Embodiments of the present disclosure are generally directed to a fluid filter, and more specifically, to a fluid filter with an electrostatic discharge mitigation sleeve.
High purity fluid handling systems have many uses in advanced technology applications. These applications include processing and manufacturing of solar panels, flat panel displays, and in the semiconductor industry for applications such as photolithography, bulk chemical delivery, chemical mechanical polishing (CMP), wet etch, and cleaning. Certain chemicals used in these applications are aggressive, high purity organic solvents precluding the use of some conventional fluid handling technology.
In order to meet the high purity requirements for such applications, suitable fluid handling systems provide filters, tubing, fittings, valves, and other elements, that are made from inert polymers. These inert polymers may include, but are not limited to, fluoropolymers such as tetrafluoroethylene polymer (PTFE), perfluoroalkoxy alkane polymer (PFA), ethylene and tetrafluoroethylene polymer (ETFE), ethylene, tetrafluoroethylene and hexafluoropropylene polymer (EFEP), and fluorinated ethylene propylene polymer (FEP). These materials are susceptible to a buildup of electrostatic charge that can lead to damage of the fluid handling system.
Built up electrostatic static charge can discharge from within the fluid handling system to the exterior environment, potentially damaging components in the fluid handling system (e.g. tubing or piping, fittings, components, containers, filters, etc.), that may lead to leaks, spills of fluid in the system, and diminished performance of components. In these situations, such discharge, may lead to potential fire or explosion when flammable, toxic and/or corrosive fluids are used in the compromised fluid handling system.
Electrostatic discharge (ESD) is an important technical issue for fluid handling systems in the semiconductor industry and in other technology applications. Frictional contact between fluids and surfaces of various operational components (e.g. tubing or piping, valves, fittings, filters, etc.) in the fluid system can result in generation and buildup of static electrical charges. The extent of charge generation depends on various factors including, but not limited to, the nature of the components and the fluid, fluid velocity, fluid viscosity, electrical conductivity of the fluid, pathways to ground, turbulence and shear in liquids, presence of air in the fluid, and surface area. There is a need to find solutions for dissipating electrostatic charge in fluid handling systems in general as well as the filters present in the fluid handling systems.
One or more embodiments of this disclosure are related to a fluid filter having an electrostatic mitigation sleeve.
In certain embodiments, an electrostatic mitigation filter comprises a filter element, a filter housing, one or more endcaps, an electrically conductive polymer sleeve, and electrically conductive polymer tie bands.
In some embodiments, the filter has one endcap; in other embodiments the filter has two end caps.
A suitable electrically conductive polymer sleeve may comprise an electrically conductive fluoropolymer such as, but not limited to, an electrically conductive polymer selected from the group consisting of tetrafluoroethylene polymer (PTFE), perfluoroalkoxy alkane polymer (PFA), ethylene and tetrafluoroethylene polymer (ETFE), ethylene, tetrafluoroethylene and hexafluoropropylene polymer (EFEP), fluorinated ethylene propylene polymer (FEP), polychlorotrifluoroethylene (PCTFE), polyvinylidene fluoride (PVDF), and mixtures thereof. In one embodiment, the electrically conductive polymer sleeve comprises perfluoroalkoxy alkane polymer. In some embodiments the electrically conductive polymer sleeve is an extruded tube, in other embodiments the electrically conductive polymer sleeve is a cylindrical sheet, in still other embodiments the electrically conductive polymer sleeve is a flat sheet or rolling mill sheet. Further, the disclosed the electrically conductive polymer sleeve may be reusable.
In some embodiments, the filter has a first electrically conductive polymer tie band to secure the electrically conductive polymer sleeve to the filter housing and for connecting to ground and a second electrically conductive polymer tie band to also secure the electrically conductive polymer sleeve to the filter housing. Suitable electrically conductive tie bands comprise electrically conductive fluoropolymers or electrically conductive polyolefins. In one embodiment, the electrically conductive tie bands comprise electrically conductive polypropylene.
