Patent Grant
6895764
The present invention relates generally to air conditioning and refrigeration systems, and more specifically to a cryogenic temperature control apparatus which is moveable into and out of thermal communication with a plurality of conditioned spaces to pull down the temperature of the conditioned spaces to predetermined set point temperatures.
Conventional temperature control apparatuses are commonly used in both stationary and mobile applications. Generally, these temperature control apparatuses are used to pull down the temperature in a conditioned space to a predetermined set point temperature and to maintain the temperature of the conditioned space within a range surrounding the set point temperature.
Typically, conventional temperature control apparatuses utilize conventional refrigerants (e.g., R-12, R-134(a), and the like) in a mechanical refrigeration cycle. The mechanical refrigeration cycle requires an evaporator, a condenser, and a refrigerant compressor driven by a prime mover, such as, for example, a diesel powered internal-combustion engine.
Mobile temperature control units are commonly mounted on refrigerated containers, refrigerated straight trucks, refrigerated tractor-trailer combinations, and the like, to maintain cargo, such as foods and beverages, at or near a desired set point temperature. In other applications, temperature control apparatuses can be used to condition air in a conditioned space to improve human comfort, such as, for example, in buses and passenger trains. Temperature controlled vehicles typically include an on-board dedicated mechanical temperature control apparatus for conditioning the air in the vehicle during transportation. Generally, the dedicated temperature control apparatus is also used to pre-cool the vehicle before the vehicle is loaded so that passengers and/or cargo are not exposed to temperatures which are significantly above the desired set point temperature. Because these dedicated temperature control apparatuses are incorporated in the vehicles, they are generally small and lightweight. Consequently, these dedicated temperature control apparatuses may have low cooling capacities. Relatively high cooling capacities are required to pull down a higher temperature conditioned space to the desired set point temperature in a relatively short time. For example, a conventional mechanical temperature control apparatus can take as long as six hours to cool the interior of a refrigerated trailer from an ambient outdoor temperature of 100° F. to a desired set point temperature of −20° F. During this time, the refrigerated trailer is generally parked in a lot and cannot be used to transport product until the desired set point temperature is achieved. Similarly, buses are often parked at a depot or warehouse while the on board mechanical temperature control apparatus pulls down the temperature of the air in the bus to a comfortable predetermined set point temperature.
In remote locations, such as in rural or under developed areas and on farms, electricity and diesel fuels are often not readily available. Therefore, it is often difficult to refrigerate large quantities of agricultural products until the agricultural products can be transported from the farms to processing facilities, which may be miles away. Additionally, because electricity and diesel fuel may not be readily available, the trucks and trailers that are used to transport agricultural products to the processing facilities are often not adequately refrigerated. Moreover, during loading, the trucks and trailers are frequently opened, allowing warm air to enter the trucks and trailers. Therefore, the agricultural products may be exposed to elevated temperatures for extended periods of time after being harvested. This exposure can cause spoilage and waste, contribute to the growth of harmful bacteria and parasites, and reduce the shelf life of the agricultural products.
Conventional mechanical temperature control apparatuses generally use conventional refrigerants. Additionally, conventional mechanical temperature control apparatuses are generally powered by internal-combustion engines, which generate relatively large quantities of exhaust. Practical alternatives to temperature control apparatuses that are driven by internal-combustion engines and that use conventional refrigerants are highly desirable.
A cryogenic temperature control apparatus may be used to pull down the temperature in a conditioned space to a predetermined set point temperature. In addition, to eliminating the need for conventional refrigerants, cryogenic temperature control apparatuses do not require a compressor and the associated prime mover.
The present invention provides a cryogenic temperature control apparatus, which is moveable into thermal communication with conditioned spaces to rapidly pull down the temperature in the conditioned spaces. The cryogenic temperature control apparatus can then be moved to pull down the temperature in another conditioned space.
More particularly, the present invention provides a cryogenic temperature control apparatus for conditioning air in a plurality of conditioned spaces. The plurality of conditioned spaces are spaced apart and are thermally separated. The cryogenic temperature control apparatus includes a storage tank housing a cryogen, and an evaporator coil. The evaporator coil is selectively moveable into and out of thermal communication with the plurality of conditioned spaces for alternately conditioning air in the plurality of conditioned spaces. The cryogenic temperature control apparatus also includes a flow path fluidly connecting the storage tank and the evaporator coil.
