Convection heating system for vacuum furnaces

Information

  • Patent Grant
  • 6756566
  • Patent Number
    6,756,566
  • Date Filed
    Thursday, May 23, 2002
    22 years ago
  • Date Issued
    Tuesday, June 29, 2004
    20 years ago
Abstract
A convection heating system includes a hot zone enclosure defining a hot zone and a plurality of gas injection nozzles for injecting a cooling gas into the heat treatment zone of furnace. Each gas injection nozzle may include a flap disposed and pivotally supported therein for substantially preventing the escape of heat from the hot zone during a heating cycle, but for permitting the injection of the cooling gas into the furnace hot zone during a cooling cycle. A gas exit port may be provided and may include a flap pivotally mounted therein for impeding the unforced outward flow of a gas from the heat treatment zone during a heating cycle.
Description




FIELD OF THE INVENTION




This invention relates generally to vacuum heat treating furnaces, and in particular, to a convection heating system for vacuum furnaces having a unique combination of features that provides significantly improved heat retention and heat transfer during heating and cooling cycles, respectively.




BACKGROUND OF THE INVENTION




Known vacuum heat treating furnaces available hitherto incorporate cooling gas injection systems to provide cooling of metal parts from the elevated heat treatment temperature. Among the components of the cooling gas injection system used in such furnaces are a plurality of nozzles for conducting the cooling gas into the furnace hot zone. The gas injection nozzles used in the known systems are generally tubular or cylindrical in shape and have an unobstructed central opening that extends along the length of the nozzle.




A problem arises when using such nozzles in a vacuum heat treating furnace. Because the known nozzles have unobstructed openings therethrough, heat can be lost from the hot zone during the heating cycle. Such heat loss occurs when the heated atmosphere in the furnace hot zone escapes the hot zone through the cooling gas nozzles and is cooled in the plenum or, in a plenumless furnace, in the space between the hot zone and the furnace wall. The heated gas is cooled as it traverses the plenum, or the annular space between the hot zone and the water-cooled furnace wall in a plenumless furnace, and reenters the hot zone at a lower temperature. This problem occurs in vacuum furnaces that utilize convection heating.




In addition, in the known vacuum heat treating furnaces with forced gas cooling, a return path is provided so that the cooling gas can be recirculated and cooled. This return path usually includes an opening in the hot zone enclosure so that the cooling gas can exit the hot zone. This opening in the hot zone wall also permits heat to escape from the hot zone during heating.




The above-described heat loss results in a non-uniform heating of the metal parts and higher energy use. When the metal parts do not uniformly attain the desired heat treating temperature, the properties desired from the parts are not achieved. Consequently, a need has arisen for a heat treating furnace having a forced gas cooling function which substantially prevents the heat in the hot zone from exiting the hot zone during a convection or other heating cycle. It would be highly desirable to have a simple device for injecting cooling gas into a vacuum heat treating furnace which substantially inhibits the escape of heated gas therethrough without the need for actuators and the mechanical linkage systems needed to operate such actuators.




SUMMARY OF THE INVENTION




In accordance with the present invention, a heat treatment furnace having forced gas cooling or quenching capability is provided. The heat treatment furnace according to this invention includes an outer furnace wall inside of which a heat shielded enclosure is provided. The heat shielded enclosure contains an interior space, or hot zone, in which a work piece may be placed/positioned for heat treatment. The enclosure is designed with substantial thermal insulation to impede the outward flow of heat from the hot zone. The enclosure includes a plurality of orifices disposed in a selected area or areas of the enclosure wall. A plurality of nozzles are provided in communication with the orifices so that a cooling gas may be injected into the hot zone through the nozzles during a cooling cycle. The nozzles include a flow control means that is adapted for allowing an inward flow of the cooling gas during a cooling cycle, but which impedes the outward flow of heat from the hot zone during a heating cycle. In a first embodiment of the flow control means, each nozzle includes a flap disposed in a channel formed through the nozzles. The flap is pivotally supported in the channel in such a manner so as to impede the outward flow of heat from the hot zone, but to permit the inward flow of the cooling gas. The furnace further includes a gas exit port disposed in a wall of the heat shielded enclosure. The gas exit port provides a passageway through which the cooling gas introduced into the hot zone via the nozzles may exit the hot zone for recirculation and cooling . The gas exit port is also configured to impede the outward flow of heat from the hot zone during a heating cycle of the furnace. In a preferred embodiment of the gas exit port, the exit port includes a pivotally mounted panel in the passageway for impeding the unforced outward flow of heat from the hot zone. The exit port panel also functions to prevent the unforced introduction of cooler gas into the hot zone. A gas circulation means is also provided within the heat shielded enclosure for providing stirring circulation of the heated atmosphere within the hot zone to convectively heat or cool a work piece that is being heat treated in the furnace. The circulation means may conveniently be provided as a fan.











