,244,749 describes parallel spaced apart banks of pipes each having external surfaces exposed to a liquid environment, such as in bath vessel. An ultrasonic cleaning array is dipped into the bath, in a space between the pipes, and then activated to cause cavitation of the liquid. The transducers are not mounted directly to a tube.
Examples embodiments of the invention are provided below, including example aspects of such embodiments. Additional features of the embodiments as well as additional example embodiments are described in the figures and the detailed description.
A cleaning system for cleaning tubes is provided. For example, the system includes: a string of multiple cleaning apparatuses in electrical communication with each other and configured to be mounted along a length of a tube; a primary control module that is in electrical connection with a first cleaning apparatus in the string of multiple cleaning apparatuses; each one of the cleaning apparatuses comprising an acoustic transducer, a releasable clamping mechanism to mount the transducer to the tube, and a microcontroller to control the transducer; and wherein the microcontroller is configured to receive a data command from the primary control module.
A method for cleaning a tube, or multiple tubes, in a furnace is provided. The method, for example, includes: filling the tube in the furnace with a liquid solvent; mechanically cleaning multiple portions an exterior surface of the tube, the multiple portions space apart from each other along a length of the tube; clamping multiple cleaning apparatuses on to the cleaned multiple portions of the tube, each of the cleaning apparatuses comprising an acoustic transducer; activating the cleaning apparatuses via a primary control module that is in electrical communication with the cleaning apparatuses; deactivating the cleaning apparatuses; flushing the tube with new liquid solvent; and removing the cleaning apparatuses from the tube.
An acoustic energy cleaning apparatus is provided for cleaning an interior surface of a tube. For example, the apparatus includes: a transducer housing that houses an acoustic transducer; a rigid seal cover that encompasses a lower portion of the transducer housing; an annular resilient seal positioned within and below the seal cover; and an injection hole that fluidly connects a space, defined at least by the annular resilient seal and a bottom surface of the acoustic transducer, to an external environment, the injection hole having an opening to receive an injection of gel.
A cleaning system for a tube is provided and it includes: the tube comprising a mechanical receiver positioned at an opening in a wall of the tube; a removable plug that can be mechanically fastened and removed from the mechanical receiver; a cleaning apparatus that can be mechanically fastened to the mechanical receiver in place of the removable plug, and can be subsequently removed from the mechanical receiver; the cleaning apparatus comprising an electromechanical device to at least one of vibrate the wall of the tube and excite liquid within the tube; and a wire extending from the cleaning apparatus to provide electric power to the electromechanical device.
Embodiments will now be described by way of example only with reference to the appended drawings wherein:
It will be appreciated that for simplicity and clarity of illustration, where considered appropriate, reference numerals may be repeated among the figures to indicate corresponding or analogous elements. In addition, numerous specific details are set forth in order to provide a thorough understanding of the example embodiments described herein. However, it will be understood by those of ordinary skill in the art that the example embodiments described herein may be practiced without these specific details. In other instances, well-known methods, procedures and components have not been described in detail so as not to obscure the example embodiments described herein. Also, the description is not to be considered as limiting the scope of the example embodiments described herein.
It is herein recognized that cleaning the inner surface of tubing in cracking furnaces and heat exchangers is difficult due to limited access, the long length of tubing, and the multiple U-bends connecting straight segments of the tubing.
Existing cleaning systems use a cleansing bath method wherein tube sections are removed and submerged into a large vessel that contains cleaning fluid. In particular, tube sections are removed from a cracking furnace and are transported to a facility that holds the large vessel. The tube sections are then submerged within the vessel, and the fluid is made to undergo cavitation by acoustic waves from ultrasonic transducers. The cavitation effect applies pressure to the tubes, dislodging built-up deposits. The treated tube sections are then transported back to the cracking furnace to be re-installed. It is herein recognized, however, that the removal, transportation, and re-installation of the tube sections requires manual effort and increases the amount of time that the cracking furnace is inoperable. Furthermore, a large amount of electrical energy is required to agitate the large amount of fluid within the vessel.