In some constructions, the flow path is a flexible fluid conduit. The flow path includes a valve for regulating the back pressure in the evaporator coil and the flow path. At least one of the conditioned spaces is a trailer and another of the conditioned spaces is a vehicle.
In some constructions, the cryogen is carbon dioxide. The cryogenic temperature control apparatus includes a fan. The fan is in fluid communication with the evaporator coil and is oriented to selectively draw air from at least one of the plurality of conditioned spaces and to direct air across the evaporator coil. The cryogenic temperature control apparatus includes a fluid conduit, which selectively fluidly connects the evaporator coil and at least one of the plurality of conditioned spaces.
Also, the present invention provides a cryogenic temperature control apparatus for conditioning the temperature of air in a plurality of thermally separated conditioned spaces. The plurality of conditioned spaces are located in a plurality of locations. The cryogenic temperature control apparatus includes a storage tank housing a cryogen and a mobile heat exchanger. The mobile heat exchanger is moveable between the plurality of locations and is alternately thermally connectable with the plurality of conditioned spaces to alternately condition air in the plurality of conditioned spaces. The mobile heat exchanger includes an evaporator coil extending through the heat exchanger and a flow path fluidly connecting the storage tank and the evaporator coil.
Further, the present invention provides a method of controlling the temperature of a plurality of conditioned spaces with a cryogenic temperature control apparatus. The method includes the acts of removably thermally connecting the evaporator coil and at least one conditioned space, transferring cryogen through the flow path from the storage tank to the evaporator coil, transferring heat from the conditioned space to the cryogen, and moving the evaporator coil out of thermal communication with the conditioned space.
In some applications, the method includes removably thermally connecting the evaporator coil and another of the plurality of conditioned spaces, transferring cryogen through the flow path from the storage tank to the evaporator coil, transferring heat from the other conditioned space to the cryogen, and moving the evaporator coil out of thermal communication with the other conditioned space.
Other independent features of the present invention will become apparent to those skilled in the art upon review of the following detailed description, claims, and drawings.
The present invention is further described with reference to the accompanying drawings, which show constructions of the present invention. However, it should be noted that the invention as disclosed in the accompanying drawings is illustrated by way of example only. The various elements and combinations of elements described below and illustrated in the drawings can be arranged and organized differently to result in constructions which are still within the spirit and scope of the present invention. Also, it is understood that the phraseology and terminology used herein is for the purpose of description and should not be regarded as limiting.
In the drawings, wherein like reference numerals indicate like parts:
As used in the following description and claims, the term “conditioned space” includes any space to be temperature and/or humidity controlled, including stationary and mobile applications for the preservation of foods, beverages, flowers, plants, and other temperature sensitive products, maintenance of a proper atmosphere for the shipment of perishable products, and the like. Additionally, as used herein and in the following claims, the term “vehicle” includes any moveable apparatus or element which includes a conditioned space, including but not limited to, trucks, buses, shipping containers, trailers, railcars, tractor-trailer combinations, and the like.
The cryogenic temperature control apparatus 10 shown in
The cryogenic temperature control apparatus 10 includes a thermally insulated or vacuum insulated storage tank 20, which is adjacent to the loading dock 12. As shown in
As shown in
As shown in
A relief valve 42 is located downstream from the filter 40 at a branch conduit. The relief valve 42 operates to prevent over pressurization. During normal operation, the pressure in the conduit 28 upstream of the relief valve 42 is between 250 and 300 psi. If the pressure in the conduit 28 exceeds a maximum pressure value, the relief valve 42 is activated to vent excess pressure. At the same time the pressure regulator 32 maintains the pressure lower than the activation pressure of the relief valve 42. The filling station 24 also includes a high-pressure cut-off switch 44 that is electrically connected to a controller 46, and is preferably set to shut off the solenoid operated fill valve 38 if the pressure in the conduit 28 rises above 200 psi downstream from the pressure regulator 32.
