This disclosure generally relates to fabrication of parts made of composite material. More specifically, this disclosure relates to apparatus and methods for consolidating and forming a pre-form made of fiber-reinforced plastic material (also referred to herein as a composite preform) to reduce voids and/or porosity.
Fiber-reinforced organic resin matrix composites have a high strength-to-weight ratio or a high stiffness-to-weight ratio and desirable fatigue characteristics that make them increasingly popular as a replacement for metal in aerospace applications. Organic resin composites may comprise thermoplastics or thermosetting plastics.
Prepregs combine continuous, woven, or chopped reinforcing fibers with an uncured, matrix resin, and usually comprise fiber sheets with a thin film of the matrix. Sheets of prepreg generally are placed (laid-up) by hand or with fiber placement machines directly upon a tool or die having a forming surface contoured to the desired shape of the completed part or are laid-up in a flat sheet which is then draped and formed over the tool or die to the contour of the tool. Then the resin in the prepreg layup is consolidated (i.e., pressed to remove any air, gas, or vapor) and cured (i.e., chemically converted to its final form usually through chain-extension) in a vacuum bag process in an autoclave (i.e., a pressure oven) to complete the part.
In hot press forming, the prepreg is laid-up, bagged (if necessary) and placed between matched metal tools that include forming surfaces that define the internal, external, or both mold lines of the completed part. The tools and composite preform are placed within a press and then the tools and preform are heated under pressure to produce a consolidated, net-shaped part.
It is known to consolidate and form composite preforms using inductively heated consolidation tools. Induction heating is a process in which an electrically conducting object (usually a metal) is heated by electromagnetic induction. During such heating, eddy currents are generated within the metal and the electrical resistance of the metal leads to Joule heating thereof. An induction heater typically comprises an electromagnet through which a high-frequency alternating current is passed. Most organic matrix composites require a susceptor in or adjacent to the composite material preform to achieve the necessary heating for consolidation or forming. The susceptor is heated inductively and transfers its heat principally through conduction to the preform sandwiched between opposing susceptor facesheets. During heating under pressure, the number of voids and/or the porosity of a composite preform can be reduced.
Recycled graphite fibers can be used in the fabrication of composite aircraft parts, such as lightweight seat back components. First, a matte product is fabricated using recycled graphite fibers and virgin thermoplastic fibers; then the matte product is consolidated and formed in matched tooling comprising opposing susceptor facesheets. These matte products produced with recycled graphite fibers can exhibit a rather matted and tangled fiber architecture. These products can also have undesirable unevenness and thickness/density variations. Furthermore, since the graphite fibers are tangled, they do not facilitate the flow of the thermoplastic material. These characteristics lead to the formation of voids and/or porosity in the final composite product due to the fact that thickness and density distribution are not uniform across the matte product. The formation of voids and/or porosity is further aided by the fact that the fibers are entangled and flow is limited and unable to “heal” porosity very effectively. Even prepreg has some variation in thickness and density distribution, which could lead to the formation of voids and/or porosity during matched tool molding of prepreg composites.
Accordingly, there is a need for a method and an apparatus that can reduce the number of voids and/or the porosity during the consolidation and formation of a composite preform having uneven thickness and/or density distribution.
The subject matter disclosed herein is directed to a method for reducing the number of voids and/or porosity during the consolidation and formation of a composite preform having uneven thickness and/or density distribution, such as a matte product comprising recycled graphite fibers and virgin thermoplastic fibers. This method is carried out using an apparatus that comprises matched molding tools. The apparatus further comprises a compliant layer that is situated between the composite preform and one of the matched molding tools for the purpose of providing a more even pressure over the entire area of the preform during the consolidation process. The compliant layer should have an offset tensile yield point (0.2% of the strain) in a range of 25-300 psi at the temperature of consolidation of the preform at strain rates of about 1% to 10% strain per minute.
