The invention relates to fluid processing and, more particularly, high pressure fluid processing devices for creating particulate structures in a fluid mixture.
The creation and processing of hard, non-compliant particles in a fluid mixture is desirable for a variety of industrial processes including, for example, the preparation of inks, paints, abrasive coatings, and the like. In addition, fluid mixtures of hard particles are used extensively in the coating of magnetic media, such as magnetic disks, magnetic tape or other magnetic media used for data storage. For magnetic media, the mixture may contain magnetic particles and a polymeric binder carried in a solvent. The coating process involves application of the mixture to a substrate, followed by a drying process to remove the solvent.
For high-density magnetic media and other industrial processes, the size and uniformity of the various particles is extremely important. To produce particles in a desired size range, industrial fluid processing techniques make use of one or more fluid processing devices. A fluid processing device processes the fluid mixture in a manner that subjects particles or other units of microstructure in the mixture to intense energy dissipation through the generation of a combination of intense shear and extensional forces. In this manner, agglomerations of the particles in the fluid mixture can be broken down into smaller sized particles.
In general, the invention is directed to a high pressure fluid processing device for shearing particles or other units of microstructure in a fluid mixture. The fluid processing device makes use of annular fluid flow paths. For example, the fluid mixture can be separated into two fluid paths which are introduced to first and second annular flow paths on opposite sides of a flow path cylinder. The two annular flow paths flow toward one another through the cylinder, and meet one another within the cylinder. An outlet extends through the cylinder where the two annular flow paths collide, allowing a fluid mixture flowing down the annular flow paths to be expelled. The shear force of the collision of the mixture flowing down one annular flow path with the mixture flowing down the other annular flow path causes particles in the mixture to be broken into smaller particles prior to expulsion through the outlet.
A cylindrical rod may be positioned within the flow path cylinder to define the inner diameter of the annular flow paths. In other words, an inner diameter of the flow path cylinder defines an outer diameter of the annular flow paths, and an outer diameter of the cylindrical rod positioned inside the flow path cylinder defines an inner diameter of the annular flow paths.
In some embodiments, the cylindrical rod may be free to move and vibrate within the flow path cylinder, which can provide an automatic anti-clog mechanism. In other words, if particles in the mixture become clogged inside the fluid processing device, the cylindrical rod which defines the inner diameter of the annular flow path can move or vibrate as a result of pressure imbalance caused by the clog. The movement of the cylindrical rod, in turn, may help to clear the clogged material and restore the pressure balance within the fluid processing device.
The outlet can be located approximately near the center of the flow path cylinder, and may have a fixed or adjustable width. In the case where the width of the outlet is adjustable, the outer diameter of the annular flow paths may be defined by the inner diameter of two cylinders positioned in series, with the outlet being defined as the lateral gap between the two cylinders. In that case, the cylindrical rod extends inside each of the two cylinders to define the inner diameter of the annular flow paths. The outlet may be adjusted by moving one or both of the cylinders laterally relative to the other.
In one embodiment, the invention provides a fluid processing device comprising a first annular flow path, a second annular flow path, and an outlet for a fluid mixture flowing within both the first and second annular flow paths.
In another embodiment, the invention provides a fluid processing device comprising a first flow path, a second flow path, and an adjustable size outlet for a fluid mixture flowing within both the first and second flow paths.
In another embodiment, the invention provides a fluid processing device comprising a flow path cylinder that defines an outer diameter of first and second annular flow paths, and a rod positioned within the flow path cylinder that defines an inner diameter of the first and second annular flow paths. In addition, an outlet for a fluid mixture flowing within the first and second annular flow paths can be formed in the flow path cylinder.
In another embodiment, the invention provides a fluid processing device comprising a first flow path cylinder that defines an outer diameter of a first annular flow path, and a second flow path cylinder that defines an outer diameter of a second annular flow path. An outlet gap can be defined by a lateral distance between the first and second flow path cylinders. A rod can be positioned within the first and second flow path cylinders to define an inner diameter of the first and second annular flow paths.
In another embodiment, the invention provides a fluid processing system comprising a mixer that mixes particles into a fluid, a pump that pumps the mixed fluid along a flow path, and a fluid processing device that receives the mixed fluid. The fluid processing device may include first and second cylindrical flow paths that receive the mixed fluid and an outlet for the mixed fluid.
In another embodiment, the invention provides a method comprising mixing a fluid mixture, and pumping the fluid mixture into two opposing annular flow paths of a fluid processing device to cause shearing of particles in the mixture.
The invention may be capable of providing a number of advantages. In general, the invention may improve industrial manufacturing of coatings, inks, paints, and the like. In particular, the use of annular flow paths may improve the shearing of particles in a mixture, producing particles with reduced size and possibly enhanced size uniformity. In particular, annular flow paths may enhance wall shear forces in the fluid processing device, e.g., because of increased wall surface area for a given flow path. The invention may be capable of handling input pressures on the order of approximately 60,000 psi (413 MPa). In addition, the invention may provide automatic anti-clog features that can improve the industrial manufacturing process by reducing or avoiding the need to manually clean and de-clog the fluid processing device. Thus, the automatic anti-clog features can reduce maintenance costs and avoid down-time of the manufacturing system. Also, the invention may improve the end product in terms of reduced particle sizes and improve particle size uniformity.
