This application is related to U.S. patent application Ser. No. 12/337,988, filed Dec. 18, 2008, titled “CENTRIFUGAL SEPARATOR DEVICES, SYSTEMS AND RELATED METHODS,” the disclosure of which application is incorporated herein in its entirety by reference.
The present invention relates to centrifugal separators and related devices and methods. More particularly, embodiments of the invention relate to centrifugal separators comprising a first fluid supply fitting configured to deliver fluid into a longitudinal fluid passage of a rotor shaft and a second fluid supply fitting sized and configured to sealingly couple with the first fluid supply fitting. Embodiments of the invention also relate to centrifugal separator systems comprising a manifold having a drain fitting and a cleaning fluid supply fitting, the manifold coupled to a movable member of a support assembly. Additionally, embodiments of the invention relate to methods of cleaning centrifugal separators.
Centrifugal separators use inertial forces resulting from the acceleration of a material, particularly the acceleration of a material in a circular path, for the separation of a heavier (more dense) material from a lighter (less dense) material. For example, such devices have been found to provide a relatively rapid method of separating immiscible liquids from one another based on different weight phases.
A centrifugal contactor is a type of centrifugal separator that is widely used for liquid-liquid separation, and particularly for solvent extraction processes. These centrifugal separators are termed “contactors” as fluid streams introduced separately into the device are brought together, or contacted, prior to a centrifugal separation of weight phases. For example, fresh water and an organic solvent contaminated with salts may be fed into separate inlets and rapidly mixed in an annular space between a spinning rotor and a stationary housing. The salts may migrate from the organic solvent to the water as they are mixed in the annular space. The water and organic solvent are then centrifugally separated and exit through separate outlets, thus washing salts from the organic solvent with the water.
During normal use, particularly when separating water/petroleum mixtures, solids suspended within the mixture tend to accumulate in the interior of the centrifugal contactor assembly. Such solids are difficult to remove from a welded, enclosed assembly, and back-flushing of the centrifugal contactor has not produced satisfactory results. Better results have been obtained by disassembling the centrifugal contactor and removing the rotor assembly. However, this is a time-consuming operation, and causes the centrifugal contactor to be removed from service for an extended period of time.
To solve this problem, inventors of the present invention disclosed in U.S. Pat. No. 5,908,376 a self-cleaning or “clean-in-place” rotor assembly that can thoroughly clean a centrifugal contactor of accumulated solids without disassembly thereof. The clean-in-place rotor assembly of the centrifugal contactor has a double-ended hollow axial shaft with a bottom end extending through the centrifugal contactor housing. In order to provide a pressurized cleaning solution to the hollow axial shaft, the bottom end of the axial shaft is coupled to a rotary union. The pressurized cleaning solution is then directed from the rotary union into the hollow axial shaft and through a plurality of spray nozzles that are fitted to the axial shaft, which impinges a stream of the pressurized cleaning solution onto the interior surfaces of the centrifugal contactor to remove accumulated solids therefrom.
However, the rotary union used to couple the cleaning fluid supply to the bottom end of the axial shaft has experienced several problems in use. The rotary union is composed of several moving parts, including a bearing and seal assembly that may wear or become damaged during normal use, or during repair or servicing of the centrifugal contactor. Because the rotary union is attached to the bottom end of the axial shaft, the rotary union is otherwise unsupported and, thus, subject to damage due to the constant stress of vibrations from fluid connections and bumps during maintenance or service. The rotary union is also subject to process fluid-related corrosion and wear, resulting in eventual leakage and failure, thus making the rotary union a weak link in centrifugal contactor reliability. This is such a widespread problem with rotary unions that rotary union manufacturers typically limit their warranty to steam, oils, water and other benign fluids. The presence of corrosives, caustics and solids in the centrifugal contactor process streams thus typically voids manufacturer's warranties, as the rotary union is continuously exposed to the process chemistry during the rotary union's installed use in such applications. Additionally, the installation and removal of a rotary union from a centrifugal contactor may require the manipulation of a tool, such as a wrench, in a space between the body of the rotary union and the bottom of the centrifugal contactor, which may be difficult and time consuming.
