1. Field of the Invention
The present invention relates to an apparatus for use during wellbore completion. More particularly, the invention relates to an improved expander tool for expanding tubular bodies downhole.
2. Description of the Related Art
Hydrocarbon and other wells are completed by forming a borehole in the earth and then lining the borehole with steel pipe or casing to form a wellbore. After a section of wellbore is formed by drilling, a section of casing is lowered into the wellbore and temporarily hung therein from the surface of the well. Using apparatus known in the art, the casing is cemented into the wellbore by circulating cement into the annular area defined between the outer wall of the casing and the borehole. The combination of cement and casing strengthens the wellbore and facilitates the isolation of certain areas of the formation behind the casing for the production of hydrocarbons.
It is common to employ more than one string of casing in a wellbore. In this respect, a first string of casing is set in the wellbore when the well is drilled to a first designated depth. The first string of casing is hung from the surface, and then cement is circulated into the annulus behind the casing. The well is then drilled to a second designated depth, and a second string of casing, or liner, is run into the well. The second string is set at a depth such that the upper portion of the second string of casing overlaps the lower portion of the first string of casing. The second liner string is then fixed or “hung” off of the existing casing by the use of slips, which utilize slip members and cones to fix the new string of liner in the wellbore. The second casing string is then cemented. This process is typically repeated with additional casing strings until the well has been drilled to total depth. In this manner, wells are typically formed with two or more strings of casing of an ever decreasing diameter.
Apparatus and methods are emerging that permit tubulars such as casing strings to be expanded in situ. The apparatus typically includes expander tools which are fluid powered and are run into the wellbore on a working string. The hydraulic expander tools include expandable members which, through fluid pressure, are urged outward radially from the body of the expander tool and into contact with a tubular therearound. As sufficient pressure is generated on a piston surface behind these expansion members, the tubular being acted upon by the expansion tool is expanded past its point of elastic deformation. In this manner, the inner and outer diameter of the tubular is increased in the wellbore. By rotating the expander tool in the wellbore and/or moving the expander tool axially in the wellbore with the expansion member actuated, a tubular can be expanded into plastic deformation along a predetermined length in a wellbore.
Multiple uses for expandable tubulars are being developed. For example, an intermediate string of casing can be hung off of a string of surface casing by expanding an upper portion of the intermediate string into frictional contact with the lower portion of surface casing therearound. This allows for the hanging of a string of casing without the need for a separate slip assembly as described above. Additional applications for the expansion of downhole tubulars exist. These include the use of an expandable sand screen, employment of an expandable seat for seating a diverter tool, and the use of an expandable seat for setting a packer.
Various types of expander tools are being developed. The most basic type employs a simple cone-shaped body which is run into a wellbore, and then mechanically actuated to expand outwardly. The expander tool is then pulled upward in the wellbore by pulling the working string from the surface. A basic arrangement of a conical expander tool is disclosed in U.S. Pat. No. 5,348,095, issued to Worrall, et al., in 1994 and that patent is incorporated herein in its entirety. Pulling the expanded conical tool has the effect of expanding a portion of a tubular into sealed engagement with a surrounding formation wall, thereby sealing off the annular region therebetween.
More recently, rotary expander tools have been developed. Rotary expander tools employ one or more rows of compliant rollers which are urged outwardly from a body of the expander tool in order to engage and to expand the surrounding tubular. The expander tool is rotated downhole so that the actuated rollers can act against the inner surface of the tubular to be expanded in order to expand the tubular body circumferentially. Radial expander tools are described in U.S. Pat. No. 6,457,532 and that patent is incorporated herein by reference in its entirety.
There are problems associated with the expansion of tubulars. One problem particularly associated with the use of rotary expander tools is the likelihood of obtaining an uneven expansion of a tubular. In this respect, the inner diameter of the tubular that is expanded tends to initially assume the shape of the compliant rollers of the expander tool, including imperfections in the rollers. Moreover, as the working string is rotated from the surface, the expander tool may temporarily stick during expansion of a tubular, then turn quickly, and then stop again. This spring-type action in the working string creates imperfections and, possibly, gaps in the expansion job.
