The present disclosure relates to a device according to the preamble of claim 1 for extracting aroma substances from vegetable aroma carriers, in particular from solid hop products such as hop pellets, into a brewing liquid. The disclosure further relates to a method for extracting aroma substances from vegetable aroma carriers into a brewing liquid.
Generic devices in the method are employed in the brewing of beer to separate solids of hop products when hopping wort and beer, which may take place at any stage during beer production. This so-called aroma hopping may take place by way of the hot brewing liquid as so-called boil hopping (Ger.: Heiβhopfung) or also after fermentation in the finished beer as so-called dry hopping or hop stuffing (Ger.: Hopfenstopfen).
In beer production, hop is added to the wort during wort production. This is also called boil hopping. In this case, it is one of the tasks of the hop to add a bitter flavor and hop aroma to the beer. Customarily, hop pellets, which contain solids, or hop extract or also natural hop is used for this purpose. In case of hopping in the boiling process, i.e. during the brewhouse process, the hop is usually added during wort boiling. To bring out the hop aroma, the hop may also be added during or after hot trub separation, i.e. in or after the whirlpool and prior to the wort cooler. In this way, the volatile hop aromas are prevented from evaporating and dissipating.
Based on changing customer demands, beer with a strongly pronounced hop aroma is increasingly sought in the market. To achieve said aroma, the beers are increasingly also dry-hopped. This means that hop is added to the beer at the cold stages, preferably after fermentation. This is called dry-hopping. Hop pellets, hop powder or natural hops are most commonly used for this purpose.
When solid hop products, in particular hop pellets, are used, there is the particular disadvantage both at the hot stages and at the cold stages that after extraction of the ingredients, large amounts of residue, so-called spent hops or hop trub particles, remain in the wort and in the beer. These solid residues have to be separated again because they are undesired in the subsequent processes and in the finished beer.
At the hot stages, when the hop is added during wort boiling, said separation subsequently takes place in the whirlpool or by means of a centrifuge, whereby hop trub particles are separated together with the protein residue, namely the hot trub.
In order to achieve proper separation, the whirlpool has to have a sufficiently large separating area so as to be able to receive and separate the hop trub. In case of beers with large amounts of hop, the whirlpool vessels will have to be dimensioned correspondingly larger, which leads to additional investment costs as well as to higher losses of wort.
During hopping, the spent hops are separated by filtration or separation, which, however, causes additional costs because the additional trub particles tend to considerably reduce the capacity and performance of the filter and because it becomes necessary to invest in a potentially custom-built centrifuge. Also, part of the hop trub particles may lie in the fermentation tank in a very compact manner, making them difficult to remove.
From DE 10 2013 101 435 A1, a device and a method for extracting aroma substances from vegetable aroma carriers into a brewing liquid are known. Either a hydrocyclone or a filter, in particular a slotted sieve filter, is used as a solids separating device for separating the insoluble hop trub particles. The use of a hydrocyclone has the disadvantage that adjustment of the capacity of said hydrocyclone to the respectively necessary capacities for hop trub separation is very intricate. Since the hydrocyclone is based on complex flow-mechanical operating principles, the dimensions of the hydrocyclone cannot be easily adjusted or changed depending on the respectively necessary capacity for hop trub separation. The use of a filter for hop trub separation has the disadvantage that these filters, in particular sieve filters, are easily clogged and will have to be laboriously cleaned for continued use.
Field tests have shown that only part of the aroma substances can be transferred into the brewing liquid in the known extraction methods. In particular, the known extraction methods fail to release all releasable aroma substances, in particular the aroma oils contained in the aroma carrier, and to transfer them into the brewing liquid. On the other hand, the known fluidized bed extraction yields insufficient results in transferring and utilizing the bitter substances contained in the aroma substances. Thus, there is always a loss in valuable α-acid, which cannot be used in dry hopping and which so far has been disposed of with the spent hops.
