Silicon of ultra-high purity is used extensively in the electronics and photovoltaic industries. High purity granular polysilicon materials with only trace of amounts of contamination measured at the part per billion levels are often required. Producing such materials is possible, but then extreme care must be taken in any handling, packaging or transportation operations to avoid subsequent contamination.
Conventional feeding and flow control technologies used to convey granular polysilicon materials includes components having metal in their construction (e.g., valves, conduits, etc.). When protective coatings or linings are compromised, or when wear occurs at the interfaces of moving parts, for example, contamination from metal parts can occur, which is unacceptable.
Valves used to regulate the flow of granular materials that rely on components that move relative to the material being conveyed, such as butterfly dampers, pinch bladders, diaphragms, gates, etc., have a disadvantage of potentially crushing granules of the material, which can both reduce its value and potentially damage the components and other equipment.
In addition, conventional feeders may not provide sufficient control over the rate of flow granular polysilicon and/or the flow rate range. Conventional vibrating tray feeders may achieve a feed rate range between a lowest controllable feed rate and a highest controllable feed rate of only about 1:50, but a much higher feed rate range is desirable. Other conventional approaches allow higher feed rate ranges to be achieved, but only with apparatus having multiple parts within the control volume of the flowing material that must move relative to each other, such as auger screws, rotary vanes and other similar structures. Multiple parts in relative motion within the control volume, however, leads to a greater risk of contamination.
Also, such conventional feeders are difficult to purge with a suitable process gas and/or clean in part because of their complicated constructions. The multi-piece constructions typically require an extensive use of seals to prevent leakage through components that move relative to each other.
Conventional vibratory solids conveyors typically have a rigid container constrained by linkages and/or springs that can be driven by an eccentric weight assembly coupled to an electric motor or an electromagnetic drive in a desired motion, such as elliptical rotation that includes horizontal and vertical components.
Conventional approaches to conveying solids, including vibratory conveyors, screw augers, belt conveyors and other similar devices, are not capable of achieving high performance over a large range of flows while ensuring that ultrahigh purity is maintained.
Described below are apparatus and methods that address some of the drawbacks in conventional approaches to feeding solids materials, including granular polysilicon.
According to a first implementation, a feeder operable to convey a divided solids material comprises a conduit and an actuator. The conduit has a hollow body with a length, a first end, a second end opposite the first end and a displaceable body segment defined along at least a portion of the length. The displaceable body segment has at least a first fixable location positionable at a first fixed location. The actuator is positioned to apply force to the conduit and controllable to cause selected flow of divided solids material in a feed direction extending generally from the first end to the second end.
In some implementations, the actuator is supported by the conduit and moves with the displaceable body segment during a feeding operation. The actuator can comprise a rotating offset mass, and the rotating offset mass can be operated to generate oscillating motion of the displaceable body segment and the attached actuator. The displaceable body segment can be cyclically displaced through a closed trajectory having at least one of a vertical component and a horizontal component.
In some implementations, the displaceable body segment has a second fixable location downstream of the first fixable location in the feeding direction and positionable at a second fixed location.
In some implementations, the displaceable body segment has a curved profile with a length longer than a shortest distance separating the first fixable location and the second end, and the actuator is attached to the displaceable body segment approximately at an inflection point for a curve of the curved profile.
In some implementations, the actuator is positioned stationarily and has a controllably movable element that contacts the displaceable body segment. In some implementations, the actuator comprises a linear actuator. In some implementations, the actuator comprises an elongate member having a distal end pivotable into contact with the displaceable body segment to selectively move the displaceable body segment and a proximal end pivotably connected to a pivot point.
In some implementations, the displaceable body segment comprises an intermediate section configured to collect a portion of the divided solids material when the displaceable body segment is at rest. The intermediate section can be configured to collect a leading edge of a flow of divided solids material received from the first end of the feeder.
In some implementations, the intermediate section is configured for positioning at a slight angle relative to horizontal, and there is a first upright section positioned upstream of the intermediate section and a second upright section positioned downstream of the intermediate section.
In some implementations, the conduit is made from a resilient material. In some implementations, the conduit comprises polyurethane hose material.
