This application claims priority from Japanese Patent Application No. 2010-012812 filed on Jan. 25, 2010, the entire contents of which are incorporated herein by reference.
Aspects of the present invention relate to a centrifugal separator having a swing rotor, and more particularly, to a centrifugal separator and a swing rotor for a centrifugal separator, which are easily used and have a longer operating life by improving a bucket.
A centrifugal separator separates purifies a sample by inserting the sample (for instance, culture solution or blood or the like) into a rotor through a tube or a bucket vessel and rotating the rotor at high speed. A set rotating speed of the rotor is different depending on a use. Products from low speed (about several thousand rotations) to high speed (a maximum rotating speed is 150,000 rpm) are provided so as to meet uses. As rotors to be used, there are various kinds of rotors, for instance, an angle rotor whose tube hole is a fixed angle type so as to meet a high rotating speed or a swing rotor in which a bucket provided with a tube is swung from a vertical state to a horizontal state in accordance with the rotation of the rotor. Further, there are rotors of various sizes such as a rotor that is rotated at a super-high rotating speed to apply a high centrifugal acceleration to a small amount of sample or a rotor that is rotated at a low rotating speed but can treat a large amount of sample. Since these rotors are used depending on the sample to be separated, the rotors are detachably attached to a rotating shaft of a driving unit such as a motor and the rotor may be exchanged.
Generally, an allowable maximum rotating speed of the swing rotor is lower than that of the angle rotor, because the swing rotor has a swing mechanism. However, in the rotor body. The bucket includes a bucket body and a hook portion formed in a cover portion of the bucket body. When the rotation is stopped, the hook portion is engaged with the arm to attach the bucket to the swing rotor. Further,
Here, when the swing rotor 120 is rotated, the buckets 130 are swung by a centrifugal force on the pins 134, in the directions shown by an arrow mark 141 as swing shafts (rotating shafts) for a swing movement. In the swing movements of the buckets 130, the buckets 130 are moved from the vertical directions to horizontal directions (immediately transversely). In an outer peripheral side of the rotor body 21, hollow portions 24 are formed which are semi-cylindrically hollowed so as not to block the swing movements of the buckets 130 by the rotor body 21 at that time. The form of the hollow portion 24 may substantially correspond to an outer line of the bucket 130 and may be formed to be slightly larger than the bucket 130 so as to exactly fit the bucket 130 thereto.
The left half of
A cap main body 133 as a main portion of the cap assembly 131 serves as a cover for sealing an inner space of the bucket body 132 and is connected to the bucket body 132 by screwing. The cap main body 133 is manufactured, for instance, by scraping a metal alloy such as aluminum and includes a cover portion 133c serving as the cover, a cylindrical portion 133a formed in an upper portion of the cover portion 133c and an external threaded portion 133d formed in a lower portion of the cover portion 133c. The external threaded portion 133d is screwed to the internal threaded portion of the bucket body 132. In the cylindrical portion 133a, a through-hole 133b of an oval form in side view is formed through which the pin 134 transversely penetrates, so as to be vertically movable by a minute distance. The pin 134 is guided by the pin insert groove 23 of the rotor body 21 on both ends thereof and used to hold the bucket 130 on the rotor body 21 so as to swing freely.
A pin holder 135 is a member for attaching the pin 134 to the cap main body 133. When attaching the cap main body 133, the pin 134 and the pin holder 135, the pin holder 135 is initially inserted from an upper end of the cylindrical portion 133a of the cap main body 133. A central position of a through-hole 135a of the pin holder 135 is aligned with a central position of the through-hole 133b of the cap main body 133, and the pin 134 is press fitted in the through-hole 135a of the pin holder 135 from a side, so as to fix the cap main body and the pin holder. Here, the inside diameter of the pin holder 135 is formed with a little clearance so that the pin holder 135 may slide relative to the cylindrical portion 133a of the cap main body 133. Further, since the through-hole 133b formed in the cap main body 133 has the shape of a slot, the pin 134 can move vertically by a minute distance within a range of the through-hole 133b.
