Patent Application
20190168131
The present invention relates to the field of gas distributors for gas/liquid contact columns and more particularly to the columns for units for the treatment of gas, for the capturing of carbon dioxide (CO2) or for the dehydration of a gas.
Units for the treatment of gas and/or for the capturing of CO2 by washing with amines and/or for distillation and/or for dehydration comprise columns for exchange of material and/or heat between a gas and a liquid. They can, for example, be columns for the absorption and regeneration of liquid or gaseous fluids. These columns operate in countercurrentwise or cocurrentwise gas/liquid flow.
In the present description, these columns for exchange of material and/or heat between a gas and a liquid are denoted without distinction as gas/liquid exchange columns or gas/liquid contact columns.
The gas/liquid contact columns used in these units for the treatment of gas and/or for the capturing of CO2 and/or for distillation and/or for dehydration generally operate on the principle of an exchange of material and/or of heat between the gas and the fluid which circulate in the columns.
When it is a matter of removing contaminants present in the gas, such as CO2, water, hydrogen sulfide (H2S) or carbonyl sulfide (COS), by processes of washing with a liquid, use is generally made of vertical gas/liquid contact columns which wash an ascending gas stream by countercurrentwise circulation with a descending liquid stream. Thus, the contaminants of the gas are retained by the liquid during the rise of the gas in the column with variable absorption rates. In the context of the absorption of contaminants in a gas, vertical contact column is also understood to mean regeneration towers, in which solvents (liquids) laden with contaminants are purified by contact with a gas, which favours the extraction of the contaminants present in the solution laden with contaminants. The units are generally composed of two gas/liquid contact columns, one devoted to the absorption of the contaminants, such as acid compounds in the gaseous form, by the solvent flowing along the absorption column, also known as absorber, and the other being devoted to the regeneration (“regenerator”) of the solvent containing the contaminants resulting from the first gas/liquid contact column, also known as enriched solvent, for example by contributing heat in the form of boiling the said solvent, so as to completely purify the solvent, which is then reused in the absorber. This regenerated solvent is also known as depleted solvent.
There exists a great variety of types of gas/liquid contact columns.
The “random” packings and the “structured” packings form the two main families of packings currently available. A packing of random type consists of a multiplicity of singular solid elements, possibly identical and generally of moderate size (of the order of a centimetre), randomly deposited within the contactors, while a packing of structured type is generally formed by steel sheets shaped and arranged in a specific manner.
As represented in
For all the types of packing, in order to have available the entire surface area developed by the transfer internal, it is advisable for each of the streams moving about countercurrentwise to flow in as uniform a manner as possible over the whole of the section of the column, and contact internals of the column. To this end, the depleted solvent DS, at the column top, is injected uniformly over the section of the top packing bed 7, using a liquid distributor 3, and the gas to be treated FTBT is introduced at the contactor bottom using the gas distributor 2. The column 1 also comprises a plurality of liquid collecting and redistribution systems (4,5) between the packing beds 7. The column 1 represented thus comprises two such liquid collecting and redistribution systems (4,5), each been placed between two successive packing beds 7, making it possible, on the one hand, to collect the descending liquid originating from the upper packing bed and to distribute the said liquid over the lower packing bed and, on the other hand, to uniformly distribute the gas originating from the lower liquid packing bed over the upper packing bed. This configuration is particularly well suited when a high gas/liquid contact height is required. These intermediate liquid collecting and redistribution systems, in this instance installed between two packing beds 7, can be of different types, such as, for example, systems comprising a liquid-collecting tray 4 comprising chimneys for the passage of the gas, combined with a distributor 5 comprising a vertical conduit emerging over a plurality of sprinklers (horizontal pipes equipped with orifices or nozzles) for the distribution of the liquid collected on the tray 4.
In general, the gas distributor 2 positioned at the bottom of the column also collects the liquid ES, which can subsequently be extracted at the bottom of column 1. The liquid ES is generally collected in a liquid-collecting zone provided on the gas distributor 2, the said zone being conventionally connected to the bottom of the column via legs emerging in a liquid guard zone from where the liquid is withdrawn from the column 1.