In view of the above, it would be advantageous to provide improved centrifugal separators and related devices, systems and methods.
In one embodiment, a centrifugal separator comprises a rotor shaft, a first fluid supply fitting proximate a tail end of the rotor shaft, a second fluid supply fitting sized and configured to sealingly couple with the first fluid supply fitting and a support assembly having a movable member coupled to the second fluid supply fitting. The rotor shaft of the centrifugal separator includes a longitudinal fluid passage therein having an opening at the tail end of the rotor shaft. The first fluid supply fitting, located proximate the tail end of the rotor shaft, is configured to deliver fluid into the longitudinal fluid passage through the opening at the tail end of the rotor shaft. The support assembly includes a fixed member coupled to the movable member, such that the movable member, which is coupled to the second fluid supply fitting, is constrained to movement along a fixed path relative to the fixed member. The support member additionally includes an actuator configured to move the movable member along the fixed path.
In another embodiment, a centrifugal separator system comprises a centrifugal separator supported in a frame, a manifold and a support assembly having a movable member coupled to the manifold. The centrifugal separator includes a drain assembly and a cleaning fluid delivery structure and the manifold includes a drain fitting and a cleaning fluid fitting. The support assembly includes a fixed member fixed relative the frame and coupled to the movable member. The support assembly also includes an actuator coupled to each of the fixed member and the movable member. The actuator is configured to move the drain fitting into sealing contact with the drain assembly and move the cleaning fluid fitting into sealing contact with the cleaning fluid delivery structure.
An additional embodiment comprises a method of cleaning a centrifugal separator. The method comprises holding a rotor shaft, and a first fluid fitting coupled to a tail end of the rotor shaft, substantially stationary. Additionally, the method comprises operating a linear actuator to move a second fluid fitting into contact with the first fluid fitting and slidably coupling the first and second fluid fittings to form a fluid-tight seal and directing a pressurized cleaning fluid from the second fluid fitting into the first fluid fitting and into a longitudinal fluid passage of the rotor shaft. The method also comprises moving the second fluid fitting out of contact with the first fluid fitting.
A centrifugal separator system, according to an embodiment of the invention, is shown in
Each centrifugal contactor 12 of the centrifugal separator system 10 may include a motor, such as an electric motor 18. Additionally, the electric motor 18 may include a shaft coupled to a rotor shaft 20 (see
Examples of such centrifugal separators and system configurations are disclosed in, for example, the aforementioned and incorporated by reference U.S. patent application Ser. No. 12/337,988, filed Dec. 18, 2008, titled “CENTRIFUGAL SEPARATOR DEVICES, SYSTEMS AND RELATED METHODS,” of Meikrantz et al.
A manifold 32 may be positioned below each centrifugal contactor 12 and may include a drain fitting 34, which corresponds to the drain assembly 28, and another fitting, such as a fluid supply fitting 36, which corresponds to the CIP fluid delivery fitting 30. The manifold 32 may be coupled to a support assembly 38 having a component fixed to the frame 14.