BRIEF DESCRIPTION OF THE DRAWINGS




The foregoing summary, as well as the following detailed description of a preferred embodiment of the present invention, will be better understood when read in conjunction with the drawings, in which:





FIG. 1

is a schematic view partially in section of a vacuum heat treating furnace in accordance with the present invention;





FIG. 1A

is a detail view of an alternative arrangement for the end wall structure of the vacuum heat treating furnace shown in

FIG. 1

;





FIG. 2

is a sectional view taken along line


2





2


of

FIG. 1

showing the end wall of the heat shielded enclosure;





FIG. 3

is a perspective view of a cooling gas nozzle in accordance with the present invention;





FIG. 4

is a cross-sectional side elevation view of the cooling gas nozzle of

FIG. 3

as viewed along line


4





4


therein;





FIG. 5

is a front elevation view of the cooling gas nozzle of

FIG. 3

;





FIG. 6

is a rear elevation view of the cooling gas nozzle of

FIG. 3

;





FIG. 7

is a perspective view of a pin for attaching the cooling gas nozzle of

FIG. 3

to a furnace hot zone wall; and





FIG. 8

is a cross-sectional side elevation view of a gas exit port in accordance with the present invention.











DETAILED DESCRIPTION




Referring now to the drawings wherein like reference numerals refer to the same or similar elements across the several views, and in particular to

FIG. 1

, there is shown a heat treating furnace generally designated


10


which includes a pressure vessel having a double outer wall


12


, preferably of generally cylindrical shape, and a domed double end wall


14


. The space between the double walls can be insulating space to impede the flow of heat or can be liquid filled and used as a cooling jacket, if desired. End wall


14


includes a cylindrical motor housing and support


16


which has a flanged outer edge


16




a


which mates with a flanged edge


18




a


of an end closure


18


for the motor housing. End closure


18


is removable for servicing the motor


20


. Although not shown here, the flanges are provided with suitable fastening means (e.g., bolts) and sealing means (e.g., gasket seal). A motor


20


is supported within the housing


16


and is provided with electrical connections which pass through motor housing wall


16


in a sealed manner.




The opposite end of the vacuum furnace


10


is provided with a double-wall end closure


24


having a sealing flange


24




a


which cooperates with a sealing flange


12




a


on the cylindrical double wall structure


12


. A furnace of the present invention may vary in size, but is typically quite large, having a diameter of perhaps six feet or more. In such large structures the end closure


24


is supported in a way not material to the present invention, but which enables it to be conveniently moved away from the end of the structure to allow the introduction into the furnace hot zone of work pieces to be heat treated, typically supported on refractory pallets. Although not shown the furnace requires heating elements


25


or other means of heating. One such heating element arrangement is shown in FIG.


2


.




As shown in

FIG. 1

, a heat shielded enclosure, or hot zone wall, generally designated


26


, conforming to the shape of the outer wall


12


is suitably supported in the pressure vessel by structure not shown, but well known in the art. In a cylindrical furnace, such as that shown in the drawings, a cylindrical hot zone wall


28


is preferably generally arranged coaxially with the longitudinal axis of the pressure vessel. The hot zone wall


28


is spaced inwardly a uniform spacing distance from the outer furnace wall


12


. In the embodiment shown in

FIG. 1

, the hot zone enclosure


26


is substantially cylindrical. However, the enclosure


26


and hot zone wall


28


may have other cross-sectional shapes such as square, rectangular, or polygonal, as needed for a particular application. The hot zone enclosure


26


is lined internally with a refractory material to resist the intense processing heat. The hot zone enclosure


26


is designed to retain the heat within the enclosure and impede its flow outwardly and to provide a hot zone


40


therein into which work pieces to be heat treated are positioned.




