The present invention relates in general to the processing of metallic materials, and more particularly to a method of fabricating continuous or semi-continuous billets or bars of metallic materials using severe plastic deformation techniques.
The metal industry continues to require new materials for fabricating products that are improved in performance and are less costly to manufacture. Because of the vast differences in the characteristics of metals themselves, some materials are uniquely adapted for special uses. Steel, for example, has a high characteristic tensile strength and is easily formable in sheet form and thus is well adapted for stamping automobile body parts as well as a host of other commercial and consumer goods. However, steel has a high density and is not suitable for lightweight applications such as those in the aerospace industry. Aluminum, on the other hand, is light weight, but has a lower tensile strength, as compared to steel, and is not easily formable in sheet form, and is thus not well adapted for use in stamping automobile body parts. When stamping contoured parts, the sheet aluminum material becomes thinned and even breaks at the high stress locations, such as areas where sharp curves and corners are formed. Because of the requirements for higher strength and light weight materials in many modern applications, titanium has become a material of choice, especially in the aerospace industry, because of its high strength and light weight properties. The demand for higher strength and lower weight materials continues to grow and is becoming very important not only in aerospace industry but also in automotive industry. The use of high strength and low density materials in the automobile industry is becoming extremely important because of more stringent requirements to control environmental pollution and to conserve the fossil energy resources.
A relatively new process has been developed for increasing the tensile strength of aluminum, or other soft metals, in an attempt to fulfill the current and future demands for high strength and low density materials, while yet being easily formable in many metal-forming areas. The tensile strength of metals can be increased by many methods, one being a process by which the grain size of the metal is reduced and made very small. With a smaller grain size, the hardness and tensile strength of the metal is increased without compromising the ductility properties. The reduction in the grain size of a metal or alloy can be achieved by thermomechanical processing (TMP) where the material undergoes an extremely high degree of deformation. It is well known that when a metal undergoes severe thermomechanical deformation, the grain structure becomes smaller, and the material becomes correspondingly stronger at low temperatures. Many metal processing techniques are known which provide extremely large material deformations, including the well-known TMP techniques, the torsional/pressure technique, extrusion, and others. While yet in an experimental stage, softer metals can be hardened by undergoing a process called Equal Channel Angular Extrusion (ECAE), which is also known also Equal Channel Angle Pressing (ECAP). Because the processes are substantially identical, except for name, the process is referred to herein as the ECAE/P process. The ECAE/P process reduces the grain size of the metal by forcing the material through an angled die so that the metal undergoes a shear deformation without a corresponding change in the cross-sectional size thereof. A number of stages can be utilized so that the billet undergoes a shear deformation along different axes of the billet. This sequential shear deformation in the material can result in an ultrafine grain size, on the order of a few microns, or less. For a better understanding of the ECAE/P process, reference is made to the following U.S. patents: U.S. Pat. No. 5,620,537 by Bampton; U.S. Pat. No. 5,809,393 by Dunlop, et al; U.S. Pat. No. 5,826,456 by Kawazoe, et al; U.S. Pat. No. 5,904,062 by Semiatin, et al; and U.S. Pat. No. 6,197,129 by Zhu, et al. The ECAE/P process is well adapted for use with softer metals such as aluminum, copper, magnesium, nickel, titanium, and their corresponding alloys, and others. The shear strain to which these materials are subjected during the ECAE/P process increases the hardness thereof. These metals can thus be used in many other applications which heretofore rendered them unacceptable.
In a conventional process, the billet 16 is pushed through the die 10 by a hydraulic ram 18. As can be appreciated, the length of the billet must be somewhat short so that the billet does not buckle at the entrance of the entry channel 12. Billet cross sections on the order of about 1 inch to 2 inches in diameter or side dimensions have been processed through ECAE/P dies in this manner. With a limitation of short billets, in connection with the diameter/length ratios noted above, there is inherently a substantial amount of waste associated with the process, it being realized that the frontal end and rear end parts of each billet may be unusable. The ECAE/P method of work hardening a metal is thus acceptable for short billets. Hence, where the fabrication of large metal work pieces is necessary, the use of ECAE/P processed metals is not presently economically feasible.
It can be seen from the foregoing that a need exists for a process that can produce long billets of metallic materials using ECAE/P methods. Another need exists for a metal processing system that can produce large quantities of ECAE/P-hardened metals, with substantially lower energy requirements for carrying out the process. Yet another need exists for a method of continuous processing of long metal billets through successive ECAE/P dies to thereby achieve large quantities of ultrafine grain, hardened materials adapted for new and existing uses. Another need exists for a process where ultrafine grain materials can be produced by severe plastic deformation techniques, with less waste.
