The present application is a national phase application of International Application PCT/JP2005/020977 filed on Nov. 9, 2005 and published as International Publication WO 2006/054564 on May 26, 2006. This application claims priority from the International Application pursuant to 35 U.S.C. §365. The present application also claims priority from Japanese Patent Application No. 2004-335598 filed on Nov. 19, 2004 under 35 U.S.C. §119. The disclosures of these applications are incorporated herein in their entireties.
The present invention relates to a facility for production of high strength steel sheet or hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability.
Recently, improvement of the fuel economy of motor vehicles and reduction of the weight of vehicle chasses have been deemed important. To reduce the weight, the usage of high strength steel sheet has been increasing. However, the higher the strength, the more difficult the formability can become. In particular, the steel material can fall in elongation. Further, depending on the member to be produced, there may be a few parts where burring is performed to expand a machined hole to form a flange. A demand has also risen for a hole expandability as possibly an important characteristic.
Therefore, to address such demand, Japanese Patent Publication (A) No. 2001-192768, Japanese Patent Publication (A) No. 2001-200338, Japanese Patent Publication (A) No. 2001-3150, Japanese Patent Publication (A) No. 2001-207235, Japanese Patent Publication (A) No. 2001-207236, Japanese Patent Publication (A) No. 2002-38248, Japanese Patent Publication (A) No. 2002-309334, and Japanese Patent Publication (A) No. 2002-302734 have been provided which describe an improvement in the hole expandability in TRIP steel or composite structure steel sheet via a technique for using tempered martensite and conducting annealing heat treatment twice.
In this way, a high strength steel sheet for which hole expandability is preferred may be increasingly provided hot dip zinc coatings. On the other hand, there may also be a demand for high hole expandability high strength steel sheet without hot dip zinc coatings. In addition, relatively soft steel sheet previously used for exterior panels of motor vehicles and steel sheet with extremely large deep drawability used for oil pans, etc. may be regularly produced.
To produce such diverse types of steel sheet stably and efficiently, with a conventional single-objective type of continuous annealing facility continuously annealing steel sheet or a continuous annealing hot dip zinc coating facility able to continuously treat steel from annealing to hot dip zinc coating by a series of facilities, a plurality of such facilities can be combined and passed through. This may provide a problem of additional construction of facilities, lengthening of the production time, and increase in the production costs.
Exemplary embodiments of the present invention facilitate an efficiently production, both cost- and time-wise, of high strength steel sheet or hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability which can be used, e.g., auto parts, etc.
Facilities for the production of high strength steel sheet or hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability have been reviewed. As a result, it was determined that by arranging in a continuous annealing facility or hot dip zinc coating facility or their joint facility or continuously with the same a quenching facility, it is possible to cool annealed steel sheet down to a temperature region of the martensite transformation point or less and a tempering facility for tempering the steel sheet, and maintaining it in temperature which enables the amount of tempered martensite to be freely controlled. This can be important in securing and improving the elongation and hole expandability. For example, according to the exemplary embodiments of the present invention, in contrast which the case where the quenching facility and the tempering facility are in separate production lines and a sheet is cooled down to ordinary temperature once between the quenching and tempering, by providing a series of continuous treatment facilities, it may be possible to freely control the quenching/tempering temperature and possible to freely control the amount of tempered martensite. This can play a large role in the securing and improvement of the elongation and hole expansion rate, and the tensile strength.
Thus, according to the exemplary embodiments of the present invention, a production facility can be provided for high strength steel sheet or hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability. Using such exemplary facility, it may be possible to arrange a tempering facility for tempering the steel sheet and holding its temperature, and a recooling facility for cooling the steel sheet to 100° C. or less. Such exemplary arrangement can be provided in a continuous annealing facility or a continuous hot dip zinc coating facility or their joint facility or continuously with the same a quenching facility able to cool steel sheet after recrystallization or after recrystallization and after hot dip zinc coating down to a temperature region of the martensite transformation point or less.
According to another exemplary embodiment of the present invention, a tempering temperature rise ΔT between the quenching facility and the tempering facility can fall in a range of the following exemplary relationship (A) obtained from the post-tempering tensile strength TS and hole expansion rate λ and in that a pre-tempering temperature T (° C.) falls in a range of the following exemplary relationship (B) found from the post-tempering tensile strength TS and hole expansion rate λ.
0.028(λ−28)TS−11.5λ−40≦ΔT≦0.028(λ−28)TS−7.5λ−90 (A)
[{−2(λ−40)^2}/10^5]×(TS−580)^2−8λ+700≦T≦[{−15(λ−45)}/10^5]×(TS−580)^2−λ+555 (B)
Further, the quenching facility can include a cooling system of atomized water cooling, mist cooling, water spray cooling, and/or deep water cooling. The tempering facility can have a heating system of induction heating.
These and other objects, features and advantages of the present invention will become apparent upon reading the following detailed description of embodiments of the invention, when taken in conjunction with the appended claims.
Further objects, features and advantages of the invention will become apparent from the following detailed description taken in conjunction with the accompanying figure showing illustrative embodiment(s), result(s) and/or feature(s) of the exemplary embodiment(s) of the present invention, in which:
Described below is an exemplary embodiment a facility for the production of high strength steel sheet or hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability according to the present invention according to the present invention with reference to examples.
