Information
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Patent Grant
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6436233
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Patent Number
6,436,233
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Date Filed
Thursday, May 18, 200024 years ago
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Date Issued
Tuesday, August 20, 200222 years ago
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Inventors
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Original Assignees
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Examiners
- Silverman; Stanley S.
- Halpern; Mark
Agents
-
CPC
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US Classifications
Field of Search
US
- 162 52
- 162 56
- 162 237
- 162 246
- 162 17
- 162 18
- 162 19
- 162 57
- 162 68
- 162 242
- 162 243
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International Classifications
- D21C110
- D21C510
- D21C706
- D21C708
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Abstract
A feed system for a cellulose pulp treating vessel (such as a continuous digester) is not limited by the required L/W ratio of the pump feeding a wood chip slurry to a high pressure transfer device, the feed system may be kept at a low temperature to minimize flashing of liquid into steam, and a return conduit from the treatment vessel to the transfer device high pressure inlet may be eliminated. Some of the liquid is removed from the slurry just before the low pressure inlet to the transfer device, and/or just after the high pressure outlet, to reduce the L/W ratio of the slurry by at least 0.25, e.g. from 3.0:1 to 2.25:1 just before the low pressure inlet, and from 7.0:1 to 5.0:1 substantially immediately after the high pressure outlet.
Description
BACKGROUND AND SUMMARY OF THE INVENTION
U.S. Pat. Nos. 5,476,572; 5,622,598; 5,635,025; 5,766,418; and 5,968,314 disclose methods and devices for feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel that have revolutionized the art of treating comminuted cellulosic fibrous material to produce cellulose pulp. The disclosed inventions, sold under the trademark LO-LEVEL® by Ahlstrom Machinery Inc., of Glens Falls, N.Y. employ one or more slurry-type pumps for treating and transferring comminuted cellulosic material to one or more treatment vessels. Not since the initial development of the continuous cooking process in the 1940s and 1950s have such dramatic improvements been made to equipment used to transfer material to a treatment vessel, for example, a continuous or batch digester. This is confirmed by the broad acceptance of this technology by the Pulping Industry.
The present invention introduces improvements to the systems and methods described in the above patents which further simplify and enhance the effectiveness of the methods and devices disclosed therein.
The prior art systems for introducing a slurry of comminuted cellulosic fibrous material, for example, as exemplified by the system disclosed in U.S. Pat. No. 5,476,572, use a two-stage pressurization and transfer of slurry. In the first stage, the slurry is pressurized to a first pressure and transferred to a high-pressure transfer device, such as, a High Pressure feeder designed and marketed by Ahlstrom Machinery. The first stage pressurization and transfer is typically performed using a specially-designed slurry pump which handles slurries of material and liquid. In the second stage the High Pressure Feeder pressurizes the slurry to a second pressure, higher than the first pressure, by exposing the material to a high pressure liquid stream, and transports the slurry to a treatment vessel, for example, a continuous or batch cellulose pulp digester. However, according to this prior art, the amount of cellulose material, such as, wood chips, that can be transferred to the High Pressure Feeder by the slurry pump, per unit volume of liquid, is limited by the capacity of the pump to transfer solid material.
Typically, the relative amount of liquid present in slurry is indicated by a “liquid-to-solids” ratio, or, in the case of transferring slurries of wood chips, a “liquid-to-chip” ratio, or, more specifically, a “liquor-to-wood” (L/W) ratio. The liquid-to-wood ratio is a dimensionless ratio of the volume of the liquid present in the slurry to the volume of the wood present in the slurry. Conventional High Pressure Feeders can accept slurries having L/W of below 3.0:1, typically even below 2.5:1. The lower limit of the L/W ratio of a slurry being introduced to a High Pressure Feeder is about 2.0:1. Note that a reduction in L/W ratio from 3.0:1 to 2.0:1 corresponds to a 25% reduction in the volume of liquid that must be accepted by the High Pressure Feeder, or a corresponding 25% increase in the volume of chips that can be processed by the High Pressure Feeder.
According to one aspect of the present invention, the volume of liquid that is transferred to the High-pressure Feeder is reduced so that more wood chips can be introduced and processed in the digester system being fed per revolution of the High Pressure Feeder. This aspect of the invention has the further advantage of allowing for the reduction in size of the High-pressure Feeder for a given project, or allowing for an increase in the capacity of a production-limited facility.
After introducing the slurry of chips to a high-pressure transfer device, for example, a High-Pressure Feeder sold by Ahlstrom Machinery, the slurry is displaced from the feeder by a flow of high-pressure liquid, typically at a pressure between about 5 and 15 bar gage, provided by a high-pressure pump. Typically this flushing of the slurry from the feeder by the liquid results in the slurry being propelled to a treatment vessel having a L/W ratio of between about 4.0:1 to 10.0:1, and is typically greater than 5:1, often greater than 7:1, sometimes greater than 9:1. For example, for a L/W ratio of 9:1, the volume of liquid present in the conduit transferring the slurry from the feeder to the treatment vessel, for example, to a pulping digester, the volume of liquid is 9 times the volume of the cellulose material, such as, wood chips. Typically, this volume of liquid is required in order to flush the chips from the pockets of the feeder. This relatively large volume of liquid requires a relatively large conduit in which to pass the slurry from the feeder to the digester and sufficient energy to propel the relatively large volume of liquid up to the top of the pressurized digester.
The L/W ratio of the slurry exiting the High Presser Feeder is also a function of the equipment which feeds the slurry to the feeder. In conventional, “suck through” systems typically having a pressurized chip chute the L/W ratio of the slurry introduced to the High Pressure Feeder is about 2.0-2.5:1. In “pump through” systems, such as Lo-Level Feed Systems sold by Ahlstrom Machinery, the L/W ratio of the slurry introduced to the High Pressure Feeder is about 3.0-3.5:1.
According to another embodiment of this invention, the liquid volume in the slurry transferred from the feeder to the treatment vessel is minimized by removing at least some of the liquid from the slurry after the slurry has been discharged from the feeder and before the slurry is introduced to the treatment vessel. One advantage of this embodiment of the invention is that, with reduced liquid volume, the diameter of the transfer conduit to the treatment vessel can be reduced. Reducing the size of this conduit has the further advantage of reducing the sizes, and hence the cost, of the associated valves and instruments that are located in this conduit.
The above embodiment of this invention is particularly effective in limiting the amount of heat returned to the feed system from the treatment vessel, for example, via what is known as the “Top Circulation” or “TC” line. As recognized in the art, exposing the feed system, for example, the High-pressure Feeder, to liquids having temperatures at or above 100° C. can cause flash-evaporation of this liquid (known as “flashing”) when the liquids are exposed to the atmospheric pressures present in the vicinity of the high-pressure feeder. However, when excess liquid is removed from the slurry when introducing the slurry to the treatment vessel, for example, by using of a Top Separator, heat present in the treatment vessel can migrate, for example, by convection, to the vicinity of the Top Separator and be drawn out of the vessel with the removal of liquid from the Top Separator. This heat can raise the temperature of the liquid returned to the feed system via the TC line. This increased TC line temperature can cause flashing and vibration in the feed system and interfere with the normal operation of the feed system.
One way of reducing the potential of returning undesirable heat to the feed system is by limiting the flow of liquid removed from the slurry as the slurry is introduced to the treatment vessel. According to this embodiment of the invention, a liquor removal device is located in the conduit which feeds the slurry to the treatment vessel, preferably, near to or adjacent the inlet of the treatment vessel. At least some liquid is removed from the slurry using this device and returned to the feed system such that less liquid needs to be removed from the slurry as the slurry is introduced to the vessel. This reduced removal of liquid from the vessel reduces the potential for heat in the vessel to be withdrawn with the removed liquor and returned to the feed system.
One embodiment of this invention is a method of feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising or consisting of: a) slurrying the material with a slurrying liquid to produce a slurry of material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure and transferring the slurry to a high-pressure transfer device; c) introducing the slurry to the high-pressure transfer device; d) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure; e) transferring the slurry from the high-pressure transfer device to the treatment vessel; f) introducing the pressurized slurry to the treatment vessel; and g) removing at least some of the liquid from the slurry between a) and c) so that the slurry introduced to the high-pressure transfer device in c) has a second liquid-to-material ratio lower than the first ratio. In a preferred embodiment, at least some of the liquid removed during step g) is used as at least some of the slurrying liquid of step a). Preferably g) is performed immediately prior to c), but f) may be performed at any time after a).
The present invention also may further include h) treating the material in the treatment vessel to produce cellulose pulp, for example, by a continuous or non-continuous (that is batch) chemical pulping process. For example, those processes disclosed in U.S. Pat. Nos. 5,489,363; 5,536,366; 5,547,012; 5,575,890; 5,620,562; 5,662,775; 5,824,188; 5,849,150; and 5,849,151 and marketed by Ahlstrom Machinery under the trademark LO-SOLIDS®.
