The present inventive concept relates to the field of centrifugal separators. More particularly it relates to an exchangeable separation insert for a centrifugal separator for separating a fluid mixture, and a centrifugal separator comprising such an exchangeable separation insert.
Centrifugal separators are generally used for separation of liquids and/or solids from a liquid mixture or a gas mixture. During operation, fluid mixture that is about to be separated is introduced into a rotating bowl and due to the centrifugal forces, heavy particles or denser liquid, such as water, accumulates at the periphery of the rotating bowl whereas less dense liquid accumulates closer to the central axis of rotation. This allows for collection of the separated fractions, e.g. by means of different outlets arranged at the periphery and close to the rotational axis, respectively.
When processing pharmaceutical products such as fermentation broths, it may be desirable to eliminate the need for cleaning-in-place processes of the rotating bowl and the separator parts that have contacted the processed product. More useful may be to exchange the rotating bowl as a whole, i.e. to use a single use solution. This is advantageous from a hygienic perspective of the process.
WO 2015/181177 discloses a separator for the centrifugal processing of a flowable product comprising a rotatable outer drum and an exchangeable inner drum arranged in the outer drum. The inner drum comprises means for clarifying the flowable product. The outer drum is driven via drive spindle by a motor arranged below the outer drum. The inner drum extends vertically upwardly through the outer drum which has fluid connections arranged at an upper end of the separator.
However, there is a need in the art for single use solutions for centrifugal separation that are compact and easy to handle for an operator.
It is an object of the invention to at least partly overcome one or more limitations of the prior art. In particular it is an object to provide an exchangeable separation insert that is compact and allows for increased manoeuvrability and handling for the operator.
Thus, an exchangeable separation insert for a centrifugal separator comprises a rotor casing enclosing a separation space in which a stack of separation discs is arranged to rotate around an axis of rotation. Said rotor casing is axially arranged between a first and a second stationary portion. The insert comprises further a feed inlet for supply of the fluid mixture to be separated to said separation space, a light phase outlet for discharge of a separated phase of a first density, and a heavy phase outlet for discharge of a separated phase of a second density higher than said first density.
Two of said feed inlet, light phase outlet and heavy phase outlet are arranged at a first axial end of said rotor casing. A first seal assembly is sealing and connecting said two of said feed inlet, light phase outlet and heavy phase outlet to corresponding inlet conduit and/or outlet conduits in said first stationary portion.
Said first seal assembly comprises a rotatable part attached to said rotor casing and a stationary part attached to said stationary portion.
Said rotatable part and said stationary part are axially aligned and seal against each other.
A first of said two of said feed inlet, light phase outlet and heavy phase outlet is arranged axially at the axis of rotation and a second of said two of said feed inlet, light phase outlet and heavy phase outlet is arranged axially outside of said first of said two of said feed inlet, light phase outlet and heavy phase outlet in such a manner that both said first and second of said two of said feed inlet, light phase outlet and heavy phase outlet are led through said rotatable part and said corresponding inlet conduit and/or outlet conduits are led through said stationary part of said first seal assembly.
Said light phase outlet may be arranged at said first axial end.
Said feed inlet may be arranged at said first axial end.
Said stationary heavy phase outlet may be arranged at said first axial end.
Said rotatable part may be a plate-formed seal element with a centre-hole for said feed inlet and at least one outlet-hole for one of the light phase or heavy phase outlets.
Said stationary part may comprise two concentrically arranged ring-formed seal elements.
The inner of said ring-formed seal elements may be arranged to engage with the rotatable part axially outside said centre-hole and axially inside said at least one outlet-hole.
At least one fluid connection may be formed within at least the inner of said two ring-formed seal elements.
At least the inner of said two ring-formed seal elements has a recess in its surface facing said rotatable part of said seal assembly, which recess is connected to said at least one fluid connection.
The at least one fluid connection may comprise a seal fluid inlet for supplying fluid to the at least one of said recesses.
The at least one fluid connection may also comprise a seal fluid outlet for removing fluid from the at least one of said recesses.
Said seal fluid inlet and said seal fluid outlet may both be attached to a container forming a closed circulation system.