In some implementations, a feeder comprises a conduit and an actuator. The conduit has an inlet end, an outlet end opposite the inlet end and a displaceable body segment along a feeding direction between the inlet end and the outlet end. The inlet end is configured for connection to a source of material to be fed by the feeder. The outlet end is configured to convey divided solids material from the feeder to a location downstream of the feeder. The outlet end is positioning at a lower height than the inlet end. The displaceable body segment is sized to have a length longer than a shortest distance between the inlet end and the outlet end and to define a curved profile with at least one inflection point when installed. When installed, the displaceable body segment defines an intermediate section configured to support accumulated material therein at an angle of repose of the material, and to reduce movement of material in the feeding direction when the displaceable body segment is at rest. The actuator is connected to the displaceable body segment to controllably displace the displaceable body segment in a feeding operation.
In some implementations, the actuator is controllable to displace the displaceable body segment in an oscillating cycle. In some implementations, the actuator is manually operable. In some implementations, the displaceable body segment extends substantially from the inlet end and substantially to the outlet end.
In some implementations, the intermediate section is caused to be displaced from a substantially lateral position at which no flow occurs to a downwardly tilted position at which flow towards the outlet end occurs.
In some implementations, the actuator can be configured to move at a rate sufficient to cause displacement of the displaceable body section such that the solids material moves at a selected rate between a low trickle flow and a high bulk filling flow.
According to a method implementation, a method of conveying a divided solids material with a feeder comprises using a sensor to monitor an amount of the divided solids material being conveyed with the feeder, receiving signals from the sensor at a controller and sending control signals from the controller to the feeder to control a flow rate of the divided solids material over a flow rate range ratio of greater than 1:50 of a low flow rate to a high flow rate.
According to some implementations, using a sensor to monitor an amount of the solid material being conveyed can comprise configuring the sensor to measure a loss of weight of the solid material from a source of the material positioned upstream of the feeder. According to some implementations, using a sensor to monitor an amount of the solid material being conveyed comprises configuring the sensor to measure a gain in weight from the solid material conveyed to a receptacle positioned downstream of the feeder.
According to some implementations, the feeder can comprise a conduit segment for receiving the solid material and that is displaceable according to the control signals from the controller to achieve a desired flow rate of the material from the feeder. In some implementations, the flow rate range ratio is greater than 1:4000.
According to another method implementation, a method of conveying divided polysilicon comprises receiving divided polysilicon from a source into a conduit of a feeder, controllably moving the conduit through an operation path in which the conduit is positioned in at least a first position at which flow through the conduit occurs and a second position at which flow through the conduit is stopped, and receiving the divided silicon material flowing through the conduit, when the conduit is positioned at least in a first position, in a receptacle positioned downstream of an outlet end of the conduit.
Desirably, the feeding and flow control technologies described herein tend not to rely on reducing the cross section of the conduit, which reduces damage to the material being conveyed and the equipment.
The foregoing and other objects, features, and advantages will become more apparent from the following detailed description, which proceeds with reference to the accompanying figures.
Referring to
The body 102 has a first end 104 and an opposite second end 106. Between the first and second ends 104, 106, there is a displaceable body segment 108 that can be caused to displace or move, or to vibrate or oscillate (and in some cases, to do so cyclically), as described below in greater detail, to cause material to be conveyed or fed from the first end 104, through the body 102 and to the second end 106. The body 102 is formed of one or more materials and to have selected dimensions such that it can be moved between different positions as desired, which is described below in more detail.
In some implementations, the material to be fed or conveyed is one or more solids materials comprising particles, such as a divided solids material. Polysilicon is one example of a material that can be provided as a divided solids or finely divided solids material. Other materials can also be fed using the described apparatus and methods. Also, the material to be fed can be a mixture of two or more different component materials.
A material is defined to be flowable if the bulk stress acting on the material exceeds the material's bulk strength. In the case of a granular material, one measurement used to indicate a material's ability to flow is the angle of repose of the material. The angle of repose of a granular material is the steepest angle of descent or dip relative to the horizontal plane to which the material can be piled without slumping (at this angle, the material on the slope face is on the verge of sliding). A material that has a lower tendency to flow may be comprised of particles with a relatively high degree of inter-particle friction, such as particles of a material having more angular shapes that tend to interlock with each other. In the same way, flowability of a material tends to be decreased if there is plastic deformation of particles, partial melting of particles, moisture present in and/or around particles and/or another factor tending to increase adhesion between particles.