The accumulator tank 26 includes an inlet conduit 49 and a check valve 50. A control valve 51 allows liquid cryogen to flow out of the accumulator tank 26 to a refrigeration circuit 52. The control valve 51 is normally closed while the accumulator tank 26 is filled so that liquid cryogen can fill the accumulator tank 26. Once the accumulator tank 26 is filled, the control valve 51 can be opened to supply cryogen to the refrigeration circuit 52. Alternatively, the control valve 51 can remain open during tank filling. A vent conduit 53 extends out of the accumulator tank 26 and is operable to vent off gaseous cryogen created as a result of flashing when the pressure of the liquid cryogen is reduced from about 300 psi to about 125-135 psi. The flash gases are preferably vented out through an outlet 57. The vent conduit 53 includes a vent shut-off valve 47 for sealing the accumulator tank 26 and a level gauge 65, which is operable to monitor cryogen volume. Additionally, in some constructions of the present invention, the level gauge 65 can be used with a controller 46 to stop cryogen filling operations after a prescribed volume of cryogen is transferred.
A back pressure regulator 55 is located upstream from the outlet 57 and preferably maintains the back pressure in the accumulator tank 26 and the vent conduit 53 at approximately 125-135 psi. A pressure line 56 interconnects the pressure regulator 55 and the cryogen vapor in the storage tank 20 to maintain the necessary pressure differential within the back pressure regulator 55 so that the back pressure regulator 55 can perform its function. Cryogenic vapor is exhausted to the atmosphere through an outlet 57, which may in some constructions include a muffler (not shown) that is operable to reduce noise during venting operations. In some constructions, the cryogenic vapor is directed to a recompression/liquefaction apparatus (not shown) that recompresses and liquefies the cryogen before returning the cryogen to the storage tank 20 to be recycled through the temperature control apparatus 10.
As shown
In operation, the accumulator tank 26 is normally filled when the control valve 51 is closed and when the shut-off valve 47 is open. However, as mentioned above, in some applications, the control valve 51 can also remain open during tank filling. The controller 46 then opens the fill valve 38. Liquid cryogen pressurized to approximately 300 psi then flows through the conduit 28 into the filling station 24. The pressure regulator 32 lowers the pressure of the liquid cryogen from approximately 300 psi to approximately 125-135 psi, causing some of the cryogen to flash into gas. The liquid/gaseous cryogen mixture then moves into the accumulator tank 26. The gaseous cryogen is expelled through the vent conduit 53 and out the outlet 57. The vent conduit 53 also includes a shut-off valve 55. Once the tank level sensor 65 determines that the accumulator tank 26 is full, the filling operation is discontinued and the solenoid-operated fill valve 38 is closed.
As described above, in some constructions, the present invention can include one or more filling stations 24, which operate to, among other things, lower the pressure of cryogen. One having ordinary skill in the art will appreciate that other assemblies and apparatuses (not shown) can also or alternately be used to lower the pressure of the cryogen before the cryogen is transferred to the refrigeration circuit 52. In other constructions, the pressure of the storage tank 20 can be maintained at a lower level and in these constructions some or all of the above-describe structure may be removed.
Referring now to
As shown in
As shown in
A flow control valve 68 (e.g., solenoid-controlled, manual, proportional, or any suitable mechanism for altering flow), is positioned along the refrigeration circuit 52 to regulate the flow of cryogen out of the storage tank 20 to the heat exchanger 66. In some constructions, the valve 68 has a number of open positions so that the valve 68 can regulate the flow of cryogen out of the accumulator tank 26 to one of the heat exchangers 66. The controller 46 electrically controls the flow of cryogen to the heat exchanger 66 by selectively opening and closing the valve 68. In constructions of the present invention having multiple heat exchangers 66, the refrigeration circuit 52 can include multiple valves 68, each controlling the flow of cryogen to one of the heat exchangers 66.
An evaporator coil 70 and a blower 71 are contained within the heat exchanger 66. Warm air from the conditioned space 16 enters the heat exchanger 66 through an inlet 72. The blower 71 conveys the warm air past the evaporator coil 70, and through an air outlet 73 of the heat exchanger 66. The conditioned air thus enters the conditioned space 16 to regulate the temperature therein. As liquid cryogen flows through the evaporator coil 70, the relatively cold liquid cryogen within the evaporator coil 70 cools the relatively warm air flowing past the evaporator coil 70 before the air is expelled into the conditioned space 16. At the same time, the cryogen in the evaporator coil 70 is vaporized. The outlet 73 includes a baffle 74, which can be opened and closed, either electronically or manually, to control airflow through the heat exchanger 66. The vaporized cryogen is then vented from the evaporator coil 44 to the atmosphere. Because the cryogen is released to the atmosphere, cryogen does not enter the conditioned space 16. In other constructions, the vaporized cryogen can be re-compressed and returned to the storage tank 20 to be recycled through the cryogenic temperature control apparatus 10.