It is also recognized that some cleaning systems use ultrasonic transducers, but these transducers are not mounted directly to a tube. This separation and distance will therefore increase the amount of energy required to clean a tube.
Furthermore, while sensor-type transducers are used for measurement, these transducers are typically lower power and are not configured for cleaning.
It is also herein recognized that tubes come in many different diameters, and that a tube may not be perfectly cylindrical. Therefore, having a cleaning system that is adaptable to the variances in tube surfaces is desirable, while still maintaining a high transfer of acoustic energy from the transducer to the tube.
It is also desirable to reduce the setup and the manual effort of a process required to clean tubing. This reduced setup includes, for example, using a reduced amount of liquid to excite.
The proposed example cleaning apparatuses, systems and methods address one or more of the above issues.
Turning to
The furnace, for example, is a hydrocracking furnace, a steam cracking furnace, a gas cracking furnace, or a liquid cracking furnace. Other types of currently known or future known cracking furnaces are applicable. It is appreciated that, while many of the examples described herein relate to furnaces, the features described herein are also applicable to other structures that have tubing. For example, a heat exchanger having tubing can benefit from the systems and methods proposed herein.
In an example embodiment, each cleaning apparatus 102 is removable and attachable to the tube.
For example, the cleaning apparatus 102 is attachable to the exterior of surface of the tube.
In another example, the cleaning apparatus 102 is inserted into a receiver on a tube. The receiver is positioned at an opening in the tube wall and the cleaning apparatus can be inserted at or within the opening, so that the cleaning apparatus is in fluidic communication with the interior of the tube.
In an example embodiment, each cleaning apparatus includes one or more ultrasonic transducers.
In an alternative example embodiment, each cleaning apparatus includes at least one of a sonic transducer an ultrasonic transducer. For example, in a cleaning system that includes a series of cleaning apparatuses, every other apparatus includes an ultrasonic transducer and every other apparatus includes a sonic transducer.
The ultrasonic transducers are powered and operated at frequency settings to cause cavitation of the liquid within the tube.
In an example embodiment, the sonic transducers include sound emitters for audible sound in the approximate frequency range 20-20,000 Hz. In another example, the sonic transducers are devices, e.g. pulsators, that emit non-audible sound, infrasound, in the approximate frequency range 2-20 Hz. In an example embodiment, the sonic transducers emit acoustic energy at frequencies in the range extending from 60 to 800 Hz.
In another example embodiment the cleaning apparatus 102 is a mechanical device or an electromechanical device that produces vibrations. This type of device is also known as a vibrator. For example, an electric motor or an electric actuator, or a combination of both, are used to generate vibrations. The vibrations are used to loosen and dislodge the build-up of material on the inner surface of a tube. The vibrations are, for example, emitted to vibrate the tube wall itself, or the liquid within the tube, or both.
It another example embodiment, the cleaning apparatus 102 includes a combination of a vibrator and an acoustic transducer (e.g. a sonic transducer or an ultrasonic transducer).
In addition or in an alternative example embodiment, the cleaning apparatus 102 includes a heating element to assist with the cleaning process.
In addition or in an alternative example embodiment, the cleaning apparatus 102 includes a light source to emit light for the purposes of cleaning. For example, the light source shines ultraviolet (UV) light to aid in the cleaning process.
Turning to
As shown by
The microcontroller housing 201 includes two electrical connection receptacles 204 to electrically connect one cleaning apparatus 102 to another cleaning apparatus 102. In particular, an electrical wire 205 has at both ends connectors 206. A given connector 206 can be inserted into a given receptacle 204.
In an example embodiment, the microcontroller housing 201 has side surfaces 202 and 203 that are at opposite ends from each other, and each of the side surfaces 202 and 203 have defined therein a receptacle 204.
The microcontroller can be programmed to activate a transducer at a desired time, or at a desired pattern, or both. The microcontroller is also programmable to control the frequency at which the transducer emits acoustic energy.
