Patent Application
20140124990
This invention relates to soluble packages such as pouches containing one or more products and to apparatus and method for producing such pouches. The invention has particular, but not exclusive, application to thermoformed packages made from two or more webs comprising polymeric substrates. The webs are soluble or dispersible in a solvent and may comprise water soluble or water dispersible films.
Thermoformed packages comprising a single compartment are typically made in four steps:
Thermoformed packages are frequently made on intermittent horizontal machines in which the web is moved through the machine in intermittent steps allowing each operation described above to be carried out whilst the web or webs are stationary.
In such machines, once the base web is moved away from the forming mould, it begins to cool and unlike many insoluble polymeric substrates, many soluble webs, including particularly those comprising substantially polyvinyl alcohol, then experience a phenomenon known as shrink-back in which the thermoformed film tries to return to its pre-thermoformed condition thereby reducing the volume of the thermoformed pocket. This represents a major problem as the pocket will have reduced in size by the time that it is filled. To take account of the shrink-back and still maintain the required fill volume, the thermoformed pocket needs to be made larger than the fill volume so that it can accept the fill volume despite the effects of shrinkback. Designing a thermoforming mould with larger cavities requires either a deeper draw depth, which in turn often requires a thicker base web provoking slower subsequent dissolution, or a greater superficial area, known as the footprint, allowing fewer cavities in either the machine direction or across the web or both, thereby reducing machine and web material efficiencies.
A continuous motion rotary thermoforming machine for making thermoformed packages is disclosed in U.S. Pat. No. 3,218,776 in which the base web is heated to a plastic condition and immediately pressed on to the surfaces of the drum surrounding the pockets. A heated metal roller is employed to press the web of film against the surfaces of the drum. The roller is heated to a temperature sufficient to render the film plastic by the time that it is pressed against the continuously rotating drum. The actual temperature will vary depending upon the film, its thickness, and the length of time that it remains in contact with the heated roller. The film, by means of the heated roller, may be heated to about 140° F. (60° C.) but it might be as low as about 100° F. (37.8° C.) or as high as 300° F. (148.9° C.). A vacuum is applied to the base of the cavity in order to draw the web of heated film that covers the cavities into the cavities and define pockets to receive subsequently the product to be packaged. The vacuum should be applied instantly after the cavity is covered with film. In a subsequent operation, the top web is pressed against the base web, by now containing filled thermoformed pockets located upon the rotating drum, by means of a second heated roller which conductively heats the top web and, by means of a spring, presses the top web over the pockets containing the packaged product during which both webs are pressed together on the surfaces surrounding the pockets to achieve a bond. In the particular case where water-soluble packages are desired, the top web, prior to arrival at the sealing station, is made adhesive by moistening with a liquid in which the film of the top web is soluble, in order that the sealing process can be effected by a combination of heat and solvent welding.
In the machine disclosed in U.S. Pat. No. 3,218,776, two heated rollers provide the sole sources of heat, a first heated roller heating the base web prior to thermoforming and a second heated roller heating the lidding web prior to closure of the pouches. This has a number of disadvantages. Firstly, the base web begins to cool as soon as it leaves the first heated roller and a high vacuum is therefore required to hold the base web to the walls of the cavities and thereby inhibit the occurence of shrink-back. Secondly, the top web begins to cool as soon as it leaves the second heated roller, thereby preventing the strongest seal from being made between the base web and the top web.
Continuous motion rotating thermoforming offers advantages compared to intermittent motion horizontal thermoforming, particularly in respect of higher productivity and reduced shrink-back. Due to the higher productivity of continuous motion rotating machines, the time interval between thermoforming and filling is reduced, thereby allowing the thermoformed web less time to cool. Nevertheless, shrinkback of soluble webs has remained a problem, even with continuous motion rotary machines such as described in U.S. Pat. No. 3,218,776.