As shown in
The CIP fluid delivery fitting 30 may additionally include a valve located proximate the tail end 40 of the rotor shaft 20. The valve may comprise a check valve 46, as shown in
In an additional embodiment, the CIP fluid delivery fitting 30 may include a poppet valve 54, as shown in
As shown in
As shown in
The poppet 74 of the drain valve assembly 70 may comprise an annular body 84, a head 86 coupled to the annular body 84 and a plurality of apertures 88 located in the annular body 84 proximate the head 86. The head 86 may be configured generally as a disc comprising the sealing portion 82 at the periphery thereof. The sealing portion 82 may include an elastic seal 90, such as an elastomer O-ring, positioned in a seal gland 92, which may be compressed against the seat 80 of the valve body 78 to form a fluid-tight seal between the head 86 and the seat 80. Additionally, an elastic seal 94 may be positioned below the apertures 88 in the annular body 84 and form a fluid-tight seal between the annular body 84 and a substantially smooth wall 96 of the valve body 78, such that fluid may not leak into the biasing mechanism 76 or outside of the drain valve assembly 70. The annular body 84 of the poppet 74 may extend out of the valve body 78 and include a sealing portion 98 comprising one or more elastic seals 100, such as elastomer O-rings, such that the annular body 84 of the poppet 74 may be sized and configured to slidably couple and seal with the drain fitting 34, as shown in
The biasing mechanism 76 of the drain valve assembly 70 may comprise one or more helical springs 102 located between a portion of the valve body 78 and the poppet 74. The springs 102 may have one end positioned against a surface of the valve body 78 and another end positioned against a surface of a structure 104 coupled to the annular body 84 of the poppet 74. For example, the structure 104 may be an annular structure encircling the annular body 84 of the poppet 74 and positioned against a retaining ring 106 that is located in a groove 108 formed in the surface of the annular body 84 of the poppet 74. The biasing mechanism 76 may be configured to apply a biasing force against the poppet 74, which may cause the head 86 of the poppet 74 to seal against the seat 80 of the valve body 78 and prevent fluid flow therethrough.
As shown in cross-sectional view in
Referring again to
The guide structure 124 may be configured to constrain the movement of the movable member 122 to a fixed path, such as a linear path, relative the fixed member 120. For example, the guide structure 124 may comprise one or more guide rods 128 having one end coupled to the movable member 122. Each guide rod 128 may be positioned at least partially within a guide sleeve 130, such that the guide sleeves 130 may constrain the movement of the guide rods 128 and the movable member 122 to a fixed linear path.
The actuator 126 may be configured to move the movable member 122, and thus the manifold 32, the fluid supply fitting 36 or 61, and the drain fitting 34, along the fixed path relative the fixed member 120. For example, the actuator 126 may be a linear actuator, such as a pressure actuated cylinder assembly (as shown) or a mechanical actuator having a rotatable screw (not shown).
The actuator 126 may comprise a cylinder body 132 fixed to the frame 14 and a piston rod 134 fixed to the movable member 122. In additional embodiments, the cylinder body 132 may be fixed to the movable member 122 and the piston rod 134 may be fixed to the frame 14.
In an additional embodiment, the actuator 126 may be a mechanical actuator (not shown) comprising a rotatable screw mated with a floating nut. The floating nut may be fixed to the movable member 122 and the rotatable screw may be coupled to the frame 14. The floating nut may be coupled to the rotatable screw, such that the floating nut may translate along the rotatable screw as the screw is rotated. The screw may include a head at one end configured to mate with and be rotated by a tool. For example, the head may be shaped as a standard hexagonal bolt head.
During a centrifugal separation process, the motor of a centrifugal separator, such as the electric motor 18 of the centrifugal contactor 12, may rotate the rotor shaft 20, thus causing the centrifugal separation of the working fluids within the separation chamber. Additionally, the manifold 32 may be in a retracted position, such that the fluid supply fitting 36 or 61 may be separated and out of contact with the CIP fluid delivery fitting 30 and the drain fitting 34 may be separated and out of contact with the drain assembly 28, as shown in
To initiate a clean-in-place procedure, the flow of additional working fluid into the centrifugal contactor 12 may be prevented. The electric motor 18 may be stopped so that the rotor shaft 20 and the CIP fluid delivery fitting 30 coupled to the tail end 40 of the rotor shaft 20 are held substantially stationary. Then the actuator 126 may be operated to move the movable member 122 from a retracted position (as shown in
If a pressure actuated cylinder is used as the actuator 126, pressurized fluid may be supplied to the actuator 126 to operate the actuator 126 and cause the movable member 122 to be moved along the linear path from the retracted position to the coupled position. For example, if a pneumatic cylinder is used, a pressurized gas, such as air, may be supplied to the pneumatic cylinder. If a hydraulic cylinder is used, a pressurized liquid, such as hydraulic oil, may be supplied to the hydraulic cylinder. Likewise, if a screw and floating nut mechanism is used, a rotational force may be applied to the screw to operate the actuator and cause the movable member to move along a fixed path.