The first liquid-to-material volume ratio is used in slurrying the material in a) is typically greater than 2.75:1, preferably about 2.75 to 3.25 to 1.0. This ratio is typically required in order for the slurry pump, for example, a Hidrostal® screw-type-impeller slurry pump manufactured by Wemco of Salt Lake City, Utah, or a pump provided by Lawrence Pumps Inc. of Lawrence, Mass. to operate properly. Though for other types of slurry pumps this L/W ratio may even be lower, for example, 2.50:1 or less. The second liquid-to-material ratio (that is, the ratio for the slurry introduced to the high-pressure feeder) is preferably about 2.50:1 or less, preferably about 1.75 to 2.25:1, or even less than about 1.75:1. In a preferred embodiment of this invention the second L/W ratio is at least 0.25 less than said first liquid-to-material ratio, most preferably at least 0.50 less than said first liquid-to-material ratio.
The first pressure to which the slurry is pressurized typically is in the range of 1 to 7 bar gage; the second pressure is typically in the range of 5 to 15 bar gage.
The present invention also includes a system for feeding comminuted cellulosic fibrous material to a treatment vessel, comprising or consisting of: a first vessel containing a slurry of comminuted cellulosic fibrous material having a first liquid-to-material volume ratio; a high-pressure transfer device having a low-pressure inlet, a low-pressure outlet, a high-pressure inlet, and a high-pressure outlet connected to the treatment vessel; means for pressuring and transferring the slurry from the first vessel to the low-pressure inlet of the high-pressure transfer device; a means for removing at least some of the liquid from the slurry located between the pressurizing means and the low-pressure inlet to provide a slurry having a liquid-to-material ratio less than the first ratio; and a means for transferring the slurry from the high-pressure outlet to the treatment vessel.
The first vessel is preferably a Chip Chute or Chip Tube provided by Ahlstrom Machinery. The high-pressure transfer device is preferably a High-pressure Feeder as sold by Ahlstrom Machinery. The means for pressurizing and transferring the slurry to the high-pressure transfer device may be a chip pump for pumping the slurry into the high-pressure transfer device or a pump (for example, a pump known as a Chip Chute Circulation Pump) for drawing the slurry into the high-pressure transfer device, or any other suitable conventional pressurizing device. The means for removing liquid from the slurry is preferably a cylindrical device having a concentric cylindrical screen through which the slurry passes and from which liquid can be removed. One such device is an In-line Drainer sold by Ahlstrom Machinery. A means for transferring the slurry from the high-pressure outlet of the high-pressure transfer device preferably comprises a high-pressure pump that provides pressurized liquid to the high-pressure inlet of the high-pressure transfer device. The preferred liquid-to-material ratios and pressures are preferably as described above.
Another aspect of the invention comprises a method of feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising or consisting of: a) slurrying the material with a slurrying liquid to produce a slurry of material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure and transferring the slurry to a high-pressure transfer device; c) introducing the slurry to the high-pressure transfer device; d) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure using a pressurized liquid and to produce a slurry of liquid having a second liquid-to-material volume ratio, higher than the first ratio; e) discharging the slurry having the second volume ratio from the high-pressure transfer device; f) transferring the slurry to the treatment vessel; g) introducing the pressurized slurry to the treatment vessel; and h) removing at least some of the liquid from the slurry between e) and g) so that the slurry introduced to the treatment vessel in g) has a third liquid-to-material ratio lower than the second ratio.
In a preferred embodiment, at least some of the liquid removed during h) is used as the pressurized slurrying liquid for d). In another preferred embodiment at least some of the liquid removed during h) is used as the slurrying liquid in a). Also h) is preferably performed immediately after e) but h) may be performed at any time after e) but before g). The present invention also may further include i) treating the material in the treatment vessel to produce cellulose pulp, for example, by a continuous or non-continuous, that is batch, chemical pulping process. For example, those processes disclosed in U.S. Pat. Nos. 5,489,363; 5,536,366; 5,547,012; 5,575,890; 5,620,562; 5,662,775; 5,824,188; 5,849,150; and 5,849,151 and marketed by Ahlstrom Machinery under the trademark LO-SOLIDS®. Also the method is preferably practiced to, between a) and c), remove some of the liquid from the slurry before the slurry is introduced into the high pressure device so that the slurry has a fourth liquid to material ratio at least about 0.25 less than the first ratio.
In one preferred embodiment of this invention, the above method is performed such that h) is practiced prior to g) so that a slurry having a third liquid-to-material ratio is introduced to the treatment vessel. This embodiment also preferably additionally includes i) removing excess liquid from the slurry during or shortly after the process of g), that is, while introducing the slurry to the treatment vessel, or shortly thereafter, and also j) combining the liquids removed at g) and i) and using at least some of the combined liquids as the pressurizing medium in d). Furthermore, j) preferably is practiced by monitoring the temperature of the combined liquids and regulating the flow of the liquids in h) and i) so that the temperature of the combined liquid is maintained below a specified value. The specified temperature value typically ranges from about 90 to 120° C. depending upon the prevailing pressure in the feed system.
The first liquid-to-material volume ratio is used in slurrying the material in a) is typically greater than 2.75:1, that is, about 2.75 to 3.25 to 1.0. This ratio is typically required in order for the slurry pump, for example, a Hidrostal® screw-type-impeller slurry pump manufactured by Wemco, to operate properly. For other types of slurry pumps this L/W ratio may even be lower, for example, 2.50:1 or less. The second liquid-to-material ratio is typically greater than 2.50:1, for example about 5.0:1 or greater, preferably about 7.0:1 or greater, or even 9.0:1 or greater. The third liquid-to-material ratio is typically at least about 0.25 less than the second liquid-to-material ratio, most preferably at least about 0.50 less than the second liquid-to-material ratio.
The first pressure to which the slurry is pressurized typically is in the range of 1 to 7 bar gage; the second pressure is typically in the range of 5 to 15 bar gage.
According to another aspect of the invention there is provided a cellulosic fibrous material treating system comprising: A material slurry vessel. A high pressure transfer device including a low pressure inlet, low pressure outlet, high pressure inlet and high pressure outlet. The slurrying vessel operatively connected to said low pressure inlet and outlet. A treatment vessel connected to the high pressure outlet. Means for removing some liquid from slurry moving between the high pressure outlet and treatment vessel and circulating the removed liquid to the high pressure inlet. And, the system devoid of a connection from the treatment vessel to the high pressure inlet. The system may also include means for removing some liquid from the slurry between said slurrying vessel and low pressure inlet, and returning removed liquid to the slurrying vessel.
The present invention also includes a system for feeding comminuted cellulosic fibrous material to a treatment vessel having an inlet, comprising or consisting of: a first vessel containing a slurry of comminuted cellulosic fibrous material having a first liquid-to-material volume ratio; a high-pressure transfer device having an low-pressure inlet, a low-pressure outlet, a high-pressure inlet and a high-pressure outlet; means for pressuring and transferring the slurry from the first vessel to the low-pressure inlet of the high-pressure transfer device; means for diluting the slurry and transferring the slurry from the high-pressure outlet to the treatment vessel at a second liquid-to- material ratio, greater than the first ratio; and means for removing at least some of the liquid from the slurry located between the high-pressure outlet of the high-pressure transfer device and the treatment vessel inlet to provide a slurry having a third liquid-to-material ratio less than the second ratio to the inlet of the treatment vessel.
The first vessel is preferably a Chip Chute or Chip Tube provided by Ahlstrom Machinery. The high-pressure transfer device is preferably a High-pressure Feeder as sold by Ahlstrom Machinery. The means for pressurizing and transferring said slurry to the high-pressure transfer device may be a chip pump for pumping the slurry into the high-pressure transfer device or a pump (for example, a pump known as a Chip Chute Circulation Pump) for drawing the slurry into the high-pressure transfer device, or any other suitable conventional pressurizing device. The means for diluting the slurry and transferring the slurry from the high-pressure outlet of the high-pressure transfer device is preferably a high-pressure pump that provides pressurized liquid to the high-pressure inlet of the high-pressure transfer device. The means for removing liquid from the slurry is preferably a cylindrical device having a concentric cylindrical screen through which the slurry passes and from which liquid can be removed. One such device is an In-line Drainer sold by Ahlstrom Machinery but the means may comprise any other suitable conventional device which can readily separate liquid from a moving slurry. The preferred liquid-to-material ratios and pressures are as described above.