According to an exemplary embodiment, a method of making a pouch from two webs comprising soluble polymeric substrates comprises the steps of rotating a former that comprises a plurality of cavities around its periphery and one or more heaters around the former for heating the cavities; heating the cavities; drawing a base web into the cavities by means of a vacuum to form pockets in the base web; filling the pockets with at least one component; closing the pockets with a top web to form a pouch; and heating the cavities and maintaining the vacuum after the step of drawing the base web into the cavities in order that, once thermoformed, the base web is held tightly to a base of the cavities through filling, sealing and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
According to another exemplary embodiment, a method of making a pouch from three webs comprising soluble polymeric substrates comprises the steps of rotating a former that comprises a plurality of cavities around its periphery and one or more heaters around the former for heating the cavities; heating the cavities; drawing a micro-perforated or porous base web into the cavities using a vacuum to form pockets in the base web; filling the pockets with at least one powder or granular product; closing the pockets with an intermediate web to create a lower compartment; evacuating the lower compartment through the micro-perforations or porosity in the base web; filling the pockets with at least one powder or granular product or liquid or gel product on top of the lower compartment; closing the pockets with a top web to create an upper compartment; and heating the cavities and maintaining the vacuum after the step of drawing the base web into the cavities in order that, once thermoformed, the base web is held tightly to a base of the cavities through filling, sealing, and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
According to another exemplary embodiment, a continuous motion rotating thermoforming machine for producing pouches made from two webs comprising soluble polymeric substrates includes a former having a plurality of pouch forming cavities around its periphery; a motor configured to continuously rotate the former so that the cavities follow an endless path in the direction of rotation of the former through forming, filling, sealing and cutting stations; one or more heaters disposed around the former for heating the cavities; and a vacuum configured to apply a vacuum through the base of each cavity in order that, once thermoformed, a base web is held tightly to the base of the cavities through filling, sealing and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
According to another exemplary embodiment, a method of making a pouch from two webs comprising soluble polymeric substrates includes providing a former having a plurality of cavities around its periphery; providing one or more heaters around the former for heating the cavities; continuously rotating the former; heating the cavities; drawing a base web into the cavities using a vacuum to form pockets in the base web; filling the pockets with at least one component; closing the pockets with a top web to form a pouch; and heating the cavities and maintaining the vacuum after the step of drawing the base web into the cavities in order that, once thermoformed, the base web is held tightly to the base of the cavities through filling, sealing and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
According to another exemplary embodiment, a method of making a pouch from three webs comprising soluble polymeric substrates wherein the base web is micro-perforated or porous comprises providing a former having a plurality of cavities around its periphery; providing one or more heaters around the former for heating the cavities; continuously rotating the former; heating the cavities; drawing a micro-perforated or porous base web into the cavities using a vacuum to form pockets in the base web; filling the pockets with at least one powder or granular product; closing the pockets with an intermediate web to create a lower compartment; evacuating the lower compartment through the micro-perforations in the base web; filling the pockets with at least one powder or granular product or liquid or gel product on top of the lower compartment; closing the upper compartment with a top web to create an upper compartment; and heating the cavities and maintaining the vacuum after drawing the base web into the cavities in order that, once thermoformed, the base web is held tightly to the base of the cavities through filling, sealing and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
The present invention is intended to overcome or at least mitigate some of the problems and disadvantages aforementioned.
More especially, this invention seeks to address the problem of shrink-back of soluble webs in continuous motion rotating thermoforming machines.
A preferred aim of this invention is to provide an improved continuous motion rotating thermoforming machine to make thermoformed soluble packages containing one or more products and comprising one or more compartments.
As used herein, the term “soluble webs” refers to webs of polymeric substrates which can be dissolved in a solvent. In many cases, the requirement is for the pouch to dissolve in water or in an aqueous medium but dissolution in other solvents can be envisaged where the pouch is required to dissolve in a solvent other than water.
As used herein, the term “water soluble” refers to materials that are capable of being dissolved in water of whatever temperature to form a homogeneous solution and the term “water dispersible” refers to materials that are capable of being dispersed in water of whatever temperature to form a permanent or temporary suspension. For convenience, where the term “water soluble” is used hereinafter in the description and claims, it will be understood this includes “water dispersible”.
As used herein, the term “mould” refers to a constituent part (containing one or more cavities) of a continuously rotatable former, the part often being designed to be easily exchanged within the former in order to produce pouches of different fill volume, the term “cavity” refers to that part of the mould into which a base web is drawn during a thermoforming operation, and the term “pocket” refers to an open container which is formed in a base web as a result of a thermoforming operation.
