The instant disclosure relates to centrifuges, and in particular to a disposable cartridge for use with a centrifuge enabling automatic discharge of solids that accumulate during separation.
Many different types of centrifugal separators are known for separating heterogeneous mixtures into components based on specific gravity. A heterogeneous mixture, which may also be referred to as feed material or feed liquid, is injected into a rotating bowl of the separator. The bowl rotates at high speeds and forces particles of the mixture, having a higher specific gravity, to separate from the liquid by sedimentation. As a result, a dense solids cake compresses tightly against the surface of the bowl, and the clarified liquid, or “centrate”, forms radially inward from the solids cake. The bowl may rotate at speeds sufficient to produce forces 20,000 times greater than gravity to separate the solids from the centrate. The solids accumulate along the wall of the bowl, and the centrate is drained off. Once it is determined that a desired amount of the solids has been accumulated, the separator is placed in a discharge mode. Various types of scrapers may be used to scrape sides of the bowl towards a discharge outlet in the bottom. The discharge outlet typically includes a valve that may be operated manually or automatically so that solids may exit the bowl and be collected in a separate container.
A centrifugal separator may include a cylindrical separator bowl, a core tube assembly for introducing a feed fluid and removing centrate, and an annular piston for extruding accumulated solids through a shuttle valve in the bottom of the bowl following centrifugation. A representative centrifugal separator is shown and described in U.S. Pat. No. 10,449,555, incorporated by reference and shown in
Core tube assembly 16 includes a pull rod 20 inside a pull rod support 22. A feed liquid port 23 above the separator housing 14 is in communication with a feed tube 24 inside of pull rod 20. Pull rod 20 is operably connected to a shuttle valve 26 in the lower portion of separator bowl 10, and is described in further detail below. The lower end of feed tube 24 is coupled to shuttle valve 26 which is proximate an opening in the lower end of separator bowl 10, and may be opened and closed via pull rod 20.
Also shown in
The centrifugal separator includes main shaft 32 on the upper portion of cylindrical separator bowl 10. Main shaft 32 operatively connects to a spherically mounted bearing and spindle assembly 40. A drive belt 33 is operatively coupled to a drive motor (not shown) that may be controllably operated to rotate the separator bowl 10 at desired speeds for separating the feed liquid. Separators described herein can also be operated using other motor and drive systems. A seal assembly 34 for main shaft 32 is also shown in
As shown in
After a quantity of feed material has been separated, it is necessary to clean and sterilize the separator. This tends to be difficult in conventional separators without significantly increasing maintenance costs, especially for companies who may use one machine for several different processes, thus requiring frequent cleaning and sterilization.
It is desirable to have a centrifugal separator that uses a disposable separator bowl liner. There is a further need to load new liners and unload used liners with minimal interaction from an operator to minimize external contamination.
The present disclosure provides a disposable cartridge for a centrifugal separator for separating sticky solids from a feed liquid and discharging the accumulated solids. In one aspect, the a centrifugal separator includes a separator housing, a spindle assembly, a main shaft retained within the spindle assembly for rotation therein and a cylindrical separator bowl, the cylindrical separator bowl having an upper end coupled to the main shaft and a lower end with an opening, the cylindrical separator bowl suspended within the separator housing from the main shaft and operative during a separation mode of operation to rotate at a high speed relative to the spindle assembly to separate feed liquid into centrate and solids, and the disposable cartridge includes a unitary bowl and support structure having a stainless steel cylindrical liner portion conforming to an inner wall of the cylindrical separator bowl and having an opening at the lower end thereof, a shaft liner conforming to an inner wall of the main shaft and in mechanical communication with the cylindrical liner portion at an upper extent thereof, and a pull rod support disposed axially along the interior length of the cylindrical separator bowl and in mechanical communication with the shaft liner at a lower extent thereof and the cylindrical bowl liner portion at a lower extent thereof; a pull rod disposed axially along the interior length of the pull rod support and the shaft liner and comprising a shuttle valve operative for axial movement relative to the pull rod support to open and close the opening in the lower end of the cylindrical liner portion; and an annular piston disposed between an inner surface of the cylindrical liner portion and an outer surface of the pull rod support, the annular piston being operative for axial movement to selectively discharge solids out of the opening in the lower end of the cylindrical liner portion.