The above methods and apparatuses in which liquid is removed prior to introducing a slurry to the high pressure transfer device or liquid is removed after the slurry is discharged from the high-pressure transfer device can be used alone or in tandem. In either case, the flow of liquid from the two liquid removal devices is preferably controlled, for example, by appropriate valves, and in one embodiment the flows can be combined. The temperature of the individual liquids or of the combined liquid is preferably monitored and limited to a temperature that will prevent flashing of the liquid in the feed system. This is preferably effected by controlling the amount of liquid removed from the respective liquor separators, for example, by appropriate valves. The temperature of the liquids may also be controlled by passing one or more of the liquids through a cooling heat exchanger. This cooling heat exchanger may be used to heat other fluids, such as dilution liquids or cooking liquor, including kraft white liquor.
The present invention also includes a system for feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel, comprising or consisting of: a first vessel containing a slurry of material and liquid having a top and a bottom, with an inlet adjacent the top and an outlet adjacent the bottom; a high-pressure transfer device having a low pressure inlet, a low pressure outlet, a high-pressure inlet, and a high-pressure outlet, the high-pressure outlet operatively connected to the treatment vessel; a pump, operatively connected to the outlet of the first vessel, for pressuring and transferring the slurry to the low-pressure inlet of the high-pressure transfer device; and means for removing liquid from the slurry located between the pump and the treatment vessel. The means for removing liquid from the slurry is distinct from the high-pressure transfer device. The treatment vessel is preferably one or more continuous digesters, or one or more batch digesters, for producing cellulose pulp.
The means for removing the liquid from the slurry is preferably a cylindrical vessel having a perforated barrier or screen that allows liquid to pass but retains the fibrous material in the slurry. One preferred device is an In-line Drainer, as described and illustrated in FIG. 2 of U.S. Pat. No. 5,401,361, the disclosure of which is included by reference herein, but the means may comprise any other suitable conventional device which can readily separate liquid from a moving slurry. This device may be located immediately upstream or downstream of the high-pressure transfer device, or two such devices may be used: one upstream of the transfer device and one downstream.
In a preferred embodiment, the means for removing liquid from the slurry comprises a first means located near to or adjacent the inlet of the treatment vessel while the treatment vessel also includes a second means for removing liquid from the slurry. In this embodiment, the liquid removed from the first means and second means is combined and returned to the high-pressure transfer device. The first means is preferably an In-line Drainer and the second means is preferably a Top Separator, Inverted Top separator, or “stilling well” arrangement located in the inlet of the treatment vessel, but other conventional devices may alternatively or additionally be utilized. The first and second means for removing liquid also preferably include a means for regulating the flow of liquid removed, for example, using conventional control valves. Also, the invention preferably includes means for measuring the temperature of the combined liquids, and means for regulating the flow of liquid from the first and the second means for removing liquid to maintain a specified maximum temperature of the combined liquids.
The present invention preferably also includes a pretreatment vessel, for example, a steaming vessel, having an inlet and an outlet which communicates with the inlet of the first vessel. The pretreatment vessel is preferably a DIAMONDBACK® steaming vessel as sold by Ahlstrom Machinery and described in U.S. Pat. Nos. 5,500,083; 5,617,975; 5,628,873; and 4,958,741, or a CHISELBACK™ vessel as described in co-pending application Ser. No. 09/055,408 filed on Apr. 6, 1998, though other more conventional screw-conveyor-type steaming vessels, or other conventional constructions, may be used. The present invention also preferably includes a metering device positioned between the pretreatment vessel and the first vessel. The metering device may be a star-type metering device, such as a Chip Meter as sold by Ahlstrom Machinery, or a screw-type metering device. In a preferred embodiment of the invention, the first vessel is a Chip Tube or Chip Chute as also sold by Ahlstrom Machinery.
As discussed above, one liquid separating device that is particularly useful in the practice of the present invention is a cylindrical device having a cylindrical screen through which the slurry passes and from which liquid is removed, for example, an In-line Drainer, as sold by Ahlstrom Machinery Inc. of Glens Falls, N.Y. An In-line Drainer is typically used to isolate a stream of liquid from a stream of liquid that typically contains at least some wood chips or fine wood particles, for example, what are known as “fines” and “pins”. However, an In-line Drainer can also be used in the practice of the present invention where a liquid is preferably removed from a slurry containing a larger amount of cellulose material, in particular wood chips.
In the conventional use of an In-line drainer, the drainer is positioned in a feed system of a continuous digester, for example, in the outlet of a Sand Separator [as shown by item
37
in
FIG. 2
herein]. The liquid passed to the drainer from the Sand Separator can typically contain at least some wood particles or other material. The In-Line Drainer is typically used to remove excess liquid from the low pressure liquor circulation associated with the feed system, that is, the Chip Chute Circulation, to control the volume of liquid, for example, in the Chip Chute or Chip Tube. Conventional drainers include cylindrical screen baskets fashioned from steel bars oriented parallel to the direction of flow so that the liquid passes through vertical slots or apertures while retaining wood particles within the circulation. However, due to the low concentration of chips, pins, and fines in the liquid passing through the drainer, the flow of liquid through the basket is such that the chips, pins, and fines are oriented in the direction of flow which is also parallel to the slots in the basket. As a result, without taking appropriate measures, the chips, pins, and fines can align with and undesirably pass through the vertical slots or become lodged in the vertical slots of the drainer.
In the drainer of the conventional art, for example, as shown in
FIG. 5
herein, the potential for chips, pins, and fines to align with and pass through the vertical slots of the drainer basket is minimized by introducing a horizontal velocity component to the liquid flow as it is passes through the drainer. This is typically achieved by introducing a helical baffle, or so-called “flight”, to the inlet of the drainer in order to impart a helical flow to the liquid as it is introduced to the drainer and passes through the drainer basket. Due to this helical flow, any chips, pins, or fines that may be present are oriented in the direction of the helical flow and thus oriented obliquely to the elongation of the slots of the vertical bars. Thus, in the conventional art, the helical flight in the inlet reduces the tendency for chips, pins, and fines to pass through the drainer basket or to be lodged in the slots of the drainer basket and cause pluggage of the drainer.
Though this conventional In-line Drainer has proven to be very effective in most applications, the flight positioned in the inlet of the conventional drainer has, in some applications, been associated with an undesirable pressure drop across the drainer. That is, the helical baffle introduces an impediment to flow which causes a decrease in hydraulic pressure from the pressure of the liquid introduced to the drainer to the pressure of the liquid leaving the drainer. This pressure drop impedes the flow of liquid through the drainer and also reduces the pressure of the liquid downstream of the drainer, which can interfere with the proper operation of downstream equipment, for example, the Level Tank or Make-up Liquor Pump. This flow impediment can also reduce the velocity of the flow and thus increase the likelihood for chips, etc. to pass through or become lodged in the screen.
According to another aspect of the present invention, the helical baffle present in the inlet of prior art In-line Drainers and the source of pressure drop associated with this baffle are eliminated yet the Drainer still functions properly. To account for the loss of the baffle's function, according to the present invention, the slots or apertures of the screen basket are aligned obliquely to the direction of elongation of the drainer, and thus obliquely to the direction of flow of the liquid through the drainer. The angle of the slots relative to the direction of elongation of the screen can range from between about 5 to 90 degrees. For example, in one embodiment the slots are oriented substantially perpendicular to the direction of elongation and direction of flow. In the preferred embodiment, the slots are oriented at an angle of about 10° to 80°, preferably about 30° to 60°, most preferably about 40° to 50°.
One embodiment of the present invention consists or comprises a liquid separating device having a cylindrical housing elongated in a direction of elongation having an inlet at a first end of the housing, an outlet at a second end, opposite, the first end, and an inside surface; a cylindrical screen assembly centrally mounted in the housing having a plurality of elongated apertures having an angle of orientation and an outside surface; an annular cavity formed by the outside surface of the screen and the inside surface of the housing; and an outlet for separated liquid located in the housing and communicating with the annular cavity; wherein the angle of orientation of the screen assembly apertures is oblique to the direction of elongation of the housing. The angle of orientation is preferably at least 5° to the direction of elongation of the housing or screen basket, but is typically between about 10° to 80°, preferably about 30° to 60°, most preferably 40° to 50° to the direction of the elongation of the housing or screen basket. For example, the orientation of the slots relative to the elongation of the housing is about 45°.
The drainer slots may be continuous slots or they may be interrupted by unperforated “land” areas. These land areas may be uniformly located throughout the screen basket so that a uniform pattern of slots and land areas is provided or the slots and land areas may be distributed non-uniformly. The orientation of the slots may also vary, for example, the angle of orientation of the slots at one elevation in the direction of elongation of the screen basket may be different from the orientation of the slots at second or an adjacent elevation. The orientation of slots at one elevation in the direction of elongation of the screen basket may also vary, for example, producing a “herring bone”-type pattern of slots. The screen slot configuration of this device may be similar or identical to the screen designs illustrated and described in U.S. Pat. Nos. 6,039,841 or 6,165,323, the disclosures of which are incorporated by reference herein.