In an upper portion of the pin holder 135, one to several wave washers 136 are inserted and an upper portion thereof is fixed by a stopper 137. The stopper 137 is strongly pressed in and fixed to an upper end of the cylindrical portion 133a of the cap main body 133. The wave washer 136 is a spring member that urges downward the pin 134 and the pin holder 135 which are slightly vertically movable relative to the cap main body 133. When the bucket 130 is supported by both end portions of the pin 134, the pin holder 135 stands still at a position where a repulsion force of the wave washer 136 and a weight of the bucket 130 are balanced.
Generally, when centrifugal separation is carried out by using the swing rotor, an allowable maximum rotating speed is lower than that when an angle rotor is used. However, a rotation at high speed is requested to the centrifugal separation using the swing rotor, and a centrifugal separator that uses the swing rotor and rotates the swing rotor at high speed such as 50,000 rpm has appeared. However, in the centrifugal separator using the swing rotor, there is a fear that, since a strong centrifugal load is applied to an attached bucket vessel by a rotating force of the rotor, when the swing rotor is repeatedly used, the strength of the bucket may be possibly lowered due to metal fatigue. Further, as recognized by experiments, when a state that the bucket is swung to be seated on a bucket receiving surface of the swing rotor is not stable, as the centrifugal load is increased, a force for rotating a pin may occasionally operate to fasten or unfasten a cap main body. Further, it is recognized that when the position of a bucket body which comes into contact with the bucket receiving surface of the swing rotor is always located at the same position, face pressure is repeatedly applied to a specific position. This is not preferable in view of operating life.
Aspects of the present invention are devised by considering the above-described background. Accordingly, it is an aspect the present invention to provide a centrifugal separator and a swing rotor for a centrifugal separator that can smoothly operate a swinging bucket and stably make the bucket seated.
Another aspect of the present invention is to provide a centrifugal separator and a swing rotor for a centrifugal separator that can be rotated at high speed by improving a bucket.
Another aspect of the present invention is to provide a centrifugal separator and a swing rotor for a centrifugal separator in which a position of a bucket body which comes into contact with a bucket receiving surface of the swing rotor can be prevented from being always located at the same position by improving a bucket, to realize long operating life.
According to an aspect of the present invention, there is provided a centrifugal separator comprising: a driving portion including a driving shaft; and a swing rotor provided at an end of the driving shaft, the swing rotor including, a rotor body, a through-hole passing through the rotor body from an upper side in an axial direction of the driving shaft, pin insert grooves which are provided to the through-hole parallel with the axial direction of the driving shaft, the pin insert grooves opposing each other in a diametric direction of the through-hole and only partially penetrating the rotor body, a cut-out portion perpendicular to the through-hole and formed outwards in a radial direction of the driving shaft, and a bucket including, a bucket body that accommodates a vessel and has a contact surface which is configured to contact the rotor body during centrifugal separation, and a cap assembly that seals the bucket body and has a swing shaft extending in a direction perpendicular to an longitudinal direction of the bucket, wherein the swing rotor is rotated when the bucket is inserted into the through-hole, to swing the bucket, and the swing shaft can be moved in the longitudinal direction of the bucket relative to the bucket body and rotated about a longitudinal central axis of the bucket.
According to another aspect of the present invention, there is provided a swing rotor for a centrifugal separator, the swing rotor comprising: a rotor body; and a bucket including, a bucket body that accommodates a vessel and has a contact surface which is configured to contact the rotor body during centrifugal separation, and a cap assembly that seals the bucket body and has a swing shaft extending in a direction perpendicular to an longitudinal direction of the bucket, wherein the swing shaft can be moved in the longitudinal direction of the bucket relative to the bucket body and rotated about a longitudinal central axis of the bucket.
Hereinafter, an exemplary embodiment of the present invention will be described by referring to the drawings. In the drawings, the same portions are designated by the same reference numerals and repeated explanation is omitted. Further, upper and lower directions described hereinafter correspond to upper and lower arrows shown in the drawings.
The swing rotor 20 includes a rotor body and a plurality of buckets 30 into which tubes having accommodated samples to be separated are inserted. By the rotation and centrifugal force of the swing rotor 20, the buckets 30 are swung in the centrifugal direction to be located in horizontal directions from vertical directions. The form of the swing rotor will be described hereinafter. The swing rotor 20 is rotated by a motor 7 included in a driving portion 6. The rotation of the motor 7 is controlled by a controller not shown in the drawing. The driving portion 6 is attached to a lower side of a partition plate 2d of the casing 2 via a damper 8.