An end wall


30


of construction similar to the hot zone wall


28


, is attached at one end thereof. A movable end wall


32


is disposed at the opposite end of the heat shielded enclosure


26


, and is of similar construction thereto. End wall


32


is dimensioned to substantially close the open end of the enclosure


26


. The movable wall


32


which completes the heat shielded enclosure


26


is affixed to and moves with the furnace end closure


24


. End closure


24


includes a cylindrical motor housing


65


and support


66


. The motor housing


65


is generally cylindrical in shape and has a central longitudinal axis substantially aligned with the central longitudinal axis of the enclosure


26


when the movable end wall


32


is engaged to close the open end of the enclosure


26


. A convection motor


70


is supported within the housing


65


on support structure


67


. The convection motor


70


is provided with electrical connections


68


which pass through and are sealed at motor housing wall. The convection motor


70


is also provided with optional water cooling by means of inlet water tubing


64




a


and outlet water tubing


64




b


which pass through and are sealed at the motor housing wall.




A convection fan


60


is attached to a hub


60




b


, which is mounted to the shaft


62


of the convection motor


70


. The hub


60




b


extends through an aperture in the movable end wall


32


so that the fan


60


is located inside the hot zone when the end closure


24


and end wall


32


are in the fully closed position. The convection fan


60


in the embodiment shown in

FIGS. 1 and 1A

has flat blades


60




a


attached to the hub


60




b


on the shaft


62


. Because the blades


60




a


, hub


60




b


, and shaft


62


are disposed within the hot zone


40


during the heating cycle of the furnace


10


, those components are preferably made of a refractory material capable of withstanding the very high temperatures attained within the hot zone


40


. One such suitable material is carbon reinforced carbon (CFC) manufactured by C-CAT, Inc. of Fort Worth, Tex., USA. In operation, the convection fan


60


circulates or stirs the gas within the hot zone


40


during a convection heating cycle to provide more rapid and uniform heating of work pieces present within the hot zone


40


. In addition, during a cooling cycle the convection fan


60


may be used to assist circulation of the cooling gas within the hot zone


40


to provide more rapid and uniform cooling of the work pieces.




The hot zone wall


28


of the heat shielded enclosure


26


is perforated with a plurality of orifices


36


. Optionally, a plurality of orifices


38


perforate the end wall


30


also. The orifices


36


,


38


are so distributed over the wall areas as to permit the flow of cooling or heat treating gas in several directions in the hot zone


40


, toward the work pieces being treated. The orifices


36


,


38


may have any shape and pattern of distribution at the enclosure wall


28


and end wall


30


that is suited to provide the desired flow of gas into the hot zone


40


. For example, the orifices


36


,


38


may comprise a series of holes in the walls


28


,


30


. Alternatively, the orifices


36


,


38


may comprise one or more longitudinal slots.




A plurality of gas injection nozzles


39


are disposed in communication with the orifices


36


,


38


to provide a means for injecting a cooling gas into the hot zone


40


during a forced gas cooling cycle of the heat treating furnace when the work pieces are rapidly cooled from the heat treating temperature. The gas injection nozzles


39


include a means for substantially preventing the egress of heat from the hot zone


40


during the heating cycle of the furnace


10


. The gas injection nozzles


39


may comprise any structure that permits the forced flow of gas therethrough, but which also impedes the flow of heat that would otherwise be induced by natural convection therethrough. For example, the nozzles


39


may comprise a baffle structure in gaseous communication with the orifices


36


,


38


. In a preferred embodiment, the nozzles


39


have a flap valve which is described more fully hereinbelow.




The gas injection nozzles


39


are fastened to the hot zone wall


28


by any appropriate means. This arrangement can be seen more easily in FIG.


6


. Suitable fastening means include pins, bolts, wires, threads, twist-lock tabs, or retaining clips. The means for attaching the nozzle


39


to the hot zone wall


28


preferably provides for easy installation and removal of the nozzle


39


to facilitate assembly and maintenance of the heat treating furnace


10


and/or its heat shielded enclosure


26


. A preferred means for attaching the nozzle


39


to the hot zone wall


28


is described more fully below.