A The slots may be fabricated from parallel-bar-type or parallel-wire-type construction or they may be machined from plate, for example, by water-jet cutting, laser cutting, EDM machining, drilling, milling, or any other conventional method of producing apertures in plate. The housing or screen basket material is typically metallic, for example, steel, steel-based alloy, stainless steel, aluminum, titanium or any other commercially available metal, but may also be manufactured from a high-performance plastic or composite material.
The drainer according to the present invention may be used in a conventional feed system, as shown by item
37
in
FIG. 2
of this application, or for treating slurries according to the method and apparatuses of the present invention, for example, as shown as items
153
and
154
of
FIG. 3
or item
254
of FIG.
4
.
The invention can be used in a feed system with or without a high pressure feeder (HPF). A feed system utilizing one or more slurry pumps that can be used according to the invention is shown in U.S. Pat. Nos. 5,735,075, 6,106,668 and 6,325,890, the disclosures of all of which are hereby incorporated by reference herein.
That is, according to his aspect of the invention there is provided a system for feeding comminuted cellulosic fibrous material to a treatment vessel, comprising: a first vessel containing a slurry of comminuted cellulosic fibrous material having a first liquid-to material volume ratio; means for pressuring and transferring the slurry from the first vessel to the treatment vessel; and means located between the first vessel and the treatment vessel for removing at least some of the liquid from the slurry. The means for removing at least some of the liquid from the slurry preferably provides a slurry having a second liquid-to-material ratio less than said first ratio, and may comprise any known removal device, as described above. The means for pressuring and transferring the slurry may comprise one or more slurry pumps, or at least one conventional high pressure transfer device (e.g. a HPF) having a low-pressure inlet, a low-pressure outlet, high pressure inlets and outlets, and one or more through-extending pockets.
The invention may also comprise a method of feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising: a) slurrying the material with a slurrying liquid to produce a slurry of material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure; c) transferring the slurry to the treatment vessel; d) introducing the pressurized slurry to the treatment vessel; and e) removing at least some of the liquid from the slurry between b) and d). In the method e) may be practiced so that the slurry introduced to the treatment vessel in d) has a second liquid-to-material ratio lower than the first ratio. Also the method may further comprise, between b) and c), f) transferring the slurry to a high-pressure transfer device; g) introducing the slurry to the high-pressure transfer device; h) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure, using a pressurized liquid, to produce a slurry of liquid having a second liquid-to-material volume ratio, higher than the first ratio; and i) discharging the slurry having the second liquid-to-material volume ratio from the high-pressure transfer device. Typically the method further comprises between b) and c), pressurizing the slurry to a second pressure, higher than the first pressure.
These and other embodiments of this invention will become more apparent upon review of the following drawings and the attached claims.
BRIEF DESCRIPTION OF THE DRAWINGS
FIG. 1
is a schematic illustration of a continuous digester system employing a prior art feed system over which the present invention is an improvement.
FIG. 2
is a detailed view of the prior art feed system used in the digester system of
FIG. 1
;
FIG. 3
is a schematic illustration of one embodiment of the present invention;
FIG. 4
is a schematic illustration of another embodiment of the present invention;
FIG. 5
is a cross-sectional view of an exemplary prior art drainer that can be used in the practice of the present invention.
FIG. 6
is a cross-sectional view, similar to
FIG. 5
, of another embodiment of drainer that can be used according to the present invention.
FIG. 7
is a detailed view of the screen basket of the drainer of
FIG. 6
; and
FIG. 8
is cross-sectional view of another embodiment of a drainer that can be used according to the invention.
DETAILED DESCRIPTION OF THE DRAWINGS
FIGS. 1 and 2
illustrate typical prior art systems for handling the feeding and treatment of comminuted cellulosic fibrous material to produce cellulose pulp.
FIG. 1
illustrates a cellulose treatment system
10
having a feed system
11
and a digester system
12
.
FIG. 2
illustrates a detailed view of a similar feed system
11
′ for introducing, steaming, slurrying and pressurizing comminuted cellulosic fibrous material, for example, hardwood or softwood chips, and feeding the slurry to a continuous digester system
12
. These systems are disclosed in U.S. Pat. Nos. 5,476,572; 5,622,598; 5,635,025; 5,766,418; and 5,968,314 and are marketed under the trademark LO-LEVEL® by Ahlstrom Machinery.
Though comminuted cellulosic fibrous material may take many forms, including sawdust; grasses, such as straw or kenaf; agricultural waste, such as bagasse; recycled paper; or sawdust, for the sake of simplicity, the term “chips” will be used when referring to comminuted cellulosic fibrous material; but any and all of the listed materials, and others not listed, may be processed by the present invention. Also, though a continuous digester in shown in
FIG. 1
, it is understood that the present invention as also applicable to feeding several continuous digesters or one or more discontinuous or batch digesters.
As shown in
FIGS. 1 and 2
, chips
13
are introduced to the system, for example, via a conveyor (not shown) from a chip storage facility, for example, a woodyard, via an isolation and metering device
14
,
14
′. For example,
FIG. 1
illustrates a star-type Air-lock Feeder as sold by Ahlstrom Machinery Inc. of Glens Falls, N.Y.
FIG. 2
illustrates a screw-type isolation device
14
′ described in U.S. Pat. No. 5,766,418 and having a similar function to device
14
of FIG.
1
. The device
14
,
14
′, driven by an electric motor (not shown), introduces the chips to chip retention and streaming vessel
16
by means of a counter-weighted gate assembly
15
. Though various types of vessels are known in the art, vessel
16
is preferably a DIAMONDBACK® Steaming vessel as marketed by Ahlstrom Machinery and described in U.S. Pat. Nos. 5,500,083; 5,617,975; 5,628,873; and 4,958,741, or a CHISELBACK™ vessel as described in co-pending application Ser. No. 09/055,408 filed on Apr. 6, 1998. This vessel typically includes a gamma-radiation level-detection system, a regulated vent for discharging gases which accumulate in the vessel and one or more steam introduction conduits (
16
′ in FIG.
2
), as is conventional. The pressure in the vessel
16
may be slightly below atmospheric pressure or slightly above atmospheric pressure, that is, the pressure in vessel
16
may vary from about −1 to 2 bar gage (that is, about 0 to 3 bar absolute).
During treatment with steam in vessel
16
, the air that is typically present in the chips is displaced by steam and the heating of the chips is initiated. The removal of air from the cavities within the chips permits the more efficient diffusion of cooking chemical into the chip and minimizes the buoyant forces on the chip during subsequent processing.
The steamed material is discharged from the bottom of the vessel
16
to a metering device
17
, for example, a star-type metering device or Chip Meter as sold by Ahlstrom Machinery, though any type of meeting device may be used. The metering device
17
is typically driven by an electric motor (not shown) and the speed of rotation of the metering device is typically controlled by operator input to define a set rate of introducing chips to the system. The chips discharged by the metering device
17
are introduced to a vertical conduit or pipe
18
, for example, a Chip Tube sold by Ahlstrom Machinery. Cooking chemical and other liquids are typically first introduced to the chips in conduit
18
by means of one or more conduits
19
such that a level of liquid is established in conduit
18
and a slurry of chips and liquid is present in the bottom of conduit
18
. This level of liquid is typically monitored and controlled by a level detection device, for example, a gamma-radiation level detection device or a “d-p” cell. The metering device
17
typically does not act as a pressure isolation device, though it may, and the pressure in conduit
18
typically varies from 0 to 2 bar gage (or 1 to 3 bar absolute).
Conduit
18
discharges the slurry of chips and liquid by means of a radiused section
20
to the inlet of slurry pump
21
. Though any slurry pump can be used, pump
21
is preferably a Hidrostal® screw centrifugal pump sold by Wemco Pump of Salt Lake City, Utah or a pump provided by Lawrence Pumps Inc. of Lawrence, Mass. Slurry pump
21
, driven by electric motor
21
′ (see FIG.
2
), pressurizes and transfers the slurry in conduit
18
via conduit
22
to the low pressure inlet
23
of a high pressure transfer device
24
. This high pressure transfer device is preferably a High-pressure Feeder as sold by Ahlstrom Machinery. High-pressure Feeder
24
includes a pocketed rotor mounted in a housing typically having a low-pressure inlet
23
, a low-pressure outlet
25
, a high-pressure inlet
26
and a high-pressure outlet
27
. The low-pressure outlet
25
typically includes a screen plate (not shown) which minimizes the passage of chips out of low-pressure outlet
25
while allowing the liquid in the slurry to pass out outlet
25
to conduit
28
, though as disclosed in pending application Ser. No. 60/138,280 filed on Jun. 9, 1999, the screen in the low-pressure outlet of feeder
24
may be omitted. The chips which are retained in the feeder by the screen are slurried with high-pressure liquid provided by pump
29
, preferably a Top Circulation Pump (TCP) provided by Ahlstrom Machinery, to inlet
26
via conduit
30
. The slurry is discharged out of high-pressure outlet
27
into conduit
31
and to the digester
32
of digester system
12
at a pressure of between about 5 and 15 bar gage, typically between about 7 to 12 bar gage.