The electrical wire 205 is used to transmit electrical energy to power each of the cleaning apparatuses that are interconnected, and to also transmit control signals. For example, the control signals synchronize the operation of the cleaning apparatuses.
The primary control module 303 includes a power source 304 and a controller device 305. The power source 304 outputs electrical power that is transmitted via the wires to each of the cleaning apparatuses in the series. The controller device 305 outputs commands that determines the operation of the power source 304. The controller device 305 also outputs commands that are receivable by the microcontroller of each cleaning apparatus and, in turn, the microcontroller uses the received command to affect its operating attributes (e.g. pattern or timing of operation, frequency output, etc.).
Turning to
The tube 406 and elements of sealing components 407, 408 and 409 are shown in a cross-sectional view. The sealing components are used to ensure that there are little or no air gaps through which the acoustic waves to dissipate. In particular, if the acoustic waves generated by a transducer pass through air, then the acoustic energy being transmitted into a tube body and into the liquid inside the tube is drastically diminished. In other words, there is a loss of energy due to an air gap, which reduces the effectiveness of the cleaning apparatus. To improve the transfer of energy from an ultrasonic transducer, or a transducer, or both to the tube wall, then various types of sealing components are herein proposed.
It will be appreciated that other types of clamping mechanisms may be used with the cleaning apparatuses described herein. For example, thread bolts, friction belts, and other devices may be used to mechanically secure the cleaning apparatus to the tube, while still allowing the cleaning apparatus to be removed after the cleaning operations are performed.
The lower portion of the transducer is encompassed by a rigid seal cover 407. The rigid seal cover protrudes outwards from the sides of the transducer, and extends downwards to define within a cavity, which holds an expandable seal 408. In particular, the expandable seal 408 is positioned around the perimeter of the lower portion of the transducer 401.
Positioned between the tube 406 and the bottom surface of the transducer is a gel 409, which transmits the acoustic energy from the transducer to the tube 406. The seal 408 helps to trap the gel 409 from leaking, so that over time, the gel remain in place. The gel is also known as an ultrasonic gel, or a coupling agent.
As shown in
In an example operation, a user places the gel on the bottom of the transducer, within the space encircled by the expandable seal, and then places the cleaning apparatus onto the tube. Alternatively, the user places the gel on to the tube itself, and then places the cleaning apparatus on to the tube having the gel. The user then tightens the clamp, which compresses the expandable seal.
In this way, there are little or no air gaps. Furthermore, the gel remains in place over an extended period of time. It will be appreciated that the expandable seal 408 may be an O-ring that is made of a resilient polymer material.
In another aspect, it is recognized that placing a sufficient amount of gel onto a vertically oriented tube can be difficult, because the gel will run down the tube due to gravity. Turning to
The embodiment shown in
The compressible seal 705 is positioned within the rigid seal cover 407. An annular compression plate 704 is positioned above the seal 705 to evenly distribute compression forces onto the seal 705. The plate 704 is rigid. In an example embodiment, an inner O-ring 706 and an outer O-ring 703 are placed on the inner and the outer edges of the plate 704, in order to act as a seal. In another example, the inner and out edges of the plate 704 are not surrounded by O-rings.
Above the plate 704 is space 702 that is defined by the plate, the outer wall of the transducer, and the inner walls of the rigid seal cover 407. An injection opening 701, which is in fluidic communication with the space 702, allows a user to inject a fluid into the space 702 in order to pressure the plate 704 downwards. As the plate 704 is pressed down, due to the pressure of the injected fluid, the seal 705 is compressed against the tube.
As shown in
Turning to
In operation, a user injects gel into the space 801 via the opening 503 of the injection hole 501. The gel travels into the space 801, into the channel 802, and then into the chamber 803. The pressure of the gel in the chamber exerts a downward pressure onto the plate 704, which in turn, presses down on, and compresses, the seal 705.