In some cases, when particles of a material are at rest and not flowing, e.g., because the angle of repose for the material has not been exceeded, the particles can nevertheless be induced to flow by disturbing them, such as through applying energy to them, e.g., in the form of vibrations.
In the case of granular polysilicon (also sometimes referred to herein as granulate polysilicon and granules), the polysilicon particles are generally spheroids having an average diameter of 0.25 to 20 mm, such as an average diameter of 0.25-10 mm, 0.25-5 mm, or 0.25 to 3.5 mm. As used herein, “average diameter” means the mathematical average diameter of a plurality of granules. Individual granules may have a diameter ranging from 0.1-30 mm, such as 0.1-20 mm, 0.1-10 mm, 0.1-5 mm, 0.1-3 mm or 0.2-4 mm. The individual particles of any given material may have generally the same size and shape, or they vary in size and shape.
The open cross section of the tubular body 102 or conduit can sized to be at least 2-3 times greater than the major dimension of the largest target particle size such that flow of particles of such size through the feeder is facilitated. In specific examples, the major dimension is a diameter that is 2-3 times, 5 times, 10 times or 100 times the diameter of the largest target particle size of the material to be conveyed.
The first end 104 can be connected to an upstream source of material to be fed, such as a material comprising solids. In the illustrated implementation, the first end 104 is connected to the outlet end of a hopper H, which is stationary. Instead of the hopper H, the feeder 100 can be connected downstream of any other component or conduit that supplies material to be fed. The second end 106 can be connected to an outlet from which material fed by the feeder 100 is discharged as shown, or to any other downstream location. As shown in
The displaceable body segment 108 can have a first fixable location 110, e.g., a location that is positionable at a first fixed location. Similarly, the displaceable body segment 108 can have a second fixable location 112, e.g., a second location that is fixable at a second fixed location. The first and second fixable locations 110, 112 define the approximate ends of the displaceable body segment 108. In the illustrated implementation, the first fixable location 110 is located in the area of the first end 104, and second fixable location 112 is located in the area of the second end 106. In other implementations, the first and second fixable locations 110, 112 can be located at points spaced from the first and second ends 104, 106, respectively, to define displaceable body segments of different lengths and characteristics.
Typically, at least the displaceable body segment 108 is configured to be sufficiently flexible to be displaced as desired, such as by selecting appropriate material(s) and their dimensions. As one example, in the illustrated implementation, the body 102, including the displaceable body segment 108, is formed of a section of flexible polyurethane hose or conduit having an appropriate uniform diameter and wall thickness. In other implementations, one or more different materials may be used for the body 102 and/or displaceable body segment 108, and/or non-uniform wall thicknesses and/or diameters may be used.
As shown in the implementation of
As also shown in
Referring to
Referring again to
By displacing or moving the displaceable body segment 108 as described in more detail below, the material M can be moved or feed through the body 102 along a feed path as indicated generally by the arrows F (see, e.g.,
The steady state cyclical motion of the feeder 100 in a representative operating scenario is shown in
As the displaceable body segment 108 moves down to the right, the material M, and specifically, the granules that make up the material M, have a relative velocity that is in a direction up to the left, thereby creating a void V in the material M as shown schematically in
Subsequently, as shown in
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As described above,
By maintaining the motion of the displaceable body segment 108 predominately in the XY plane, feeding efficiency is maximized, and potential drawbacks from motion with components in the Z direction (i.e., perpendicular to the page), which could introduce torsional vibrations adverse to feeding, can be avoided. Thus, the motor 130 (as well as the cylinder 230 described below) can be positioned such that the forces they produce act predominately in the XY plane. For the motor 130, the mounting can also be configured so that the swinging mass does not introduce torsional vibration effects that would tend to counteract smooth feeding.