Additional details of one or more embodiments are set forth in the accompanying drawings and the description below. Other features, objects, and advantages of the invention will be apparent from the description and drawings, and from the claims.
As shown in
One or more intensifier pumps 20, for example, may be capable of generating approximately 100 to 60,000 psi (690 kPa to 413 MPa) of fluid pressure. Fluid processing device 12, as described herein, may be capable of handling pressures greater than approximately 10,000 psi (68,950 kPa), greater than approximately 30,000 psi (207 MPa), greater than approximately 50,000 psi (345 MPa) or greater than approximately 60,000 psi (413 MPa). Following pressurization by intensifier pumps 20, the mixture is delivered to fluid processing device 12. Fluid processing device 12 causes shearing to reduce the size of the particles in the mixture. In other words, fluid processing device 12 serves to break down the particles in the mixture into smaller-sized particles, and thereby produce a finely dispersed solution of particles having a desired size range. Heat exchangers (not shown) may be used to dissipate excess thermal energy generated in the mixture during processing and shearing.
A filtration element may be used to filter particles in the mixture. For example, the filtration element may comprise one or more porous membranes, mesh screens, or the like, to filter the mixture. The output of filtration element may then be used for magnetic coating (in the case of magnetic media manufacture), or other industrial processes. In some cases, the output may be packaged and sold, e.g., in the case of inks, paints, dyes or the like. A back pressure regulator (not shown) may be added downstream of filtration element to help maintain constant pressure in system 10 and provide a return path to supply vessel 14 for the mixture.
As described in greater detail below, fluid processing device 12 makes use of opposing, annular fluid flow paths. In particular, fluid processing device 12 may include a flow path cylinder and a rod positioned inside the flow path cylinder. Annular flow paths are defined by the outer diameter of the rod and the inner diameter of the flow path cylinder. Specifically, two annular flow paths flow toward one another through the cylinder, and meet within the cylinder, such as near the center of the cylinder. The opposing forces created by the fluid transmitted along the annular flow paths creates shear forces. An outlet extends through the cylinder where fluid mixtures flowing down the two annular flow paths collide, allowing the mixture to be expelled through the outlet. The shear force of the collision of the fluid mixtures causes particles in the mixture to be broken-up prior to expulsion through the gap, producing particles of reduced size. Moreover, annular flow paths may enhance wall shear forces in fluid processing device 12 by increasing surface area associated with a given flow path.
The rod may be cylindrical, and can be positioned within the flow path cylinder to define the inner diameter of the annular flow paths. In other words, an inner diameter of the flow path cylinder defines an outer diameter of the annular flow paths, and an outer diameter of the cylindrical rod positioned inside the flow path cylinder defines an inner diameter of the annular flow paths. In some embodiments, the cylindrical rod may be free to move and vibrate within the flow path cylinder, which can provide an automatic anti-clog mechanism. Also, the outlet may be an adjustable gap defined by two separate flow path cylinders positioned in series, with the rod extending into both cylinders. In that case, the mixture flows down the cylinders in opposing directions and meets at the adjustable gap defined by separation of the two separate flow path cylinders
In particular, the inner diameter of flow path cylinder 30 defines an outer diameter of annular flow paths that feed toward one another to meet at the center of cylinder 30. Rod 32 is positioned inside flow path cylinder 30. For example, rod 32 may define first and second ends. A first end of rod 32 extends into annular flow path 33 and a second end of rod 32 extends into second annular flow path 34. The outer diameter of rod 32 defines the inner diameter of the annular flow paths. Accordingly, flow paths 25 and 26 respectively feed into annular flow paths 33, 34 defined by flow path cylinder 30 and rod 32.
The mixture flows down annular flow paths 33, 34 and collides at or near outlet 36 formed in flow path cylinder 30, e.g., approximately at the lateral center of cylinder 30. The shear force of the collision of the mixture flowing down the annular flow paths 33, 34 causes agglomerations in the mixture to be broken up into smaller sized particles. Moreover, annular flow paths 33, 34 may enhance wall shear forces in fluid processing device 12 by increasing surface area associated with the flow paths. In this manner, fluid processing device 12 can be used to shear particles in a mixture. After shearing, the mixture is expelled through outlet 36 and exits fluid processing device 12 (as indicated at output 38).
As further shown in
Substantially identical flows of the mixtures down the respective annular flow paths 33, 34, e.g., in terms of pressure or temperature, is indicative of a non-clogged condition. Temperature monitoring, in particular, can be used to identify when a clogged condition occurs, and may be used to identify when an anti-clogging measures should be taken, e.g., application of a pulsated short term pressure increase in the input flow to clear the clog.