In a further embodiment, the pull rod includes a feed tube along a first interior length of the pull rod and a feed bore along a second interior length of the pull rod, the feed tube and feed bore forming a feed flow path through the length of the pull rod and wherein the feed flow path is in fluid communication with the interior of the cylindrical liner portion when the shuttle valve has closed the opening in the lower end of the cylindrical liner portion.
In another embodiment, the feed flow path is in fluid communication with the interior of the cylindrical liner portion via at least one feed acceleration channel disposed in the shuttle valve. Further, the pull rod support includes at least one slot intermediate the interior of the cylindrical liner portion and the opening in the lower end of the cylindrical liner portion, wherein solids may be extruded out of the opening in the lower end of the cylindrical liner portion through the at least one slot by the annular piston when the lower portion of the shuttle valve has opened the opening in the lower end of the cylindrical liner portion.
In yet another embodiment, the pull rod support includes plural lateral centrate passages, each having an opening on the outer surface of the pull rod support, wherein the pull rod comprises a centrate channel intermediate a feed tube outer surface and a pull rod inner surface, the plural centrate passages being in fluid communication with the centrate channel, and wherein the centrate channel is in fluid communication with a centrate port, thereby allowing removal of centrate from the cylindrical liner portion.
In any of the above embodiments, the disposable cartridge further includes at least one coupler at an upper end of the shaft liner for coupling to a feed port and a centrate port.
In any of the above embodiments, the annular piston includes at least one magnet, and the separator housing comprises an array of magnetic sensors for detecting the position of the annular piston through selective interaction with the at least one annular piston magnet.
In any of the above embodiments, the lower end of the cylindrical liner portion and a lower portion of the annular piston are complementarily shaped.
In any of the above embodiments, wherein the lower end of the cylindrical liner portion and the lower portion of the annular piston are substantially conically shaped.
In an embodiment, a method for discharging solids from a centrifugal separator comprising a disposable cartridge includes providing a centrifugal separator comprising a separator housing and a cylindrical separator bowl, the cylindrical separator bowl having an upper end, and a lower end with an opening, the cylindrical separator bowl disposed in the separator housing and operative during a separation mode of operation to rotate at a high speed to separate feed liquid into centrate and solids; providing a disposable cartridge including a cylindrical liner conforming to an inner wall of the cylindrical separator bowl; shaft liner conforming to the main shaft; a pull rod support in mechanical communication with the shaft liner at a lower extent thereof and with the cylindrical liner at a lower extent thereof and disposed axially along the interior length of the disposable cartridge, the core tube assembly comprising a shuttle valve operative for axial movement to open and close an opening in the lower end of the cylindrical separator bowl; an annular piston disposed between an inner surface of the cylindrical liner and an outer surface of the core tube assembly, the annular piston being operative for axial movement to discharge solids out of the opening in the lower end of the disposable bowl liner; a process seal coupler operatively coupled to an upper end of the shaft liner; and a cap for securing a lower end of the cylindrical liner within the cylindrical separator bowl; securing the disposable cartridge within the cylindrical separator bowl via the process seal coupler and the cap; and introducing gas to press against an upper surface of the annular piston to drive the annular piston downward to discharge solids accumulated within the cylindrical liner through the opening in the lower end of the cylindrical liner portion.
In a further embodiment, the pull rod support further includes a pull rod disposed axially along the interior length of the pull rod support and the shaft liner and in mechanical communication with the shuttle valve at a respective lower extent thereof, wherein the pull rod comprises a feed tube along a first interior length of the pull rod and a feed bore along a second interior length of the pull rod, the feed tube and feed bore forming a feed flow path through the length of the pull rod and wherein the feed flow path is in fluid communication with the interior of the cylindrical liner when the shuttle valve has closed the opening in the lower end of the cylindrical liner, the method further including selectively positioning the pull rod in a downward position whereby the shuttle valve has closed the opening in the lower end of the cylindrical liner; flowing feed liquid having a solids component suspended therein through the feed flow path and into the interior of the cylindrical liner via the shuttle valve; and rotating the cylindrical separator bowl whereby the feed liquid is separated into solids that accumulate on an inner surface of the cylindrical liner below the annular piston and centrate.
In another embodiment, the method includes drawing the pull rod upwardly within the pull rod support prior to the step of introducing gas to press against an upper surface of the annular piston support, whereby the shuttle valve has opened the opening in the lower end of the disposable bowl liner.