A pump may be arranged in said seal fluid inlet to supply liquid to said first seal assembly.
Said container may be pre-pressurized to supply liquid to said first seal assembly.
The exchangeable separation insert is configured to be inserted and secured within a rotatable member journaled in a stationary frame, both comprised by the centrifugal separator.
According to another aspect of the invention a centrifugal separator comprises a stationary frame and a rotatable member journaled in said stationary frame, comprising an exchangeable separation insert, which exchangeable separation insert is arranged in such manner that said rotor casing is fitted in said rotatable member, and said first and second stationary portions are fitted in said stationary frame.
The above, as well as additional objects, features and advantages of the present inventive concept, will be better understood through the following illustrative and non-limiting detailed description, with reference to the appended drawings. In the drawings like reference numerals will be used for like elements unless stated otherwise.
The feed inlet is in this example arranged at the first axial lower end 5, and the feed is supplied via a stationary inlet conduit 7 arranged in the first stationary portion 3. The stationary inlet conduit 7 is arranged at the rotational axis (X). The first stationary portion 3 further comprises a stationary outlet conduit 9 for the separated liquid phase of lower density, also called the separated liquid light phase.
There is further a stationary outlet conduit 8 arranged in the upper stationary portion 4 for discharge of the separated phase of higher density, also called the liquid heavy phase. Thus, in this embodiment, the feed is supplied via the lower axial end 5, the separated light phase is discharged via the lower axial end 5, whereas the separated heavy phase is discharged via the upper axial end 6.
The outer surface of the rotor casing 2 comprises a first 10 and second 11 frustoconical portion. The first frustoconical portion 10 is arranged axially below the second frustoconical portion 11. The outer surface is arranged such that the imaginary apex of the first 10 and second 11 frustoconical portions both point in the same axial direction along the rotational axis (X), which in this case is axially down towards the lower axial end 5 of the insert 1.
Furthermore, the first frustoconical portion 10 has an opening angle that is larger than the opening angle of the second frustoconical portion 11. The opening angle of the first frustoconical portion 10 may be substantially the same as the opening angle of a stack of separation discs contained within the separation space 17 of the rotor casing 2. The opening angle of the second frustoconical portion 11 may be smaller than the opening angle of a stack of separation discs contained within the separation space of the rotor casing 2. As an example, the opening angle of the second frustoconical portion 11 may be such that the outer surface forms an angle α with rotational axis that is less than 10 degrees, such as less than 5 degrees. The rotor casing 2 having the two frustoconical portions 10 and 11 with imaginary apexes pointing downwards allows for the insert 1 to be inserted into a rotatable member 31 from above. Thus, the shape of the outer surface increases the compatibility with an external rotatable member 31, which may engage the whole, or part of the outer surface of the rotor casing 2, such as engage the first 10 and second 11 frustoconical portions.
There is a lower rotatable seal arranged within lower seal housing 12 which separates the rotor casing 2 from the first stationary portion 3 and an upper rotatable seal arranged within upper seal housing 13 which separates the rotor casing 2 from the second stationary portion 4. The axial position of the sealing interface within the lower seal housing 12 is denoted 15c, and the axial position of the sealing interface within the upper seal housing 13 is denoted 16c. Thus, the sealing interfaces formed between such stationary part 15a, 16a and rotatable part 15b, 16b of the first 15 and second 16 rotatable seals also form the interfaces or border between the rotor casing 2 and the first 15 and second 16 stationary portions of the insert 1.
There are further a seal fluid inlet 15d and a seal fluid outlet 15e for supplying and withdrawing a seal fluid, such as a cooling liquid, to the first rotatable seal 15 and in analogy, a seal fluid inlet 16d and a seal fluid outlet 16e for supplying and withdrawing a seal fluid, such as a cooling liquid, to the second rotatable seal 16.
