The present disclosure relates to a cryostat for experiments at temperatures in the range below 2K.
Cryostats and in particular dilution cryostats for temperatures in the range below 2K are currently required and built essentially for the development of quantum computers and quantum communication devices. The arrangement of the individual temperature levels or cold plates and thus also the arrangement of experimentation places is given by the vertical arrangement of conventional cryostats
A first cooling device not shown in detail, e.g., a first level of a Gifford-McMahon (GM) cooler, comprises a first cold plate 8-1 with the first experimentation place 4-1 arranged below the first cold plate 8-1. The first cooling level 2-1 provides a temperature level of about 50K for the first experimentation place 4-1.
A second cooling device not shown in detail, e.g., a second level of the GM cooler, comprises a second cold plate 8-2 arranged below the first experimentation place 4-1. The second cold plate 8-2 or the second cooling level 2-2 has a temperature level of about 4K. The second experimentation place 4-2 is arranged below the second cold plate 8-2 at the temperature level of the second cooling level 2-2. A third cold plate 8-3 of a third cooling level 2-3 having a temperature level of about 1K is arranged below the second experimentation place 4-2. The third cooling level 2-3 is cooled by a third cooling device not shown in detail, e.g., a Joule-Thomson level.
A fourth cooling device not shown in detail, e.g., a 3He/4He dilution refrigerator system, provides the temperature levels of the fourth, fifth and sixth cooling levels 2-4, 2-5 and 2-6. The third experimentation place 4-3 is disposed on the fourth cooling level 2-4 between the fourth cold plate 8-4 and the fifth cold plate 8-5. A sixth cold plate 8-6 of the lowest cooling level 2-6 is disposed below the third experimentation place 4-3 and below the fifth cold plate 8-5. The temperature level of the fourth cold plate 8-4 is in the range between 500-700 mK. The temperature level of the fifth cold plate 8-5 is between 100-200 mK. The lowest temperature level of the sixth cold plate 8-6 and the fourth experimentation place 4-4 located below it is in the range of <100 mK.
The entire arrangement is arranged in a vacuum chamber 10. Within the vacuum chamber 10, all six cooling levels 2-1 to 2-6 are surrounded by a first heat shield 12-1. Within the first heat shield 12-1, the second to sixth cooling levels 6-2 to 6-6 are surrounded by a second heat shield 12-2. Within the second heat shield 12-2, the fourth to sixth cooling levels 2-4 to 2-6 are surrounded by a third heat shield 12-3. The lowest, sixth cooling level 2-6 is shielded by a fourth heat shield 12-4.
This conventional arrangement has the advantage that the individual temperature levels lie inside each other like onion skins and are easy to manufacture, as shown in
A so-called tabletop dilution cryostat is described in the article by Kurt Uhlig, “Concepts for a low-vibration and cryogen-free tabletop dilution refrigerator,” in Cryogencis 87 (2017) 29-34. The tabletop dilution cryostat allows a smaller construction volume due to the arrangement of still and mixing chambers, but has the same disadvantage as the prior art according to
DE 102014015665B4 describes an optical table that has a single cold plate integrated into the tabletop.
DE102016214731B3, DE102005041383A1 and DE102011115303A1 disclose NMR apparatuses or cryogenic devices in which sample head components are arranged on different temperature levels when viewed from above, below or above each other. The figure of DE102011115303A1 shows that two sample heads are arranged horizontally and are vertically offset from each other. However, DE102011115303A1 provides no written disclosure of this arrangement.
It is therefore the object of the present invention to provide a cryostat that allows improved accessibility of the experimentation places and at the same time requires a smaller construction volume.
