This invention relates to a means of crushing crystal granules in a solution to maintain granule size, shape, and texture. This is done by an inline crushing and grinding mill with fluted rollers rotating at different speeds equipped with an emergency fluidic bypass channel and a follow-on emergency fluidic waste drain.
Aspects of the present invention relate to a mechanical means of controlling the physical characteristics of aqueous crystals involved in crystallization, including, but not limited to: size, shape, and varied size distribution through mechanical means. Managing these attributes enhances the crystallization rate by increasing the absorption and precipitation from the aqueous media by maintaining a steady state of crystal particle size.
The mechanical means of controlling the physical characteristics of the crystals and other media involved in the crystallizing process are important, because, for a given shape, the surface to area volume (SA:V) ratio is inversely proportional to size. The SA:V ratio is the amount of surface area per unit volume of an object or collection of objects. In chemical reactions involving a solid material, the SA:V ratio governs the reactivity, that is, the rate at which the chemical reaction will proceed.
For a given volume, the object with the smallest surface area (and therefore with the smallest SA:V) is a sphere, because it has the same cross-sectional perimeter in any dimension.
By contrast, objects with tiny spikes have a very large surface area for a given volume. Small crystals with spikes have a larger SA:V ratio compared to larger more spherical crystals and thus have a greater influence on crystallization rates. Where many variably sized small crystals are present, a higher proportion of crystal growth can occur, thereby reducing the growth rates of larger more spherical crystals.
The larger a crystal grows the smoother and more uniform it becomes thus reducing its reactivity and reducing the growth equilibrium. Therefore, a mechanical means of cracking and shearing larger more spherical crystals into smaller particles with a variety of shapes and sizes with rough surface texture improves the overall crystallization rate of the solution.
The invention is intended to be used in a circulating system where reactions occur between components fluidically transported by the system. Such devices may be found in a system that process leachate from landfill sites, runoff from agricultural land, effluent from industrial processes, industrial process water, municipal wastewater, animal wastes, phosphogypsum carrying pond water, commercial fertilizer production and processing, along with natural occurring aqueous solution. Also, urea, potassium sulfate, thiamine nitrate, calcium chloride, H2S hydrate crystal, methane hydrate crystal, struvite crystal, vivianite crystal, sugar, carbonate apatite in aqueous solution (which may come from a wide range of sources), various prepared solutions, and so on, may be processed using the invention.
The device is comprised of a grinding element which is itself comprised of at least two fluted grinding rollers. The grinding rollers are powered by at least one electric, or any other kind, of motor affixed to mill drive coupling gears that have different diameters. As a result, the grinding rollers rotate at different speeds. Material in the system is cracked and broken down from larger particles or crystals that have a low surface area to volume (SA:V) ratio into smaller particles or crystals that have a higher SA:V ratio. The invention has an emergency bypass pathway to divert an excess volume of large particles or crystals around the grinding roller assembly if the grinding roller assembly is temporarily overloaded. Also, the invention has an emergency dump pathway where particles are dumped to a drain if the system overloads further.
In the following description, numerous specific details regarding possible componentry (e.g., standard pipe connectors, flanges, bearing housings, gears, and rollers) are set forth. Those skilled in the art will recognize, however, that the invention may be practiced apart from these specific details. For example, the invention may be constructed of polyvinylchloride (PVC) pipe, metal, or other structural components and assembled by means of glue or adhesive, welding, fastening, bolting, and/or screwing. All such variations in materials used to construct the present invention are specifically included in the spirit and scope of the disclosure.
Similarly, details well known and widely used in the process of manufacturing such equipment (e.g., threading and assembling pipe, plastic injection molding, metal casting techniques for assembling mechanical devices, etc.) and various miscellaneous components have been omitted, so as not to unnecessarily obscure the present invention.
Referring now to
Connected to the bottom of the influent material fluid containment section 100 is standard pipe flange adapter 103 used to affix mill body 112 inlet 104 and influent material fluid containment section 100 by means of standard pipe flange adapter 103. Connected to the top end of the influent material fluid containment section 100 is sanitary drain port 105. The mill body 112 containing at least two fluted mill rollers 113a and 113b is connected to the bottom of the influent material containment section 100. The mill body 112 outlet 106 is affixed to the upper end of effluent material fluid containment section 107 by means of a standard pipe flange adapter 108.
The effluent material fluid containment section 107 comprises an inlet bypass conduit or pipe 109 externally connected to the influent material fluid containment section 100 by means of outlet bypass conduit or pipe 102. This pathway comprises an overflow pathway should material become stuck or trapped in the crushing rollers of the mill. The effluent material fluid containment section 107 is fitted at both ends with standard pipe connectors. Connected to the input end of the effluent material fluid containment section 107 is mill body 112 outlet 106. Connected to the bottom end of effluent material fluid containment section 107 is eductor pump 110. Eductor pump 110 has a high velocity input pipe 110a and a corresponding low velocity output pipe 110b. Cracked crystals are recirculated to the separate system (not shown) by means of low velocity output pipe 110b. Standard pipe flange adaptors 103 and 108 are affixed to the mill by means of gaskets.
Referring now to
The invention is used as follows: 1) Fluidically carried crystalline material is input to the influent material fluid from the attached operating device (not shown) to the influent material fluid containment section 100 by means of inlet conduit or pipe 101; 2) Fluidically carried crystalline material is conveyed by means of gravity into fluted mill rotors 113a and 113b. Mill material guides 126 cover the outer edges of fluted mill rotors 113a and 113b thus causing fluidically transported crystalline matter into the gap between fluted mill rotors 113a and 113b; 3) Larger crystals of fluidically transported material are crushed and cracked into smaller crystals of fluidically transported material; 4) Smaller crystals of fluidically transported material are transported into effluent material fluid containment section 107 where they are returned to the attached operating device (not shown) by means of eductor pump 110; 5) If larger fluidically carried crystalline material overloads the gap between fluted mill rotors 113a and 113b, it bypasses them by means of outlet bypass conduit or pipe 102. In this case, larger fluidically carried crystalline material is transported from outlet bypass conduit or pipe 102 to inlet bypass conduit or pipe 109 to the effluent material fluid containment section 107 where they are returned to the attached operating device (not shown) by means of eductor pump 110; 6) Finally, if larger fluidically carried crystalline material overloads the gap between fluted mill rotors 113a and 113b and the outlet bypass conduit or pipe 102, larger fluidically carried crystalline material is transported out of the system to a drain by means of sanitary drain port 105.
Those having skill in the art will recognize that other embodiments of the present invention are conceivable. For example, more than two fluted mill rollers 113a and 113b may be used. These additional fluted mill rollers may be arranged such that their rotating axes are above, below, parallel, perpendicular, or at any angle with respect to one another, and that these and all other embodiments are included, by reference, in the present invention.
This application makes reference to U.S. Prov. Pat. No. 63/049660 filed Jul. 9, 2020 and incorporates that application, in its entirety, by reference.
Filing Document | Filing Date | Country | Kind |
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PCT/US2021/040228 | 7/2/2021 | WO |
Number | Date | Country | |
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63049660 | Jul 2020 | US |