Shown in
The exchangeable separation insert 1 has a compact form that increases the manoeuvrability and handling of the insert 1 by an operator. As an example, the axial distance between the separation space 17 and the first stationary portion 3 at the lower axial end 5 of the insert may be less than 20 cm, such as less than 15 cm. This distance is denoted d1 in
The exchangeable separation insert 1 is inserted and secured within rotatable member 31. The rotatable member 31 thus comprises an inner surface for engaging with the outer surface of the rotor casing 2. The upper and lower ball bearings 33a, 33b are both positioned axially below the separation space 17 within the rotor casing 2 such that the cylindrical portion 14 of the outer surface of the rotor casing 2 is positioned axially at the bearing planes. The cylindrical portion 14 thus facilitates mounting of the insert within at least one large ball bearing. The upper and lower ball bearings 33a, 33b may have an inner diameter of at least 80 mm, such as at least 120 mm.
Further, as seen in
Moreover, the separation insert is mounted within the separator 1 such that the axial lower end 5 of the insert 1 is positioned axially below the supporting means, i.e. the upper and lower bearings 33a, 33b. The rotor casing 2 is in this example arranged to be solely externally supported by the rotatable member 31. The separation insert 1 is further mounted within the separator 100 to allow easy access to the inlet and outlets at the top and bottom of the insert 1.
The feed inlet 20 is in this example arranged at the axial lower end 5, and the feed is supplied via a corresponding stationary inlet conduit 7 arranged in the first stationary portion 3. The stationary inlet conduit 7 may comprise a tubing, such as a plastic tubing.
The stationary inlet conduit 7 is arranged at the rotational axis (X) so that the material to be separated is supplied at the rotational centre. The feed inlet 20 is for receiving the fluid mixture to be separated.
The feed inlet 20 is in this embodiment arranged at the apex of an inlet cone 10a, which on the outside of the insert 1 also forms the first frustoconical outer surface 10. There is further a distributor 24 arranged in the feed inlet for distributing the fluid mixture from the inlet 20 to the separation space 17.
The separation space 17 comprises an outer heavy phase collection space 17c that extends axially from a first, lower axial position 17a to a second, upper axial position 17b. The separation space 17 further comprises a radially inner space formed by the interspaces between the separation discs of the stack 19.
The distributor 24 has in this embodiment a conical outer surface with the apex at the rotational axis (X) and pointing toward the lower end 5 of the insert 1. The outer surface of the distributor 24 has the same conical angle as the inlet cone 10a. There is further a plurality of distributing channels 24a extending along the outer surface for guiding the fluid mixture to be separated continuously axially upwards from an axially lower position at the inlet 20 to a radially upper position in the separation space 17. This axially upper position is substantially the same as the first, lower axial position 17a of the heavy phase collection space 17c of the separation space 17. The distribution channels 24a may for example have a straight shape or a curved shape, and thus extend between the outer surface of the distributor 24 and the inlet cone 10a. The distribution channels 24a may be diverging from an axial lower position to an axial upper position. Furthermore, the distribution channels 24a may be in the form of tubes extending from an axial lower position to an axial upper position.
There is further a stack 19 of frustoconical separation discs arranged coaxially in the separation space 17. The separation discs in the stack 19 are arranged with the imaginary apex pointing to the axially lower end 5 of the separation insert 1, i.e. towards the inlet 20. The imaginary apex 18 of the lowermost separation disc in the stack 19 may be arranged at a distance that is less than 10 cm from the first stationary portion 3 in the axial lower end 5 of the insert 1. The stack 19 may comprise at least 20 separation discs, such as at least 40 separation discs, such as at least 50 separation discs, such as at least 100 separation discs, such as at least 150 separation discs. For clarity reasons, only a few discs are shown in
The heavy phase collection space 17c of the separation space 17 has in this embodiment an inner diameter that continuously increases from the first, lower axial position 17a to the second, upper axial position 17b. There is further an outlet conduit 23 for transporting a separated heavy phase from the separation space 17. This conduit 23 extends from a radially outer position of the separation space 17 to the heavy phase outlet 22. In this example, the conduit 23 is in the form of a single pipe extending from a central position radially out into the separation space 17. However, there may be at least two such outlet conduits 23, such as at least three, such as at least five, outlet conduits 23. The outlet conduit 23 has thus a conduit inlet 23a arranged at a radially outer position and a conduit outlet 23b at a radially inner position, and the outlet conduit 23 is arranged with an upward tilt from the conduit inlet 23a to the conduit outlet 23b. As an example, the outlet conduit 23 may be tilted with an upward tilt of at least 2 degrees, such as at least five degrees, such as at least ten degrees, relative the radial plane.