Various embodiments of the disclosed filter have electric charge and resistivity properties. In one embodiment, the filter has measured charge of about +/−1 kV when a charge-generating fluid flows through the filter. In other embodiments, the electrically conductive polymer sleeve has an outer surface resistivity of about less than about 1 E+4 ohm, from 1 E ohm to about 1 E+4 ohm, or about 0.9 E+2 ohm to about 4 E+3 ohm, preferably the conductive polymer sleeve has an outer surface resistivity of about 1 E+3 ohm to about 3 E+3 ohm. In some embodiments, the electrically conductive polymer sleeve has an inner surface resistivity less than about 1 E+4 ohm, from 1 E ohm to about 1 E+4 ohm, or form about of about 0.9 E+2 ohm to about 2 E+3 ohm, preferably the conductive polymer sleeve has an inner surface resistivity of about 1 E+3 ohm to about 1.5 E+3 ohm. In some embodiments, the conductive tie bands have a resistivity of less than about 1 E+4 ohm, from 1 E ohm to about 1 E+4 ohm, or about 2 E+3 ohm to about 4 E+3 ohm.
One or more disclosed embodiments may include an electrostatic discharge kit comprising an electrically conductive polymer sleeve and electrically conductive polymer tie bands.
Additional embodiments may include a fluid handling system comprising an electrostatic mitigation filter.
Additional embodiments may also include a method of mitigating electrostatic discharge in a fluid handling system comprising installing an electrostatic mitigation filter in the fluid handling system.
The above summary is not intended to describe each illustrated embodiment or every implementation of the present disclosure. The embodiments of this disclosure are amenable to various modifications and alternative forms, and certain specifics have been shown, for example, in the drawings and will be described in detail. It is understood that the intention is not to limit the disclosure to the particular embodiments described; the intention is to cover all modifications, equivalents, and alternatives falling within the spirit and scope of this disclosure.
The drawings included in this disclosure illustrate embodiments of the present disclosure and, along with the description, serve to explain the principles of the disclosure. The drawings are only illustrative of certain embodiments and do not limit the disclosure.
This disclosure reports embodiments of a fluid filter for ESD mitigation having a conductive polymer sleeve. Embodiments of this filter may include a conductive sleeve and tie bands to mitigate electrostatic discharge.
In certain embodiments as illustrated in
The ESD mitigation filter of this disclosure may be used in ESD mitigation fluid circuits. Representative ESD mitigation circuits are reported, for example, in International patent application, WO 2017/210293, which is incorporated herein by reference, except for express definitions or patent claims contained therein.
An exemplary ESD circuit includes a fluid handling system 450 illustrated in
Various embodiments of the disclosed ESD mitigation filter have electric charge and resistivity properties. In one embodiment, the filter has measured charge of less than +1 kV (a range of about −1 KV to about +1 kV) when a charge-generating fluid flows through the filter. In some embodiment, the conduction polymer sleeve has a resistivity of about 1 E+1 to about 1 E+4. In other embodiments, the conductive polymer sleeve has an outer surface resistivity of about 0.9 E+2 ohm to about 4 E+3 ohm, preferably the conductive polymer sleeve has an outer surface resistivity of about 1 E+3 ohm to about 3 E+3 ohm. In some embodiments, the conductive polymer sleeve has an inner surface resistivity of about 1 E to about +4 E ohm, from about 0.9 E+2 ohm to about 2 E+3 ohm, preferably the conductive polymer sleeve has an inner surface resistivity of about 1 E+3 ohm to about 1.5 E+3 ohm. In some embodiments, the conductive tie bands have a resistivity of about of about 1 E+1 ohm to about 1 E+4 ohm. In other embodiments, the conductive tie bands have a resistivity of about of about 2 E+3 ohm to about 4 E+3 ohm.
This example measured the amount of electric charge generated by flowing propylene glycol methyl ether acetate (PGMEA) through two commercially available filters, an IMPACT 8G 7 nm PTFE filter and an IMPACT 2 AT 0.05 μm filter (both available from Entegris, Inc., Billerica, MA). The buildup of charge was measured with an ESD meter for a filter having an ESD sleeve according to this disclosure and for a filter not having an ESD sleeve. The ESD was measured a flow rates of 50, 100, 200 and 300 ml/min at room temperature. The measured charge is shown in
The data demonstrates that the ESD charge values (kV) for the filters with an ESD sleeve are lower than for the filters without the ESD sleeve.