In another example embodiment, the “A” cleaning apparatus represents an ultrasonic transducer that is affixed to the tube with a gel interface, and the “B” cleaning apparatus represents on with an ultrasonic transducer that is affixed to the tube without a gel interface. The “B” cleaning apparatus is configured to cause a larger portion of the tube to be excited with the acoustic energy.
Turning to
At block 1, the furnace is turned off. At block 2, tubes are flushed are filled with a liquid, such as, but not necessarily, a cleaning solvent. At block 3, a user mechanically cleans portions of the tube surfaces at which multiple cleaning apparatuses will be placed. For example, a user may use a wire brush to clean an outer surface of the tube.
At block 4, the user mounts a cleaning apparatus to each of the cleaned surface portions. This may include using the clamping mechanism of the cleaning apparatus and injecting gel into the cleaning apparatus to ensure there is a seal.
At block 5, the user electronically connects each of the cleaning apparatuses together in a series, and connects the series to a primary control module. At block 6, the cleaning apparatuses are activated via the primary control module. For example, the primary control module activates the series of the cleaning apparatuses according to a pre-defined sequence (block 7). While being activated, cavitation of the liquid within the tubing causes the scaling and build-up of material to be dislodged.
At block 8, the series of the ultrasonic transducers are deactivated by the primary control module. At block 9, the liquid within the tubing is flushed.
If the process is repeated at least one or more times, as per block 10, then at block 11, the liquid inside the tubing is flushed out and then refilled with new liquid. The process repeats by returning to block 6. It will be appreciated that the cleaning process may repeat multiple times.
If the process is not to be repeated, then the user disconnects the cleaning apparatuses from each other and also removes the cleaning apparatuses (block 12). At block 13, the furnace is then returned to operational settings.
It will be appreciated that any module or component exemplified herein that executes instructions may include or otherwise have access to computer readable media such as storage media, computer storage media, or data storage devices (removable and/or non-removable) such as, for example, magnetic disks, optical disks, or tape. Computer storage media may include volatile and non-volatile, removable and non-removable media implemented in any method or technology for storage of information, such as computer readable instructions, data structures, program modules, or other data. Examples of computer storage media include RAM, ROM, EEPROM, flash memory or other memory technology, CD-ROM, digital versatile disks (DVD) or other optical storage, magnetic cassettes, magnetic tape, magnetic disk storage or other magnetic storage devices, or any other medium which can be used to store the desired information and which can be accessed by an application, module, or both. Any such computer storage media may be part of the primary control module 303, or a controller 201, or accessible or connectable thereto. Any application or module herein described may be implemented using computer readable/executable instructions that may be stored or otherwise held by such computer readable media.
In another aspect, it is herein recognized that it is also desirable to place a cleaning apparatus within the wall of the tube or directly within the flow of the tube, or both, in order to clean the inner surface of the tube.
It is also recognized that an ultrasonic transducer may be permanently placed within the flow of the tube. However, placing the ultrasonic transducer within the tube may disrupt the flow of the fluid within the tube, thereby reducing performance when the cracking furnace or other heat exchanger mechanism is in operation. It is also recognized that an ultrasonic transducer may degrade if placed within a cracking furnace due to the extreme heat. Therefore, it is herein recognized that it is also desirable to remove an ultrasonic transducer, or another type of sensitive cleaning apparatus, from a tube when the cracking furnace is in operation.
Turning to
As best seen in the cross-section views in
The plug 1801 is removable and can be switched with an ultrasonic transducer, or other cleaning apparatus, during cleaning operations. An example of this is shown in
Turning to
In a further example embodiment, either in addition or in the alternative, an ultrasonic transducer 1902 extends from the plug 1901 into the tube cavity. The transducer 1902 excites the liquid within the tube 1800.
It an example embodiment, there are multiple tapered holes with plugs 1801 along the length of the tube. During a cleaning operation, each of the plugs 1802 are removed and the cleaning apparatuses are attached instead. The wires 1903 or 2003 may be connected together, so as to power multiple cleaning apparatuses at the same time.