The facility for production of a high strength steel sheet or hot dip zinc coating according to the exemplary embodiment of the present invention, as shown in
It is possible to produce hot rolled or cold rolled steel sheet, in particular high strength steel sheet excellent in elongation and hole expandability, for example, hot rolled or cold rolled steel sheet containing by wt % C: 0.01 to 0.3%, Si: 0.005 to 2%, Mn: 0.1 to 3.3%, P: 0.001 to 0.06%, S: 0.001 to 0.01%, Al: 0.01 to 1.8%, and N: 0.0005 to 0.01% and having the balance of Fe and unavoidable impurities is heated by an annealing and heating facility 1 to Ac1 to Ac3+100° C. in temperature over 30 seconds to 30 minutes, then cooled by an annealing and cooling facility 2 by 1° C./sec or more of a cooling rate to 450 to 600° C. in temperature. Further, it is possible to hold such sheet via a holding facility 3 at 150 to 500° C. in temperature for 10 seconds to 30 minutes, then, in the case of the “no-plating pass” of
When producing an exemplary embodiment of a hot rolled or cold rolled hot dip zinc coated high strength steel sheet, in particular, the hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability, for example, a plating sheet containing by wt % C: 0.01 to 0.3%, Si: 0.005 to 2%, Mn: 0.1 to 3.3%, P: 0.001 to 0.06%, S: 0.001 to 0.01%, Al: 0.01 to 1.8%, and N: 0.0005 to 0.01% and having the balance of Fe and unavoidable impurities, such steel sheet can be heated by the annealing and heating facility 1 to the Ac1 to Ac3+100° C. in temperature over 30 seconds to 30 minutes, then cooled by the annealing and cooling facility 2 by 1° C./sec or more of a cooling rate down to 450 to 600° C. in temperature. Next, it is possible to maintain such sheet by the holding facility 3 at 150 to 500° C. in temperature for 10 seconds to 30 minutes, then passed the sheet along the “plating pass” of
When producing the exemplary embodiment of the hot rolled or cold rolled hot dip zinc coated high strength steel sheet, in particular hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability, for example a plating sheet containing by wt % C: 0.01 to 0.3%, Si: 0.005 to 2%, Mn: 0.1 to 3.3%, P: 0.001 to 0.06%, S: 0.001 to 0.01%, Al: 0.01 to 1.8%, and N: 0.0005 to 0.01% and having the balance of Fe and unavoidable impurities, it is possible to heat such sheet by the annealing and heating facility 1 to the Ac1 to Ac3+100° C. in temperature over 30 seconds to 30 minutes, then cooled it by the annealing and cooling facility 2 used as a quenching facility in the same or approximately the same way as the quenching facility 6 of Example 2 by 1° C./sec or more of a cooling rate down to the temperature region of the martensite transformation point or less. The sheet can be raised by the holding facility 3 used as a tempering facility in the same or approximately the same way as the tempering facility 7 of Example 2 to 200° C. to 500° C. in temperature, and the sheet can be maintained there for 1 second to 5 minutes.
Further, the steel sheet can be passed along the “plating pass” of
As described above with reference to Examples 1-3, the quenching/tempering facility can be arranged inside the continuous annealing facility or continuous hot dip zinc coating facility or their joint facility or continuously with the same. Further, as an exemplary arrangement, in the case of a continuous annealing facility, the quenching/tempering facility can be arranged at the exit side of the annealing and cooling facility 2 or the exit side of the holding facility 3, while in the case of a continuous hot dip zinc coating facility, the quenching/tempering facility may be arranged continuously with the hot dip zinc coating facility 4 or alloying treatment facility 5. In the case of a joint facility of a continuous annealing facility and continuous hot dip zinc coating facility, it is possible to employ an arrangement of the quenching/tempering facility alone or in combination. In the case of a double use facility, arranging a quenching/tempering facility as shown in
It is possible to arrange the quenching/tempering facility in the continuous annealing facility or hot dip zinc coating facility or their joint facility or continuously with the same being preferable, and the relationship between the tempering conditions and the hole expansion rate has been reviewed. It has been determined that the pre-tempering temperature, tempering temperature rise, post-tempering tensile strength, and hole expansion rate are in the exemplary relationships such as those shown in the graphs of
Therefore, based on these exemplary relationships, it has been ascertained that when the pre-tempering temperature, tempering temperature rise, post-tempering tensile strength, and hole expansion rate satisfy the exemplary relationship (A) and the exemplary relationship (B), the necessary tempered martensite can be secured and superior formability and hole expandability can be obtained.
0.028(λ−28)TS−11.5λ−40≦ΔT≦0.028(λ−28)TS−7.5λ−90 (A)
[{−2(λ−40)2}/105]×(TS−580)2−8λ+700≦T≦[{−15(λ−45)}/105]×(TS−580)2−λ+555 (B)
If falling in the ranges of the above-described exemplary relationships (A) and (B) and/or if controlling them in the ranges in accordance with need or preference, it is possible to obtain high strength steel sheet or hot dip zinc coated high strength steel sheet having a balance of the tensile strength and hole expansion rate in accordance with the user demands or preferences.