Another obstacle to smooth expansion relates to the phenomenon of pipe stretch. Those of ordinary skill in the art will understand that raising a working string a selected distance at the surface does not necessarily result in the raising of a tool at the lower end of a working string by that same selected distance. The potential for pipe stretch is great during the process of expanding a tubular. Once the expander tool is actuated at a selected depth, an expanded profile is created within the expanded tubular. This profile creates an immediate obstacle to the raising or lowering of the expander tool. Merely raising the working string a few feet from the surface will not, in many instances, result in the raising of the expander tool; rather, it will only result in stretching of the working string. Applying further tensile force in order to unstick the expander tool may cause a sudden recoil, causing the expander tool to move uphole too quickly, again leaving gaps in the tubular to be expanded.
The same problem exists in the context of pipe compression. In this respect, the lowering of the working string from the surface does not typically result in a reciprocal lowering of the expander tool at the bottom of the hole. This problem is exacerbated by rotational sticking, as discussed above. The overall result of these sticking problems is that the inner diameter of the expanded tubular may not have a uniform inner circumference.
In still other cases, an expander tool can displace material as it travels along the interior of a tubing, forming a “wave” of material that can grow longer and ultimately jam the extendable member of the tool.
Further, expansion apparatus are frequently used to expand a smaller tubular into frictional engagement with larger tubulars therearound. Because there are no real indicators of the relative positions of the tubulars, an operator at the surface can never be completely sure that there is frictional contact between the tubulars.
There is a need, therefore, for an improved apparatus for expanding a portion of casing or other tubular within a wellbore. Further, there is a need for an apparatus which will provide information to the operator at the surface as to the location of the expander tool downhole. Correspondingly, there is a need for an improved expander tool which informs the operator at the surface as to the depth of the expander tool, and the extent of tubular expansion at that particular depth during the expansion process.
The present invention provides an improved expander tool for expanding a tubular body in a wellbore. According to the present invention, an expander tool is provided which includes one or more sensing devices. In operation, the expander tool is run into the wellbore on a working string, along with the sensing devices. The sensors provide information to the operator at the surface, such as the depth of the expander tool and a variety of other downhole variables.
In one embodiment, the expander tool includes a sensor for sensing the wall thickness of the expandable tubular during expansion. Thickness readings are transmitted to the operator at the surface. Once the tubular wall has been expanded to a desired amount as reflected in the wall thickness measurements, the expander tool can be translated vertically to produce a continuous, expanded length of tubular. After the tubular has been expanded along a desired length, pressure actuation of the hydraulic expander tool is relieved and the tool is removed from the wellbore.
The expander tool may also include, in one arrangement, a central processing unit for controlling the transmission of data from a sensor to the surface. The expander tool may further optionally include a recording device electronically connected to the sensor. The recording device can be retrieved from the wellbore along with the expander tool after the expansion operation is completed. Data from the recording device can then be downloaded and reviewed by the operator. The recording device provides visual confirmation to the operator and to the customer that the expansion job has been completed satisfactorily.
In yet another aspect of the expander tool of the present invention, a data transmission device is provided. The data transmission device transmits data from the sensors downhole to a server at the surface. Examples of data transmission devices include an electrical line, a fluid pulse telemetry system, and a low frequency electromagnetic wave system. In this way, the operator at the surface can monitor progress of the expansion operation downhole in real time.
So that the manner in which the above recited features of the present invention are attained and can be understood in detail, a more particular description of the invention, briefly summarized above, may be had by reference to the appended drawings. It is to be noted, however, that the appended drawings illustrate only typical embodiments of this invention and are therefore not to be considered limiting of its scope, for the invention may admit to other equally effective embodiments.
An upper annulus 105 is seen between the upper string of casing 110 and the wellbore formation 108. Likewise, a lower annulus 308 is seen between the lower string of casing 120 and the wellbore formation 108. Cement is depicted in the annular area 105 outside of the upper string of casing 110, demonstrating that the upper string of casing 110 has been cemented in place. However, the annular area 308 between the lower string of casing 120 and the formation 108 has not yet been cemented in place.
In the arrangement of
A sealing member 210 is optionally disposed on the outer surface of the lower string of casing 120. The sealing member 210 serves to provide a fluid seal between the outer surface of the lower string of casing 120U and the inner surface of the upper string of casing 110L after the lower casing string 120U has been expanded. The sealing member 210 may define one or more simple rings formed circumferentially around the lower string of casing 120U. However, it is preferred that the sealing member 210 define a deformable material lodged within a matrix of grooves 230.
