The present invention relates to extrusion dies and a method for forming an extrusion die that may be utilized for forming honeycomb structures. More particularly, the invention relates to high-strength, single-piece, integrally-formed extrusion dies and methods for forming such extrusion dies.
Honeycomb structures having traverse cross-sectional cellular densities of approximately one tenth to one hundred or more per square centimeter have several uses, including catalysts substrates, solid particulate filter bodies and stationary heat exchangers. The manufacture of these honeycomb structures from plasticized powder batches comprising inorganic powders dispersed in appropriate binders is well known. U.S. Pat. Nos. 3,790,654; 3,885,977; and 3,905,743 describe extrusion dies, processes, and compositions for such manufacture, while U.S. Pat. Nos. 4,992,233 and 5,011,529 describe honeycombs of similar cellular structure extruded from batches incorporating metal powders.
As an example, reference numeral 10 (
A typical method for manufacturing the honeycomb structure 12 described above includes the steps of mixing various batch constituents with an aqueous vehicle to form a plasticized batch, extruding the plasticized batch through a die to form the walls 14, 15 of the honeycomb structure 12 and the greenware honeycomb structure, and cutting the greenware honeycomb structure to a particular length. The method also includes firing the greenware honeycomb structure to form a hardened honeycomb log structure, cutting the hardened honeycomb log structure to length, masking the end faces 18, 20 of the honeycomb structure 12, plugging certain cell channels 22 of the honeycomb structure 12, and drying the plugged honeycomb structure 12 to form a hardened filter 10.
One of the critical steps in producing these filters is the extrusion formation of the honeycomb structure through an extrusion die. While continually evolving, current commercial honeycomb structure die designs do not depart fundamentally from the die designs shown in the patents as noted herein, being mostly fabricated by the machining of solid metal blocks or billets. To make such a die, multiple apertures (feed holes) are first drilled into one face of the steel billet to form a feed hole array into which a plasticized batch material to be extruded can be supplied at high pressure. A discharge face of the die is thereafter formed by cutting a criss-crossing array of finely machined discharge slots into the billet face opposite the drilled inlet face, the slots being cut to a depth intersecting the ends of the feed holes extending from the inlet face, thereby providing fluid communication therebetween. As a result, plasticized batch material delivered through the feed holes into the intersecting discharge slots is continuously shaped by, and discharged from, the slots to form the intersecting walls and channels of the honeycomb structure.
A number of machining techniques have been adapted for the shaping of metal billets into honeycomb extrusion dies. For softer steels, the feed hole array is typically formed by mechanically drilling, while the discharge slots may be formed by a sawing procedure. If the die is formed of a harder, slower-wearing material such as a stainless steel, electrochemical machining (ECM) and electrical discharge machining (EDM) are more widely used. Generally, inlet face designs continue to feature feed holes in the shape of linear cylinders of a reasonably constant radius and a diameter in spacing dictated by the slot spacing or density of the honeycomb structure of the die.
Heretofore, most machining techniques utilized for forming these extrusion dies are limited to “line-of-sight” elements. Specifically, these techniques cannot be employed to form elements located within an interior of the die that may not be easily accessed or accessed in a straight line from an outer surface of the billet from which the die is machined. These “blind elements” may be extremely useful by allowing adjustment of the flow of the extruded material through the die during the manufacture of the honeycomb structure, such as to reduce back pressure, decrease die wear, improve part fill and proper formation of the honeycomb structure, and the like.