In a further embodiment, flowing the feed liquid further includes flowing the feed liquid into the interior of the cylindrical liner via at least one feed acceleration channel disposed in the shuttle valve.
In a further embodiment, the pull rod support includes plural lateral centrate passages, each having an opening on the outer surface of the pull rod support, and a centrate channel intermediate a feed tube outer surface and a pull rod inner surface, the plural centrate passages being in fluid communication with the centrate channel, and the method further includes flowing the centrate through the plural centrate passages, into the centrate channel, and to an exit thereof.
In yet another embodiment, the method includes stopping the rotation of the cylindrical separator bowl prior to the step of introducing gas to press against an upper surface of the annular piston.
In any of the above embodiments, the method includes after the step of introducing gas to press against an upper surface of the annular piston, removing the process seal coupler and the cap from the disposable cartridge and removing the disposable cartridge from the cylindrical separator bowl.
The centrifugal separator of
A disposable bottom cap 78 is attached to housing 14 to help secure cartridge 70 in the centrifugal separator 104. Bottom cap 78 also includes solids discharge outlet 80 and cartridge leakage drain 82. A tight labyrinth gap 91 is formed between disposable bottom cap 78 and clamp ring 77 to help prevent solid and centrate from leaking from solids discharge outlet 80 into central region 11 of housing 14. In embodiments, hand nut 74, bowl adapter ring 76, clamp ring 77 and bottom cap 78 may be fabricated from Class VI plastic materials.
Cartridge 70 includes a cylindrical liner portion 84 adapted to fit within separator bowl 10 and a shaft liner 86 adapted to fit within main shaft 32. Core tube assembly 88 is disposed axially along the interior length of assembly 70. Core tube assembly 88 includes pull rod 87 disposed within pull rod support 85. Shuttle valve 90 is located at a lower end of liner portion 84 and may be opened and closed using pull rod 87. Annular piston 92 is disposed within the cylindrical liner portion 84 and is used to remove solids from disposable cartridge 70. Gas passages 94 in cartridge 70 communicate with gas passages 56 in separator bowl 10 via a recessed shoulder ring 57 at the upper extent of the cylindrical liner portion 84 so that compressed gas injected into discharge case 50 may force annular piston 94 downward to remove solids when shuttle valve 90 is raised and opened by core tube assembly 88. The recessed shoulder ring 57 enables communication between the gas passages 56 and gas passages 94 without requiring alignment therebetween.
Solids discharge outlet 80 receives solids from disposable cartridge 70. In embodiments, outlet 80 may discharge solids to a variety of containers, such as an Ezi-Dock® aseptic valve with a plastic paste collection bag, or a paste bag with disposable re-suspension agitator from Pall Corporation.
With reference to
Due to the high rate of speed achieved by centrifugal separator 104, vibration bushings 117 and 119 are provided to isolate support frame 105. The flexibility afforded by vibration bushings 117 and 119 may make it difficult to insert disposable cartridge 70. Frame and case motion lock cylinder 118 prevents support frame 105 and housing 14 from moving while the cartridge 70 is removed or inserted. After cartridge 70 is inserted in centrifuge 104, hand nut 74 (
The operation of disposable cartridge 70 with a centrifugal separator will now be described. In embodiments,
During a fill mode of operation, cartridge 70 (and separator bowl 10) are not spinning, as it is being filled with feed fluid or buffer liquid. Isolation valve 54 is open, allowing gas (e.g. air) to pass between the discharge case 50 and central region 11. Shuttle valve 90 is urged into a closed position within the opening in the lower end of the cylindrical liner portion 84 by operation of the shuttle valve actuator 130 and by pressure provided by spring 132, located between pull rod 87 and pull rod support 85. Feed fluid is introduced through feed port 60 and down through feed tube 136, exiting into the lower end of the cylindrical liner portion 84 through feed acceleration channels 144 of shuttle valve 90. The feed acceleration channels 144 are angled slightly upward, at the same angle as the lower end of the cylindrical liner portion 84, to create angular acceleration of feed liquid as it enters the cylindrical liner portion 84. Cylinders 135 may be machined inside core tube assembly 88 to reduce weight. In embodiments, there may be 2-8 cylinders around the circumference of core tube assembly 88.