Therefore, the object of the present disclosure is to propose a new device and a new method for extracting aroma substances from vegetable aroma carriers, in particular hop products, into a brewing liquid, by means of which the above-described disadvantages regarding transfer and utilization of bitter substances present in the aroma carriers are avoided.
This object is attained by a device and by a method according to the teaching of the independent claims.
Advantageous embodiments of the disclosure are the subject-matter of the dependent claims.
The disclosure is based on the idea to retrofit the known devices for extracting aroma substances, which use a solids separating device, with a heater by means of which the suspension of brewing liquid and aroma carriers can be heated to an isomerization temperature. This additional option of heating the suspension to the isomerization temperature allows the α-acid contained in the aroma carriers to be converted into iso-α-acid, which is a bitter substance desired in beers. In other words, this means that the additional heat treatment using the added heater increases the formation of iso-α-acids in the suspension of brewing liquid and aroma carriers, allowing these desired bitter substances to be subsequently transferred to the brewing process.
The type of solids separating device used to perform extraction is basically optional. Different solids separating devices are known for this purpose. Extraction using a fluidized bed extractor is particularly effective and economical. The fluidized bed extractor can accommodate a suspension bed formed by the brewing liquid and the solids contained in the aroma carriers. The fluidized bed extractor additionally has at least one inlet and one outlet for the brewing liquid, wherein the brewing liquid can be pumped from the inlet through the fluidized bed extractor to the outlet by means of a feed pump. The feeding speed of the feed pump is set to a value at which the average vertical feeding speed of the brewing liquid in the fluidized bed extractor is lower than the average vertical sedimentation speed of the solid particles in the fluidized bed extractor.
The way in which the heater for heating the suspension is constructively designed is basically optional. The suspension of brewing liquid and aroma carriers can be heated in a particular simple way if a heating element installed on the fluidized bed extractor is used. In this way, the suspension contained in the fluidized bed extractor can be heated by operating the heating element until the isomerization temperature is achieved or exceeded.
As an alternative to the heating of the suspension of brewing liquid and aroma carriers in the fluidized bed extractor, the device can additionally also be retrofitted with a buffer vessel. After extraction of aroma substances, for which the fluidized bed extractor is used, the suspension will be pumped into said buffer vessel, where it can be heated for isomerization and/or cooled after isomerization. The additional buffer vessel allows the sub-process for extracting aroma substances on the one hand, which is carried out in the fluidized bed extractor, and the sub-process for isomerizing the iso-α-acids in the buffer vessel on the other hand to be carried out separately and to be decoupled. Also, the use of the buffer vessel makes it possible to temporarily store the brewing liquid with the iso-α-acids contained therein as obtained from isomerization.
As an alternative to the heater being installed directly on the fluidized bed extractor or directly on the buffer vessel, separate flow heaters may be used. They may be a heat exchanger, for example, in particular a plate heat exchanger. During heating, the suspension may also flow through the flow heater multiple times and is heated during passage by heat transfer. A suitable heat transfer medium, such as steam or hot water, may be used to heat the flow heater.
Tests have shown that an excessively long exposure to heat during isomerization of the bitter substances on the other hand can cause negative decomposition processes of the bitter substances. Thus, for the isomerization to have optimum success, the temperature has to drop back to below the isomerization temperature after a certain exposure time. To achieve that, the device can additionally be quipped with a cooler. Said cooler then serves to cool the suspension of brewing liquid and aroma carriers to a cooling temperature below the isomerization temperature after isomerization.
The type of the cooler is basically optional. A particularly simple way of cooling the suspension of brewing liquid and aroma carriers uses a cooling element that is installed on the fluidized bed extractor. With regard to a cooling of the suspension being as effective as possible, a flow cooler, such as a heat exchanger, in particular a plate heat exchanger, can again be used. The suspension will be pumped through the flow cooler by means of a pump and will be cooled by heat transfer to a coolant, such as cold water. As the case may be, cold brewing water in the flow cooler can also be heated to the desired brewing water temperature.