Referring now to

FIGS. 3-7

, an embodiment of the gas injection nozzle


39


will be described in greater detail. The gas injection nozzle


39


is formed of a forward portion


21


which is exposed in the hot zone


40


and a rear portion


25


which is attached to the hot zone wall


28


and end wall


30


to communicate with orifices


36


and orifices


38


, respectively. A first central opening


23


is formed through the length of the forward portion


21


and a second central opening


27


is formed through the length of the rear portion


25


. The first central opening


23


and the second central opening


27


are aligned to form a continuous channel through the nozzle


39


. The rear portion


25


has an annular recess


29


formed at the end thereof. The annular recess


29


is formed to accommodate a boss on the hot zone wall


28


around the orifice


36


as shown in FIG.


4


.




A pair of boreholes


33




a


and


33




b


are formed or machined in the nozzle


39


for receiving metal attachment pins that attach the nozzle


39


to the hot zone wall


28


. A preferred construction for the attachment pins is shown in

FIG. 7. A

pin


41


has a first end on which a plurality of screw threads


43


are formed to permit the pin


41


to be threaded into a threaded hole (not shown) in the hot zone wall. It will be appreciated that instead of the screw threads


43


, the first end of pin


41


can be provided with twist-lock tabs, or a transverse hole for accommodating a retaining clip. The other end of the attachment pin


41


has a transverse hole


45


formed therethrough for receiving a retaining clip (not shown) to hold the nozzle


39


in place.




A flap


31


is disposed in the first central opening


23


and is pivotally supported therein by a pin


33


which traverses holes in the sidewalls


35




a


,


35




b


of forward portion


21


. The flap


31


is positioned and dimensioned so as to close the central opening


23


when it is in a first position, thereby preventing, or at least substantially limiting, the transfer of heat out of the hot zone


40


and the unforced introduction of cooler gas into the hot zone through the central channel of the nozzle


39


. In a second position of the flap, as shown in phantom in

FIG. 4

, the central opening


23


is open to permit the forced flow of cooling gas therethrough into the hot zone


40


during a cooling or quenching cycle. For simplicity, the flap


31


is maintained in the first or closed position by the force of gravity. In such an arrangement the nozzle


39


is preferably oriented such that the flap will be normally closed. In a horizontally oriented vacuum furnace, as shown in the embodiment of

FIG. 1

, some of the nozzles


39


in the upper half of the hot zone


40


will necessarily be open a small amount because of the orientation of the nozzles


39


and the effect of gravity on the flap


31


. When it is desired to maintain the flaps


31


of such nozzles


39


in the normally closed position, biasing means, such as a counterweight or a spring, can be used. The biasing means should provide sufficient biasing force to maintain the flap


31


in the normally closed position, but the biasing force of the biasing means should be less than the force of the cooling gas on the flap


31


when it is being injected so that the flap


31


can be readily moved to the open position by the flow of the cooling gas.




The nozzle


39


and the flap


31


are preferably formed from a refractory material such as molybdenum, graphite, or CFC. They may also be formed of a ceramic material if desired. In the embodiment shown, the forward portion


21


is rectangular in cross section and the rear portion


25


is circular in cross section. However, the shapes of the forward and rear portions of nozzle


39


are not critical. Similarly, the shapes of the first and second central openings


23


,


27


are not critical. The first central opening


23


is preferably square or rectangular for ease of fabrication and the second central opening


27


is preferably circular for ease of adaptation with the opening in the hot zone wall


28


.




Referring back now to

FIG. 1

, cooling gas is preferably supplied to the nozzles


39


through a plenum


47


. Accordingly, the orifices


36


,


38


are provided over an area of the enclosure wall


28


and end wall


30


selected to provide passageways for gaseous communication between the hot zone


40


and the plenum


47


. The plenum


47


is disposed in the passage between the furnace wall


12


and the enclosure wall


28


and extends around the back thereof, over the orifices


36


,


38


. The plenum


47


includes a plenum wall


42


connected to the heat shielded enclosure wall


28


by radially inwardly extending plenum end wall


44


located between the orifices


36


and the open end


37


of the enclosure


26


to provide an annular flow channel around the hot zone wall


28


. The plenum wall


42


extends beyond the end wall


30


of the heat shielded enclosure


26


and the plenum


47


is continued by a planar plenum end wall


46


extending radially inwardly to a cowling


48


. A blower fan


50


is attached at hub


50




b


to shaft


52


of motor


20


. In the embodiment shown in

FIG. 1

, a heat shield


55


is mounted between the fan


50


and hot zone enclosure


26


in order to protect the fan and motor from the intense heat generated in the hot zone