Disclosed is a method of fabricating ultrafine grain-hardened metals using a Continuous Severe Plastic Deformation (CSPD) method, where the process is carried out on a continuous or semi-continuous basis so that longer and larger billets of ultrafine grain, hardened metals can be produced. The CSPD dies are very similar to the ECAE/P dies but with different channel diameter/length ratios. The channel lengths of the CSPD dies are made shorter to reduce the friction between the billet and the CSPD die. In accordance with the principles and concepts of the invention, large and/or long billets of a metal are continuously fed to one or more CSPD dies arranged in a series. In a preferred form of the invention, the raw billets are continuously fed to a CSPD die by a set of push/pull rolls that grip or roll the billet and force it through the die. The set of push rolls are arranged on opposing sides of the long billet for gripping or rolling the billet and for pushing the billet into the die. The pull rolls also grip or roll the billet in a similar manner and are arranged to pull the billet from the die. Hence, the rolls can operate on continuous lengths of billets to thereby allow much longer billets of processed metals to be produced. When employed in a series of dies, the pull rolls of one die station can also function as the push rolls for the next downstream die station. The downstream dies are oriented in such a way that they can provide the effect of rotating the continuous billet in a desired angle as it is moved through the CSPD dies in a sequence. These die orientations can be changed in a manner so that the process can produce either equiaxed or elongated microstructure metals.
In accordance with an optional feature of the invention, a small annular constriction can be formed in the exit channel of a CSPD die to reduce the friction between the die and the billet. In this case, the cross section of the billet moving through the entry channel of the die is reduced slightly, thus producing less friction as the billet is moved through the exit channel. Another optional feature is that the rolls used in the plastic deformation process can be flat or shaped. In either case, the billet, as it is rolled, can be deformed in a variable amount depending on the roll shape, rolling, and billet configuration. In addition, the force generated by the rolling operation before entering and after exiting the die can be applied by a conveyor type or tank-wheel track arrangement powered by one or more sets of rolls.
According to one aspect of the invention, there is disclosed a method of processing metallic materials by severe plastic deformation thereof, comprising the steps of providing at least one die with an angled bore through which a billet of the metallic material is moved, where the angled bore is structured so that the billet undergoes a severe plastic deformation when moved therethrough, and using a transport mechanism for gripping a side surface of the billet and moving the billet through the die, whereby a long length billet can be processed.
According to another aspect of the invention, there is disclosed a method of processing metallic billets by severe plastic deformation thereof, comprising the steps of providing at least a first and second die for causing severe plastic deformation of the billets when moved through the respective dies, arranging the dies in series such that at least a portion of the billet being processed is positioned in both said dies at the same time, and moving the billet simultaneously through said first and second dies so that severe plastic deformation of the billet occurs at different locations thereof at the same time, whereby long length billets can be processed.
According to a further aspect of the invention, there is disclosed a die for use in severe plastic deformation of a metallic material, comprising a body with an angled bore formed therein so that when the metallic material is forced through the angled bore of said die, the metallic material experiences severe plastic deformation, the angled bore is characterized by an entrance channel and an exit channel, the respective axial axes of the entrance channel and the exit channel are angled, and wherein a channel diameter/length ratio of the die is in the range of about 1:1 to about 1:2.
Further features and advantages will become apparent from the following and more particular description of the preferred and other embodiments of the invention, as illustrated in the accompanying drawings in which like reference characters generally refer to the same parts, elements, or components throughout the views, and in which:
With reference now to
In one embodiment of the invention shown in
A third set of rolls 26 is located adjacent the exit channel 14 of the CSPD die 10. The third set of rolls 26 functions to grip the side surfaces of the billet 16 and exert a pulling force to pull the billet 16 from the die 10. In the event that the CSPD die 10 is disposed in a plastic deformation system upstream of another die, then a fourth set 28 of rolls can be utilized to exert a pushing force for pushing the billet 16 into the entry channel of the subsequent downstream die (not shown). With this arrangement of push and pull pinch rolls, the length of the billet 16 is not limited, and the billet 16 can be routed through a multi-station system.