Gland nuts 47, 48 may be used to secure flow path cylinder 30 in the proper location within fluid processing device 12. Moreover, gland nuts 47, 48 can be formed with channels (indicated by the dotted lines) that allow fluid to flow freely through flow paths 25, 26 and into annular flow paths 33, 34.
Rod 32 may be cylindrically shaped, although the invention is not necessarily limited in that respect. For example, other shapes of rod 32 may further enhance wall shear forces in the annular flow paths. Rod 32 may be free to move and vibrate within the flow path cylinder 30. In particular, rod 32 may be unsupported within flow path cylinder 30. Free movement of rod 32 relative to flow path cylinder 30 can provide an automatic anti-clogging mechanism to fluid processing device 12. If particles or agglomerations in the mixture become clogged inside the fluid processing device 12, e.g., at the edges of annular flow paths 33, 34, rod 32 may respond to local pressure imbalances by moving or vibrating. In other words, a clog within cylinder 30 or in proximity of annular flow paths 33, 34 may result in a local pressure imbalance that causes rod 32 to move or vibrate. The movement and/or vibration of the rod 32, in turn, may help to clear the clog and return the pressure balance within fluid processing device 12. In this manner, allowing rod 32 to be free to move and vibrate within the flow path cylinder 30 can facilitate automatic clog removal.
To further improve clog removal, a pulsated short term pressure increase in the input flow can be performed upon identifying a clog. For example, as mentioned above, temperature sensors 41, 42 may identify temperature changes in flow paths 25, 26 occur, which may be indicative of a clogged condition. In response, a short term pressure increase, e.g., a two-fold pressure increase for approximately five seconds, can cause more substantial movement and/or vibration of the rod 32 to facilitate clog removal. The pulsated short term pressure increase in the input flow can be performed in response to identifying a clogged condition, or on a periodic basis. For example, intensifier pump 20 (
In different embodiments, outlet 36 can have a fixed or adjustable size. For example, outlet 36 may take the form of a gap with an adjustable width. Flow path cylinder 30 and rod 32 may define substantially constant diameters, or one or both of flow path cylinder 30 and rod 32 may define diameters that vary or change along the annular flow paths. The components of fluid processing device 12, including flow path cylinder 30 and rod 32 may be formed of a hard durable material such as steel or a carbide material. As one example, flow path cylinder 30 and rod 32 can be formed of tungsten carbide containing approximately six percent tungsten by weight.
Again, annular flow paths 33, 34 are defined by flow path cylinder 30 and rod 32. Flow path cylinder 30 may define a minimum width that remains substantially constant along the annular flow paths. Rod 32 may be cylindrically shaped, and can be free to move and vibrate within the flow path cylinder 30. Ordinarily rod 32 is concentric with the annular flow paths, having a center axis that is aligned with the central longitudinal axis of flow path cylinder 30. Fluid dynamic forces and uniform balance of rod 32 can force rod 32 toward the lateral and longitudinal center of the annular flow path. Movement and vibration of rod 32 within the flow path cylinder 30 can facilitate automatic clog removal.
The minimum width of the inner diameter of flow path cylinder 30 may be in the range of approximately 0.1 inch (0.254 cm) to 0.001 inch (0.00254 cm). For example, the width of the inner diameter of flow path cylinder 30 may be approximately 0.0290 inch (0.07366 cm). The width of the outer diameter of rod 32 may be slightly smaller than the minimum inner diameter of flow path cylinder 30. For example, if the width of the inner diameter of flow path cylinder 30 is approximately 0.0290 inch (0.07366 cm), the width of the outer diameter of rod 32 may be between approximately 0.0260 inch (0.06604 cm) and 0.0280 inch (0.07112 cm). Other sizes, widths and shapes of flow path cylinder 30 and rod 32 could also be used in accordance with the invention.
By way of example, the width of outlet 36 may be approximately between 0.0001 inch (0.000254 cm) and 0.1 inch (0.254 cm). As one example, the width of outlet 36 at the outer diameter of flow path cylinder 30 is approximately between 0.006 inch (0.01524 cm) and 0.010 inch (0.0254 cm). Outlet 36 may extend approximately 180 degrees around cylinder 30, or may extend to a lesser or greater extent, if desired. Other sizes and shapes of outlet 36 could also be used.
In the configuration of
In the configuration of
Rod 32 is positioned inside flow path cylinder 30, thereby creating flow paths that are annular. Rod 32 may have a length that is longer, shorter, or approximately the same length as flow path cylinder 30. Preferably, rod 32 may have a length that is longer than the length of flow path cylinder 30, but shorter than a distance between input nozzles (not shown) or gland nuts (not shown) through which fluid is introduced into flow path cylinder 30.
In an alternative embodiment shown in
A number of embodiments of the invention have been described. Nevertheless, it is understood that various modifications may be made without departing from the spirit and scope of the invention. For example, the fluid processing device may be used in other industrial systems that may or may not include the components illustrated in FIG. 1. Accordingly, other embodiments are within the scope of the following claims.
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Number | Date | Country | |
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20040050430 A1 | Mar 2004 | US |