The present document discloses a cryostat for experiments in temperatures below 2K which permits improved accessibility for the experimentation places and also a smaller construction volume. Because the experimentation places are arranged next to one another instead of one below the other, after removal of the respective heat shields these places are accessible from above and from the side, whereas in the prior art they are accessible only from the side. This simplifies various experiments and more generally the handling of the cryostat during use. The side-by-side arrangement of the experimentation places also substantially reduces the construction height of the cryostat, and it is possible to operate the cryostat in standard-height laboratory spaces, which is not possible with cryostats having a vertically suspended arrangement. Although the side-by-side arrangement of the experimentation places can lead to heat shields having a larger surface area, this drawback (increased cooling power from the various coolers being necessary for operation) is compensated by the ability to use the cryostat in standard-height laboratory spaces.
In one embodiment, a novel cryostat with improved accessibility for experiments includes a cooling device, a vacuum chamber and multiple cooling levels, heat shields and experimentation places. The cooling device is thermally coupled to multiple cooling levels that have different temperature levels during operation of the cryostat. The experimentation places are at the temperature levels of the cooling levels and are arranged side by side when viewed from above such that each of the experimentation places is accessible from above and from the side. The heat shields are associated with the cooling levels and enclose the experimentation places. The vacuum chamber encloses the cooling levels. For example, the cold plate of a second cooling level is arranged above the cold plate of a first cooling level such that a portion of the first cold plate protrudes laterally out from under the second cold plate. An experimentation place is disposed above the laterally protruding portion of the first cold plate and is accessible from above the cryostat and from the side of the cryostat.
In another embodiment, a cryostat includes first and second cold plates, first and second heat shields, first and second cooling devices, and a vacuum chamber. The first cold plate forms a first base of a first cooling level. The first heat shield encloses the first cooling level above the first cold plate. The second cold plate forms a second base of a second cooling level. The second heat shield encloses the second cooling level above the second cold plate. The second cooling level is enclosed by the first cooling level. The first cooling device is thermally coupled by a first heat conductor to the first cold plate. The second cooling device is disposed within the second cooling level and is thermally coupled by a second heat conductor to the second cold plate. The second cold plate is disposed above the first cold plate. A portion of the first cold plate protrudes laterally out from under the second cold plate such that the laterally protruding portion of the first cold plate is not covered by the second cold plate. A first experimentation place is disposed above the laterally protruding portion of the first cold plate. The first heat shield encloses the first experimentation place. The vacuum chamber encloses the first cooling level and the second cooling level.
A second experimentation place is disposed above the second cold plate, and the second heat shield encloses the second experimentation place. The second experimentation place is accessible from above the cryostat and from the side of the cryostat. The first experimentation place and the second experimentation place are arranged side by side when viewed from above the cryostat. Both the first and second experimentation places are accessible from above the cryostat and from the side of the cryostat.
Other embodiments and advantages are described in the detailed description below. This summary does not purport to define the invention. The invention is defined by the claims.
The accompanying drawings, where like numerals indicate like components, illustrate embodiments of the invention.
Reference will now be made in detail to some embodiments of the invention, examples of which are illustrated in the accompanying drawings.
The arrangement of the experimentation places of the cryostat 50 simplifies various experiments and generally the handling of the cryostat in use. By arranging the experimentation places 4-1 to 4-5 side by side, the construction height of the cryostat 50 is also significantly reduced, and it is possible to operate the cryostat in laboratory rooms of standard height, which is not possible with cryostats that have a vertically suspended arrangement. Although the side-by-side arrangement of the experimentation places of the cryostat 50 may lead to heat shields 32-1 to 32-4 with a larger surface area, this disadvantage (increased cooling power of the various coolers is required for operation) is accepted by the possibility of use in laboratory rooms with standard height.
In a preferred configuration of the cryostat 50, care is taken in the side-by-side arrangement of the experimentation places 4-1 to 4-5 to ensure that they are accessible from above and from one side.
A second cold plate 8-2 is provided which is spaced from the base plate 20 by support elements 28 and which is in thermal contact with the pulse tube refrigerator 26 and which also has a lateral circumferential border 22. In the right edge region of the second cold plate 8-2, a support element 28 supports a second partial cold plate 30-2 which is offset upwards and is located in the plane of the first partial cold plate 30-1. The second cold plate 8-2 and the second partial cold plate 30-2 are at a second temperature level of approximately 50K. A second experimentation place 4-2 is located on or above the second partial cold plate 30-2. Starting from the second cold plate 8-2, a second heat shield 32-2 encloses the second experimentation place 4-2.