The chamber 2c is formed so as to be sealed by the door 5. Under a state that the door 5 is opened, the swing rotor 20 can be attached to or detached from the rotor chamber 4 in the chamber 2c through an opening portion 2a in an upper side. Though not shown in the drawing, a cooling device that maintains an inner portion of the rotor chamber 4 at a desired low temperature and a vacuum pump that maintains an inner portion to a prescribed pressure reduced state is connected to the chamber 2c. During the operation of a centrifugal separation, an inner portion of the rotor chamber 4 is maintained in a set environment by a control by the controller. In a side portion (a right side) of the door 5, an operation and display portion 9 is arranged, in which a user inputs conditions such as a rotating speed of the rotor or a centrifugal separation time, and on which various kinds of information is displayed. The operation and display portion 9 is formed with, for instance, a combination of a liquid crystal display device and operating buttons or a touch type liquid crystal panel. Further, between the driving portion 6 and a lower portion of the protective wall 2b, a bellows 11 is provided so as to surround the rotating shaft 7a. Thus, when the pressure in the chamber 2c is reduced by the vacuum pump not shown in the drawing, atmospheric air is prevented from entering from a through-hole 12 through which the rotating shaft 7a passes.
The rotor body 21 may be formed substantially in a circular shape when the rotor body is seen from the upper side. However, in order to reduce a mass of the swing rotor 20, the swing rotor is formed to decrease a thickness except for portions that a below-described bucket accommodating space 29 (see
In an upper portion of a bucket body 32, a flange portion 32b expanding in the diametric direction is formed. A contact surface 32a which comes into contact with the rotor body 21 is formed to a lower portion of the flange portion 32b. The contact surface 32a is formed with a linear inclined surface 32g continuous in a circumferential direction and extending to a lower tapered portion 32f, which will be described later, from the flange portion 32b. The inclined surface is connected to the tapered portion 32f by an R portion 32h. On the other hand, in the vicinity of the connecting portion of the bucket accommodating cavity 27 and the hollow portion 24 of the rotor body 21, a bucket receiving surface 25 is formed which effectively comes into contact with the contact surface 32a. Further, a clearance groove 26 is formed adjacently to the bucket receiving surface 25. The clearance groove 26 is a corner removed portion or cut-out portion so that when the bucket 30 is swung to be located in a horizontal position or the bucket receiving surface 25 comes into contact with the contact surface 32a, the R portion 32h of the bucket body 32 does not collide with the corners of the bucket accommodating cavity 27 and the hollow portion 24.
When the rotating speed of the swing rotor 20 is increased from the state that the bucket 30 is located in the horizontal position, since a strong centrifugal load is applied to the bucket 30 in the direction shown by an arrow mark 45, the wave washer 36 is bent as shown in the right side of the drawing to move the bucket 30 outwards in the longitudinal direction thereof and decrease a clearance between the rotor body 21 and the bucket 30. As a result, the bucket body 32 and the stopper 37 are moved in the direction shown by an arrow mark 46 to reduce the thickness of the wave washer 36, and at a position shown by an arrow mark 47, the contact surface 32a effectively comes into face contact with the bucket receiving surface 25 to be seated thereon. The rotating speed when the contact surface 32a is seated on the bucket receiving surface 25 is, for instance, about 3000 rpm. The area of the bucket that face contacts the bucket receiving surface 25 is shown by a contact area 48, which is substantially half of an upper side of the contact surface 32a of the bucket 30. In such a way, when the rotating speed of the swing rotor 20 is sufficiently high, the centrifugal load of the bucket 30 is received by a wide area of the bucket receiving surface 25 formed in the rotor body 21. Thus, the centrifugal load applied to the bucket portion 30 does not act on the pivot pins 34. In the present exemplary embodiment, even when the bucket 30 is located in the horizontal position, the pivot pins 34 are not restrained from not only moving in the direction of a bucket central axis 51 (a longitudinal direction), but also moving in the direction of rotating about the bucket central axis 51.