The present invention relates in particular to such a device for the distribution of gas and collecting of liquid, positioned at the bottom of a column for exchange of material and/or of heat between a gas and a liquid. Such a device does not have the role of the redistribution of liquid, such as the intermediate liquid collecting and redistribution systems between packing beds illustrated in
As mentioned above in the description of the column represented in
In particular, the quality of the distribution of the gas becomes better as the diameter of the column increases and as the packing used to bring the gas and the liquid into contact becomes more capacitive. Capacitive packing is understood to mean a packing having a high capacity. Capacity of a packing refers to the maximum amount of gas which can circulate without obstructing the column, with respect to a given liquid flow rate, that is to say without creating an accumulation of liquid in a part of the packing. The capacity of a packing depends on numerous factors (angle of the channels, shapes of the elements, and the like); it is generally inversely proportional to its specific surface (also known as geometric area), which is the contact surface area per unit of volume (expressed in m2/m3). This is because the use of a capacitive packing makes it possible to delay the phenomenon of obstruction of the column and also makes it possible to reduce the pressure drop per unit length in the packing. Pressure drop per unit length is understood to mean the total pressure drop of the packing in relation to its height.
Thus, more particularly for large-diameter columns for exchange of material and/or of heat between a gas and a liquid, typically having a diameter of greater than or equal to 1 m, the system for distribution of the gas at the column bottom proves to be important.
Among the existing systems for distribution of the gas at the column bottom, chimney trays are widely employed. Such a type of gas distributor is illustrated in
The tray 2 has a circular general shape, according to a top view, and comprises a first flat portion 2′ supporting the chimneys 8, having a truncated circle shape, according to a top view, a second flat portion 9″ substantially parallel to the first flat portion, located at a lower level than that of the first portion of the tray and connected to the first portion via the weir 9′, which is a third flat orthogonal portion of the tray. The collecting zone 9 is thus the volume formed in part by the weir 9′ and the second flat portion 9″ of the tray, the other part being the wall of the shell of the column (not represented).
On the tray 2 represented, 12 chimneys in rectangular parallelepiped form, laid out along an axis parallel to the plane formed by the weir 9′, are thus positioned in a way aligned in pairs on either side of a central conduit dividing the first portion of the tray into two equal parts, the said conduit emerging in the collecting region 9 delimited by the weir 9′ and the second lower flat portion 9″ of the tray.
In other gas distributors of chimney tray type according to the prior art, the chimneys for passage of the gas can have other shapes and another arrangement than those of the gas distributor tray illustrated in
However, the gas distributors of chimney tray type according to the prior art are not always satisfactory and may exhibit gas velocities which are not completely homogeneous, in particular on the edges of such trays, this becoming more accentuated as the diameter of the column increases.
In addition, it is always desired to reduce the height of a column, in particular constrained by the size of the internals which it contains, and of which the gas distributor placed at the column bottom forms part.
The present invention is thus targeted at providing an improved gas distributor of chimney tray type, in particular to be used in the case of large-diameter columns (typically with a diameter at least equal to 1 m), making possible in particular better homogenization of the gas velocity downstream of the distributor (downstream being defined with respect to the direction of the gas stream ascending in the column), while minimizing the bulkiness, that is to say the height of the gas distributor and thus of the column in which is incorporated.
Thus, in order to achieve at least one of the objectives targeted above, among others, the present invention provides, according to a first aspect, a gas-distributing tray for a column for exchange of heat and/or of material between a gas and a liquid comprising an upper face and a lower face, a plurality of protruding chimneys which are substantially parallelepipedal and parallel to one another over a portion of the upper face of the tray for the exclusive passage of the gas through the tray, and a zone for collecting the liquid comprising two diametrically opposite weirs for collecting the liquid on the tray, the chimneys each comprising an element for distribution of the gas of the same shape as the chimney, the element for distribution of the gas of at least one of the said chimneys partially overlapping the zone for collecting the said liquid.
According to one embodiment, the chimneys have substantially a right-angled parallelepiped shape.
According to one embodiment, the chimneys extend between the weirs.
According to one embodiment, the length of the element for distribution of the gas of at least one of the said chimneys is greater than the width of the portion of the upper face of the tray supporting the chimneys, which is defined as being the distance separating the two diametrically opposite weirs.
According to one embodiment, each chimney additionally comprises a raising chamber on which the element for distribution of the gas rests, the element for distribution of the gas thus being raised with respect to the said portion of the upper face of the tray, preferably by a height (h2) of between 0 and 0.20 m.