The sealing member 210 is fabricated from a suitable material based upon the service environment that exists within the wellbore 100. Factors to be considered when selecting a suitable sealing member 210 include the chemicals likely to contact the sealing member, the prolonged impact of hydrocarbon contact on the sealing member, the presence and concentration of erosive compounds such as hydrogen sulfide or chlorine, and the pressure and temperature at which the sealing member must operate. An elastomeric material is most commonly preferred for the sealing member 210; however, non-elastomeric materials or polymers may be employed as well, so long as they substantially prevent production fluids from passing upwardly between the outer surface of the lower string of casing 120U and the inner surface of the upper string of casing 110L after the expandable section 120U of the casing 120 has been expanded.
Also seen on the outer surface of the lower string of casing 120 in
The lower string of casing 120 is supported on the working string 310 by a releasable carrying mechanism 300. The carrying mechanism 300 may be a threaded connection, a fluid actuated connection, or other known carrying device. In the embodiment of
In order to expand the lower string of casing 120, an expander tool 400 is provided. An exemplary expander tool 400 is shown in side view in
The expander tool 400 has a central body 402 which is hollow and generally tubular. Connectors 404 and 406 are provided at opposite ends of the body 402 for connection to other downhole components. The upper connector 404 is shown in
The central body 402 allows the passage of fluids through a hollow fluid passageway 415 of the expander tool 400, and through the connectors 404 and 406. The central body 402 has a plurality of recesses 414 to hold a respective roller 416. Each of the recesses 414 has parallel sides and holds a roller 416 capable of extending radially from the radially perforated fluid passageway 415.
In one embodiment of the expander tool 400, rollers 416 are near-cylindrical and slightly barreled. Each of the rollers 416 is supported by a shaft 418 at each end of the respective roller 416 for rotation about a respective rotational axis. The rollers 416 are generally parallel to the longitudinal axis of the tool 400. The plurality of rollers 416 are radially offset at mutual circumferential separations around the central body 402. In the arrangement shown in
While the rollers 416 illustrated in
Referring again to
The expander tool 400 is preferably designed for use at or near the end of the working string 310. In order to actuate the expander tool 400, fluid is injected into the working string 310. Fluid under pressure then travels downhole through the working string 310 and into the perforated tubular bore 415 of the tool 400. From there, fluid contacts the backs of the pistons 420. As hydraulic pressure is increased, fluid forces the pistons 420 from their respective recesses 414. This, in turn, causes the rollers 416 to make contact with the inner surface of the liner 400. Fluid finally exits the expander tool 400 through connector 406 at the base of the tool 400.
The circulation of fluids to and within the expander tool 400 may optionally be regulated so that the contact between and the force applied to the inner wall of liner 120 is controlled. The pressurized fluid causes the roller assembly 416 to extend radially outward and into contact with the inner surface of the lower string of casing 120. With a predetermined amount of fluid pressure acting on the piston surface 420, the lower string of casing 120 is expanded past its elastic limits.
A fluid outlet 325 is provided at the lower end of the working string 310. The fluid outlet 325 may serve as a fluid conduit for cement to be circulated into the wellbore 100 so that the lower string of casing 120 can be cemented into the wellbore 100 during the well completion process.
As noted, the lower connector 406 is connected to a downhole swivel 360. The swivel 360 allows the expander tool 400 to rotate within the wellbore 100 without upsetting the connection between the expandable tubular 120 and the working string 310. The expander tool 400 rotates within the wellbore 100 in order to rotate the actuated rollers 416, thereby radially expanding the lower string of casing 120 or other expandable tubular at the desired depth in the wellbore 100. The swivel 360 allows the body 402 of the expander tool 400 to be rotated by the working tubular 310 while the releasable connection 300 remains stationary. The swivel 360 is shown schematically in
The expander tool 400 of the present invention may be of any type or configuration. In this respect, it is again noted that the expander tool 400 depicted in
In order to monitor the progress of the expander tool 400 during the expansion process, the expander tool 400 of the present invention incorporates one or more sensing features. In
One type of sensing device 500 which might be used in the expander tool 400 of the present invention is a device for sensing the wall dimensions of the expandable tubular 120U. An example of such a dimensions sensor is a caliper log. Caliper logs have known utility in connection with casing inspections. A caliper log operates to detect the inner diameter of a string of pipe, and is able to detect even small irregularities therein. Caliper logs are commonly used to detect perforations or wear in a string of casing. As used in the present invention, the caliper log is run into the hole proximate to the expander body 402. The caliper log employs a number of feelers (not shown) on various sizes of calipers in order to detect the diameter of the casing wall. The wall at issue in the present application would be the inner diameter of the upper portion 120U of the lower string of casing 120. In this way, the caliper log can detect when the inner diameter of the lower string of casing 120 has been adequately expanded.