The effectiveness of the isomerization process also depends on the isomerization temperature selected in each case. The isomerization is particularly effective if an isomerization temperature in a range higher than 120° C. is selected. However, such high temperatures can only be achieved in the suspension—which is a water-based mixture of liquid and solids—if the isomerization takes place under pressure because otherwise undesired evaporation of the brewing liquid occurs. To allow for isomerization under pressure, it is particularly advantageous if the vessel used for isomerizing the suspension, i.e. the fluidized bed extractor or the buffer vessel, is realized as a pressure vessel.
Furthermore, it is of great importance for the success of the isomerization that the isomerization temperature is distributed as homogeneously as possible in the suspension. To achieve that, it is particularly advantageous if a mixing element by means of which the suspension can be mixed is disposed in the vessel used for isomerization, i.e. in the fluidized bed extractor or in the buffer vessel. The mixing element can be a mechanical mixer, in particular a shear stirrer, or a circulation pump by means of which the suspension can be circulated in the vessel.
To be able to avoid additional installation of a heater, it is also possible for a heater present in the brewhouse anyway to be used for isomerizing the suspension. For this purpose, the heater can be realized in the manner of a brewhouse vessel, in particular in the manner of a wort kettle. In this case, the device comprises a transfer line in which the suspension of brewing liquid and aroma carriers can be pumped into the brewhouse vessel after the extraction of aroma substances. The suspension of brewing liquid and aroma carriers can be boiled together with the wort in the brewhouse vessel for isomerization.
The method according to the disclosure is based on the idea that prior to and/or during and/or after release of the aroma substances in the solids separating device, at least part of the suspension of brewing liquid and aroma carriers is heated to an isomerization temperature at which the α-acids contained in the aroma carriers are converted into iso-α-acids. In other words, this means that the heat treatment of the suspension is carried out prior to the releasing process, during the releasing process or after completion of the releasing process. However, it is particularly preferred for the heat treatment to be carried out by heating the suspension to an isomerization temperature after the releasing process.
Preferably, the method according to the disclosure is carried out using a fluidized bed extractor as the solids separating device.
To avoid negative decomposition processes caused by an excessively long heat treatment of the suspension, it is particularly advantageous if the suspension is cooled to a cooling temperature below the isomerization temperature after a certain isomerization time.
It is particularly advantageous if an additional buffer vessel is used to untangle the processes for releasing the aroma substances by using the fluidized bed extractor on the one hand and to convert the α-acids into the iso-α-acids by heat treatment. After sufficient release of the aroma substances by corresponding processing in the fluidized bed extractor, the suspension can subsequently be pumped into a buffer vessel where it is heated to isomerize the bitter substances or cooled to interrupt the isomerization process.
The process for isomerizing or for interrupting the isomerization is particularly effective if the suspension is heated in flow or is cooled in flow.
Isomerization is particularly effective if an isomerization temperature greater than 100° C., in particular an isomerization temperature greater than 120° C., is selected. To this end, the suspension should be heated under pressure in order to avoid undesired evaporation processes.
To achieve a temperature distribution of the isomerization temperature being as homogenous as possible in the suspension, the suspension should be mixed by a mixing element during heat treatment for isomerization and/or during cooling after completion of the isomerization.
The aroma substances composing the suspension are basically optional. It is particularly advantageous if a hop product is used, in particular hop pellets. When forming the suspension, an alcoholic brewing liquid, in particular fermenting or matured beer, should be used as the brewing liquid.
To be able to avoid additional installation of a heater, it is also possible for a heater present in the brewhouse anyway to be used for isomerizing the suspension. To this end, at least part of the suspension remaining after sufficient release of the aroma substances is pumped into a brewhouse vessel, in particular into a wort kettle. In the brewhouse vessel, the suspension of brewing liquid and aroma carriers is boiled together with the wort for isomerization. A buffer vessel in which the suspension of brewing liquid and aroma carriers can be buffered may also be used in the brewhouse for temporarily storing the suspension.