According to a first aspect of the invention, we provide a continuous motion rotating thermoforming machine for producing soluble pouches made from two or more webs comprising soluble polymeric substrates, the machine including a plurality of pocket forming cavities and means to heat the cavities.
As used herein, the terms “continuous motion rotating thermoforming machine” refers to a machine in which thermoforming is effected by means of cavities in a former that continues to turn while sequential operations required for the production of soluble pouches are carried out.
Preferably, means is provided for rotating the former so that the cavities follow an endless path in the direction of rotation of the former through forming, filling, sealing and cutting stations. The rotating means may comprise a motor, for example an electric motor, more preferably a variable speed electric motor.
The former may comprise a continuously rotating drum with cavities opening to the outer surface of the drum. Cavities may be arranged across the width of the drum and/or around the circumference of the drum. Alternatively, the former may comprise a continuously rotating endless belt with cavities opening to the outer surface of the belt. Cavities may be arranged across the width of the belt and/or along the length of the belt.
The arrangement and disposition of the cavities across and along an endless belt can be similar to the arrangement and disposition of the cavities around a drum. In either case, the cavities are heated and a vacuum is preferably maintained through the base of each cavity in order that, once thermoformed, a base web is held tightly to the base of the cavities through subsequent filling, sealing and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
A rotating endless belt may allow the possibility of greater space for sequential operations, namely thermoforming, filling, and sealing, required for the production of soluble pouches from two or more webs according to this invention. Where the invention is practiced using a rotating endless belt rather than a rotating drum, the greater space that may be made available for sequential operations along that portion of the rotating endless belt that is disposed horizontally, may be of particular value. The length of the rotating endless belt that is disposed horizontally can be varied in order to increase or decrease the space required to carry out sequential operations. The number of sequential operations will increase as the number of compartments in the soluble pouch increases. Thus, a rotating endless belt may be of particular value in the production of multi-compartment soluble pouches comprising more than two webs, where successive webs may be thermoformed, and the successive pockets so formed may be filled and sealed. However many compartments are contained within the soluble pouch, the top web that is sealed to the uppermost thermoformed web is not itself thermoformed.
The machine has particular application for the manufacture of water soluble pouches. Depending upon whether they are required for edible or non-edible applications, water-soluble webs can be substantially based upon polyvinyl alcohol (PVOH), polyethylene oxide, modified celluloses such as carboxy-methyl cellulose (CMC) and hydroxy-propyl methyl cellulose (HPMC), pullulan, certain types of starch, dextrin, guar gum, gelatine and their derivatives. In the case where one or more webs is based upon PVOH, their solubility at a given temperature may be adjusted by selecting a grade of PVOH with a specific molecular weight and a specific % saponification. By way of example only, to obtain solubilisation of a water-soluble film made substantially from PVOH in an aqueous medium at a temperature at or above 60° C., the PVOH should preferably be of a fully saponified type i.e. the degree of saponification ranging from 90-99.5%, and to obtain solubilisation in an aqueous medium at a temperature of 25° C. and below, the PVOH should be of a partially saponified type i.e. the degree of saponification ranging from 71-90%. Hence, the lower the degree of saponification, the lower the temperature of water required to dissolve a water soluble film made substantially from PVOH.
The heating means may be arranged externally and/or internally of the former and may be of any suitable type for heating the cavities. The cavities may be heated by convection, for example hot air heating, or radiation, for example infra-red heating or conduction, for example electrical heating. Preferably, the surface temperature of the cavities of the drum or endless belt is at least 60° C. According to a preferred embodiment of the invention, the drum or endless belt is heated to a temperature of between 60° C. and 200° C. (140° F. and 392° F.) in order to reduce or preferably eliminate the incidence of shrink-back and thereby improve the quality of thermoforming. This has the benefit of making the complete volume of the cavity available to receive the product to be filled. A further benefit is that the reduction or elimination of shrink-back allows the vacuum within the drum or endless belt to hold the filled pouches on the drum or endless belt, even after they are separated by cutting, until the vacuum is removed and the pouches are released from the drum or endless belt on to a conveyor or other suitable means for collecting/and or transferring the pouches away from the machine, for example to a packing unit. It will be evident that where shrink-back is pronounced, the base web of the filled pouches can draw itself away from the internal surfaces of the cavity thereby breaking the vacuum holding the filled pouches on the drum or endless belt. As a consequence, the filled pouches, after being separated from each other by cutting knives, will no longer be held tightly to the drum or endless belt and will fall away from the drum or endless belt before they arrive at the conveyor. For effective operation of continuous motion rotating thermoforming machines, it is essential that the pouches are held tightly to the drum or endless belt until they are released on to the conveyor.