As shown in
The loading dock's internal electrical circuit (not shown) supplies electricity to the blower 71, the controller 46, and other components within the temperature control apparatus 10. It will be readily apparent to one of ordinary skill in the art that the electricity used to operate the blower 71, the controller 46, and other components within the temperature control apparatus 10 can alternatively come from other conventional power sources (not shown), such as, for example, a battery, generator, or fuel cell.
The cryogen flowing through the evaporator coil 70 is often very cold relative to the air to be conditioned. Therefore, water vapor present in the air may accumulate on the exterior of the evaporator coil 70 in the form of frost or ice, reducing heat transfer between the cryogen in the evaporator coil 44 and air in the heat exchanger 36. Therefore, the controller 46 is programmed to periodically operate the cryogenic temperature control apparatus 10 in a defrost mode.
The cryogenic temperature control apparatus 10 shown in
During a defrost mode, the controller 46 is programmed to close valve 68, preventing cryogen from entering the evaporator coil 70 and to activate the heating element 78. Additionally, the controller 46 closes the baffle 74. The heating element 78 heats the air in the heat exchanger 36, melting any ice or frost which may have formed on the evaporator coil 44. Alternatively or in addition, the blower 71 may be turned off during the defrost mode.
In some applications it may be necessary to heat the conditioned space 16, particularly in relatively cold climates. For example, heating may be desirable when the ambient air temperature is below the desired conditioned space set point temperature. When heating is required, the controller 46 is programmed to activate the heating element 78 and to close the valve 68, preventing cryogen from entering the evaporator coil 70. The baffle 74 remains open so that the blower 71 can blow air from the conditioned space 16 across the heating element 78. The heated air is then returned to the conditioned space 16 through the outlet 73.
Referring now to
In operation, a trailer 18 is backed up to the cooling chamber 80 and a seal is formed between the skirt 82 and the trailer 18. Air from the trailer 18 is then cycled through the heat exchanger 66 to condition the temperature of air in the trailer 18.
The cryogenic temperature control apparatus 110 includes a thermally insulated storage tank 120, which is adjacent to the cooling wall 111. The storage tank 120 contains a supply of cryogen, such as carbon dioxide (CO2) or nitrogen (N2). The pressure of the storage tank 120 is maintained at a pre-determined pressure value, such as, for example 300 psi. The storage tank 120 preferably operates with a filling station 124 and an accumulator tank 126 as explained above to reduce the pressure of the cryogen to approximately 125-135 psi.
A refrigeration circuit 152 extends along the cooling wall 111 fluidly connecting the accumulator tank 126 and heat exchangers 166. As shown in
The cryogenic temperature control apparatus 110 also includes flow control valves 168 positioned along the refrigeration circuit 152 for controlling the flow of cryogen from the accumulator tank 126 to the heat exchangers 166. A controller 146 preferably electrically controls the flow of cryogen to the heat exchangers 166 by selectively opening and closing the valves 168.
An evaporator coil 170 and a blower 171 are contained within each of the heat exchangers 166. Warm air from the conditioned spaces 116 enters the heat exchangers 166 through inlets 172. The blowers 171 convey the warm air past the evaporator coils 170, and through air-outlets 173 of the heat exchangers 166. The conditioned air thus enters the conditioned spaces 116 to regulate the temperature therein. As the cryogen flows through the evaporator coils 170, the relatively cold liquid cryogen within the evaporator coils 170 cools the relatively warm air flowing past them before the air is expelled into the conditioned spaces 116. The cryogen in the evaporator coils 170 is vaporized and the vaporized cryogen is then vented to the atmosphere.