Thus, there is flexibility of time between the formation of the suspension and its isomerization in the brewhouse vessel.
In the figures:
In the variant of use illustrated in
In its core, the device 01 consists of a fluidized bed extractor 09, through which different media can be pumped from various pipes and different check valves by being driven via a controllable feed pump 10. Before the actual process for extraction begins, first, CO2 from the CO2 supply duct 07 is fed into the device 01, and the different pipes and the fluidized bed extractor 09 are flooded with CO2, as illustrated in
As soon as the device 01 is flooded with CO2, first, the fluidized bed extractor is filled with dry hop pellets 12, as illustrated in
After filling-in of the hop pellets, the device 01 and in particular the fluidized bed extractor 09 is filled with beer 03. To this end, the beer is pumped by operation of the feed pump 10 out of the fermentation tank 02 through the outlet 06 and the feed line 15 into the fluidized bed extractor 09 from below until the latter is completely filled with beer and the beer flows back to the feed line 15 via a circulation duct 16. The gas contained in the system is removed from the device via the discharge 11.
Once the fluidized bed extractor 09 and the circulation duct 16 are completely flooded with beer, the outlet 06 of the fermentation tank 02 is disconnected from the device 01 by switching a valve and, as illustrated in
As soon as the hop pellets 12 are completely crushed and the hop particles contained in the hop pellets form a finely distributed suspension together with the beer 03, the feed pump 10 is briefly turned off, as illustrated in
Once the suspension bed 18 has sufficiently settled, the circulation duct 16 is closed and the outlet 06 of the fermentation tank 02 is connected to the device 01 again by opening the corresponding valve. Subsequently, as illustrated in
If it is possible within the parameters of the process, the fine filter device 21 may also be entirely omitted. The fine solid particles would then reach the fermentation tank 02 and would have to be removed from the beer 03 in another way. This decision, too, has to be made by the user in consideration of the intended use.
The circulation of the beer 03 from the fermentation tank 02 as illustrated in
In general, the process steps for forming the suspension, as illustrated in
As soon as a sufficient degree of leaching of the hop particles is reached, the outlet 06 of the fermentation tank 02 is closed.
Then, as illustrated in
After isomerization, brewing water from the brewing water supply duct 08 is pressed into the feed line 15, as illustrated in
Once the beer 03 has been completely removed from the device 01, a suitable cleaning fluid, preferably brewing water 08, is pressed into the fluidized bed extractor 09 via a duct 23, as illustrated in
To homogenize the concentration of the aroma substances dissolved in the beer 03, the beer 03 can be pumped through a circulation duct 25 and can be mixed by operation of the feed pump 10 in the fermentation tank 02, as illustrated in
The process state of the device 28 as illustrated in
In the two illustrated embodiments of the disclosure, the isomerized content of the fluidized bed extractor or of the buffer vessel was introduced into the fermentation tank. Of course, the content can also be introduced into any vessel or at any point in the brewhouse (such as into the wort kettle). Alternatively or additionally to the hop addition, the suspension can also be used during wort production. Further buffering in another buffer vessel is possible, as well, because this allows better buffering of delays between production of the isomerized suspension and its use. This use in the brewhouse, too, saves costs in connection with the addition of bitter substances during beer production.
The process state of the device 34 as illustrated in
Then, by operating a pump 37 and by suitably switching the check valves, the suspension 33 contained in the fluidized bed extractor 29 is pumped into the brewhouse vessel 36, where it is mixed with wort which is yet to be boiled. The suspension 33 is then heated and isomerized during wort boiling in the brewhouse vessel 36.
Number | Date | Country | Kind |
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10 2016 121 249.0 | Nov 2016 | DE | national |
Filing Document | Filing Date | Country | Kind |
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PCT/EP2017/078404 | 11/7/2017 | WO | 00 |