Further, the above-described exemplary hole expansion rate λ is the rate when punching a 150 mm square test piece by a conical punch having a punching hole diameter of 10 mm, a clearance of 12%, and a peak angle of 60° and expanding the hole in a direction so that its burrs can become external portion(s) or side(s) by a forming speed of 0.5 mm/sec.
The amount of the tempered martensite of the high strength steel sheet obtained by the exemplary embodiments of the present invention can be, in terms of the area ratio, 0.5 to 60% in range. The tempered martensite may be evaluated by the exemplary method of observation under an optical microscope, observation of the martensite by LePera etching, quantization by LePera etching, polishing of the sample (alumina finish), dipping in a corrosive solution (mixed solution of pure water, sodium pyrosulfite, ethyl alcohol, and picric acid) for 10 seconds, then again polishing, rinsing, then drying the sample by cold air. After drying, the structure of the sample can be examined at, e.g., 1000× for a 100 μm×100 μm area by a Luzex apparatus and measured for area to determine the area of the tempered martensite. Further, the tensile strength and elongation can be evaluated by, e.g., conducting a tensile test in a direction perpendicular to the rolling direction of a JIS No. 5 tensile test piece.
Regarding the specifications of this exemplary quenching facility, since a certain extent of rapid cooling down to the martensite transformation point or less may be preferred, atomized water cooling, mist cooling, water spray cooling, or deep water cooling can be preferable, and even gas cooling may be used if giving an equal or better cooling rate as with atomized water cooling, mist cooling, water spray cooling, or deep water cooling.
Further, regarding the specifications of this tempering facility, to obtain an exemplary greater compactness of the facility or a reliable tempering effect in a short time, the heating system is preferably induction heating, but tempering by a gas burner, radiant tube oven, or electric heater oven may also be used if giving the same extent of greater compactness and reliable tempering effect in a relatively short time as with the induction heating. The exemplary cooling system of this exemplary re-cooling facility is not limited, and if considering the unnecessary oxidation and discoloration of zinc plating, gas cooling can be preferable.
The continuous annealing facility or hot dip zinc coating facility or joint facility of the same for installation of the quenching/tempering facility may also include a pre-plating facility for improving the plating adhesion. Further, for adding surface lubrication, corrosion resistance, and chemical conversion treatment, various post-treatment facilities may also be provided at the exit sides of the continuous annealing facility or hot dip zinc coating facility or joint facility of the same.
Further, the exemplary use of the exemplary embodiment of the facility according to the present invention can be advantageous for the elongation and hole expandability of high strength steel sheet, as described herein.
For example, the exemplary steel having the composition of ingredients of Table 1 can be produced by a vacuum melting furnace, cooled to solidify, then reheated up to 1200 to 1240° C. and finish rolled at 880 to 920° C. (sheet thickness of 2.3 mm), cooled, then held at 600° C. for 1 hour so as to reproduce the coiling heat treatment of hot rolling. Such obtained hot rolled steel sheet may be descaled by polishing, 7 cold rolled (1.2 mm), then annealed using a continuous annealing simulator at 750 to 880° C.×75 seconds, hot dip zinc coated at 490° C., then alloyed at 510° C. Thereafter, such steel sheet can be treated under the conditions of Table 2 to confirm the effects of the exemplary embodiments of the facilities according to the present invention.
Experiments [1]-[3] of Table 2 below are comparative examples, wherein experiment [1] shows the case of quenching as is with no tempering, experiments [2] and [3] show the case of passage through a conventional continuous hot dip zinc coating facility and cooling (quenching) to ordinary temperature, then tempering by a separate line, and experiments [4]-[7] show the case of treatment by the exemplary embodiments of the facility according to the present invention.
As described herein, the improvement in the material quality can be due to tempering by the exemplary embodiments of the facility according to the present invention by providing an improvement of the hole expandability, in addition, the improvement can also be provided by the ability to control the quenching/ tempering temperature conditions to any conditions gives an effect of improvement of the material quality including an improvement of the elongation.
According to the exemplary embodiments of the present invention, it is possible to provide a facility able to efficiently produce, both cost-wise and time-wise, high strength steel sheet or hot dip zinc coated high strength steel sheet excellent in elongation and hole expandability used for auto parts etc. and is extremely high in value industrially.
The foregoing merely illustrates the exemplary principles of the present invention. Various modifications and alterations to the described embodiments will be apparent to those skilled in the art in view of the teachings herein. It will thus be appreciated that those skilled in the art will be able to devise numerous modification to the exemplary embodiments of the present invention which, although not explicitly shown or described herein, embody the principles of the invention and are thus within the spirit and scope of the invention. All publications, applications and patents cited above are incorporated herein by reference in their entireties.
Number | Date | Country | Kind |
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2004-335598 | Nov 2004 | JP | national |
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PCT/JP2005/020977 | 11/9/2005 | WO | 00 | 3/11/2009 |
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WO2006/054564 | 5/26/2006 | WO | A |
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