Each of the heat exchangers 166 preferably include backpressure regulators 175 and temperature sensors 176 for regulating the flow of cryogen through the evaporator coils 170. However, as explained above with respect to the first construction of the present invention, when the cryogen is nitrogen, the cryogenic temperature control apparatus 110 can operate without backpressure regulators 175. The heat exchangers 166 also include heating elements 178 for operating the heat exchangers 166 in heating and defrost modes. As shown in
The cryogenic temperature control apparatus 210 includes a storage tank 220 and a heat exchanger 266, both of which are mounted on the vehicle V. The cryogenic temperature control apparatus 210 also includes two fluid conduits for moving air between the conditioned space 216 and the cryogenic temperature control apparatus 210. The first conduit is an air supply tube 267 and the second conduit is an air return tube 268. To improve air flow between the conditioned space 216 and the heat exchanger 266, fans and blowers (not shown) can be positioned within the conditioned space 216 or can be included in the air supply and return tubes 267, 268.
Cryogen flows along a flow path from the storage tank 220 into an evaporator coil (not shown), which extends through the heat exchanger 266 as described above. The blowers draw air from the conditioned space 216 through the air supply tube 267 into the heat exchanger 266 and blow the air across the evaporator coil. As the warm conditioned space air flows across the evaporator coil, the cryogen absorbs heat from the air and is vaporized. The vaporized cryogen is vented to the atmosphere and the cooled air is vented through the air return tube 268 back into the conditioned space 216.
The cryogenic temperature control apparatus 210 can also include a heating element (not shown) for defrosting the heat exchanger 266 and for heating the conditioned space 216, as described above with respect to the other constructions. The heating element is preferably a conventional electric heating coil powered by a power source 270. The power source 270 is preferably mounted on the vehicle V for movement with the cryogenic temperature control apparatus 210 between locations and can also supply power to other elements of the cryogenic temperature control apparatus 210. Alternatively, an external power source such as a battery, generator, or fuel cell (not shown) can supply power to the cryogenic temperature control apparatus 210. In still other constructions, the vehicle's engine can supply power to the temperature control apparatus 210.
Once the temperature of the conditioned space 116 is pulled down to the desired set point temperature, the vehicle V and the cryogenic temperature control apparatus 210 can be moved to a new location to condition the air in other conditioned spaces. Alternatively, the cryogenic temperature control apparatus 210 can be used to maintain the conditioned space 216 at the desired set point temperature for an extended time.
The cryogenic temperature control apparatus 210 can also be used to condition the air in buildings and temporary structures. As shown in
The cryogenic temperature control apparatus 310 includes a thermally insulated or vacuum storage tank 320, which contains a supply of cryogen, such as carbon dioxide (CO2) or nitrogen (N2) that has an elevated pressure. In the illustrated construction, the storage tank 320 is a stationary storage tank. However, in other constructions (not shown), the storage tank 320 can be a moveable storage tank. More particularly, in some constructions, the storage tank 320 can be mounted on a vehicle that is moveable between remote locations to condition a number of conditioned spaces. For example, the cryogenic temperature control apparatus 310 can be used to condition a conditioned space defined by a trailer, which is parked in a remote location (e.g., a farm field). After the cryogenic temperature control apparatus 310 pulls down the temperature of the conditioned space to a predetermined set point temperature, the cryogenic temperature control apparatus 310 can maintain the temperature of the conditioned space within a desired range surrounding the predetermined set point temperature. Alternatively, the cryogenic temperature control apparatus 310 can be moved to a new location to pull down the temperature of another conditioned space.
In applications of the present invention in which the storage tank 320 houses carbon dioxide, the carbon dioxide is preferably maintained at approximately 275-300 psi. In other applications, the cryogen can be maintained at other pressures, depending, at least in part, upon the particular cryogen used. The storage tank 320 operates with a filling station 324 and an accumulator tank 326 to reduce the pressure of the cryogen from the storage tank 320 to a pressure of approximately 125-135 psi as explained above with respect to the other constructions of the present invention.
Flexible supply conduits 352 are connected to the accumulator tank 326 and are used to supply cryogen to condition conditioned spaces in vehicles. As shown in
The truck T and the bus B define conditioned spaces 316. The temperature control apparatus 310 of the present invention is preferably operable to rapidly pull down and maintain the temperatures in the air-conditioned spaces 316 at predetermined set point temperatures. Alternatively or in addition, the temperature control apparatus 310 can provide supplemental cooling to the conditioned spaces 316, acting with on-board mobile cooling systems to condition the air in the conditioned spaces 316.
As shown in
Warm conditioned space air flows into the inlets 338, continues across the evaporator coils 334 and is discharged through the outlets 340. As the refrigerant flows through the evaporator coils 334, the refrigerant absorbs heat from the conditioned space air, and in this way pulls down or maintains the temperature of the conditioned spaces 316 at predetermined set point temperatures.