In accordance with one embodiment, a sheet of magnesium base alloy is used to act as the compliant layer or shim to compensate for uneven thickness or density over the area of a composite preform, for example, a matte product comprising recycled graphite fibers and virgin thermoplastic fibers. Magnesium base alloy makes an excellent candidate for a compliant layer for high-performance thermoplastic resins due to the fact that some magnesium alloys become very soft at temperatures useful for assisting the consolidation and molding of thermoplastic composites (i.e., 600-750° F.) and do not melt until above 1000° F. As the temperature and pressure increase inside the apparatus during consolidation of the composite preform, the magnesium alloy sheet softens and forms into the areas of relatively lower pressure. The magnesium alloy sheet can be reused due to the soft nature of the material. Other alloys can be used instead of a magnesium base alloy provided that the alloy has an offset tensile yield point (0.2% of the strain) in a range of 25-300 psi at the temperature of consolidation of the preform at strain rates of about 1% to 10% strain per minute
In accordance with one aspect, a method is disclosed for consolidating a preform made of composite material with reduced number of voids and/or porosity. The preform and a compliant metal alloy sheet are placed between less compliant matched confronting forming/molding surfaces with the preform being sandwiched between the metal alloy sheet and one of the matched confronting surfaces. The matched confronting surfaces are inductively heated (which heats the compliant metal alloy sheet by conduction) until the preform reaches at least a consolidation temperature of the composite material. During heating, force is applied so that the matched confronting surfaces exert sufficient compressive force on the preform and metal alloy sheet to cause the composite material to consolidate at the consolidation temperature. The compliant metal alloy sheet has a tensile yield point in a range of 25-300 psi at the consolidation temperature at a strain rate of about 1% to 10% strain per minute.
Another aspect of the disclosed subject matter is an apparatus for consolidating a preform made of composite material at a consolidation temperature, comprising: first and second tool assemblies having matched confronting surfaces; a metal alloy sheet disposed between said matched confronting surfaces, wherein said metal alloy sheet has a tensile yield point in a range of 25-300 psi at the consolidation temperature at a strain rate of about 10% strain per minute; means for heating at least the matched confronting surfaces of the first and second tool assemblies; and means for applying force to one or both of the first and second tool assemblies so that the matched confronting surfaces are capable of exerting compressive force on the preform and metal alloy sheet.
A further aspect is a method for consolidating a composite preform made of recycled graphite fibers and organic resin fibers, comprising: placing the composite preform and a metal alloy sheet between matched confronting surfaces of first and second tool assemblies, the matched confronting surfaces being less compliant than the metal alloy sheet; heating the matched confronting surfaces of the first and second tool assemblies and the metal alloy sheet during a heating cycle; and applying force to one or both of the first and second tool assemblies so that the matched confronting surfaces exert sufficient compressive force on the composite preform and metal alloy sheet to cause thermal coupling of one matched surface to one side of the composite preform, the other side of the composite preform to the metal alloy sheet, and the metal alloy sheet to the other matched confronting surface. The force is applied during at least a portion of the heating cycle. The metal alloy sheet has a tensile yield point in a range of 25-300 psi at a consolidation temperature at a strain rate of about 1% to 10% strain per minute.
Other aspects of the invention are disclosed and claimed below.
Various embodiments will be hereinafter described with reference to drawings for the purpose of illustrating the foregoing and other aspects of the invention.
Reference will hereinafter be made to the drawings in which similar elements in different drawings bear the same reference numerals.
The following detailed disclosure describes a method and an apparatus for consolidating and molding/forming a composite preform having an uneven thickness and/or density distribution. In accordance with the disclosed method, a compliant layer is placed between the composite preform and one heated consolidation tool. The compliant layer is designed to distribute the molding pressure more evenly over the entire area of the uneven preform during the consolidation process.
One known apparatus for matched tool consolidation of composite preforms is partly depicted in
Still referring to
The consolidation/molding apparatus shown in
In a typical implementation of a composite consolidation and molding process, the composite preform 22 is initially positioned between the upper and lower tooling dies of the stacked tooling apparatus, as shown in
After a predetermined interval of time, the cooling system 14 will be operated to apply a cooling medium to the tooling dies 4 and 10, thereby also cooling the susceptors 18 and 20 and the composite preform 22 therebetween. The composite preform 22 remains sandwiched between the susceptors for a predetermined period of time until complete cooling of the composite preform has occurred. This allows the molded and consolidated composite preform 22 to retain the structural shape which is defined by the contoured surfaces of the susceptors 18 and 20. The tooling dies are then opened and the composite preform can be removed. The formed and cooled composite preform is removed from the stacked tooling apparatus without loss of dimensional accuracy when it is cooled at an appropriate property-enhancing rate.