Digester
32
(see
FIG. 1
) may be a single or multiple-vessel digester and may be a hydraulic or steam-phase digester. Digester
32
may also consist or comprise one or more batch digesters. The cellulose material with added cooking chemical is treated under temperature and pressure in digester
32
and essentially fully-treated chemical cellulose pulp is discharged into conduit
50
at the bottom of the digester. Digester
32
typically includes a plurality of screen assemblies
51
,
52
,
53
, and
54
; liquor circulations
55
,
56
, and
57
having pumps
58
,
59
, and
60
and heat exchangers
61
,
62
, and
63
; cooking liquor introduction conduits
64
,
65
, and
66
, supplied by pump
67
, as is conventional, in order to treat the cellulose material. Though many types of processes may be performed in digester
32
, one preferred process is the process described in U.S. Pat. Nos. 5,489,363; 5,536,366; 5,547,012; 5,575,890; 5,620,562; 5,662,775; 5,824,188; 5,849,150; and 5,849,151 and marketed by Ahlstrom Machinery under the trademark LO-SOLIDS®. According to this preferred process, one or more dilution liquid (for example, wash filtrate) introduction conduits
68
,
69
, and
70
are provided which are supplied by filtrate pump
71
, also known as a Cold Blow Pump (CBP). The liquid pressurized by pump
71
may be heated or cooled as desired by heat exchangers
72
and
73
. The process performed in digester
32
may also be one of the processes disclosed in U.S. Pat. Nos. 5,635,026 or 5,779,856 and marketed under the name EAPC™ cooking by Ahlstrom Machinery.
As shown in
FIG. 1
, excess liquor in the slurry in conduit
31
at the top of the digester
32
is separated from the slurry by a liquor separator
33
and returned to the feed system
11
by means of conduit
34
(again, also shown in FIG.
2
). The liquid in conduit
34
is pressurized by pump
29
, driven by electric motor
29
′ (FIG.
2
), and provides the pressurized slurrying liquid introduced to the high-pressure inlet
26
of feeder
24
via conduit
30
. Feeder
24
is typically driven by an electric motor (not shown), the speed of which is monitored and controlled.
As shown in both
FIGS. 1 and 2
, the liquid discharged from the low-pressure outlet
25
of high-pressure feeding device
24
passes via conduit
28
to a cyclone-type separator
35
which isolates undesirable material and debris, such as sand, stones, etc., from the liquid in conduit
28
. Separator
35
is preferably a Sand Separator as sold by Ahlstrom Machinery. Liquid having little or no undesirable material or debris is discharged from separator
35
and is passed through a liquor separating device
37
via conduit
36
. At least some liquid is removed from the liquid separator
35
, which is preferably an Inline Drainer as sold by Ahlstrom Machinery, via conduit
38
and sent to vessel
39
. Vessel
39
is preferably a Level Tank as sold by Ahlstrom Machinery. Liquid is discharged from vessel
39
to conduit
40
and pump
41
and is supplied to digester
32
(see
FIG. 1
) as liquor make-up as needed via conduit
42
. Pump
41
is preferably a Make-Up Liquor Pump (MLP) as sold by Ahlstrom Machinery. As also disclosed in pending application Ser. No. 60/138,280 the Sand Separator
35
, Level Tank
36
, and In-line Drainer
37
can be omitted without interfering with the ultimate function of the feed system
11
.
The liquid discharged from separator
37
into conduit
43
may be supplemented with cooking chemical, for example, kraft white, green, orange (that is, liquid containing polysulfide additives) or black liquor, introduced via conduit
44
(see
FIG. 1
) prior to being introduced to tank
45
. Tank
45
is preferably a Liquor Surge Tank as sold by Ahlstrom Machinery and described in U.S. Pat. No. 5,622,598. The cooking chemical introduced via conduit
44
may be heated or, preferably, cooled as needed by heat exchanger
46
(see FIG.
1
). Some of the liquid in conduit
43
may bypass tank
45
and be introduced via conduit
19
to conduit
18
as described above. Tank
45
communicates with conduit
18
and the inlet of pump
21
via conduits
47
and
20
. As disclosed in pending application Ser. No. 60/124,890 filed on Mar. 18, 1999, tank
45
may comprise or consist of an integral vessel concentric with conduit
18
.
According to the prior art system shown in
FIGS. 1 and 2
, the amount of liquid in the slurry transferred in conduit
22
by pump
21
is governed by the capacity of the pump
21
. That is, typically screw-type-impeller slurry pumps, such as the Wemco Hidrostal® pump, are limited to pumping slurries having a minimum liquid content, that is, a minimum liquid-to-solid, or, in this case, a limited liquid-to-wood chip, ratio. Thus, in prior art systems, the amount of solid material that can be subsequently transferred by the high-pressure transfer device
24
is governed and limited by the solid transfer capacity of the pump
21
. The present invention overcomes this limitation of the prior art.
FIG. 3
illustrates one embodiment of the present invention.
FIG. 3
illustrates a feed system
111
including many of the components found in feed system
11
of FIG.
1
and feed system
11
′ of FIG.
2
. Similar components in
FIG. 3
to those shown in
FIGS. 1 and 2
are identified by the same reference numerals shown in
FIGS. 1 and 2
but preceded by the a “
1
”.
Steamed chips
113
are introduced to horizontal metering-screw conveyor
117
in FIG.
3
. Conveyor
117
performs a similar function as metering device
17
in
FIGS. 1 and 2
. Chips, or other comminuted cellulosic fibrous material,
113
are typically steamed in a steaming vessel prior to being introduced to conveyor
117
, for example, the chips are steamed in a DIAMONDBACK® steaming vessel such as vessel
16
shown in FIG.
2
. The chips
113
are discharged from metering screw
117
into a vertical conduit or vessel
118
, which is preferably a Chip Tube or Chip Chute. Conduit or vessel
118
may include a radiused tramp material separation device as disclosed in copending application Ser. No. 08/905,324 filed on Aug. 4, 1997 [Attorney. Ref. 10-1213], the disclosure of which is included by reference herein. In a preferred embodiment, the Chip Tube includes a radiused discharge
120
which feeds a slurry pump
121
. The slurry pump
121
is preferably a Hidrostal® pump or a Lawrence Pump. Slurrying liquid is introduced to conduits
118
and
120
via conduits
119
and
147
. The liquid introduced via conduits
119
and
147
typically includes some form of chip treatment liquid, for example, kraft white, green, or black liquor, weak black liquor, soda liquor, or liquor including some form of strength or yield enhancing, or metal sequesting additive, such as polysulfide, anthraquinone, chelating agents (such as EDTA and DPTA and their equivalents), surfactants, penetrants, or their equivalents or derivatives. The treatment liquid is introduced via conduit
144
. Pump
121
pressurizes and transfers the slurry via conduit
122
to a high-pressure transfer device
124
, for example, a High Pressure Feeder sold by Ahlstrom Machinery.
Slurry pumps, such as the Hidrostal pump, typically require that the slurry being pumped have a minimum content of liquid, that is, a minimum liquid-to-wood (L/W) volume ratio. For the Wemco Hidrostal slurry pump
121
shown, the L/W ratio of the slurry must be at least 2.75:1, preferably at least 3.0:1. That means that the slurry passing through conduit
122
and being introduced to feeder
124
also has approximately this same L/W ratio. In conventional systems, the pump
121
requirement limits the L/W ratio of the slurry introduced to and transferred by the feeder
124
.
However, according to the present invention, the L/W ratio of the slurry introduced to the feeder
124
is not limited by the L/W ratio that can be transferred by the slurry pump
121
. According to the present invention, some form of liquid removal device
153
is provided upstream of the feeder
124
which removes at least some of the liquid in the slurry in conduit
122
so that the slurry introduced to the feeder
124
has a lower L/W ratio, typically at least about 0.25 lower, preferably at least about 0.5 lower, than the slurry transferred by pump
121
.