As the fluid supply fitting 36 or 61 is moved into contact with and is slid into the CIP fluid delivery valve 30 the smooth surface portion 64 of the fluid supply fitting 36 or 61 may be pressed against and compress the elastic seals 66 of the CIP fluid delivery fitting 30 between the fluid supply fitting 36 or 61 and the CIP fluid delivery fitting 30 creating a fluid-tight seal between the coupled fittings 30 and 36 or 61. If the CIP fluid delivery fitting 30 includes a poppet valve 54, such as shown in
Meanwhile, the drain fitting 34 may be moved into contact with and slid over the annular body 84 of the movable poppet 74 of the drain valve assembly 70. A substantially smooth portion 136 of the drain fitting 34 may be pressed against the elastic seals 100 of the sealing portion 98 of the annular body 84 and compress the seals 100 between the drain fitting 34 and the annular body 84 of the poppet 74 to form a fluid-tight seal. Substantially simultaneously, the drain fitting 34 may apply a force to the annular body 84 of the poppet 74 and displace the poppet 74 to unseal the sealing portion 82 of the poppet 74 from the seat 80 of the valve body 78, thus causing the drain valve assembly 70 to open, as shown in
After the working fluids have been substantially drained from the centrifugal contactor 12 a pressurized cleaning fluid may be directed from the fluid supply fitting 36 or 61 into the CIP fluid delivery fitting 30 and into the longitudinal fluid passage 42 of the rotor shaft 20. For example, the pressurized cleaning fluid may comprise at least one of a solvent, an organic solvent, detergent, and water. Directing the fluid through the CIP fluid deliver fitting 30 may comprise directing the fluid through the check valve 46 (as shown in
The pressurized cleaning fluid may then be directed through the longitudinal fluid passage 42 of the rotor shaft 20 and be sprayed out of one or more nozzles (not shown) located along the rotor shaft 20. The spray from the nozzles may wash debris from surfaces of the separation chamber. The debris may be directed by gravity and the flow of the cleaning fluid through the apertures 118 in the bottom plate 112 of the centrifugal contactor 12 and into the solids collection chamber 110. The debris and cleaning fluid may then flow out of the solids collection chamber 110 through the drain valve assembly 70 in a manner similar to the prior draining of the working fluids.
Optionally, after supplying the cleaning fluid, a rinsing fluid, such as substantially pure water, may be directed through the longitudinal fluid passage 42 of the rotor shaft 20 in a manner similar to the cleaning fluid. The rinsing fluid may be used to rinse the cleaning fluid from the separation chamber of the centrifugal contactor 12 and out the drain assembly 28.
After the cleaning fluid and, optionally, the rinsing fluid, have been substantially drained from the centrifugal contactor 12, the actuator 126 may be operated to retract the movable member 122 and manifold 32. This may substantially simultaneously move the fluid supply fitting 36 out of contact with the CIP fluid delivery fitting 30, move the drain fitting 34 out of contact with the drain assembly 28, cause the poppet 74 of the drain valve assembly 70 to be biased to a closed position and optionally cause the poppet 56 of the poppet valve 54 of the CIP fluid delivery fitting 30 to be biased to a closed position. Working fluids may then be reintroduced into the separation chamber, the electric motor 18 may cause the rotor shaft 20 to rotate and the centrifugal contactor 12 may be returned to regular fluid separation service.
While specific embodiments of the invention have been shown by way of example in the drawings and have been described in detail herein, the invention is not limited to the particular forms disclosed. Rather, the invention includes all modifications, equivalents, and alternatives falling within the scope of the invention as defined by the following appended claims and their legal equivalents.
This invention was made with government support under Contract Number DE-AC07-05ID14517 awarded by the United States Department of Energy. The government has certain rights in the invention.
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