After the cleaning operations are complete, the cleaning apparatus is removed from the tube and the plug 1801 is put back into the hole of the tube for nominal operation.
During a cleaning operation, the plug 2102 is removed from the tube 2100. As shown in
In other words, the cleaning apparatus includes an outer threaded surface, and the mechanical receiver (e.g. flange 2101) comprises an inner threaded surface, and the cleaning apparatus is configured to screw into the mechanical receiver.
Turning to
In another example embodiment, either in addition or in alternative to the above, one or more ultrasonic transducers 2301 are positioned below the threaded body 2201a. In other words, the one or more transducers 2301 are within the flow of the liquid in the tube, and are positioned to excite the liquid (e.g. to cause cavitation).
Turning to
As best seen in
Turning to
In another example, either in addition or in the alternative, a protruding body 2603 protrudes from the main body 2601. The protruding body 2603 includes one or more ultrasonic transducers to excite the liquid within the tube.
Turning to
Turning to
As better seen in the exploded view of
In a preferred example, the bottom of the nested portion 2802 is curved to match the inner radius of, and to be flush with, the inner surface of the tube 2800. This is best shown in
In a preferred example embodiment, the plug 2802 is configured to withstand the same or similar environmental and operating conditions (e.g. temperature and pressure) as the tube 2800.
Turning to
One or more ultrasonic transducers are embedded within the main body 2901 and, when excited, can cause the walls of the tube 2800 to vibrate.
In another example, either in the alternative or in addition, a secondary body 2902 protrudes from the main body and into the flow of liquid in the tube. The secondary body includes one or more ultrasonic transducers and excites the liquid in the tube.
In another example embodiment, another configuration of a cleaning apparatus is attached to the receiving flange 2801 as shown in
A cover plate 3001 is secured to the receiving flange 2801. A wire 3003 passes through a sealed opening in the cover plate. At the end of the wire is a body 3002 that is positioned within the cavity of the tube. The body 3002 contains one or more ultrasonic transducers for exciting the liquid within the tube. The wire 3003 provides electric power to the one or more transducers.
It will be appreciated that the above examples shown in
In another example embodiment, the cleaning apparatus is located on a bend portion of a tube.
In particular, turning to
As can be seen in
It will be appreciated that although an example orientation of the U bend is shown relative to the furnace wall 3101, other orientations are applicable.
Turning to
A push mechanism is positioned within the jacket 3201 that exerts a pushing force against the exterior bracing surface 3208 of the removable bend cap 3202 to push a seating surface 3210 of the removable bend cap against an end surface 3223 of the two sections of the tubing. The example push mechanism in
In particular, continuing with
It will be appreciated that the jacket 3201, the bracket 3203, and the blind flange 3207 are shown in a cross-sectional view, with the bracket 3203 nested within the jacket 3201.
The interior of the removable bend cap 3202 includes a rounded surface 3209 that defines an interior bend space 3211. Therefore, the straight passages 3110 are in fluidic communication with the interior bend space 3211, allowing the fluid to flow around the bend between different straight portions of tubing.
In the example of
The system also includes a blind flange 3207 that is braced against the flange 3222 of the jacking bracket 3214. In particular, the bolts 3204 hold together the blind flange 3207, the jacking bracket 3203 and the jacket 3201. Although bolts and nuts are shown, it will be appreciated that other clamping mechanisms or mechanical fasteners could be used.
The blind flange 3207 includes an exterior surface 3206 and an opposite interior surface 3215. The interior surface 3215 of the blind flange 3207 faces the exterior surface 3214 of the jacking bracket 3203, and these surfaces together define a space 3218 there-between.
Opposite to the exterior surface 3214 of the jacket bracket 3203 is the interior surface 3213 of the jacking bracket 3203. The bracing surface 3208 of the removable bend cap faces the interior surface 3213 of the jacking bracket 3203, and these surfaces, together with the interior surface 3229 of the jacket 3201 define another space 3217.
