1. Field of the Invention
This invention lies in the field of pulse dampers for reciprocating pumps.
2. Description of the Prior Art
Certain laboratory systems, prominent among which are high-performance liquid chromatography (HPLC) systems, require a continuous and steady flow of liquid. In HPLC, the continuous and steady flow assures that the chromatogram for any given sample will be readily readable and sufficiently standardized so that components can be identified by their retention times, properly quantified if desired, and generally reproducible. A dual-headed reciprocating pump system is often used to produce the flow, and a common example of such a system is one with two pump chambers, each with its own piston but with the pistons coordinated by a common motor to drive the pistons in alternating manner. A common problem with dual-headed reciprocating systems is the occurrence of pressure pulsations that occur when the system switches over from one piston to the other. Pressure pulsations cause pulsations in the output flow, and hence the flow rate of the output flow, from the system. When the liquid is a mixture formed by combining two liquids of different compositions either outside of or within the pump chambers, the resulting mixture will often contain ripples in its composition, i.e., fluctuations in the proportion of one liquid relative to the other downstream of the mixing site, in addition to pressure pulsations. Composition ripples occur at elevated pumping pressures and are the result of compression and decompression of the fluid in each pump at the beginning and end of each stroke, respectively. Dampers can be added to individual pumps to dampen the pressure pulsations, but the composition ripples often remain.
The present invention resides in a pressure vessel that reduces, and in many cases eliminates entirely, both pressure pulsations and composition ripples in the output of a dual-headed reciprocating pump. The invention also resides in a dual-headed reciprocating pump that includes such a pressure vessel, and further resides in a method of continuously pumping fluid by use of such a dual-headed reciprocating pump and pressure vessel. The pressure vessel is a single enclosure with two flow-through compartments that are closed from each other so that liquid from one compartment does not enter the other and liquids flow independently through both compartments. Each compartment has its own inlet port and outlet port to allow discharges from the two pump chambers to pass through the compartments separately, and the two compartments are separated by a diaphragm that is fluid-impermeable and yet flexible. The diaphragm responds to surges or other variations in pressure from either side by flexing and thereby allows both momentary pressure surges and momentary drops in pressure to be absorbed within the vessel and removed from the liquid leaving the vessel. In certain embodiments of the invention, the pressure vessel contains two such diaphragms with a volume between them that is filled with compressible fluid. Pressure variations can then be absorbed by the compressible fluid as well as both diaphragms.
The term “flexible” as used herein in connection with the diaphragm(s), refers to diaphragms that can bow or bend in either direction in response to pressure differentials, as well as diaphragms that are elastic and can therefore stretch in response to pressure differentials. The term “fluid-impermeable” denotes diaphragms that do not allow the passage of either liquid or gas at the fluid pressures at which the pumps typically operate. Diaphragms made of a wide array of polymers that meet these descriptions are available and well known in the art. For embodiments of the invention involving the use of a compressible fluid, the fluid can be a gas or a liquid at operating temperatures; such fluids are likewise well known in the art. Examples of compressible liquids are isopropyl alcohol and silicone oil. Examples of compressible gases are air, nitrogen, and any other common gas. Liquids and gases that are not flammable are preferred.
The two pump chambers and their associated pistons can be motor-driven syringe pumps, or any such pumps that have a limited chamber volume and are refilled by the system between each discharge. The pistons will typically operate in a smooth manner, i.e., at constant velocity, although deceleration will typically occur at the beginning and end of each stroke, contributing to the pressure pulsations and composition ripples that are addressed by the present invention. Once the diaphragm(s) or the compressible fluid, or both, are stressed at the beginning or end of a stroke, the stressed component, be it diaphragm or fluid, will induce a flow of its own to compensate for the aberration in the flow entering the pressure vessel. The reciprocating motion of the two pistons is achieved by a common motor such as one with a cam drive, and in some cases a cam of elliptical shape to produce overlap in the changeover between pump chambers.
The figures attached hereto and the following descriptions refer to one example of a reciprocating pump and pressure vessel in accordance with the present invention.
In the claims appended hereto, the term “a” or “an” is intended to mean “one or more.” The term “comprise” and variations thereof such as “comprises” and “comprising,” when preceding the recitation of a step or an element, are intended to mean that the addition of further steps or elements is optional and not excluded. All patents, patent applications, and other published reference materials cited in this specification are hereby incorporated herein by reference in their entirety. Any discrepancy between any reference material cited herein or any prior art in general and an explicit teaching of this specification is intended to be resolved in favor of the teaching in this specification. This includes any discrepancy between an art-understood definition of a word or phrase and a definition explicitly provided in this specification of the same word or phrase.
This application claims the benefit of U.S. Provisional Patent Application No. 61/550,598, filed Oct. 24, 2011, the contents of which are incorporated herein by reference in their entirety.
Number | Date | Country | |
---|---|---|---|
61550598 | Oct 2011 | US |