The liquid removal device, or dewatering device,
153
shown schematically in
FIG. 3
may be an isolated device or it may be integral with the feeder
124
. The device
153
typically includes a liquid permeable barrier or screen
153
′, for example, a perforated cylinder, which retains the material (chips) in the flow of slurry while removing at least some of the liquid from the slurry into conduit
150
. The screen or barrier
153
′ may be made from perforated plate, for example, screen plate having circular or slotted holes, or may be made from parallel bar-type screen construction. Device
153
may include rotating, reciprocating, vibrating, or otherwise movable components which by their movement minimize or prevent the pluggage of the screen or barrier. The device
153
may also include some form of conventional back-flush mechanism (not shown) which periodically forces a flow of liquid in a direction opposite the direction that the liquid is typically removed to again minimize or prevent pluggage of the screen or barrier. One device that may be used for dewatering device
153
is an In-line Drainer as sold be Ahlstrom Machinery (this device is illustrated in FIG. 2 of U.S. Pat. No. 5,401,361, the disclosure of which is included by reference herein).
Conduit
150
transports the liquid removed from the slurry back to conduits
118
and
120
via conduits
143
,
119
, and
147
to provide the slurrying liquid to conduits
118
,
120
. This flow of liquid is typically supplemented with treatment chemical, as described above, via conduit
144
. The flow of liquid through conduit
150
,
143
is typically regulated by a (preferably solenoid operated) flow control valve
151
. Conduit
143
may include a conventional Sand Separator (item
35
in FIG.
2
), In-line Drainer (item
37
in FIG.
2
), Level Tank (item
39
in FIG.
2
), and Liquor Surge Tank (item
45
in FIG.
2
), if desired.
The slurry having reduced liquid content is then introduced to the low-pressure inlet
123
of feeder
124
. The operation and components of feeder
124
are described in U.S. Pat. Nos. 5,236,285 and 5,236,286, the disclosures of which are included by reference herein. The pocketed rotor (not shown) of the feeder
124
accepts the slurry having reduced liquid content and, through rotation, exposes the slurry to high-pressure liquid supplied to the high-pressure inlet
126
by high pressure pump
129
via conduit
130
. This high-pressure flow flushes the chips from the rotor pocket and discharges them out of high pressure outlet
127
and into conduit
131
. The slurry, now diluted with pressurized liquid introduced by pump
129
, is then propelled to the top of a treatment vessel (item
32
shown in
FIG. 1
) via conduit
131
. Conventionally, the slurry in conduit
131
typically has a L/W ratio greater than 6.0:1, possibly even greater than 8.0:1. Again, this treatment vessel may be one or more continuous digesters or one or more batch digesters. The continuous digester may be a hydraulic or vapor-phase digester having one or more vessels, for example, the digester may include an impregnation vessel.
As is conventional, excess liquid may be removed from the slurry upon introduction to the digester, such as by using a liquid separation device, for example, a Top Separator (item
33
in FIG.
1
). This separated liquid is returned to feed system
111
via conduit
134
to supply at least some of the liquid provided by pump
129
to the high-pressure inlet
126
of feeder
124
.
As the slurry is introduced to feeder
124
via conduit
122
at least some of the liquid in the slurry passes through the rotor pocket (again, not shown) and is discharged from the feeder
124
via low-pressure outlet
125
. The outlet
125
may include a conventional screen element to prevent the passage of chips out of outlet
125
or no screen element may be present. As in conventional operation, the liquid moving through outlet
125
, which is under pressure supplied by pump
121
, is passed via conduit
128
to conduits
119
and
147
to provide the source of slurrying liquid in conduits
118
and
120
. However, in the embodiment of the present invention shown in
FIG. 3
, the slurrying liquid is also provided to conduits
118
,
120
via conduits
119
,
147
,
150
and
143
from dewatering device
153
. Since the liquid in line
128
may be hotter than 100° C. and the pressure in conduits
143
,
147
,
118
,
119
, or
120
may be lower than 1 atm, to prevent flash evaporation, the liquid in line
128
may be cooled by heat exchanger
156
prior to introducing the liquor to line
143
.
Another advantage of the present invention is that by removing liquid from the slurry in conduit
122
via separator
153
, prior to exposing this liquid to the hotter temperature liquid in feeder
124
(for example, the hot liquid returned from the treatment vessel via conduits
134
and
130
), the temperature of the liquid returned to the typically unpressurized conduits
118
and
120
may be cooler. Therefore, the liquid in conduits
150
,
143
,
147
and
119
typically will not have to be cooled to prevent flash evaporation in these conduits or in conduits
118
and
120
.
In another embodiment of the invention, a liquor separator
154
may also be introduced adjacent to the high-pressure outlet
127
of feeder
124
. This separator
154
typically is similar to separator
153
described above and typically includes a barrier or screen
154
′ and, again, may be integral with the feeder
124
or separate from feeder
124
. The separator
154
may be used in place of separator
153
or in conjunction with separator
153
to remove additional liquid from the slurry prior to passing the slurry via conduit
131
to the treatment vessel. The liquid removed using the separator
154
, since it is pressurized and typically hotter than 100° C., is preferably passed via conduit
157
to conduit
134
, which is also typically pressurized and hotter. The flow of liquid out of separator
154
and through conduit
157
is typically regulated by control valve
158
, which is desirably automatically operated.
The liquid removed by means of separator
154
may also be returned to conduits
118
and
120
directly or via conduit
150
via conduit
159
, shown in phantom. Since the liquid in conduit
159
may be hotter than 100° C., the liquid in conduit
159
will typically require some form of cooling prior to introducing it to conduit
150
, for example, by passing it through heat exchanger
160
. The flow of liquid through conduit
159
is typically regulated by valve
161
.
In one mode of operation, the liquid removed from the slurry by separators
153
or
154
is of sufficient volume so that little or no excess liquor is introduced to the treatment vessel via conduit
131
, so that in turn little or no liquid need be returned to the feed system via conduit
134
, and conduit
134
may be eliminated. In such a case, the liquor separation device (item
33
in
FIG. 1
) is unnecessary and this device may be eliminated along with its associated cost and maintenance. Furthermore, by eliminating this return of liquid to the feed system from the treatment vessel, little or no heat that is typically returned with this liquid is introduced to the feed system. As a result, the impact of this heat upon the operation of the feed system, for example, undesirable liquid flashing, and upon the treatment of the material is reduced or substantially eliminated. For example, by employing this mode of operation, the cooler impregnation processes disclosed in U.S. Pat. Nos. 5,736,006 and 5,958,181 are more readily implemented.
Furthermore, should sluicing liquid be desired and the top separator (
33
in
FIG. 1
) and the return line
134
from the top separator have been eliminated, sluicing liquor may also be obtained from one or more of the liquor circulations associated with digester
32
(see
FIG. 1
) which are closer in proximity than separator
33
. In conventional pulp mill installations, pump
29
is physically located in an area adjacent to the pumps associated with the liquor circulations of digester
32
, for example, pumps
50
,
59
, or
60
in FIG.
1
. By using the liquors in these circulations, for example, the liquor extracted from the upper cooking circulation screens
51
and pressurized by pump
50
, a more accessible source of sluicing liquor is obtained. For example, only a short pipe run need be required from the piping associated with pump
50
to the inlet of pump
29
, instead of the long pipe run from the Top Separator
33
(in
FIG. 1
) at the top of the digester to pump
29
adjacent the feeder
24
. In addition, the active cooking chemical, that is, the alkali, present in the circulations associated with the digester may offset the alkali typically needed in the feed system. The sluicing liquors obtained from these cooking circulations may also contain at least some sulfide which, as is known in the art, is beneficial to have in the treatment liquors used early in the cooking process, for example, in the sluicing liquor in conduit
34
,
134
.
Another embodiment of the present invention is shown in FIG.
4
.
FIG. 4
partially illustrates a feed system
211
similar to feed systems
11
,
11
′, and
111
described above, which feeds a continuous digester
232
, similar to digester
32
in FIG.
1
. Components in
FIG. 4
comparable to those in
FIGS. 1-3
are shown by the same two digit reference numeral but preceded by a “
2
”.
In feed system
211
, a slurry of comminuted cellulosic fibrous material
222
is introduced to a high-pressure transfer device
224
, similar to devices
24
and
124
above. This slurry
222
may be pressurized by a slurry pump, such as pumps
21
and
121
in
FIGS. 1
,
2
, and
3
, or may simply be provided by a conventional Chip Chute from a horizontal screw-type steaming vessel. The feeder
224
pressurizes and transfers the slurry to digester
232
via conduit
231
. Though not shown in
FIG. 4
, liquid removal devices
153
and
154
may also be present adjacent the feeder
224
as shown in FIG.
3
.
The inlet of the digester
232
includes a conventional liquor removal device
233
, a Top Separator, such as item
33
in
FIG. 1
, having a screw conveyor
261
, driven by electric motor
274
, and a perforated cylindrical screen
262
. The conveyor transfers the chips to the vessel in the direction of arrow
263
while removing liquid from the slurry as shown by arrow
264
and returning the liquid via conduits
265
and
234
, the TC line, to pump
229
and to feeder
224
via conduit
230
, as is conventional. The lower section of the separator housing
266
is preferably non-permeable so that little or no heated liquor can migrate from the exothermic reactions that are occurring in the chip column
267
in the vessel
232
.