Preferably, the length of the raising chamber of each chimney is less than or equal to the width of the portion of the upper face of the tray supporting the chimneys, which is defined as being the distance separating the two weirs, and is less than or equal to the length of the element for distribution of the gas.
According to one embodiment, the element for distribution of the gas of the chimneys is surmounted by a cap for preventing the passage of the liquid through the chimneys, the cap being raised with respect to the top of the element for distribution of the gas so as to leave a space for the passage of the gas.
According to one embodiment, at least one of the chimneys, and preferably all of the chimneys, comprises an element which is dispersive with respect to the gas positioned inside the element for distribution of the gas of the chimney.
The dispersive element can comprise a perforated plate comprising circular orifices or slits for the passage of the gas.
The dispersive element can comprise a random or structured packing, preferably uniformly disseminated inside the element for distribution of the gas of the chimney in the direction of its height and along a plane orthogonal to its height.
According to one embodiment, the two weirs are located at the periphery of the tray in two diametrically opposite zones of the tray and are orthogonal to the portion of the upper face of the tray supporting the chimneys.
According to one embodiment, the collecting zone comprises two distinct volumes, each volume being partially delimited by one of the two weirs and a basal portion of the tray.
According to one embodiment, the tray comprises between 2 and 100 chimneys.
According to a second aspect, the present invention relates to a column for exchange of heat and/or of material between a gas and a liquid, comprising at least one gas/liquid contactor which brings the gas and the liquid into contact and at least one gas-distributing tray according to the invention, positioned at the bottom of the column upstream of any gas/liquid contactor in order to distribute the gas at the base of the gas/liquid contactor.
According to a second aspect, the present invention relates to the use of a column according to the invention for a process for the treatment of gas, for capturing CO2, for the dehydration of a gas or for distillation.
Other subject-matters and advantages of the invention will become apparent on reading the description which follows of specific exemplary embodiments of the invention, given by way of nonlimiting examples, the description being made with reference to the appended figures described below.
In the figures, the same references denote identical or analogous elements.
The present invention relates to a gas-distributing tray for a column for exchange of heat and/or of material between a gas and a liquid, comprising a plurality of protruding chimneys over a portion of the upper face of the tray for the exclusive passage of the gas through the tray and a zone for collecting the liquid comprising diametrically opposite weirs for collecting the liquid on the tray. The chimneys have substantially a, preferably right-angled, parallelepiped shape, are positioned parallel to one another and each comprise an element for distribution of the gas of the same shape as the chimney. The element for distribution of the gas of at least one of the chimneys partially overlaps the zone for collecting the liquid.
By virtue of this overlapping, the gas-distributing tray according to the invention exhibits a high surface area open to the passage of the gas, making it possible to provide better quality of distribution of the gas. It is thus distinguished from the known gas distributors, in which the chimneys are restricted to a zone for distribution of the gas without overlapping with the zone for collecting the liquid.
The distributing tray according to the invention is also compact in height by virtue of this overlapping. This is because such an overlapping makes possible better flexibility regarding the proportioning of the collecting zone and in particular a design of the tray which is more compact in height. For a given volume of the zone for collecting the liquid, the height of the zone for collecting the liquid of the distributing tray according to the invention can be reduced as the surface area of the collecting zone can be increased, owing to the fact that the surface of opening to the passage of the gas partially overlaps the surface of the zone for collecting the liquid.
The gas-distributing tray according to the invention is appropriate to being employed at the bottom of a column for exchange of heat and/or of material between a gas and a liquid operating according to a countercurrentwise flow, the gas rising from the bottom of the column through the chimneys of the gas-distributing tray for the exclusive passage of the gas and the descending liquid being collected in the zone for collecting the liquid, which can then be subsequently discharged out of the said column.
The gas-distributing tray 20 is represented according to a perspective view in
The gas-distributing tray 20 comprises a plurality of chimneys 80, for example 7 chimneys 80 as represented in the figures, for the exclusive passage of the gas g through the tray 20. Plurality of chimneys is understood to mean at least two chimneys. The number of chimneys is variable and depends on the design of the tray, in particular on parameters such as the size of the tray, the degree of opening desired, the volume of the collecting zone, and the like. Solely by way of indication, without any limitation, the gas-distributing tray 20 can comprise between 2 and 100 chimneys 80. The chimneys 80 protrude over a portion 21 of the upper face of the tray.