Different levels of vacuum may be provided at different positions around the drum or endless belt as it rotates according to the demands of the production being carried out. By way of example which is by no means limiting, the level of vacuum required to draw the heated base web into the cavities and hold the base web in position, thereby avoiding shrink-back, until filling has been completed will be less than that required to hold the filled and sealed pouches on the drum or endless belt until they are ejected from the drum or endless belt by means of air blow off and fall on to the conveyor transporting the pouches away from the machine.
The heating of the drum or endless belt may be provided by precisely placed heaters, some examples of which are described below:
Externally mounted hot air heaters (shown at 125 in
Externally mounted infra-red heaters (shown at 225 in
Internally mounted electrical heaters (shown at 335 in
A combination of externally and internally mounted heaters of the type shown in
The machine may produce soluble pouches made from two or more water-soluble polymeric substrates. The dissolution temperature of the two webs may be identical. Alternatively, the dissolution temperature of the two webs may be different. Preferably, means is provided for sealing a top web to the base web (in the case where pouches are made from two webs) or to an intermediate web (in the case where pouches are made from more than two webs). Such means may comprise at least one heat sealing roller. The strength of the seal between the webs may be enhanced by sequentially mounted heated sealing rollers. According to a preferred embodiment of the invention, a second heated sealing roller (shown at 21 in
Preferably, means is provided to coat or print a web in-line. For example, a web may be coated or printed in line by a roller mounted between the web unwind and a heated sealing roller. A third web may be introduced in order to produce two compartment pouches. In the case of multi-compartment pouches wherein the webs comprising polymeric substrates are water-soluble, the compartments of a pouch may open sequentially as a result of changes in water temperature or pH.
A coated web may be required to form the base or top web. The coating may be a colouring or any other coating that is sufficiently miscible with the solvent to form a homogeneous coating medium. This is usually achieved by procuring differently coated webs from film suppliers, which is costly and may present logistical problems, especially when there is a requirement to produce pouches of the same size with different coatings.
According to a preferred embodiment of the invention, illustrated schematically in
The machine may produce pouches made from two or more polymeric substrates. The polymeric substrates may be water-soluble. The dissolution temperature of the two webs may be identical. Alternatively, the dissolution temperature of the two webs may be different. In the case of multi-compartment pouches wherein the webs comprising polymeric substrates are water-soluble, the compartments of a pouch may open sequentially as a result of changes in water temperature or pH.
In one preferred embodiment, the present invention provides a continuous motion rotating thermoforming machine for producing water-soluble pouches made from two or more webs comprising water-soluble polymeric substrates including a rotating former having a plurality of pouch forming cavities around its periphery, wherein the former has means to be heated and means to apply a vacuum through the base of each cavity in order that, once thermoformed, a base web is held tightly to the base of the cavities through filling, sealing and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
The base web may be micro-perforated or made porous by other means. Two webs (a base web and a top web) may be employed for pouches having a single compartment. One or more additional webs (intermediate webs) may be employed for pouches having two or more compartments.
For pouches having two or more compartments, the webs may dissolve under the same conditions. In this way, the compartments may open at substantially the same time. Alternatively, the webs may dissolve under different conditions. In this way the compartments may open at different times. Preferably, the compartments of the pouches open sequentially as a result of changes in water temperature or pH.