Another example of a sensor 500 for sensing the progress of expansion is a sonic log. Sonic logs are typically utilized to determine the density or porosity of a surrounding formation downhole. However, a sonic log may also be employed to determine the thickness of a surrounding steel casing. In the context of tubular expansion, a sonic log will detect an increase in wall thickness which occurs when the expandable tubular is expanded into contact with the surrounding second tubular.
A sonic log utilizes a transmitter (not shown) which emits a pulse of energy at a designated frequency and cycle. Two or more receivers are positioned to receive the pulses. The spacing of the receivers depends upon the sonde design. The time differential between when the acoustic wave train reaches the first receiver and the second receiver defines the log. The log readout will vary depending upon the thickness of the surrounding casing. Thus, the sonic log is able to detect when the lower string of casing 120U has been expanded into contact with the upper string 110.
The sonic log defines any acoustic-type log for measuring density. Such would encompass a density log and an ultrasonic log. The sonic log may be utilized in conjunction with, or in lieu of, the caliper log.
Another example of a sensor for sensing the progress of expansion is an electromagnetic thickness tool. Electromagnetic thickness tools typically consist of a transmitter coil (not shown) and a receiver coil (not shown). An alternating current is sent through the transmitter coil. This creates an alternating magnetic field which interacts both with the surrounding casing 110, 120U and the receiver coil. The signal induced in the receiver coil will be out of phase with the transmitted signal. In general the phase difference is controlled by the thickness of the casing wall. Thus, the raw log measurement is one of phase lag. In the context of tubular expansion, an electromagnetic thickness tool will detect an increase in wall thickness which occurs when the expandable tubular is expanded into contact with the surrounding second tubular.
The electromagnetic thickness tool may be utilized in conjunction with, or in lieu of, the caliper log or the sonic log. It is within the scope of the present invention to utilize any known means for sensing the thickness of the casing wall or otherwise detecting expansion of the upper portion 120U of the lower string of casing 120 into the upper string of casing 110.
The details of a sensing log, such as a caliper log, a sonic log, or an electromagnetic thickness tool are not depicted in
One of the sensors, e.g., 500′, may be a pressure gauge. The pressure gauge would be disposed in or at least proximate to the bore 415 of the expander tool 400 in order to measure fluid pressure therein. Alternatively, or in addition, sensor 500′ could be a pressure differential gauge for measuring the difference in internal and external fluid pressure of the body 402 of the expander tool 400. A pressure sensor located adjacent the expansion tool is useful for measuring the pressure of fluid used to actuate the slidable pistons of the expander tool.
In another variation, the sensors used with the expander tool are proximity sensors that measure the position of the fluid actuated pistons in relation to the body of the expander tool. In this manner, the distance of the actuated roller from the body can be calculated, and the relative distance of the tubular wall from the body can also be calculated.
In response to the problem created as material is displaced at the leading edge of the expander tool, a sensor could be placed in a position just in front of the tool in order to measure the material that is gathering at that location. For example, using sonic or magnetic sensors that are known in the art, the amount and/or dimension of the material could be gauged and the operation of the expander tool adjusted accordingly.
In yet another embodiment, contact between an expanded tubular and the wellbore therearound could be monitored with a sensor using a sonic or acoustic-type tool to produce sounds emanating from the area of expansion. The sensor that receives the sound then differentiates a sound produced by a tubular in contact with a wellbore, cement, or another tubular therearound from a sound produced by the same tubular not in contact with the wellbore, cement, or another tubular.
A means is needed in order to provide power to the sensors 500, 500′. The use of any power supply arrangement is within the scope and spirit of the present invention. Examples include downhole batteries, an electrical line run in on jointed or coiled tubing, or a downhole turbine which generates electricity in response to the circulation of drilling mud. Another example is the use of pipe as the working string which includes specially embedded wires or other conductive materials for placing downhole tools in electrical communication with a power source at the surface.
In one arrangement of the present invention, it is necessary to transmit measurements taken by the sensors, such as sensor 500, to the operator at the surface. The operator monitors data generated by the sensors 500 in real time. When the operator determines that sufficient expansion has occurred at a particular depth, the operator translates the expander tool 400 axially within the wellbore 100. This would typically occur by raising and/or lowering the drill string 310 from the surface. However, means are being developed for controllably translating the expander tool 400 through a downhole translation device (not shown). It is understood that the present invention is not limited by the means in which the expander tool is translated in the wellbore.