40


during operation of the furnace. The cowling


48


has a curved or flared entry throat to minimize turbulence and promote efficient flow of the cooling gas from the blower fan


50


. The fan in the embodiment shown in

FIG. 1

preferably has curved blades. The outward flow of air from blower fan


50


is directed in a generally radial direction throughout 360° in the space defined by the plenum


47


. The plenum


47


itself is adapted to handle the pressure and to keep the gaseous atmosphere relatively confined so as to cause relatively even flow through the nozzles


39


into the not zone


40


. Heat exchange coils


54


are preferably disposed in the recirculation channel between walls


46


and


14


to cool the recirculated cooling gas. Whether the coils are wound in helical layers as suggested in

FIG. 1

is a matter of choice. The actual configuration of coils is not critical and may be varied a great deal.




During a cooling cycle, the cooling gas, after entering the hot zone


40


, flows out of the hot zone


40


and into a coolant recirculation channel through the gas exit ports


34


as shown by the arrows “A”. The gas exit ports


34


may be provided in one or more of the movable end wall


32


, enclosure wall


28


, and end wall


30


. In the embodiments shown in

FIGS. 1 and 1A

, the gas exit ports are provided in the movable end wall


32


. The recirculation channel is defined by the furnace wall


12


and the outer plenum wall


42


and by the walls


46


and


14


. The gas exit ports


34


may comprise any structure that permits the forced flow of gas therethrough and also prevents the flow of heated gas therethrough that is induced by natural convection.




A preferred arrangement of the gas exit port


34


is shown in FIG.


8


. The gas exit port


34


comprises an exit port panel or flap


61


similar in function to the flap


31


of a nozzle


39


. The exit port flap


61


is disposed in exit port opening


63


which is formed in the movable end wall


32


. The exit port flap


61


is pivotally supported within the exit port opening


63


by a pin


69


which is held within the movable end wall


32


. The exit port flap


61


is positioned and dimensioned so as to close the exit port opening


63


when the flap is in a first position, thereby preventing, or at least substantially limiting, the transfer of heat out of the hot zone


40


and preventing the unforced introduction of cooler gas into the hot zone


40


through the exit port opening


63


. To enhance this function, the flap


61


is lined with thermal insulation


61


. In a second position of the flap


61


, as shown in phantom, the exit port opening


63


is open to permit the forced flow of cooling gas therethrough from the hot zone


40


during a cooling or quenching cycle. For simplicity, the exit port flap


61


is maintained in the first or closed position by the force of gravity. In such an arrangement the exit port flap


61


is preferably oriented such that it will be normally closed. The exit port flap


61


is preferably formed from a refractory material such as molybdenum, graphite, or CFC. The exit port flap


61


may also be formed of a ceramic material if desired. The shapes of the exit port opening


63


and exit port flap


61


are not critical. The exit port opening


63


and exit port flap


61


are preferably square or rectangular for ease of fabrication.




Referring back to

FIG. 1

, a vacuum pump, shown schematically as block


159


, is provided for evacuating the furnace chamber. A controlled pressure gas supply


160


is also provided to introduce the processing gas into the furnace chamber. The processing gas is typically introduced at pressures elevated substantially above atmospheric pressure. Separate fluid supply and circulating means may be provided to supply coolant fluid to the furnace jacket


12


,


14


and the end enclosure


24


and to the heat exchanger coils


54


, as needed.




It will be recognized by those skilled in the art that changes or modifications may be made to the above described embodiments without departing from the broad, inventive concepts of the invention. It is understood, therefore, that the invention is not limited to the particular embodiment(s) disclosed, but is intended to cover all modifications and changes which are within the scope and spirit of the invention as defined in the appended claims. For example, the convection heating system according to this invention can be used in a vacuum heat treating furnace in which the cooling fan and heat exchanger coils are external to the furnace vessel.