The sectional view shown in
Still referring to
As best seen in
Preferably each induction coil 34 is fabricated from copper tubing which is lightly drawn. A lightly drawn condition of the tubing enables precision bending by numerically controlled bending machines. Numerically controlled bending of the tubes allows accurate placement of the tubing relative to the changing contours of the susceptors, thereby improving the degree to which the each susceptor is uniformly inductively coupled to the induction heater across the length and width of the susceptor. However, it should be understood that the compliant layer disclosed hereinafter can be employed also in cases wherein the susceptors are planar rather than concave/convex. Optionally the coils 34 also remove thermal energy by serving as a conduit for a coolant fluid, such as water. After being bent and installed, the coils include straight tubing sections connected by flexible tubing sections. The flexible tubing sections connect the straight tubing sections and also allow the dies to be separated. The accurate placement of the tubing of the induction coils 34 promotes uniformity in the amount of heat generated by the magnetic flux field and the amount of heat removed by flow of the coolant fluid.
As disclosed in U.S. Pat. No. 6,528,771, the induction coils 34 can be connected to a temperature control system that includes a power supply, a controlling element, a sensor and a fluid coolant supply preferably containing water (not shown). The power supply supplies an alternating current to the induction coils 34 which causes the coils to generate the electromagnetic flux field. The fluid coolant supply supplies water to the induction coils 34 for circulation through the coils and the removal of thermal energy from the dies. The sensor is capable of measuring the power supplied by the power supply. Alternatively, or in addition to measuring the power supply, the sensor may include a voltmeter that can measure the voltage drop across the induction coils 34. The controlling element receives the sensor output and uses the measurements in a feedback loop to adjust the power being supplied by the power supply. The controlling element can include hardware, software, firmware, or a combination thereof that is capable of using feedback to adjust the voltage output by the power supply.
The system described with reference to
In accordance with various embodiments, the consolidation apparatus further comprises a compliant layer that is situated between the composite preform and one of the matched molding tools for the purpose of providing a more even pressure over the entire area of the preform during the consolidation process. The compliant layer should have an offset tensile yield point (0.2% of the strain) in a range of 25-300 psi at the temperature of consolidation of the preform at strain rates of about 1% to 10% strain per minute.
In accordance with one embodiment shown in
More specifically, a suitable magnesium alloy sheet material is Elektron AZ31B Sheet, which is commercially available from Magnesium Elektron UK in Manchester, England. AZ31B is a wrought magnesium base alloy, is non-magnetic, has high electrical and thermal conductivity, and has a melting range of 1050-1170° F. Superplastic forming of AZ31B can occur during the preform consolidation process. The chemical composition of AZ31B magnesium base alloy is: 2.5-3.5% aluminum; 0.7-1.3% zinc; 0.20-1.0% manganese; balance magnesium.
Other magnesium base alloys can be used instead of AZ31B provided that the alloy has an offset tensile yield point (0.2% of the strain) in a range of 25-300 psi at the temperature of consolidation of the preform at strain rates of about 1% to 10% strain per minute. Alternatively, metal alloys having a base element different than magnesium, such as aluminum, can be used provided that they have the aforementioned tensile yield property.
A system incorporating a compliant layer 44 the type described above is shown in
A compliant layer of the type described above also has application in the consolidation and forming/molding of composite preforms other than the matte product described herein. For example, the compliant layer can be used in the consolidation of composite preforms that comprise reinforcing fibers embedded in a matrix made of either thermoplastic or thermosetting plastic material.
While the invention has been described with reference to various embodiments, it will be understood by those skilled in the art that various changes may be made and equivalents may be substituted for elements thereof without departing from the scope of the invention. For example, a compliant layer can be used with heated consolidation tools that lack susceptors. In cases wherein the tooling dies have heated matched surfaces, the compliant layer can be placed between one of those heated matched surfaces and the composite preform. In addition, many modifications may be made to adapt a particular situation to the teachings herein without departing from the essential scope thereof. Therefore it is intended that the claims not be limited to the particular embodiments disclosed.
The method claims set forth hereinafter should not be construed to require that the steps recited therein be performed in alphabetical order or in the order in which they are recited, and should not be construed to exclude two or more steps being performed concurrently.