In another preferred embodiment, the present invention provides a continuous motion rotating thermoforming machine for producing water-soluble pouches containing two or more compartments made from a plurality of webs comprising water-soluble polymeric substrates, including a continuously rotating former having a plurality of cavities around its periphery, wherein the former has means to be heated and means to apply a vacuum through the base of each cavity, in order that, once thermoformed, a base web is held tightly to the base of the cavities through filling, sealing and cutting stations until the vacuum is released and the filled and sealed pouch is ejected from its cavity.
The base web may be micro-perforated or made porous by other means. In the case of pouches containing two compartments, a third web may be provided.
The machine may produce pouches made from three polymeric substrates. The polymeric substrates may be water-soluble. The dissolution temperature of the three webs may be identical. In this way, the compartments may open at substantially the same time. Alternatively, the dissolution temperature of the three webs may be different. In this way the compartments may open at different times. Preferably, the compartments of the pouches open sequentially as a result of changes in water temperature. Alternatively or additionally, the pouches may open as a result of changes in pH or any other factor affecting solubility of the polymeric materials employed.
According to a preferred embodiment, the third web is mounted on the machine in order to provide pouches having two compartments as schematically illustrated in
Other porous means can include the inclusion of mineral particles of a suitable size in a web thereby making the web porous due to the creation of minute air channels around the particles, but this means is by no means limiting. Where mineral particles are included in a web to create porosity, the particle size is typically greater than the thickness of the web.
According to a second aspect of the invention, one or more novel filling operations may be employed for varying the contents of the pouch. Examples of these operations can be seen in
In one filling operation, a spherical, hemispherical, ellipsoidal or any other three dimensional shaped object, for example a tablet or capsule although these examples are by no means limiting, may be placed in a thermoformed pocket either prior to, at the same time as, or following, the filling of a liquid, gel, granular or powder composition into one or more compartments of a water-soluble pouch.
Such a three dimensional shaped object may contain an active material not present in the liquid or gel. In the case where one or more of the materials comprised within the three dimensional shaped object is antagonistic with one or more materials comprised within the liquid or gel, the three dimensional shaped object can be coated with a water-soluble polymer, which may for example comprise the same or similar polymeric materials as comprise one or more of the webs used to make the pouch.
The three dimensional shaped object may not necessarily completely dissolve when the pouch is placed in contact with an aqueous medium. For example, it can be hollow, insoluble in an aqueous medium, and perforated such that its contents are released when placed in contact with an aqueous medium but the perforated shell of the three dimensional shaped object survives undissolved.
In another filling operation, with or without the additional presence within a compartment of a three dimensional shaped object, a combination of one or more of a liquid or gel and a granular or powder product may be present in a compartment of the water-soluble pouch. In order to prevent the components mixing with each other thereby destroying the visual identity of each, the liquid or gel may be filled at a sufficiently high temperature for it to be in molten form. At least the upper surface of the molten material solidifies so rapidly within the pocket that a granular or powder product can be subsequently filled without the components mixing substantially with each other. The temperature of the molten liquid or gel must not sufficiently high to cause any distortion of the thermoformed water-soluble web within the pocket. Where the water-soluble web within the pocket receiving the molten liquid or gel comprises substantially poly-vinyl alcohol, the temperature of the molten liquid on contact with the thermoformed web should not exceed 10° C. below the melting point of the web if distortion is to be avoided.
The base web can be micro-perforated either in-line whilst mounted on the machine or off line by the film supplier or a sub-contractor thereof, by mechanical means or by means of lasers or by any other suitable means such as a needle located in the base of each cavity. The porosity of the micro-perforated base web can be adjusted by varying the number and/or pattern of micro-perforations per square meter, or by varying the diameter of the micro-perforations. At least one micro-perforation is required in each portion of the base web that is subsequently thermoformed to comprise the base of the lower compartment.
In a third aspect, the present invention provides a continuous motion rotating thermoforming machine wherein the seal between a top web and a second web is enhanced by at least one further heated sealing roller mounted after a first heated sealing roller.
In a fourth aspect, the present invention provides a continuous motion rotating thermoforming machine wherein one or more webs is coated or printed in line on either face by a roller mounted between a web unwind and a heated sealing roller.
Machines according to the third and fourth aspects of the invention may include any of the features of the machine according to the first aspect of the invention.
The invention also provides a method of using a machine according to any preceding aspect of the invention to produce soluble pouches from two or more polymeric substrates, preferably, water soluble pouches.