The transmission of data generated downhole may be accomplished in various ways. In its simplest embodiment, a free electrical wire is connected to a server 520 at the surface. A free electrical wire 515 is depicted schematically in
Numerous other techniques exist for transmitting data from downhole to an operator at the surface. One example is the use of a system for transmitting low frequency electromagnetic waves through the earth to a receiver at the surface. Alternatively, measured data values may be communicated using “fluid pulse telemetry” (FPT), also called “mud pulse telemetry” (MPT). FPT, such as described in U.S. Pat. No. 4,535,429, requires that the well fluid be circulated to transmit data to the well surface. This arrangement is oftentimes used in connection with measurement-while-drilling, or “MWD.”
Yet another alternative is the use of so called “smart pipe.” This is a working string having a conductive medium embedded in the steel wall capable of transmitting data through the pipe structure itself. In one arrangement, the smart pipe may have wires embedded within the steel walls and which are in electrical communication along the length of the pipe system. In another arrangement, the metal composition of the pipe itself may permit electrical communication along its length. In still a further system of data transmission, a wireless digital communication system may be employed. Again, however, it is within the scope of the present invention to employ any means for transmitting downhole data to the surface.
In one aspect of the present invention, the expansion process is automated. To accomplish this, a central processing unit (CPU) is first employed. The CPU may be a part of the server 520 at the surface. Alternatively, or in addition, the CPU 510 may be positioned downhole with the sensor 500. A downhole CPU 510 is depicted schematically in
As shown in
A power supply (not shown) may be provided with CPU 510 to provide adequate electrical power (e.g., a suitably sized battery) needed in the operation of CPU 510. The CPU 510 may also include a timing circuit that may be activated in coordination with surface pumping operations so that measurements recorded by recorder 530 may be more readily compared with surface instrument measurements. The central processing unit 510 controls the transmission and recording of data from the at least one sensor 500. In one automated arrangement for the expander tool 400 of the present invention, the CPU 510 transmits signals to a downhole translation apparatus (not shown) causing the expander tool 400 to be translated from downhole without raising or lowering the drill string 310 from the surface. Such signals would be transmitted when the sensor 500 confirms engagement of the expandable tubular 120U with the inner surface of the lower string of casing 110L. For example, a signal could be sent causing the downhole translation apparatus to operate for a period of time necessary to translate the expander tool 400 upward by a length of 4 inches. This cycle would be repeated for a preset number of times which is dependent upon the desired length of tubular expansion.
After the lower casing string 120 has been expanded into frictional contact with the inner wall of the upper casing string 110L, the expander tool 400 is deactivated. In this regard, fluid pressure supplied to the pistons 420 is reduced or released, allowing the pistons 420 to return to the recesses 414 within the central body 402 of the tool 400. The expander tool 400 can then be withdrawn from the wellbore 100 by pulling the run-in tubular 310. The expander tool 400 is then removed.
While the foregoing is directed to embodiments of the present invention, other and further embodiments of the invention may be devised without departing from the basic scope thereof, and the scope thereof is determined by the claims that follow.
