1. Field of the Invention
The present invention relates to diamond membranes and more particularly, to the structure of a diamond membrane and its preparation.
2. Description of the Related Art
A diamond membrane is made by means of forming a bonding layer by means of adhesion, electroplating or any other forming techniques, and then affixing diamond grains to the bonding layer.
When an electroplating technique is employed to form a bonding layer on a substrate for the bonding of diamond grains, the bonding power between the bonding layer and the substrate is not excellent, resulting in poor fixation of the diamond grains. Accordingly, an improvement is this regards is necessary.
The present invention has been accomplished under the circumstances in view. It is the main object of the present invention to provide a diamond membrane and its preparation that effectively enhances the bonding between the bonding layer and the substrate.
It is another object of the present invention to provide a diamond membrane and its preparation that enhances fixation of diamond grains to the bonding layer.
To achieve these and other objects of the present invention, a diamond membrane comprises a substrate having a substrate surface and defining a normal line perpendicular to the substrate surface, a first bonding layer formed on the substrate surface of the substrate with the major axes of the bonding crystals thereof extending at an angle within 0˜45-degrees relative to the normal line, diamond grains evenly distributed over the exposed outer surface of the first bonding layer to force gaps among the bonding crystals of the first bonding layer sideways for enabling the diamond grains to be partially engaged into the first bonding layer and partially protruding over the exposed outer surface of the first bonding layer, and a second bonding layer formed on the surface of the first bonding layer and the periphery of the diamond grains with the major axes of the bonding crystals thereof extending at an angle within 45˜90-degrees to let the diamond grains partially protrude over the second bonding layer.
To achieve these and other objects of the present invention, the diamond membrane preparation method includes the steps of: a) providing a substrate having a substrate surface and defining a normal line perpendicular to the substrate surface; b) bonding first bonding crystals to the substrate surface of the substrate in the form of a narrow elongated strip to form a first bonding layer on the substrate surface of the substrate to have the major axis of the first bonding crystal of the first bonding layer be controlled at an angle within 0°˜45° relative to the normal line, so that a gap is defined between each two adjacent first bonding crystals; c) evenly spreading diamond grains on the exposed outer surface of the first bonding layer to impart a pressure to the first bonding layer that forces the gaps among the first bonding crystals sideways for enabling the diamond grains to be partially engaged into the first bonding layer and partially protruding over the outer surface of the first bonding layer subject to a predetermined range; and d) bonding second bonding crystals to the outer surface of the first bonding layer and the periphery of the diamond grains to form a second bonding layer on the outer surface of the first bonding layer and a part of the surfaces of the diamond grains that protrude over the first bonding layer, and to let the diamond grains protrude over the second bonding layer at a predetermined range.
Referring to
The preparation of the diamond membrane includes the steps of:
a) providing a substrate 10 having a surface 11 and defining a normal line that is perpendicular to the surface 11;
b) bonding first bonding crystals E1 to the surface 11 of the substrate 10 in the form of a narrow elongated strip to form a first bonding layer L1 on the surface 11 of the substrate 10, wherein the first bonding crystals E1 may be kept in parallel or intersected with one another; the first bonding crystals E1 are formed of nickel, cobalt, copper, tin solder, gold, palladium, tin or silver, by means of an electroplating technique; a static treatment is employed during the electroplating process to control the direction of the major axis of each first bonding crystal E1 of the first bonding layer L1 at a predetermined angle within 0°˜45°, or preferably at zero degree relative to the aforesaid normal line, i.e., to be perpendicular to the surface 11, so that gaps G1 are defined among the first bonding crystals E1;
c) evenly spreading diamond grains D on the exposed outer surface S1 of the first bonding layer L1 to impart a pressure to the first bonding layer L1 that forces the gaps G1 sideways, enabling the diamond grains D to be partially engaged into the first bonding layer L1 and partially protruding over the outer surface S1 of the first bonding layer L1 subject to a predetermined range; and
d) bonding second bonding crystals E2 to the outer surface S1 of the first bonding layer L1 and the periphery of the diamond grains D to form a second bonding layer L2 on the outer surface S1 of the first bonding layer L1 and a part of the periphery of the diamond grains D, for enabling the diamond grains D to protrude over the second bonding layer L2 at a predetermined range, wherein the second bonding crystals E2 may be kept in parallel or intersected with one another; the second bonding crystals E2 are formed of nickel, cobalt, copper, tin solder, gold, palladium, tin or silver, by means of an electroplating technique; a static treatment is employed during the electroplating process to control the direction of the major axis of the second bonding crystal E2 of the second bonding layer L2 at a predetermined angle within 45°˜90°, or preferably, at 90 degrees relative to the aforesaid normal line, i.e., to be in parallel to the surface 11, so that gaps G1 are defined among the bonding crystals E1.
Based on the aforesaid preparation, the invention has the following features and benefits:
At first, the diamond membrane made according to the present invention has the mechanical characteristics of high hardness, low friction coefficient and high stability, therefore the diamond membrane has the nature of wear resistance and effectively improves processing precision.
Further, according to conventional techniques, a surface treatment layer of high bonding power must be formed on the surface of the tool to facilitate bonding of the second bonding layer before coating the surface of the tool with a coating layer. The invention allows direct bonding of the second bonding layer L2 without preparation of the surface treatment layer, more particularly, when a non-conductive target material is used, the bonding power will be much higher than the pre-processed deposition layer. Further, the invention has the benefit of formation step simplification.
Because the major axis of the bonding crystals E1 of the first bonding layer L1 extends at an angle within 0°˜45° relative to the normal line, pressing down the diamond grains D and the second bonding layer L2 compacts the bonding crystals E1 of the first bonding layer L1 and enhances the positioning of the diamond grains D.
In an alternate form of the present invention, the major axis of the bonding crystals E1 of the first bonding layer L1 can extend at an angle within 45°˜90° relative to the normal line, and the major axis of the second bonding crystal E2 of the second bonding layer L2 can extend at and angle within 0°˜45° relative to the normal line.
Further, a third bonding layer (not shown) may be formed on the bonding crystals E1 of the first bonding layer L1 where the major axis of the bonding crystals (not shown) of this third bonding layer extends at an angle within 0°˜45° relative to the normal line. After formation of the third bonding layer on the bonding crystals E1 of the first bonding layer L1, the bonding crystals E2 of the second bonding layer L2 is then formed on the bonding crystals of the third bonding layer.
In other words, in each two adjacent bonding layers, the major axis of the bonding crystal of one bonding layer extends at and angle within 0°˜45° relative to the normal line while the major axis of the bonding crystal of the other bonding layer extends at and angle within 45°˜90° relative to the normal line.
Thus, when compared to the conventional diamond membrane formation method, the invention eliminates the drawbacks of rough coating surface and low coating bonding power and improves the mechanical properties of the tool. Therefore, a tool made according to the present invention has high stability and long work life characteristics.
Although particular embodiments of the invention have been described in detail for purposes of illustration, various modifications and enhancements may be made without departing from the spirit and scope of the invention. Accordingly, the invention is not to be limited except as by the appended claims.
Number | Date | Country | Kind |
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97211972 | Jul 2008 | TW | national |