The outlet conduit 23 is arranged at an axially upper position in the separation space 17, such that the outlet conduit inlet 23a is arranged for transporting separated heavy phase from the axially uppermost position 17b of the separation space 17. The outlet conduit 23 further extends radially out into the separation space 17 so that outlet conduit inlet 23a is arranged for transporting separated heavy phase from the periphery of the separation space 17, i.e. from the radially outermost position in the separation space 17 at the inner surface of the separation space 17.
The conduit outlet 23b of the stationary outlet conduit 23 ends at the heavy phase outlet 22, which is connected to a corresponding stationary outlet conduit 8 arranged in the second, upper stationary portion 4. Separated heavy phase is thus discharged via the top, i.e. at the upper axial end 6, of the separation insert 1.
Furthermore, separated liquid light phase, which has passed radially inwards in the separation space 17 through the stack of separation discs 19, is collected in the liquid light phase outlet 21 arranged at the axially lower end of the rotor casing 2. The liquid light phase outlet 21 is connected to a corresponding stationary outlet conduit 9 arranged in the first, lower stationary portion 3 of the insert 1. Thus, separated liquid light phase is discharged via the first, lower, axial end 5 of the exchangeable separation insert 1.
The stationary outlet conduit 9 arranged in the first stationary portion 3 and the stationary heavy phase outlet conduit 8 arranged in the second stationary portion 4 may comprise tubing, such as plastic tubing.
In
The lower rotatable seal 15 may be attached directly to the inlet cone 10a without any additional inlet pipe, i.e. the feed inlet 20 may be formed at the apex of the inlet cone 10a directly axially above the lower first rotatable seal 15. Such an arrangement enables a firm attachment of the lower first mechanical seal 15 at a large diameter to minimize axial run-out.
The lower first rotatable seal 15 seals and connects both the inlet 20 to the stationary inlet conduit 7 and seals and connects the liquid light phase outlet 21 to the stationary liquid light phase conduit 9. The lower first rotatable 15 seal thus forms a concentric double mechanical seal, which allows for easy assembly with few parts.
The lower first rotatable seal 15 comprises a stationary part 15a arranged in the first stationary portion 3 of the insert 1 and a rotatable part 15b arranged in the axially lower portion of the rotor casing 2. The rotatable part 15b comprises in the embodiment shown in
In analogy,
Furthermore,
Moreover, during transport, there is an upper securing means 27a, b that secures the position of the second stationary portion 4 relative the rotor casing 2. The upper securing means is in the form of an engagement member 27a arranged on the rotor casing 2 that engages with an engagement member 27b on the second stationary portion 4, thereby securing the axial position of the second stationary portion 4. Further, there is a sleeve member 26 arranged in a transport or setup position in sealing abutment with the rotor casing 2 and the second stationary portion 4. The sleeve member 26 is further resilient and may be in the form of a rubber sleeve. The sleeve member 26 is removable from the transport or setup position for permitting the rotor casing 2 to rotate in relation to the second stationary portion 4. Thus, the sleeve member 26 seals radially against the rotor casing 2 and radially against the second stationary portion 4 in the setup or transport position. Upon mounting the exchangeable insert 1 in a rotating assembly, the sleeve member 26 may be removed and an axial space between engagement members 27a and 27b may be created in order to allow rotation of the rotor casing 2 relative the second stationary portion 4.
The lower and upper rotatable seals 15, 16 are mechanical seals, hermetically sealing the inlet and the two outlets. During operation, the exchangeable separation insert 1, inserted into a rotatable member 31, is brought into rotation around rotational axis (X). Liquid mixture to be separated is supplied via stationary inlet conduit 7 to the inlet 20 of the insert, and is then guided by the distributing channels 24a of the distributor 24 to the separation space 17. Thus, the liquid mixture to be separated is guided solely along an axially upwards path from the inlet conduit 7 to the separation space 17. Due to a density difference the liquid mixture is separated into a liquid light phase and a liquid heavy phase. This separation is facilitated by the interspaces between the separation discs of the stack 19 fitted in the separation space 17. The separated liquid heavy phase is collected from the periphery of the separation space 17 by outlet conduit 23 and is forced out via the heavy phase outlet 22 arranged at the rotational axis (X) to the stationary heavy phase outlet conduit 8. Separated liquid light phase is forced radially inwards through the stack 19 of separation discs and led via the liquid light phase outlet 21 out to the stationary light phase conduit 9.