Again spaced apart by support elements 28, a third cold plate 8-3 is arranged on the second cold plate 8-2 and is again thermally coupled to the pulse tube refrigerator 26 and provides a temperature level of about 4K. A support element 28 on the right side of the third cold plate 8-3 supports a third partial cold plate 30-3 offset upwards. The third partial cold plate 30-3 is located in the plane of the first and second partial cold plates 30-1 and 30-2. A third experimentation place 4-3 with a temperature level of approximately 4K is located on or above the third partial cold plate 30-3. Starting from the third cold plate 8-3, a third heat shield 32-3 encloses the third experimentation place 4-3.
Again spaced apart by support elements 28, a fourth cold plate 8-4 is arranged above the third cold plate 8-3 and has the components of a 3He/4He dilution refrigerator 34 arranged thereon. On the right side of the fourth cold plate 8-4, a support element 28 supports a fourth partial cold plate 30-4 offset upwards at the height level of the other partial cold plates 30-1 to 30-3.
In other embodiments, the cooler arranged on the fourth cold plate 8-4 is a Joule-Thomson cooler, a 1-K pot, a 3He level refrigerator, or an adiabatic demagnetization refrigerator (ADR) cooler.
Via further support elements or support walls 28, a fifth cold plate 8-5 is arranged above the fourth cold plate 8-4 at the height level of the partial cold plates 30-i at the lowest temperature level of approximately 30 mK. A fifth experimentation place 4-5 is arranged above or on the fifth cold plate 8-5. Starting from the fifth cold plate 8-5, a fifth heat shield 32-5 surrounds the fifth experimentation place 8-5.
The 3He/4He dilution refrigerator 34 between the fourth and fifth cold plates 8-4, 8-5 includes a still 36 with concentric heat exchanger 38, a mixing chamber 40, and ports 42. The still 36 is thermally coupled to the fourth cold plate 8-4 and to the fourth partial cold plate 30-4. The mixing chamber 40 is thermally coupled to the fifth cold plate 8-5.
The thermal coupling of the individual cold plates 8-i with the partial cold plates 30-i and the pulse tube refrigerator 26 or the 3He/4He dilution refrigerator 34 takes place through heat conductors 44. The pulse tube refrigerator 26 is mounted in the vacuum chamber 10 via a vibration decoupler 46.
As can be seen from the sectional views in
Although the present invention has been described in connection with certain specific embodiments for instructional purposes, the present invention is not limited thereto. Accordingly, various modifications, adaptations, and combinations of various features of the described embodiments can be practiced without departing from the scope of the invention as set forth in the claims.
Number | Date | Country | Kind |
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102019203341.5 | Mar 2019 | DE | national |
PCT/EP2020/056053 | Mar 2020 | WO | international |
This application is filed under 35 U.S.C. § 111(a) and is based on and hereby claims priority under 35 U.S.C. § 120 and § 365(c) from International Application No. PCT/EP2020/056053, filed on Mar. 6, 2020, and published as WO 2020/182671 A1 on Sep. 17, 2020, which in turn claims priority from German Application No. 102019203341.5, filed in Germany on Mar. 12, 2019. This application is a continuation-in-part of International Application No. PCT/EP2020/056053, which is a continuation of German Application No. 102019203341.5. International Application No. PCT/EP2020/056053 is pending as of the filing date of this application, and the United States is an elected state in International Application No. PCT/EP2020/056053. This application claims the benefit under 35 U.S.C. § 119 from German Application No. 102019203341.5. The disclosure of each of the foregoing documents is incorporated herein by reference.
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Number | Date | Country | |
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20210402407 A1 | Dec 2021 | US |
Number | Date | Country | |
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Parent | PCT/EP2020/056053 | Mar 2020 | WO |
Child | 17474021 | US |