The rolls utilized for the push and pull functions can be of conventional construction, such as the type well known for use with rolling mills. Indeed, a rolling mill station can be employed to initially form the billet 16 in a desired cross-sectional shape prior to undergoing severe plastic deformation in a CSPD die. The rolls are machined or otherwise formed with a peripheral edge having a shape complementary to the shape of the outer surface of the billet 16. This provides for a large surface area for frictional contact between the roll gripping surface and the billet 16. As can be appreciated, the larger the surface area contact between the rolls and the billet 16, the larger the push/pull force that can be imparted to the billet 16. Various structures can be utilized to increase the gripping area between the roll surface and the billet 16. For example, the rolls can have a knurled gripping surface area to achieve a better bite on the side surface of the billet 16. Other surface configurations of rolls can be used to maximize the friction between the roll surface and the billet 16. In the event the billet 16 is of a material that is somewhat hard, additional sets of rolls can be used to push or pull the billet in a forward direction. In other words, by employing a severe plastic deformation system using CSPD die(s), there may be plural sets of drive rolls located at the entry channel of a die, and plural sets of rolls located at the exit channel of the die. Because the billet 16 continues to become harder after it undergoes a series of severe plastic deformations, an increased force is necessary to drive the billet 16 through the downstream dies. As such, an increased number of roll sets may be required to move the billet 16 through the respective dies. Conversely, the plastic deformation stations located at the input end of the system may not need a set of pull rolls and a separate set of push rolls between dies. Rather, one set of rolls may be adequate for providing a pull function on the billet 16 for the upstream billet, and for also providing a push function on the billet 16 for the adjacent downstream die. An adequate frictional contact is required between the gripping surfaces of the rolls and the billet 16, while at the same time it is desired to minimize the friction between the billet 16 and the inner surfaces of the CSPD die channels. It is contemplated that the billet 16 will be lubricated as it is forced through each CSPD die. An oil type of lubricant can be sprayed on the billet as it enters the entry channel of each die.
While not shown, a billet guide structure may be employed between each set of push rolls and respective dies. The guide structure may have a funnel-shaped bore for guiding the frontal end of the billet 16 into the entry channel of the die. The continuous movement of the billet 16 from one die to a subsequent die is thus facilitated, thereby eliminating labor efforts in manually feeding a billet 16 from one severe plastic deformation station to another.
Those skilled in the art may find that billets of certain cross-sectional shapes may be better adapted for gripping on the side surfaces thereof, especially by roller mechanisms. For example, billets having a round or oval cross-sectional shape provide a substantial surface area for contact with a complementary-shaped roller. Accordingly, it may be advantageous to utilize a set of shaped rolls to form the billet into a desired cross-sectional shape for movement through the dies, and use a final mill roll set to form the billet in the final cross-sectional shape for other uses. It is preferable, although not absolutely necessary, to utilize die channels with the same shape as the billet being processed. Hence, mill rolls providing desired billet shapes can be used in conjunction with other rolls that function solely to grip the billet and provide a continuous movement thereof through the multi-die system. In order to optimize the efficiency of the system, the mill rolls can be designed and driven so as to provide both the function of shaping and the function of movement of the billet in a forward direction.
As noted above, the process of hardening the billets can also be semi-continuous. A semi-continuous process can be one in which the hardening procedure is interrupted for various reasons. For example, such a process may be employed when the billet must undergo eight passes through a CSPD die system, and there are only four dies in the system. In this event, when the billet has completed four plastic deformations through the four dies, the process is momentarily interrupted so that the processed billet can be brought back to the input of the system to undergo four additional plastic deformations. While each pass through the system may be considered continuous, the overall procedure may be periodically interrupted and thus be thought of as semi-continuous. Other examples of a semi-continuous process may be where the billet is processed to utilize only one direction of a die to achieve special microstructures, or where only a single die is used for multiple passes of a billet therethrough.
The first CSPD die 30 receives the billet 16 as it is moved forwardly by a set of push rolls 32 and a set of pull rolls 34. The roller set 36 may be a pull roller from an upstream processing station, or may function to shape the billet 16 into a desired cross-sectional shape. It is assumed for purposes of example that the billet 16 is square in cross-sectional shape. The first CSPD die 30 functions to make the grain size of the billet 16 smaller. The depiction of the die 30′ shows the axial orientation of the die 30, particularly the entry channel 38 with respect to the exit channel 40, which is oriented upwardly. The billet 16 is pulled from the exit channel 40 by the pull roll set 34. The billet 16 is moved from the pull roll set 34 to the push roll set 42 of the next downstream CSPD die 44. The second die 44 of the system is rotated 90 degrees, as shown by the die 44′. Here, the second die 44 is rotated so that the exit channel 48 is directed to the right with respect to the entry channel 46. The pull roller set 50 directs the billet 16 from the second station to the push roll set 52 of the third station.