As described above, since a degree of freedom of the pivot pins 34 is increased relative to a body portion of the bucket 30, even if the centrifugal load may be increased so that the bucket 30 is swung not in an ideal state, but in a slightly obliquely twisted state and one side of the body portion of the bucket 30 may possibly initially abut on the bucket receiving surface 25, load is not applied to the pivot pins 34. That is, even when the load is occasionally applied to the pivot pins 34, the pivot pins 34 are rotated in the axial direction or in the rotating direction so that such a load may be avoided from being applied to the pivot pins 34. As a result, the bucket 30 is not restrained by the pivot pins 34 and can be guided to a position where the contact surface 32a effectively comes into face contact with the bucket receiving surface 25.
Hereinafter, detailed structure of the bucket 30 will be described by referring to
A cap main body 33 as a main portion of the cap assembly 31 serves as a cover for sealing an inner space of the bucket body 32 and is attached to the opening portion 32c of the bucket body 32 by screwing. The cap main body 33 is manufactured, for instance, by scraping a metal alloy such as aluminum, and has an external threaded portion 33d formed in a lower portion which is screwed to the internal threaded portion of the bucket body 32. In an upper portion of the cap main body 33, the pivot pins 34 are provided which are inserted into the pin insert grooves 23 formed in the swing rotor 20. In an upper portion of the pivot pins 34, one or more wave washers 36 are inserted and the stopper 37 is attached from an upper portion thereof. In the present exemplary embodiment, three wave washers 36 are inserted. The number of the wave washers 36 may be suitably set by considering the maximum rotating speed of a centrifugal separation or the weight of the bucket. At a central portion of the stopper 37, a screw-hole is opened and the stopper is fixed to the cap main body 33 by a screw 38. The pivot pins 34 are supported so that the pivot pins may be rotated about the bucket central axis 51 (a longitudinal central axis: a longitudinal direction of the screw 38) of the bucket 30. In the cap assembly 31 of the present exemplary embodiment, since the pivot pins 34 rotate about the bucket central axis 51, which is different from the cap assembly 131 of the related-art shown in
The hollow circle ring 39 contacts an outer circumferential surface of a cylindrical hollow portion provided lower to an external threaded portion 33d, which will be described later, of the cap main body 33, so as to seal the inner space 32e. A threaded portion is not formed to the outer circumferential surface of the cylindrical hollow portion to which the hollow circle ring 39 contacts.
The cap main body 33 includes a cover portion 33c serving as the cover, a cylindrical portion 33a formed in an upper portion of the cover portion 33c and a cylindrical hollow portion 33e formed in a lower portion of the cover portion 33c. The external threaded portion 33d is formed in an outer peripheral portion of the cylindrical form. At a center of an upper portion of the cylindrical portion 33a, a screw-hole 33f is formed and the stopper 37 is fixed to the cylindrical portion 33a by the screw 38. In
The pivot pin 34 are manufactured by scraping metal such as a titanium alloy and two shaft portions 34b are formed which extend outward from an annular member having a through-hole 34a. The shaft portions 34b serve as swing shafts. The directions in which the shaft portions 34b are extended are located on one straight line, opposite to each other and perpendicular to the bucket central axis (the longitudinal central axis) 51 of the bucket 30. An inside diameter of the through-hole 34a formed in the pivot pin 34 is formed to be a little larger than an outside diameter of the cylindrical portion 33a so that the pivot pin 34 may be smoothly rotated relative to the cap main body 33 and may be moved in the longitudinal direction of the bucket 30.
In an upper portion of the pivot pin portions 34, one to several wave washers 36 are inserted and the stopper 37 is fixed to an upper portion thereof. The stopper 37 has a through-hole 37a and a screw portion of the screw 38 passing through the through-hole 37a is screwed to the screw-hole 33f formed on an upper end of the cylindrical portion 33a of the cap main body 33 to fix the stopper. In such a way, the pivot pin portions 34 are prevented from slipping out by the stopper 37 attached to the terminal end of the cylindrical portion 33a through the wave washers 36.