The invention also provides a machine as defined in claim 1. Preferred features of the machine are defined in claims 2 to 15. A method of using the machine is defined in claims 16 to 23, a pouch made by the method is defined in claim 24, and a method of forming a pouch is defined in claim 25.
In the following description, like reference numerals are used to indicate the same or similar parts and the arrangement and operation of these parts in later embodiments will be understood from the description of earlier embodiments.
Referring first to
In each of
The drum 10 is rotated in the direction indicated by arrow 12. Soluble pouches are formed from two webs that are drawn respectively from rolls 13 and 20. The webs preferably comprise soluble polymeric substrates such as water soluble films which may dissolve at the same temperature. The first (base) web from roll 13 is guided around a heated roller 14 which presses it tightly over cavities 11 located around the circumference of the drum into which the film is drawn by suction from within the drum 10, thus forming pockets. The surface temperature within the cavities 11 and the temperature of the heated roller 14 will depend on the type of film, its thickness, and the speed of rotation of the drum. Preferably, the surface temperature within the cavities is at least 60° C. The surface of the drum surrounding the cavities should be smooth, preferably polished. The pockets are filled at the top (12 o'clock) of the drum 10 from a filling hopper or injector 18 and in the case of a granular or powder product, the fill is smoothed by wipers (not shown) which also clean product from the upper surface of the film surrounding the pockets. The second (top or lidding) web from roll 20 is made adhesive by moistening to a sufficient extent by means of a felt roller 15 rotating within a bath of liquid in which the top web is soluble. It is important that the amount of liquid applied to the surface of the top web to make it adhesive is controlled very accurately. If too little liquid is applied, the required adhesiveness will not be obtained. If too much liquid is applied, the film will be weakened and in the limit, even dissolved. It has been found that the amount of liquid can be controlled very accurately by moving the web from roll 20 along a vertical path, which in
Referring now to
Referring now to
Referring now to
Other methods of producing multi-compartment pouches may be used avoiding the need for micro-perforation of the base web. The base web may be made porous by means other than micro-perforation such as by impregnating the base web with particulate matter providing minute path ways through the web, although this example of how the base web may be rendered porous is by no means limiting. By whatever method the base web is rendered porous, the second web may be pulled down into the cavity by means of the vacuum within the drum in a similar manner to that described above where the base web was perforated. Alternatively, the base web may not be rendered porous and instead of using the vacuum within the drum or endless belt to pull down the second web into the cavity, the second web may be pressed into the base of the cavity by mechanical means or by means of air jets placed externally across the web immediately prior to the filling station.
In this embodiment of the invention, when the base web has been rendered porous by whatever means, the product contained within the lower compartment is preferably granular or powdery in nature in order to prevent escape of product through the porous web. In the case of pouches comprising two or more compartments, in which at least the lower compartment contains either a liquid or a gel, the base web is typically not rendered porous.
Referring now to
In
In
It will be understood that the cavities contained within the endless belt 100 in
Referring now to
It will be understood that the invention in its various aspects is not limited to the embodiments above-described which are provided by way of example only and that features of any of the embodiments may be employed separately or in combination with features of any other embodiments.
List of References Used in the Drawings:
| Number | Date | Country | Kind |
|---|---|---|---|
| 0920445.4 | Nov 2009 | GB | national |
The present application is a Divisional of U.S. patent application Ser. No. 13/474,493, filed May 17, 2012, which is a Continuation of International Application No. PCT/IB2010/003144, filed Nov. 23, 2010, which claims the benefit of and priority to United Kingdom Patent Application No. 0920445.4, filed Nov. 23, 2009. The entire disclosures of U.S. patent application Ser. No. 13/474,493, International Application PCT/IB2010/003144, and United Kingdom Patent Application No. 0920445.4 are incorporated herein by reference.
| Number | Date | Country | |
|---|---|---|---|
| Parent | 13474493 | May 2012 | US |
| Child | 14151655 | US |
| Number | Date | Country | |
|---|---|---|---|
| Parent | PCT/IB2010/003144 | Nov 2010 | US |
| Child | 13474493 | US |