As described, the motion of the displaceable body segment 108, and the resulting performance of the feeder, is influenced by a number of variables. One such variable is the direction in which the motor is rotated relative to the shape or profile of the displaceable body section 108, including whether the motor's rotation tends constrict or relax the curved sections in the displaceable body segment 108. Another variable concerns the magnitude and direction of residual forces in the displaceable body segment 108 tending to resist the action of the motor (e.g., due to the stiffness of the hose material and/or its configuration). Depending upon the particular needs for a specific situation, the user may determine that one direction of rotation is preferred over the other and/or that the displaceable body segment should be configured to have selected characteristics.
At high speeds, the eccentric weight of the motor 130 provides both a high centrifugal force and a high frequency to produce a high feed rate. Conversely, at low speeds, the eccentric weight provides a low centrifugal force amplitude at a low frequency. The motion of a representative feeder was studied using video analysis. Feed rate data corresponding to the video analysis was obtained by evaluating a mass vs. time relationship of the feeder's discharge. The mass of the material collected from the discharge was weighed in a container supported by a load cell (such as, e.g., a Model RAP3 single point load cell provided by Loadstar Sensors of Fremont, Calif.). Comparisons of this measured feed rate data with a calculated feed rate based on modelling the feeder as a positive displacement pump show excellent agreement.
By way of contrast to conventional vibratory feeders, the feeder 100 operates in a different frequency-amplitude regime. Referring again to
The electric motor 130 may be configured to be controlled by a variable frequency drive (VFD), either as a separate component or provided integrally with the motor. Such a VFD-controlled motor provides precise control over the speed of the motor, and thus allows a desired flow rate to be achieved. As a result of the frequency-amplitude control of the feeder, the feeder is capable of a flow rate range of 1:4700, which is far greater than the flow rate range of about 1:50 achievable with a conventional vibrating tray feeder.
Because the feeder 100 can achieve flow rates ranging from a trickle flow at very low motor speeds to very high flow rates at high motor speeds, it can be operated in a variety of different ways, which increases the flexibility of its use. As one example, in operating the feeder to reach a target weight of material to be output, the feeder can be operated at high speed for an initial period and then at low speed for a subsequent period as the target weight is approached. Thus, the feeder is very well suited for use in a continuous process where flow control of material is required. The feeder can be used as a gravimetric feeder in bulk filling applications.
As also shown in
Another implementation of the feeder can be described in connection with
The member 420 has a distal end 421 that is configured to contact the body 102 within the displaceable body segment 108, and an opposite proximal end 423. The proximal end 423 of the member 420 is pivotably supported to pivot about a pivot point 414. As is described below in more detail, it is only the member 420 that is connected at the pivot point 414, and not any part of the body 102. Rather, the displaceable body segment 108 of the body 102 is contacted by the distal end 421 of the member 420. In the illustrated implementation, the displaceable body segment 108 is contacted by a band clamp 422 that at least partially encircles it and extends lengthwise from the distal end 421 proximally over a length of the band clamp 422.
By moving the member 420, e.g., by pivoting the member 420 about the pivot point 414, the displaceable body segment 108 is moved and more specifically, an intermediate section I thereof can be rotated to a selected angle, such as to shut off feeding (zero feed rate), to allow for feeding at a maximum rate and/or to allow for feeding at rates between the zero feed rate and the maximum feed rate. In some implementations, the member 420 extends along the displaceable body segment over at least a portion of the length of the member 420.
The pivoting operation can be accomplished in discrete operations or as in cyclical operations. Further, the rotation of the intermediate section I can be accomplished manually or as step in an automatic feeding process. In the illustrated implementation, the member 420 has a forked end (not shown) that straddles the body 102 and is pivotably supported at the pivot point 414.
The intermediate section I (which tends to move greater distances that other sections of the displaceable body segment 108 during operation) is shown schematically in
The geometry of the intermediate section I, including its slope, the radii of its bends and inflection point, are selectively controlled by a number of factors, including the length and path of the body 102/displaceable body segment 108, the location of the pivot point 414 (i.e., the vertical distance of the pivot point 414 below and the horizontal distance offset from the first end 104), the geometry of the member 420, the angle of rotation of the member 420 and the flexural properties of the body 102. For a displaceable body segment 108 formed of a length of hose, the flexural properties of the body account for the type of hose, the thickness of the hose material and other similar properties. Desirably, moving the member 420 to cause the intermediate section I to rotate as described does not collapse displaceable body segment 108 or otherwise interfere with feeding taking place within it except as intended.