While other techniques have been employed to allow the formation of extrusion dies with blind-elements therein, these techniques do not allow for sufficient flexibility of design and are incapable of forming certain die details. One such method includes forming an extrusion die out of a plurality of die sections or pieces. The die sections are welded or secured to one another via binders thereby forming the entire die. One shortcoming of such dies is added cost and time required in forming such dies, as well as a relative decreased structural integrity as a result of forming the die out of multiple bonded pieces as compared to forming the die from a single-piece billet. Rapid prototyping techniques have employed the process of sintering powdered metals combined with a binding material such as a polymer or wax-based binder. In these processes, the die is constructed from the powdered metal and binder combination and then sintered into a solid die. These methods allow for the formation of die details unavailable via convention methods utilizing machined billets. However, the required use of the binder within these processes necessarily results in limitations for their use. Specifically, certain details formed within the pre-sintered dies do not retain sufficient shape, or in some cases cannot survive, the sintering process. More specifically, a pre-sintered die typically has a strength of within the range of 10 to 20 psi that allows gentle manipulation of the part, with the binder providing the structural integrity. However, as the part is sintered, a significant portion of the binder material is burned off and the strength of part approaches 3000 psi to 5000 psi prior just to sintering of the metal powder. As a result, distortion of fragile details may occur within the die. Further, certain details, such as those that would be suspended from a portion of the pre-sintered die, do not survive the sintering process.
Any one of the methods described above may also be relatively time consuming and expensive, with the average time to building ranging from days to weeks, at significant cost.
A method for manufacturing an extrusion die that provides the die with a relatively high structural integrity, while allowing blind-elements to be formed on the interior thereof so as to improve the flow characteristics of the extrusion die is desired. Further, the desired method should reduce the time and cost typically associated with the formation of extrusion dies.
According to a first aspect, the present invention is a method of forming an extrusion die, comprising the steps of depositing at least one layer of a binder-free sinterable material in an x-y plane creating a layer of unsintered material; applying irradiation to the at least one layer of unsintered material along a pattern creating a layer of sintered material; and forming the extrusion die as a single, integrally formed piece by repeating the steps of depositing and applying in a z coordinate direction that is substantially orthogonal to the x-y plane, wherein a new layer is superposed on a previously-formed layer of sintered material wherein the extrusion die includes an inlet section having a die inlet face and a plurality of open-ended feed channels extending from the inlet face toward a honeycomb forming section that is spaced from the inlet face and terminates in a die outlet face that includes a criss-crossing array of open discharge slots, and wherein the feed channels are in fluid communication with the discharge slots.
According to further embodiments of the invention, a method for forming an extrusion die is provided comprising the steps of depositing at least one layer of a sinterable material creating a layer of unsintered material; irradiating the at least one layer of unsintered material along a pattern creating a layer of sintered material; and forming the extrusion die as a single, integrally formed piece by repeating the depositing and irradiating steps, wherein a new layer is superposed on a previously-formed layer of sintered material, the extrusion die includes an inlet section having a die inlet face and a plurality of open-ended feed channels extending from the inlet face toward a honeycomb forming section that is spaced from the inlet face and terminates in a die outlet face that includes a criss-crossing array of open discharge slots interconnected with the discharge slots, the forming step includes forming the extrusion die such that the criss-crossing array of open discharge slots are formed by a plurality of pins, and wherein at least two of the pins are coupled to one another by a structural element extending between the pins and spaced along a length of the pins.
In yet another embodiment, a method of forming an extrusion die is provided, comprising the steps of depositing at least one layer of a sinterable material in an x-y plane creating a layer of unsintered material; applying a laser to the at least one layer of unsintered material along a pattern creating a layer of sintered material; and forming the extrusion die as a single, integrally formed piece by repeating steps (a) and (b) in a z coordinate direction that is substantially orthogonal to the x-y plane, wherein a new layer is superposed on a previously-formed layer of sintered material, the extrusion die includes an inlet section having a die inlet face and a plurality of open-ended feed channels extending from the inlet face toward a honeycomb forming section that is spaced from the inlet face and terminates in a die outlet face that includes a criss-crossing array of open discharge slots, the feed channels are in fluid communication with the discharge slots, and wherein the forming step includes forming the honeycomb forming section prior to forming the inlet section.