According to this embodiment of the invention, a liquor removal device
254
is located in conduit
231
. This liquid removal device is preferably similar to devices
153
and
154
discussed above, and is preferably an In-line Drainer-type device as also discussed above. According to this invention, at least some liquid is removed from the slurry via device
254
via conduit
257
, such that less liquid is introduced to the vessel
232
via conduit
260
. As a result, less liquid need be removed from the slurry by separator device
233
and less heat is withdrawn from the vessel and returned to the feed system where the heat can cause operational problems. In addition, by reducing the temperature of the liquid returned to the feed system, cooler, more beneficial treatments of the cellulose can be performed in the feed system, for example, those methods disclosed in U.S. Pat. Nos. 5,736,006 and 5,958,181.
As shown in
FIG. 4
, the temperature of the liquid in line
234
is preferably monitored by temperature sensor
270
. The temperature measured by sensor
270
can be used to regulate the flow of liquid from liquid separators
254
and
233
, for example, control signals
275
and
276
and automatic flow control valves
271
and
272
. Should the temperature of the liquid in line
234
exceed a specified value, for example, 100° C., the flow of hotter liquid through valve
271
can be reduced and the flow of cooler liquid through valve
272
can be increased. Also, the pressure drop across the inlet of the vessel, from conduit
260
to the outlet of the liquid separator at conduit
265
, can be monitored by pressure difference sensor
273
. This pressure difference can be limited to a specified value by controlling the speed of the screw of separator
233
. The speed of this screw can be varied by varying the speed of the motor
274
driving the screw.
The invention particularly contemplates all specific narrow ranges within a broad range. For example a L/W ratio of between about 4.0:1 and 10:0:1 means 8.5:1 to 10.0:1, 4.5:1 to 6.5:1, 5.0:1 to 9.0:1, and all other narrower ranges within that broad range.
One example of a liquor separating device that can be used in the practice of the present invention or as item
37
of
FIG. 2
is shown in FIG.
5
.
FIG. 5
illustrates a conventional In-line Drainer
300
as sold by Ahlstrom Machinery having an inlet
301
for a particulate-bearing liquid to be strained, an outlet
302
for liquid that has been strained, and an outlet
303
for the strained liquid. Drainer
300
includes a cylindrical housing
304
, having a cover plate
305
at a first or inlet end having the inlet opening
301
and a second or outlet end having end cover plate
306
. The cover plate
306
typically includes a lifting eye
307
and appropriate mounting hardware
308
, for example, threaded studs and nuts. The drainer
300
includes a cylindrical screen basket
309
positioned in the housing
304
. The upper end the screen basket
309
is mounted to the housing
304
by means of a annular mounting flange
310
on the housing and appropriate mounting hardware
311
, for example, threaded screws. The lower end of the screen basket
309
is snugly fit into a machined surface in the inlet
301
. The screen basket
309
is positioned in the housing
304
so that an annular cavity
312
is created between the outside surface of the screen basket
309
and the inside surface of the housing
304
. The screen basket
309
may also include a lifting eye
313
for removing the basked for replacement or servicing. The housing
304
also typically includes a gusseted mounting flange
314
for installing the drainer in the desired location and a steam purge inlet
315
for introducing steam for periodic steam cleaning of the drainer.
Though the centerline of the outlet
302
shown in
FIG. 5
is positioned at a right angle to the centerline of the housing
304
, the outlet
302
may also positioned in the top plate
306
so that its centerline is essentially collinear with the centerline of the housing. An outlet collinear with the centerline of the housing, and thus with the direction of flow, may be more desirable when the invention is used in the systems shown in
FIGS. 3 and 4
, that is, where the concentration of cellulose material is greater and abrupt changes in flow direction can cause undesirable flow restrictions and stagnation. The right-angled outlet orientation shown in
FIG. 5
is preferred when the drainer
300
is used as shown by item
37
in FIG.
2
.
In the conventional drainer
300
shown in
FIG. 5
, the screen basket
309
is fabricated from a series of evenly-spaced vertical bars
316
supported by a series of external annular rings
317
so that a straining surface is provided having a series of vertical slots
318
between the bars
316
. The bars
316
are typically welded to the rings
317
and to support rings
319
and
320
located at either end of the basket. The screen basket
309
also typically includes unperforated cylindrical sections
321
and
322
at each end of the screen basket
309
.
According to the prior art shown in
FIG. 5
, the lower cylindrical section
322
of the basket
309
includes a helical baffle
323
, which is typically referred to as the “flight”. As discussed above, this flight
323
induces a helical flow to the liquid introduced under pressure to inlet
301
so that the orientation of any chips, pins or fines that may be present in the slurry is less likely to be aligned with the vertical slots of the screen basket
309
.
The device shown in
FIG. 5
operates as follows. A pressurized flow of liquid, typically containing at least some wood chips, pins, or fines, or a slurry of liquid and chips, is introduced to the inlet
301
of the drainer
300
. When used as item
37
in
FIG. 2
, the liquid typically has a pressure ranging from about 0 to about 5 bar gage. When used as item
153
or
154
of
FIG. 3
or item
254
of
FIG. 4
, the pressure of the slurry introduced to the inlet
301
typically ranges from about 0 to about 30 bar gage. The design of the housing
304
and basket
309
will vary depending, among other things, upon this pressure. The helical baffle
323
imparts a tangential velocity component to this liquid flow so that the flow through the screen basket
309
is somewhat helical. As the liquid passes through the cylindrical screen basket
309
at least some liquid passes through the apertures, that is, the slots
318
, of the screen
309
, collects in annular cavity
312
, and is discharged out of outlet
303
. The liquid from outlet
303
can be forwarded to any appropriate location but is typically forwarded to Level Tank
39
when used in a feed system, as in
FIG. 2
, or can be recirculated as shown in
FIGS. 3 and 4
. The liquid and chips, fines, and pins and other material which do not pass through the screen basket
309
continue to and are discharged from the outlet
302
. When used as item
37
in
FIG. 2
, the liquid discharged from outlet
302
is typically passed to a conduit leading to the inlet of a High-pressure Feeder, such as a Chip Tube (item
18
in FIG.
2
), Chip Chute, or Liquor Surge Tank (item
45
in FIG.
2
). When used as item
153
or
154
of
FIG. 3
or item
254
of
FIG. 4
, the liquid discharged from outlet
302
is typically passed to a High-pressure Feeder (item
126
in FIG.
3
), or to a digester (via conduit
131
in
FIG. 3
or via conduit
260
in FIG.
4
).
The slot width and slot spacing will typically be a function of the content of the slurry passing through the drainer
300
and the desired pressure drop across the slots
318
. In the conventional use of the device
300
, for example, as used to treat a low-solid concentration slurry with smaller particles, as in as item
37
in
FIG. 2
, the slot
318
width may vary from between about 1 to 4 mm and the slots
318
are typically evenly spaced by about 2 to 6 mm. In the application of the present invention, for example, shown by item
153
or
154
in
FIG. 4
, when treating a slurry having a higher solid concentration with larger particles, the slot
318
width will typically vary between about 4 and 8 mm and typically be uniformly spaced by about 3 to 7 mm.
In the prior art device
300
shown in
FIG. 5
, the helical baffle
323
which induces a helical flow to the slurry or liquid passing through the drainer, in some instances, can produce an undesirable pressure drop across the drainer. According to the present invention, this baffle or flight
323
and the restriction to flow, or pressure drop, it can create are eliminated. Though this baffle or flight
323
may be used in conjunction with the obliquely oriented slots
318
of the present invention, it is preferred that this baffle or flight
323
be eliminated.
Two embodiments of the present invention are shown in
FIGS. 6
,
7
and
8
. The items in
FIGS. 6
,
7
, and
8
that are essentially identical to those found in
FIG. 5
are identified by the same reference numbers. The distinctions between the prior art and the present invention are identified by the same two digit reference numerals but are prefaced by the numerals “
4
” and “
5
”, respectively, instead of by the numeral “
3
” as shown in FIG.
5
.
FIG. 6
illustrates one embodiment of the present invention in which the screen basket slots are oriented obliquely to the direction of elongation of the housing. First, note that the “flight”, item
323
in
FIG. 5
, has been eliminated in FIG.
6
. That is, the inlet
301
is substantially devoid of any flow director or impediment, i.e., is substantially completely hollow. In addition, according to the present invention, in the screen basket
409
of
FIG. 6
, the slots
418
formed by bars
416
and supported by annular rings
417
, are oriented at an oblique angle α to the direction of elongation of the screen basket
409
and the direction of elongation of the cylindrical housing
404
so that slots
418
are also oriented at an angle α to the direction of flow of liquid through the screen basket
409
. This is more clearly shown in the detail schematic of FIG.