At the beginning of the bowl fill mode, annular piston 92 is positioned at the bottom of the cylindrical liner portion 84. As feed fluid is introduced into the cylindrical liner portion 84, the increasing volume of feed liquid inside the cylindrical liner portion 84 urges annular piston 92 upward, minimizing air contact with the feed liquid. This lack of air/liquid interface reduces foaming and oxidation of the feed liquid and thus ensuring the solids in the feed liquid are better preserved during the separation process.
Next, during separation mode, separator bowl 10 together with disposable cartridge 70 are spun at high speed by motor 146 and drive belt 148 to separate solid particles suspended in the feed liquid. As the feed liquid exits feed acceleration channels 144 into the cylindrical liner portion 84, Coriolis acceleration effects track the feed liquid along the outer diameter of core tube assembly 88 to the top of the cylindrical liner portion 84 and into at least one centrate passage 150 which terminates in a ring-shaped depression in pull rod support 85. The presence of a ring-shaped depression allows some alignment flexibility between centrate passage 150 and a corresponding centrate passage in pull rod 87. The centrate continues into a corresponding centrate passage 154 in the pull rod 87, travels up centrate tube 152 between shaft liner 86 and feed tube 136, then out of the centrifugal separator via centrate ports 62. O-ring seals that are above and below the exterior termination of 154 and are also on the pull rod 87 to seal passages 150 when the pull rod 87 is pulled upward.
Separated solids collect on the inner diameter of the cylindrical liner portion 84, packing into a cake with paste-like consistency. As centrate is removed, additional feed liquid may be introduced via feed tube 136. The sedimentation of feed liquid may continue until the desired bowl volume of solids is reached (e.g., 25% to 98% of bowl volume filled with solids). In embodiments, other methods of determining when to stop providing feed liquid to the cylindrical liner portion 84 may also be used.
Finally, in solids discharge mode, rotation ceases and shuttle valve actuator 130 is actuated to open shuttle valve 90, while compressing spring 132 as shown on the right side of
Isolation valve 54 is closed while gas (e.g. air) pumped into gas port 52 and through passage 56 urges annular piston 92 downward. O-ring seal 155 is provided to provide a seal between the annular piston 92 and cylindrical liner portion 84 and pull rod support 85. As annular piston 92 moves downward through cylindrical liner portion 84, accumulated solids are extruded through slots 134 then out of opening 80. Once the annular piston 92 has reached the bottom of its stroke, shuttle valve 90 is closed using shuttle valve actuator 130 and/or spring 132. The process of closing shuttle valve 90 covers slots 134 in core tube assembly 88 with the outer surface of shuttle valve 90, and thereby severs any remaining tube of accumulated solids paste hanging from the opening in cylindrical liner portion 84.
Annular piston 92 includes magnet 156 which may be used by reed switches or corresponding magnetic sensors disposed along the outside of housing 14 to sense a position of annular piston 92 as it moves up and down within the cylindrical liner portion 84. Magnetic sensors may be placed in a variety of locations inside or outside of housing 14 as long as they are able to sense the vertical position of magnet 156. These sensors enable an associated controller to have an accurate determination of the position of the annular piston 92 within the cylindrical liner portion 84.
While the present invention has been described in conjunction with a preferred embodiment, one of ordinary skill in the art, after reading the foregoing specification, will be able to effect various changes, substitutions of equivalents and other alterations to the compositions, articles, methods and apparatuses set forth herein. For example, fluid pressure may be replaced in other embodiments by, without limitation, an electromechanical force. Similarly, the lower portion and end of the piston and bowl, respectively, may not be conical in shape, although it is preferable for solids recovery that their shapes be complimentary.
Moreover, the invention also contemplates that the various passages, valves, pistons, actuators, assemblies, ports, members and the like described herein can be in any configuration or arrangement that would be suitable for operation of a centrifugal separator. The embodiments described above may also each include or incorporate any of the variations of all other embodiments. It is therefore intended that the protection granted by Letter Patent hereon be limited only by the definitions contained in the appended claims and equivalents thereof.
This application claims the benefit of priority to U.S. Patent Application No. 62/875,690, filed on Jul. 18, 2019, the entire disclosure of which is incorporated herein by reference.
Number | Date | Country | |
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62875690 | Jul 2019 | US |