The third station employs a third CSPD die 54 for providing further plastic deformation of the billet 16. The orientation of the third die 54 is axially rotated another 90 degrees, as shown by the die 54′. In the third station, the exit channel 56 is oriented downwardly with respect to the entry channel 58. The plastic deformation of the billet 16 in the third station occurs along yet another plane of the billet 16, thereby making the grains of the billet 16 finer and more homogenous. As can be appreciated, with the metal deformation resulting from each station, the billet 16 becomes harder and stronger. Importantly, the cross-sectional shape and size of the billet 16 does not substantially change when processed through the CSPD die system. Lastly, the billet 16 is pulled from the station three die 54 by pull roll set 60 and again pushed into the entry channel 66 of the station four CSPD die 64. In the processing of the billet 16 in station four, severe plastic deformation of the metal is achieved at a different angular orientation. The fourth die 64 is oriented at an angle such that the exit channel 68 is directed to the left with respect to the entry channel 66. In the event that the CSPD dies are formed with 90 degree (Φ) channels, a maximum strain can be achieved in the billet 16. After the billet 16 undergoes a severe plastic deformation in each die, the strain imparted thereto either approaches or is substantially equal to unity. After the billet 16 undergoes processing through four such dies, the accumulated strain in the billet 16 may be on the order of about four. A uniform and fine grained (nanocrystalline) structure can thereby be achieved in a very efficient and cost effective process.
The foregoing process in which the billet undergoes sequential CSPD station processing is much preferred over prior extrusion processes where a billet undergoes strain by way of plastic deformation caused by extrusion dies. When processed through an extrusion die, the cross-sectional shape of the billet changes. The strain required to produce fine grains in metals can range from 2 to 6. This range of strains corresponds to extrusion ratios in the range of about 7:1 to 300:1, the latter ratio of which may be required for breaking prior particle boundaries of PM processed material. The extrusion process is limited by the amount of product that can be produced because of limitations in the size of the extrusion chamber and the large frictional stresses that can develop between the workpiece and the extrusion chamber.
In the utilization of a drawing process in conjunction with an ECAE die, a limitation is the tensile strength of the billet. The tensile failure of the billet limits the maximum strain to about 0.63. An additional limitation of using a drawing process with an ECAE die is separation of the billet material from the sidewall of the die, especially at the outer corner of the angle between the entry and exit channels. This problem is generally overcome by using draw rolls in conjunction with push rolls (where the rotational speed of the rolls is the same), and the use of ECAE-type dies where the cross-sectional area of the billet does not substantially change during the process. When such a combination of processing steps and equipment is employed, separation of the billet from the sidewalls of the die is either substantially minimized or eliminated altogether.
In the system of
While the embodiment of the billet processing system shown in
While rolls can function as one transport mechanism for moving the billet through the CSPD dies, other transport mechanisms may also be adapted for forcing the billets in a forward direction. In the event a large frictional grip is needed to produce a correspondingly large force on the billet, a moving track transport mechanism can be used. An example of a motive conveyor or track system is shown in FIG. 5. Such an apparatus may function similar to tracks on a military tank or earth moving equipment. The track itself can have a number of grips for gripping the opposing side surfaces of the billet. Alternatively, the tracks may be comprised of a train of concave plates connected together for engaging the opposing surfaces of the billet. Preferably, one track mechanism would be positioned on each side of the billet. With this arrangement, a large surface area of the billet is engaged with the track mechanism, thereby providing a large frictional contact therewith.
With specific reference to the motive track system shown in
The linked nature of the track, for example track 86, is shown in
Assuming a flow stress of 20,000 psi for a conventional material such as aluminum, the force required to move the 8-inch square aluminum billet through the CSPD die is about 1,280,000 lbs, or 640 tons. This force must be imparted to the opposite side surfaces of the square billet. Further assuming a sticking friction of about 10,000 psi (about one-half of the flow stress), the required contact area between the tracks 110 and 112 is about 64 square inches. If an efficiency of 50% is assumed, with a friction factor of 0.5 (rather than 1.0 for sticking friction), the required linear contact length of the transport mechanism on the billet is 32 inches. As can be seen, the 48 inch surface area length of the transport drive mechanism of
In accordance with the foregoing, another advantage can be realized from the processing of billets characterized with ultrafine grain sizes. While these billets are characterized by a high hardness factor at room temperature, such material often becomes easily forgeable when subjected to higher temperatures. When the equicohesive temperature of a metal is exceeded (about fifty percent of the absolute melting temperature), a decrease in the grain size leads to a decrease in the flow stress of the material. The reduction in the flow stress that typically occurs can be mathematically represented as the amount that the grain size has been made smaller, raised to the power of about 1.5 to about 2.5. In other words, a decrease in the grain size by a factor of 2 can potentially decrease the flow stress by a factor of about 2 to 6. For example, in the processing of aluminum billets according to the invention, the resulting ultrafine grain metal can be forged at a temperature of 600 degrees F., rather than the traditional forging temperature of 900 degrees F. This makes the fabrication or forging of products more economical and requires less energy for the fabrication steps. Moreover, with the availability of large billets having ultrafine grain structures, many more products can be fabricated.
While the preferred and other embodiments of the invention have been disclosed with reference to specific apparatus and techniques, it is to be understood that changes in detail may be made as a matter of engineering and design choices without departing from the spirit and scope of the invention, as defined by the appended claims.
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