Number | Name | Date | Kind |
---|---|---|---|
761518 | Lykken | May 1904 | A |
1324303 | Carmichael | Dec 1919 | A |
1545039 | Deavers | Jul 1925 | A |
1561418 | Duda | Nov 1925 | A |
1569729 | Duda | Jan 1926 | A |
1597212 | Spengler | Aug 1926 | A |
1930825 | Raymond | Oct 1933 | A |
2383214 | Prout | Aug 1945 | A |
2499630 | Clark | Mar 1950 | A |
2575938 | Brenneke | Nov 1951 | A |
2627891 | Clark | Feb 1953 | A |
2663073 | Bieber et al. | Dec 1953 | A |
2898971 | Hempel | Aug 1959 | A |
3087546 | Wooley | Apr 1963 | A |
3186485 | Owen | Jun 1965 | A |
3191677 | Kinley | Jun 1965 | A |
3195646 | Brown | Jul 1965 | A |
3203483 | Vincent | Aug 1965 | A |
3208531 | Tamplen | Sep 1965 | A |
3385369 | Saurenman | May 1968 | A |
3412565 | Lindsey et al. | Nov 1968 | A |
3467180 | Pensotti | Sep 1969 | A |
3498376 | Sizer et al. | Mar 1970 | A |
3669190 | Sizer et al. | Jun 1972 | A |
3712376 | Owen et al. | Jan 1973 | A |
3746091 | Owen et al. | Jul 1973 | A |
3776307 | Young | Dec 1973 | A |
3818734 | Bateman | Jun 1974 | A |
3911707 | Minakov et al. | Oct 1975 | A |
3948321 | Owen et al. | Apr 1976 | A |
4069573 | Rogers, Jr. et al. | Jan 1978 | A |
4127168 | Hanson et al. | Nov 1978 | A |
4159564 | Cooper, Jr. | Jul 1979 | A |
4288082 | Setterberg, Jr. | Sep 1981 | A |
4292588 | Smith | Sep 1981 | A |
4324407 | Upham et al. | Apr 1982 | A |
4429620 | Burkhardt et al. | Feb 1984 | A |
4531581 | Pringle et al. | Jul 1985 | A |
4588030 | Blizzard | May 1986 | A |
4697640 | Szarka | Oct 1987 | A |
4848469 | Baugh et al. | Jul 1989 | A |
4980682 | Klein et al. | Dec 1990 | A |
5130705 | Allen et al. | Jul 1992 | A |
5271472 | Leturno | Dec 1993 | A |
5398754 | Dinhoble | Mar 1995 | A |
5409059 | McHardy | Apr 1995 | A |
5409060 | Carter | Apr 1995 | A |
5435400 | Smith | Jul 1995 | A |
5472057 | Winfree | Dec 1995 | A |
5533573 | Jordan, Jr. et al. | Jul 1996 | A |
5560426 | Trahan et al. | Oct 1996 | A |
5685369 | Ellis et al. | Nov 1997 | A |
5901787 | Boyle | May 1999 | A |
6006834 | Skinner | Dec 1999 | A |
6012516 | Brunet | Jan 2000 | A |
6021850 | Wood et al. | Feb 2000 | A |
6098717 | Bailey et al. | Aug 2000 | A |
6186233 | Brunet | Feb 2001 | B1 |
6325148 | Trahan et al. | Dec 2001 | B1 |
6425444 | Metcalfe et al. | Jul 2002 | B1 |
6446323 | Metcalfe et al. | Sep 2002 | B1 |
6457532 | Simpson | Oct 2002 | B1 |
6478091 | Gano | Nov 2002 | B1 |
6488095 | Buytaert | Dec 2002 | B2 |
6561271 | Baugh et al. | May 2003 | B2 |
6789621 | Wetzel et al. | Sep 2004 | B2 |
6799637 | Schetky et al. | Oct 2004 | B2 |
20010020532 | Baugh et al. | Sep 2001 | A1 |
20010045284 | Simpson et al. | Nov 2001 | A1 |
20020145281 | Metcalfe et al. | Oct 2002 | A1 |
20020166668 | Metcalfe et al. | Nov 2002 | A1 |
20030056947 | Cameron | Mar 2003 | A1 |
20030075323 | Vercaemer et al. | Apr 2003 | A1 |
20030075339 | Gano et al. | Apr 2003 | A1 |
20030111234 | McClurkin et al. | Jun 2003 | A1 |
Number | Date | Country |
---|---|---|
2 406 490 | Apr 2003 | CA |
2 446 115 | Apr 2003 | CA |
2 414 432 | Jun 2003 | CA |
0 961 007 | Dec 1999 | EP |
1 306 519 | May 2003 | EP |
2 320 734 | Jul 1998 | GB |
2 345 308 | Jul 2000 | GB |
2 379 690 | Mar 2003 | GB |
2 381 021 | Apr 2003 | GB |
2 386 625 | Sep 2003 | GB |
WO 9324728 | Dec 1993 | WO |
WO 9918328 | Apr 1999 | WO |
WO 9923354 | May 1999 | WO |
WO 0037766 | Jun 2000 | WO |
WO 0037767 | Jun 2000 | WO |
WO 0037768 | Jun 2000 | WO |
WO 0037772 | Jun 2000 | WO |
WO 0037773 | Jun 2000 | WO |
WO 0160545 | Aug 2001 | WO |
WO 03004819 | Jan 2003 | WO |
WO 03042486 | May 2003 | WO |
Number | Date | Country | |
---|---|---|---|
20040065446 A1 | Apr 2004 | US |