Consequently, in this embodiment, the feed is supplied via the lower axial end 5, the separated light phase is discharged via the lower axial end 5, whereas the separated heavy phase is discharged via the upper axial end 6.
Further due to the arrangement of the feed inlet 20, distributor 24, stack 19 of separation discs and the outlet conduit 23 as disclosed above, the exchangeable separation insert 1 is de-aerated automatically, i.e. the presence of air-pockets is eliminated or decreased so that any air present within the rotor casing 2 is forced to travel unhindered upwards and out via the heavy phase outlet 22. Thus, at standstill, there are no air pockets, and if the insert 1 is filled up through the feed inlet 20 all air may be vented out through the heavy phase outlet 22. This also facilitates filling the separation insert 1 at standstill and start rotating the rotor casing 2 when liquid mixture to be separated or buffer fluid for the liquid mixture is present within the insert 1.
As also seen in
The rotor casing 2 has a mechanically hermetically sealed liquid outlet 21 for discharge of a separated liquid light phase, and a heavy phase outlet 22 for discharge of a phase of higher density than the separated liquid light phase. There is a single outlet conduit 23 in the form of a pipe for transporting separated heavy phase from the separation space 17. This conduit 23 extends from a radially outer position of the separation space 17 to the heavy phase outlet 22. The conduit 23 has a conduit inlet 23a arranged at the radially outer position and a conduit outlet 23b arranged at a radially inner position. Further the outlet conduit 23 is arranged with an upward tilt relative the radial plane from the conduit inlet 23a to the conduit outlet 23b.
There is also a mechanically hermetically sealed inlet 20 for supply of the liquid mixture to be processed to said separation space 17. The inlet 20 is in this embodiment connected to a central duct 41 extending through the spindle 40, which thus takes the form of a hollow, tubular member. Introducing the liquid material from the bottom provides a gentle acceleration of the liquid material. The spindle 40 is further connected to a stationary inlet pipe 7 at the bottom axial end of the centrifugal separator 100 via a hermetic seal 15, such that the liquid mixture to be separated may be transported to the central duct 41, e.g. by means of a pump. The separated liquid light phase is in this embodiment discharged via an outer annular duct 42 in said spindle 40. Consequently, the separated liquid phase of lower density is discharged via the bottom of the separator 100.
A first mechanical hermetic seal 15 is arranged at the bottom end to seal the hollow spindle 40 to the stationary inlet pipe 7. The hermetic seal 15 is an annular seal that surrounds the bottom end of the spindle 40 and the stationary pipe 7. The first hermetic seal 15 is a concentric double seal that seals both the inlet 21 to the stationary inlet pipe 7 and the liquid light phase outlet 21 to a stationary outlet pipe 9. There is also a second mechanical hermetic seal 16 that seals the heavy phase outlet 22 at the top of the separator 100 to a stationary outlet pipe 8.
As seen in
The centrifugal separator 100 is further provided with a drive motor 34. This motor 34 may for example comprise a stationary element and a rotatable element, which rotatable element surrounds and is connected to the spindle 40 such that it transmits driving torque to the spindle 40 and hence to the rotor casing 2 during operation. The drive motor 34 may be an electric motor. Furthermore, the drive motor 34 may be connected to the spindle 40 by transmission means. The transmission means may be in the form of a worm gear which comprises a pinion and an element connected to the spindle 40 in order to receive driving torque. The transmission means may alternatively take the form of a propeller shaft, drive belts or the like, and the drive motor 34 may alternatively be connected directly to the spindle 40.