Claims
  • 1. A heat treatment furnace having gas cooling or quenching capability comprising:an outer furnace wall; a heat shielded enclosure surrounding a heat treatment zone within the outer furnace wall, said enclosure being designed to retain heat within the zone and impede its outward flow therefrom, said enclosure having a plurality of orifices formed therein; and a plurality of nozzles, each in communication with one of said orifices, for injecting a cooling gas into the heat treatment zone, each of said nozzles including a flow control means for impeding unforced flow of heated gas from the heat treatment zone, said flow control means movable to an open position in response to a forced inward flow of gas to the heat treatment zone to permit the inflow of gas through the nozzle into the heat treatment zone.
  • 2. The heat treatment furnace according to claim 1 wherein the nozzles each comprise:a channel formed therethrough; a flap disposed in the channel for impeding the outward flow of a heated gas from the heat treatment zone; and means for pivotally supporting said flap in said channel.
  • 3. The heat treatment furnace according to claim 1, comprising a gas exit port disposed in a wall of the heat shielded enclosure, said gas exit port comprising a flow control means for impeding unforced outward flow of the heated gas from the heat treatment zone, said exit port flow control means movable to an open position in response to a forced outward flow of gas from the heat treatment zone to permit the outward flow of gas from the heat treatment zone.
  • 4. The heat treatment furnace according to claim 1 comprising a gas circulation means for providing circulation of a processing gas within the heat treatment zone to convectively heat or cool a work piece in the heat treatment zone.
  • 5. The heat treatment furnace according to claim 1 wherein the gas circulation means comprises a fan and a motor operatively coupled to said fan for driving said fun, wherein said fan is disposed in said heat treatment zone and said motor is mounted to said outer furnace wall externally to said heat treatment zone.
  • 6. The heat treatment furnace according to claim 1 wherein the heat shielded enclosure comprises a side wall and first and second end walls, said second end wall being movable relative to the side wall for providing access to the heat treatment zone and for closing off the heat treatment zone.
  • 7. The heat treatment furnace according to claim 6 wherein the orifices are formed in one or both of the side wall and the first end wall of the heat shielded enclosure.
  • 8. A heat treatment furnace having gas cooling or quenching capability comprising:an outer furnace wall; a heat shielded enclosure surrounding a heat treatment zone within the outer furnace wall, said enclosure being designed to retain heat within the zone and impede its outward flow therefrom, said enclosure having a plurality of orifices formed therein, said heat shielded enclosure comprising a side wall and first and second end walls, said second end wall being movable relative to the side wall for providing access to the heat treatment zone and for closing off the heat treatment zone; a plurality of nozzles each in communication with one of said orifices, for injecting a cooling gas into the heat treatment zone, each of said nozzles including a flow control means for impeding unforced flow of heated gas from the heat treatment zone and for allowing forced inflow of a process gas to the heat treatment zone; a gas exit port disposed in a wall of the heat shielded enclosure, said gas exit port comprising a flow control means for impeding unforced outward flow of the heated gas from the heat treatment zone and for allowing a forced outward flow of a gas from the heat treatment zone; and a plenum extending around the side wall and first end wall of the heat shielded enclosure over the orifices and extending along a path between the outer furnace wall and the heat shielded enclosure to divide the space between the outer furnace wall and the heat shielded enclosure into gas flow paths having opposite directions on opposite sides of the plenum, said gas flow paths including an inner path within said plenum for directing the cooling gas toward and through the orifices in the heat treatment zone and an outer path between said plenum and the outer furnace wall for directing cooling gas exiting the heat treatment zone to a heat exchanger and recirculation means.
  • 9. The heat treatment furnace according to claim 1, wherein the nozzle flow control means comprises a flap moveable by said forced inflow of gas.
  • 10. The heat treatment furnace according to claim 3 wherein the gas exit port comprises an opening formed in the beat shielded enclosure and a panel pivotally mounted in said opening for impeding the unforced outward flow of a gas from the heat treatment zone and for allowing the forced flow of cooling gas from the heat treatment zone.
  • 11. The heat treatment furnace according to claim 3, wherein the exit port flow control means comprises a flap moveable by said forced outward flow of gas.
Parent Case Info

This application is a continuation-in-part of application Ser. No. 09/597,496 filed on Jun. 20, 2000, now U.S. Pat. No. 6,533,991 the disclosure of which is incorporated herein by reference.

US Referenced Citations (3)
Number Name Date Kind
2734738 Even Feb 1956 A
4285504 Colvin Aug 1981 A
4610435 Pfau et al. Sep 1986 A
Non-Patent Literature Citations (3)
Entry
Technical data, Seco/Warwick, Jun. 2001.
Technical data, Abar Ipsen.
Technical data, VFS, Sep. 1998.
Continuation in Parts (1)
Number Date Country
Parent 09/597496 Jun 2000 US
Child 10/154457 US