In the present exemplary embodiment, since the pivot pin portions 34 serving as the swing shafts can be longitudinally moved relative to the bucket body 32 and rotated about the bucket central axis 51, the degree of freedom of the movement of the pivot pin portions 34 relative to the bucket body 32 can be increased. As a result, since a torsional torque is not transmitted to the cap assembly 31 from the pivot pin portions 34, in the bucket for the swing rotor of a structure in which the weight of the bucket is supported by the rotor body during a rotation at high speed, the structure, in which the fastening of the cap assembly is not influenced even when an abutment of a seated surface of the bucket is nonuniform, is realized.
Further, since an unfastening operation or a tightening operation is not applied to the screw portion of the cap assembly 31 during a centrifugal separation, even when the cap assembly 31 is fastened to the bucket body 32 by the screw, it can be avoided that the cap assembly 31 is unfastened or the cap assembly 31 is difficult to be detached from the bucket body 32 due to the tightening operation, after the centrifugal separating operation. Further, in the cap assembly having an elastic body (the wave washer) to ensure a prescribed clearance between the rotor body and the bucket while the bucket is swung to be seated on the rotor body, the same function can be achieved by using five portions compared to six portions used in a related-art product. That is, the same function can be achieved by a smaller number of portions compared to that of the related-art product. Thus, a product having the same quality as that of the related-art product can be manufactured by lower cost.
According to the above-described disclosure, about a centrifugal separator including a bucket which can be swung on a swing shaft and having a contact surface which contacts a rotor body during centrifugal separation, since the swing shaft can be moved in a longitudinal direction of the bucket relative to a bucket body and rotated by a prescribed angle or more about a longitudinal central axis of the bucket, the flexibility of a pivot pin that moves relative to the bucket body can be increased. As a result, even when a centrifugal load is increased so that the bucket is swung not in an ideal state, but in a slightly obliquely twisted state, the bucket is not restrained by the pivot pin and can be guided to a position where the contact surface effectively comes into face contact with a bucket receiving surface.
Further, according to the above-described disclosure, since the swing shaft can be rotated by a prescribed angle or more about the longitudinal central axis of the bucket relative to the bucket body, a position of the bucket body that comes into contact with the bucket receiving surface of the swing rotor can be distributed. Thus, the operating life of the bucket can be greatly extended.
Further, according to the above-described disclosure, since the swing shaft can be continuously rotated about the longitudinal central axis of the bucket, relative to the bucket body, a position of the bucket body that comes into contact with the bucket receiving surface of the swing rotor is not the same. Thus, the operating life of the bucket can be greatly extended.
Further, according to the above-described disclosure, since a cap assembly is provided with a rotating portion for rotating the cap assembly relative to the bucket body, the cap assembly can be easily fastened or unfastened relative to the bucket body by rotating the rotating portion, without using the swing shaft.
Further, according to the above-described disclosure, since the swing shaft has two shaft portions extending in opposed directions from an annular member, and the cylindrical portion penetrates the annular member so as to support the swing shaft, the swing shaft can be easily manufactured and has a sufficient strength. Further, in an assembling operation of the bucket, a work such as a pressing-in operation is not necessary, so that the bucket can be easily assembled.
Further, according to the above-described disclosure, since a wave washer is arranged in an upper side of the swing shaft, and, a stopper member that fixes the swing shaft and the wave washer to the cylindrical portion is provided to an upper side of the wave washer, the bucket body can be held so as not to come into contact with the swing rotor during a swing operation by an urging operation of the wave washer. Thus, the swing operation can be smoothly carried out.
Further, according to the above-described disclosure, since an external threaded portion is formed in a lower portion of the cover portion, an internal threaded portion is formed in an inner peripheral side of the opening portion of the bucket body and the cap assembly is screwed to the bucket body with an hollow circle ring sandwiched therebetween, an inside of the bucket rotated under a pressure reduced condition can be sealed from external. Thus, a sample can be prevented from leaking from the bucket.
The present invention has been described in accordance with the exemplary embodiment. However, the present invention is not limited to the above-described exemplary embodiment, and various changes may be made therein without departing form the spirit and scope of the invention. For instance, an attaching method of the pivot pin to the cap main body is not limited to the method described in the exemplary embodiment. If a pivot pin is formed so as to move in the longitudinal direction of the bucket body and rotate by a prescribed angle or more about the bucket central axis, other arbitrary structures or attaching methods may be employed.
Number | Date | Country | Kind |
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2010-012812 | Jan 2010 | JP | national |