In another aspect, the invention is a method of forming an extrusion die, comprising the steps of creating a layer of unsintered material; sintering the layer of unsintered material to creating a layer of sintered material; and forming the extrusion die by repeating steps of creating and sintering wherein new layers are superposed on a previously-formed layers of sintered material, the extrusion die including an inlet section having a die inlet face and a plurality of feed channels extending from the inlet face toward a honeycomb forming section that is spaced from the inlet face and terminates in a die outlet face that includes discharge slots, the feed channels are interconnected with the discharge slots, and wherein the step of forming includes forming the honeycomb forming section prior to forming the inlet section.
According to yet another aspect of the invention, a method of forming an extrusion die is provided, comprising the steps of applying a first layer of sintered material; and thereafter forming new layers superposed on the first layer of sintered material, the extrusion die including an inlet section having a die inlet face and a plurality of feed channels extending from the inlet face toward a honeycomb forming section that is spaced from the inlet face and terminates in a die outlet face that includes discharge slots, the feed channels are interconnected with the discharge slots, and wherein the step of forming includes forming the honeycomb forming section prior to forming the inlet section.
According to further embodiments, a method of forming an extrusion die is provided, comprising the steps of applying a first layer of sintered material; and thereafter forming new layers superposed on the first layer of sintered material, the extrusion die including an inlet section having a die inlet face and a plurality of feed channels extending from the inlet face toward a honeycomb forming section that is spaced from the inlet face and terminates in a die outlet face that includes discharge slots, the feed channels are interconnected with the discharge slots, and wherein the sintered material is binder-free in a pre-sintered state.
According to further embodiment, the invention is an extrusion die, comprising an inlet section having a die inlet face and a plurality of feed channels extending from the inlet face toward a honeycomb forming section that is spaced from the inlet face and terminates in a die outlet face that includes an array of discharge slots interconnected with the discharge slots wherein the discharge slots are formed by an arrangement of pins, said pins having a pin root and an end at the outlet face and at least two of the pins are coupled to one another by a structural element other than at the pin root.
The present inventive method for manufacturing an extrusion die produces a single-piece, integrally-formed die with a relatively high structural integrity, while allowing blind-elements to be formed on the interior thereof so as to improve the flow characteristics of the extrusion die as desired. Further, the desired method reduces the time and cost typically associated with the formation of extrusion dies, and is particularly well suited for the required purpose.
These and other advantages of the invention will be further understood and appreciated by those skilled in the art by reference to the following written specification, claims and appended drawings.
For purposes of description herein, the terms “upper,” “lower,” “right,” “left,” “rear,” “front,” “vertical,” “horizontal,” and derivatives thereof shall relate to the invention as oriented in
The present inventive method includes the solidifying of superposed layers of powdered materials, such as metals and ceramics, to form an extrusion die 28 (
The depositing step includes depositing a layer of an unsintered, powdered material such as a metal, ceramic, or metal and ceramic combination. These powdered materials preferably comprise tool steels and more preferably comprise corrosive resistant super alloys such as high-strength stainless steels, however, other materials suitable for the formation of the extrusion die 28 may be utilized. It is noted that the powdered material does not include any binder materials therein, such as polymers or wax-based binders. Preferably, a layer of the powdered material at a depth of between 0.0001 inches and 0.01 inches, or even 0.0002 inches and 0.002 inches is deposited on a substrate (
As an example of the extrusion die configurations available when employing the inventive method disclosed herein,
Another embodiment of the extrusion die 28a formed via the present inventive process is illustrated in
In another embodiment, the inlet section 30b (
A square-type extrusion die is illustrated in
The present inventive process further allows construction of the extrusion die 28 in a pin-down orientation. Specifically, the pins 42 are constructed first so as to minimize the movement thereof as the die is constructed. Specifically, a building platform 74 (
In certain situations, the length and/or configuration of the pins 42 may require structural reinforcement or bracing of the same during construction of the extrusion die 28.
The present inventive method for manufacturing an extrusion die produces a single-piece, integrally-formed die with a relatively high structural integrity, while allowing blind-elements to be formed on the interior thereof so as to improve the flow characteristics of the extrusion die as desired. Further, the desired method reduces the time and cost typically associated with the formation of extrusion dies, and is particularly well suited for the required purpose.