In the feeder 400, the second end 106 of the body 102 can be fixed or movable. If the second end 106 is fixed, it may be relatively aligned in the vertical direction with the first end 104 as shown in
The member 420 can be described as defining an offset radius (or pivot length) between the point at which it acts on the displaceable body segment 108 (i.e., at the member/body interface, which is at the location of the band clamp 422 in the illustrated implementation) and the pivot point 414.
Overall, the geometry of the member 420 and the location of the pivot point 414 are influenced by the design envelope of the feeder 400. As shown in
Given a larger allowed envelope in which to provide flexing of the body 102 between at least the first fixed end 104 and the member/body interface (as well as between the member/body interface and any downstream fixed point, such as a fixed second send 106, if present), the length of the body 102/displaceable body segment 108 could be extended, permitting the member/body interface (band clamp 422) to be positioned to coincide with the pivot point 422. In this case, the member 420 is configured to rotate about itself without changing in height or horizontal position (i.e., a zero radius offset), while at the same time keeping stresses experienced in the body within acceptable levels. For example, as shown in
Instead of the member 420, other arrangements can be used. For example, an actuator similar to the actuator 230 could be configured to move the displaceable body segment 108. Other approaches to generating an appropriate torque and/or force applied at a suitable location(s) are also possible. As another example, it is also possible to have the force or torque applied very close to or at the pivot point 414.
In one operation mode, the member 420 is moved manually to change the angle of the intermediate section I of the body 108.
As illustrated in
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In the representative implementation of
As stated, the feeder 400 can be implemented for manual operation, e.g., using a lever or other device to move the intermediate section as desired. Thus, the feeder 400 can be controlled manually to shutoff flow, to deliver maximum flow or to deliver material at any intermediate flow rate. Optionally, such a manual implementation could be achieved without requiring a source of power or any control circuit.
In other implementations, the feeder 400 can be implemented with a system having at least some automated control of feeding. For example, the member 420 or other device could be configured for control by a control circuit and one or more servo motors to control the angle of the member 420, which could optionally be varied during a feeding cycle.
In the described feeder implementations, only the segments of the body and structures attached to it (such as a motor or a member) move during operation, so there are no internal moving parts. In the illustrated implementations, the feeders typically eliminate at least one valve, which is one specific component having internal moving parts. As a result, the feeders tend to be less costly to produce and maintain and more reliable than conventional feeding technologies having internal parts. Many internal parts are subject to fouling during operation and are prone to wear faster, particularly in applications where feeding of granular polysilicon material is involved. Maintenance or repair of such internal parts requires considerable downtime.
In the described feeder, there are fewer components and fewer different materials that contact the material being fed than in conventional feeders. As a result, there is a much lower risk of contamination to the material being fed. In some implementations of the feeder used for feeding high purity granular polysilicon, the body 102 is made of a single length of polyurethane hose that poses little contamination risk.
As stated, at least the displaceable body segment 108, or the entire body 102, can be configured to be flexible so that it can be resiliently deformed or distorted, e.g., through the positions shown in
In the illustrated implementation, the suction hood 300 is positioned recessed from the outlet 307 by a selected distance R, which also helps adjust the effect of the suction force to prevent it from adversely affect the feeding of material. In some implementations, the suction hood 300 is recessed from the end of the outlet by about 0.5 inch.
In view of the many possible embodiments to which the disclosed principles may be applied, it should be recognized that the illustrated embodiments are only preferred examples and should not be taken as limiting in scope. Rather, the scope is defined by the following claims. I therefore claim all that comes within the scope and spirit of these claims.
Filing Document | Filing Date | Country | Kind |
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PCT/US2017/057448 | 10/19/2017 | WO | 00 |
Number | Date | Country | |
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Parent | 15333652 | Oct 2016 | US |
Child | 16344790 | US |