During operation of the separator in
In the hermetic type of inlet 20, the acceleration of the liquid material is initiated at a small radius and is gradually increased while the liquid leaves the inlet 20 and enters the separation space 17. The separation space 17 is intended to be completely filled with liquid during operation. In principle, this means that preferably no air or free liquid surfaces is meant to be present within the rotor casing 2. However, liquid mixture may be introduced when the rotor is already running at its operational speed or at standstill. Liquid mixture may thus be continuously introduced into the rotor casing 2.
Due to a density difference, the liquid mixture is separated into a liquid light phase and a heavy phase. This separation is facilitated by the interspaces between the separation discs of the stack 19 fitted in the separation space 17. The separated heavy phase is collected from the periphery of the separation space 17 by conduit 23 and forced out through outlet 22 arranged at the rotational axis (X), whereas separated liquid light phase is forced radially inwards through the stack 19 and then led out through the annular outer duct 42 in the spindle 40.
In
The lower rotatable seal 15 may be attached directly to the inlet cone 10a without any additional inlet pipe, i.e. the feed inlet 20 may be formed at the apex of the inlet cone 10a directly axially above the lower first rotatable seal 15. Such an arrangement enables a firm attachment of the lower first mechanical seal 15 at a large diameter to minimize axial run-out.
The lower first rotatable seal 15 seals and connects both the inlet 20 to the stationary inlet conduit 7 and seals and connects the liquid light phase outlet 21 to the stationary liquid light phase conduit 9. The lower first rotatable 15 seal thus forms a concentric double mechanical seal, which allows for easy assembly with few parts. The lower first rotatable seal 15 comprises a stationary part 15a arranged in the first stationary portion 3 of the insert 1 and a rotatable part 15b arranged in the axially lower portion of the rotor casing 2. The rotatable part 15b comprises in the embodiment shown in
In analogy,
In another embodiment, not shown, instead of arranging the feed inlet and the light phase outlet in a first axial end, the feed inlet and the heavy phase outlet are arranged in this end of the rotor casing. The heavy phase outlet conduit is arranged between said two concentrical sealing rings and the inlet conduit is arranged in the inner ring at the axis of rotation X.
The first seal assembly is then sealing and connecting said feed inlet to a stationary inlet conduit and said heavy phase outlet to a stationary heavy phase outlet conduit, in said first stationary portion.
The feed inlet is thus arranged axially at the axis of rotation and the heavy phase outlet is arranged axially outside of said feed inlet in such a manner that both the feed inlet and the heavy phase outlet are led through the rotatable part and connected to said stationary feed inlet conduit and said stationary heavy phase outlet conduit, respectively, which are led through said stationary part of said first seal assembly.
In yet another embodiment, not shown, instead of arranging the feed inlet and the light phase outlet in a first axial end, the light phase outlet and the heavy phase outlet are arranged in this end of the rotor casing. The light phase outlet conduit is arranged between said two concentrical sealing rings and the heavy phase conduit is arranged in the inner ring at the axis of rotation X.
The first seal assembly 15 is then sealing and connecting said light phase outlet to the stationary light phase conduit and said heavy phase outlet to the stationary heavy phase outlet conduit, in said first stationary portion.
The heavy phase outlet is thus arranged axially at the axis of rotation and the light phase outlet is arranged axially outside of said heavy phase outlet in such a manner that both the light phase outlet and the heavy phase outlet are led through the rotatable part 15a and connected to said stationary light phase outlet conduit and said stationary heavy phase outlet conduit, respectively, which are led through said stationary part 15b of said first seal assembly 15.
In these embodiments not shown are the sealings formed in the same manner as in the embodiment described in connections with the Figs as are the circuits of the cooling liquid, buffer liquid or barrier liquid. To a person skilled in the art it is obvious how the interior of the bowl is to be adapted to these embodiments e.g. the position of the disc stack and distributor may be turned so their apex always is pointing towards the inlet.
In the above the inventive concept has mainly been described with reference to a limited number of examples. However, as is readily appreciated by a person skilled in the art, other examples than the ones disclosed above are equally possible within the scope of the inventive concept, as defined by the appended claims.
Filing Document | Filing Date | Country | Kind |
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PCT/EP2019/084149 | 12/9/2019 | WO | 00 |