In an example embodiment, one of, or both of, the spaces 3217 and 3218 are filled with a thermal insulator material, such as a thermal insulator gas, liquid, vapor, or plasma. In an example embodiment, the thermal insulator is ethylene.
In another example embodiment, one of, or both of, the spaces 3217 and 3218 are filled with the same fluid that is passing through the tubing.
In another example embodiment, one of, or both of, the spaces 3217 and 3218 are filled with the same fluid that is within the furnace enclosure, but is exterior to the tubing.
In another example embodiment, the thermal insulator is at a higher pressure in spaces 3217 or 3218, or both, compared to the pressure within the tubing. In this way, if there is leakage between the tubing and the removable bend cap, the insulator leaks into the tubing. For example, the insulator is a desirable product of a cracking process, such as ethylene, propylene, butadiene or some other hydrocarbon.
To remove the removable bend cap, the blind flange 3207 is first removed. The jacking bracket 3203 is then removed, which provides access to the removable bend cap 3202. After the jacking bracket is removed, the removable bend cap 3202 is removed. The removable bend cap can then be inspected or cleaned, or both. Similarly, the tubing portions 3106, 3107, 3109 can also be inspected or cleaned, or both.
In this way, personnel can access the bend portion of the tubing from outside of the furnace (e.g. at the exterior space 105), as well as to remove the removable bend cap 202 for inspection and cleaning while being outside the furnace. This is very convenient as it saves time. In particular, personnel do not need to wait for the furnace to cool down to enter the interior of the furnace.
The removable bend cap 3202 includes an aperture 3802 that holds a cleaning apparatus device 3801. In an example embodiment, a portion of the cleaning apparatus 3801 is in direct contact with the removable bend cap and another portion is contact with the fluid that fills the tubing.
For example, a liquid fills the tubing and the liquid and the cleaning apparatus are in contact with each other. The cleaning apparatus then emits energy, which is transmitted through the liquid, to clean the inner surfaces of the tubing.
A passage 3803 is defined in the jacking plate and a passage 3804 is defined in the blind flange to allow a wire 3805 to pass through, to connect to the cleaning apparatus 3801. For example, the wire supplies electrical power to the cleaning device.
In another example embodiment, the cleaning apparatus 3801 is battery powered, so that the wire 3805 is not required.
As shown in
It will be appreciated that the wires described above may also include control signals that control the operation of the one or more electromechanical devices. In an example embodiment, the electromechanical devices are ultrasonic transducers.
It will also be appreciated that other types of energy activated cleaning apparatuses may be used in addition to, in alternative to, ultrasonic transducers. Other types include mechanical vibration devices, electromechanical vibration devices, light sources (e.g. UV light or other light), heating elements, vibratory transducers (e.g. piezoelectric elements), and other types of acoustic transducers.
It will be appreciated that different features of the example embodiments of the system, the method and the apparatus, as described herein, may be combined with each other in different ways. In other words, different modules, operations and components may be used together according to other example embodiments, although not specifically stated.
The steps or operations in the flow diagrams described herein are just for example. There may be many variations to these steps or operations without departing from the spirit of the invention or inventions. For instance, the steps may be performed in a differing order, or steps may be added, deleted, or modified.
Although the above has been described with reference to certain specific embodiments, various modifications thereof will be apparent to those skilled in the art without departing from the scope of the claims appended hereto.
This patent application claims priority to U.S. Patent Application No. 62/427,366, titled “Acoustic Transducer Apparatus, System and Method for Cleaning Inner Surfaces of Tubing”, and filed on Nov. 29, 2016, and to U.S. Patent Application No. 62/447,673, titled “Apparatus, System and Method for Cleaning Inner Surfaces of Tubing”, and filed on Jan. 18, 2017, the entire contents of which are herein incorporated by reference.
Number | Date | Country | |
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62427366 | Nov 2016 | US | |
62447673 | Jan 2017 | US |