Secondary evaporator coils 344 extend through the heat exchanger housings 336. Ports 348 are positioned on the outside of the bus B and the truck T and communicate with the evaporator coils 344. When rapid pull down or supplemental cooling is required, the flexible supply conduits 352 are connected to the ports 348 via quick-connect couplers 354. The quick-connect couplers 354 preferably include check valves (not shown) that operate to prevent cryogen flow after the flexible supply conduits 352 have been disconnected from the ports 348.
Warm air from the conditioned spaces 316 enters the heat exchanger housings 336 through the inlets 338. Blowers 346 convey the warm air past the secondary evaporator coils 344, and through the outlets 340. The conditioned air thus enters the conditioned spaces 316 to regulate the temperature therein. As the liquid cryogen flows through the secondary evaporator coils 344, the relatively warm air vaporizes the cryogen. The vaporized cryogen continues through the secondary evaporator coils 344 and is vented to the atmosphere through a discharge flow path 349 and a discharge vent 350. Alternatively, a recovery conduit (not shown) can be connected to the discharge vent 350 to recover the vaporized cryogen. The recovered cryogen can then be directed to a compressor (not shown) and a condenser (not shown) that re-compresses and re-condenses the cryogen so that the cryogen can be recycled through the cryogenic temperature control apparatus 310.
Backpressure regulators (not shown) and temperature sensors 360 are positioned on the discharge flow paths 349 between the secondary evaporator coils 344 and the atmosphere. The backpressure regulators and the temperature sensors 360 are operable to further regulate the flow of cryogen through the secondary evaporator coils 344.
The cryogenic temperature control apparatus 410 is mounted on a wheeled cart 412 for movement between locations. The cryogenic temperature control apparatus 410 also includes a cooling chamber 414, an outer wall 416 that at least partially encloses the cooling chamber 414, and an opening 418 that extends through the outer wall 416 into the interior of the cooling chamber 414.
In operation, the wheeled cart 412 is moved into position adjacent to a vehicle, such as a truck, trailer, bus, van or the like so that the opening 418 communicates with the interior of the vehicle. In this manner, the cryogenic temperature control apparatus can condition air within a conditioned space defined by the truck or the trailer.
As shown in
The storage tank 420 contains a supply of cryogen, such as carbon dioxide (CO2) or nitrogen (N2). A fluid conduit 422 connects the storage tank 420 and a heat exchanger 424.
A flow control valve 426 (e.g., solenoid-controlled, manual, proportional, or any other suitable mechanism for altering flow), is positioned along the fluid conduit 422 to regulate the flow of cryogen out of the storage tank 420 to the heat exchanger 424. Preferably, a controller 428 controls the flow of cryogen to the heat exchanger 424 by selectively opening and closing the valve 426.
The heat exchanger 424 houses an evaporator coil 432 and a blower 434. The evaporator coil 432 is in fluid communication with the fluid conduit 422 to receive cryogen from the storage tank 420. When the cryogenic temperature control apparatus 410 is connected to a vehicle, warm air from the vehicle enters the heat exchanger 424 through an inlet 438. The blower 434 conveys the warm air past the evaporator coil 432, and through an air outlet 440 of the heat exchanger 424. The conditioned air thus re-enters the vehicle to regulate the temperature therein. As the liquid cryogen flows through the evaporator coil 432, the relatively cold liquid cryogen within the evaporator coil 432 cools the relatively warm air flowing past it before the air is returned to the vehicle. Contact with the relatively warm air vaporizes the cryogen in the evaporator coil 432. The vaporized cryogen is vented from the evaporator coil 432 through a vent conduit 442 to the atmosphere.
A back pressure regulator 444 is positioned along the vent conduit 442 for further controlling the flow of cryogen through the evaporator coil 432. The back pressure regulator 444 is preferably a spring actuated back pressure valve but can also be a manually operated pressure valve, a pneumatic operated valve, or any other conventional regulating valve.
As shown in
Various independent features of the present invention are set forth in the following claims.
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| Number | Date | Country |
|---|---|---|
| 2217646 | Jun 1974 | FR |
| Number | Date | Country | |
|---|---|---|---|
| 20040216469 A1 | Nov 2004 | US |