In a first aspect, an electrostatic mitigation filter comprises a filter element, a filter housing, one or more endcaps, an electrically conductive polymer sleeve, and one or more electrically conductive polymer tie bands.
A second aspect according to the first aspect, wherein the filter has one endcap.
A third aspect according to the first aspect, wherein the filter has two end caps.
A fourth aspect according to the first aspect, wherein a first electrically conductive polymer tie band for connecting to ground and a second electrically conductive polymer tie band to secure the electrically conductive polymer sleeve to the filter housing.
A fifth aspect according to any of the previous aspects, wherein the electrically conductive polymer sleeve comprises electrically conductive fluoropolymers.
A sixth aspect according to any of the previous aspects, wherein the electrically conductive polymer sleeve comprises an electrically conductive polymer selected from the group consisting of tetrafluoroethylene polymer (PTFE), perfluoroalkoxy alkane polymer (PFA), ethylene and tetrafluoroethylene polymer (ETFE), ethylene, tetrafluoroethylene and hexafluoropropylene polymer (EFEP), fluorinated ethylene propylene polymer (FEP), polychlorotrifluoroethylene (PCTFE), polyvinylidene fluoride (PVDF), and mixtures thereof.
A seventh aspect according to any of the previous aspects, wherein the electrically conductive polymer sleeve comprises perfluoroalkoxy alkane polymer.
An eighth aspect according to any of the previous aspects, wherein the one or more electrically conductive polymer tie bands comprise electrically conductive fluoropolymers or electrically conductive polyolefins.
A ninth aspect according to any of the previous aspects, wherein the one or more electrically conductive polymer tie bands comprise electrically conductive polypropylene.
A tenth aspect according to any of the previous aspects, wherein the electrically conductive polymer sleeve is an extruded tube.
An eleventh aspect according to any of the previous aspects, wherein the electrically conductive polymer sleeve is a cylindrical sheet.
A twelfth aspect according to any of the previous aspects, having a measured charge of less than +/−1 kV when a charge-generating fluid flows through the filter.
A thirteenth aspect according to any of the previous aspects, wherein the electrically conductive polymer sleeve has an outer surface resistivity of about 0.9 E+2 ohm to about 1 E+4 ohm.
A fourteenth aspect according to any of the first through twelfth aspects, wherein the electrically conductive polymer sleeve has an outer surface resistivity of about 1 E+3 ohm to about 1 E+4 ohm.
A fifteenth aspect according to any of the first through twelfth aspects, wherein the electrically conductive polymer sleeve has an inner surface resistivity of about 0.9 E+2 ohm to about 1 E+4 ohm.
A sixteenth aspect according to any of the first through twelfth aspects, wherein the electrically conductive polymer sleeve has an inner surface resistivity of about 1 E+3 ohm to about 1 E+4 ohm.
A seventeenth aspect according to any of the previous aspects, wherein the one or more electrically conductive polymer tie bands have a resistivity of about of about 1 E ohm to about 1 E+4 ohm.
An eighteenth aspect according to any of the previous aspects, wherein the electrically conductive polymer sleeve is reusable.
In a nineteenth aspect, an electrostatic discharge kit comprises an electrically conductive polymer sleeve and electrically conductive tie bands.
In a twentieth aspect, a fluid handling system comprises an electrostatic mitigation filter of any one of the first through eighteenth aspects.
In a twenty-first aspect, a method of mitigating electrostatic discharge in a fluid handling system comprises installing an electrostatic mitigation filter of any one of the first through eighteenth aspects in the fluid handling system.
The descriptions of the various embodiments of the present disclosure have been presented for purposes of illustration, but are not intended to be exhaustive or limited to the embodiments disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art without departing from the scope and spirit of the described embodiments. The terminology used herein was chosen to explain the principles of the embodiments, the practical application or technical improvement over technologies found in the marketplace, or to enable others of ordinary skill in the art to understand the embodiments disclosed herein.
This application claims the benefit of U.S. Application No. 62/842,942 filed on May 3, 2019, which is hereby incorporated by reference in its entirety.
Number | Date | Country | |
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62842942 | May 2019 | US |
Number | Date | Country | |
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Parent | 16857918 | Apr 2020 | US |
Child | 18434634 | US |