7
.
FIG. 7
illustrates a detailed cross-section of a partial view of the screen basket
409
. Though the angle α shown in
FIG. 7
is illustrated at a preferred orientation of the slots
418
of approximately 45°, it is to be understood that according to this invention the angle α may range from plus or minus 5° to plus or minus 90° from the direction of elongation of the housing
404
. For example, in the embodiment of
FIG. 8
, the angle α is approximately plus 90°, that is, if the housing
404
is vertically elongated, the slots
518
are essentially horizontal. Again, in
FIG. 8
, the helical baffle
323
shown in
FIG. 5
is eliminated. All other features of
FIGS. 6 and 8
are essentially the same as FIG.
5
.
Though the embodiments shown in
FIGS. 6
,
7
, and
8
, illustrate parallel bar type construction, the present invention also includes machined-plate type construction. For example, the slots
418
,
518
, either continuous or discontinuous, may be fabricated from metal plate by any appropriate machining means including, but not limited to, water-jet cutting, laser cutting, EDM machining, drilling, milling, or any other conventional method of producing apertures in plate.
Also, the slots
418
,
518
may be continuous slots or they may be discontinuous slots interrupted by unperforated “land” areas. These land areas may be uniformly distributed throughout the screen basket
409
,
509
so that a uniform pattern of slots and land areas is established or the slots and land areas may be distributed non-uniformly. The orientation of the slots may also vary, for example, the angle of orientation of the slots
418
,
518
at one elevation in the direction of elongation of the screen basket may be different from the orientation of the slots at second or an adjacent elevation. The orientation of slots at one elevation in the direction of elongation of the screen basket may also vary, for example, producing a “herring bone”-type pattern of slots. The angle α of the slots may also vary from one elevation to another or adjacent elevation or the angle α of the slots may vary within a given elevation.
The slots
418
,
518
of the screen basket
409
,
509
are preferably uniformly spaced and have a width of between about 1 to 20 mm and a distance between slots
418
,
518
that may vary from about 1 to 20 mm, depending upon the slurry treated by the drainer
400
,
500
and the desired pressure drop across the slots
418
,
518
. When used as item
37
in
FIG. 2
, the slurry being treated will typically have a relatively lower concentration of cellulose material and the slots
418
,
518
will have a width of about 0.5 to 10 mm, typically about 1 to 6 mm, preferably about 2 to 4 mm, and a distance between slots will be about 1 to 10 mm, typically about 1 to 6 mm, preferably about 3 to 4 mm. When used as item
153
or
154
of
FIG. 3
or item
254
of
FIG. 4
, the slurry being treated typically will have a relatively higher concentration of cellulose material and the slots
418
,
518
will have a width of about 0.5 to 15 mm, typically about 3 to 9 mm, preferably about 5 to 7 mm and a distance between slots of about 1 to 10, typically about 2 to 8 mm, preferably about 4 to 6 mm.
The invention shown in
FIGS. 6
,
7
, and
8
can be used in any desired location where liquid separation from a slurry of liquid and cellulose material is desired. The invention shown in
FIGS. 6
,
7
, and
8
may be used in a feed system for a digester, for example, as the device
37
in the feed system shown in
FIG. 2
herein. The invention shown in
FIGS. 6
,
7
, and
8
may also be used for treating slurries being handled by a High-pressure Feeder or being fed to a digester, either continues or batch, as shown as item
153
or
154
of
FIG. 3
or item
254
of FIG.
4
.
The present invention provides a more effective system and method of introducing a slurry of comminuted cellulosic fibrous material to a treatment vessel. Unlike the prior art, the present invention is not limited to the solids transfer capacity of the pumping device. The present invention can transfer more material and less liquid so that more material can be introduced and treated per unit time than as in prior art systems, or the size and cost of the feed system reduced. As described above, the present invention also has various other benefits compared to the prior art.
While the invention has been described in connection with what is presently considered to be the most practical and preferred embodiment, it is to be understood that the invention is not to be limited to the disclosed embodiment, but on the contrary, is intended to cover various modifications and equivalent arrangements and methods included within the spirit and scope of the appended claims.
Claims
- 1. A method of feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising:a) slurrying a comminuted cellulosic fibrous material with a slurrying liquid to produce a slurry of the comminuted cellulosic fibrous material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure and transferring the slurry pressurized at said first pressure to a high-pressure transfer device; c) introducing the slurry pressurized at said first pressure into the high-pressure transfer device; d) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure; e) transferring the slurry pressurized at said second pressure from the high-pressure transfer device to a treatment vessel; f) introducing the slurry pressurized at said second pressure and transferred from the high-pressure transfer device into the treatment vessel; and g) removing at least some of the liquid from the slurry between a) and c) so that the slurry introduced to the high-pressure transfer device in c) has a second liquid-to-material volume ratio lower than the first liquid-to-material volume ratio.
- 2. A method as recited in claim 1 wherein at least some of the liquid removed during g) is used as at least some of the slurrying liquid in a).
- 3. A method as recited in claim 1 wherein g) is practiced immediately prior to step c).
- 4. A method as recited in claim 1 further comprising h) treating the material in the treatment vessel to produce cellulose pulp.
- 5. A method as recited in claim 1 wherein a) is practiced so that the first liquid-to-material volume ratio is about 2.50:1 or greater.
- 6. A method as recited in claim 5 wherein a) is practiced so that the first liquid-to-material volume ratio is about 3.0:1 or greater.
- 7. A method as recited in claim 1 wherein a) and g) are practiced so that the second liquid-to-material volume ratio is at least 0.25 less than the first liquid-to-material volume ratio.
- 8. A method as recited in claim 6 wherein a) and g) are practiced so that the second liquid-to-material ratio is at least 0.50 less than the first liquid-to-material ratio.
- 9. A method of feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising:a) slurrying comminuted cellulosic fibrous material with a slurrying liquid to produce a slurry of the comminuted cellulosic fibrous material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure and transferring the slurry pressurized at said first pressure to a high-pressure transfer device; c) introducing the slurry pressurized at said first pressure into the high-pressure transfer device; d) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure, using a pressurized liquid, to produce a slurry of liquid having a second liquid-to-material volume ratio, higher than the first liquid-to-material volume ratio; e) discharging the slurry having the second liquid-to-material volume ratio from the high-pressure transfer device; f) transferring the slurry pressurized at said second pressure from the high pressure transfer device to a treatment vessel; g) introducing the slurry pressurized at said second pressure into the treatment vessel; and h) removing at least some of the liquid from the slurry between e) and g) so that the slurry introduced to the treatment vessel in g) has a third liquid-to-material volume ratio lower than the second liquid-to-material volume ratio.
- 10. A method as recited in claim 9 wherein at least some of the liquid removed during h) is used as the pressurized slurrying liquid of d).
- 11. A method as recited in claim 9 wherein at least some of the liquid removed during h) is used as the slurrying liquid in a).
- 12. A method as recited in claim 9 wherein h) is performed substantially immediately after e).
- 13. A method as recited in claim 9 further comprising i) treating the material in the treatment vessel to produce cellulose pulp.
- 14. A method as recited in claim 9 wherein h) is performed prior to g) so that a slurry having a third liquid-to-material volume ratio is introduced to the treatment vessel; and further comprising i) removing excess liquid from the slurry during or shortly after the practice of g).
- 15. A method as recited in claim 14 further comprising j) combining the liquids removed at g) and i) and using at least some of the combined liquids as the pressurizing medium in d).
- 16. A method as recited in claim 15 further comprising k) monitoring the temperature of the combined liquids and l) regulating the flow of the liquids in h) and i) so that the temperature of the combined liquid is maintained below a specified value.
- 17. A method as recited in claim 9 wherein a) is practiced so that the first liquid-to-material volume ratio is about 2.50:1 or greater.
- 18. A method as recited in claim 17 wherein a) is practiced so that the first liquid-to-material volume ratio is about 3.0:1 or greater.
- 19. A method as recited in claim 9 wherein h) is practiced so that the third liquid-to-material volume ratio is at least 0.25 less than the second liquid-to-material volume ratio.
- 20. A method as in claim 18 wherein h) is practiced so that the third liquid-to-material ratio is at least about 0.50 less than the second liquid-to-material ratio.
- 21. A method as recited in claim 20 further comprising, between a) and c), removing some of the liquid from the slurry so that the liquid introduced into the high pressure device has a fourth liquid to material ratio at least about 0.25 less than the first ratio.
US Referenced Citations (32)
Foreign Referenced Citations (2)
Number |
Date |
Country |
WO 9626315 |
Aug 1996 |
WO |
WO 0006282 |
Feb 2000 |
WO |