Upper face of the gas-distributing tray 20 refers to the face of the distributing tray which is directed towards the top of the exchange column. In contrast, the lower face of the distributing tray 20 is that directed towards the bottom of the column by which the gas to be distributed arrives.
The chimneys 80 are substantially parallelepipedal, for example in right-angled parallelepiped form, as represented, and are positioned parallel to one another. Preferably, a regular spacing separates the chimneys 80. Such a form of the chimneys makes possible a wide opening to the passage of the gas, in particular in comparison with known cylindrical chimneys, which makes it possible to limit the pressure drops.
The distributing tray also comprises a zone for collecting the liquid 90 comprising two diametrically opposite weirs (91, 92) for the collecting of the liquid l on the tray 20.
Weir is understood to mean a portion of the tray which is inclined, typically substantially orthogonal, with respect to the portion 21 of the upper face of the tray 20 supporting the chimneys 80, which is positioned at the periphery of the tray and which makes it possible for the liquid l to pour out towards the base 93 of the tray located at a lower elevation than that of the portion 21 of the upper face of the tray 20. The elevations are evaluated when the tray 20 is in the non-inclined position (i.e. portion 21 of the tray supporting the chimneys in a substantially horizontal plane) and positioned so that a vertical axis Z passes through the chimneys 80 positioned on the tray, corresponding to the position of use of the tray in the gas/liquid exchange column. This is transposable to all the elevations mentioned in the present description.
According to the invention, the weirs (91, 92) are preferably located at the periphery of the gas-distributing tray in two diametrically opposite zones, and are orthogonal to the portion 21 supporting the chimneys 80. These are, for example, flat plates connecting the portion 21 which is the support of the chimneys 80 and the base 93 of the distributing tray 20, orthogonal to the planes formed by the portion 21 and the base 93 of the tray 20.
The collecting zone 90 is equivalent to a volume which can be calculated from the diameter ϕ of the cylinder in which the gas-distributing tray 20 is inscribed, from the height h1 of the collecting zone defined between the base 93 of the tray and the portion 21 which is the support of the chimneys, and from the width L of the portion 21 of the tray.
The collecting zone 90 preferably comprises, and in particular consists of, two distinct volumes, each volume being partially delimited by one of the two weirs and a basal portion 93 of the tray. When the tray is positioned in the gas/liquid contact column, each of the two volumes is then also delimited by the internal wall of the column to which the tray is attached. The two volumes are open towards the top of the tray, that is to say on the side of the chimneys 80, so as to collect the liquid l, and closed towards the bottom of the tray, that is to say at the level of the base 93 of the tray. Means for discharging the liquid collected, such as openings in the tray and pipes, not represented, can be provided in the collecting zone 90, in particular in the two volumes of the collecting zone. Thus, the liquid can be discharged from the collecting zone towards the bottom of the column in a zone of the column where a liquid guard is formed and from where it can subsequently be extracted out of the column.
According to the embodiment illustrated in
According to the invention, the element for distribution of the gas 82 of at least one of the chimneys 80 partially overlaps the zone for collecting the liquid 90. More specifically, the element for distribution of the gas 82 partially overlaps the region for collecting the liquid 90, that is to say the zone which recovers the liquid descending in the column and falling onto the portion 21 of the tray 20 between the chimneys 80, this collecting zone preferably being formed by the two distinct volumes formed between the basal portion of the tray 93 and the weirs (91, 92). The element for distribution of the gas 82 thus juts out from the portion 21 of the tray over the said collecting zone (90).
The raised element for distribution of the gas 82 is located at higher elevations than those of the raising chamber 81 of the chimney 80. It thus constitutes an upper part of the chimney and the raising chamber 81 constitutes a lower part of the chimney. As illustrated in particular in
The raising chamber 81 of the chimney comprises, at its base, the arrival opening for the gas g originating from the lower part of the distributing tray 20, and the element for distribution of the gas 82 of the chimney comprises, at its top, the opening for escape of the gas which has passed through the chimney 80. In the embodiment where the chimneys do not comprise raising chambers, the element for distribution of the gas 82 comprises, at its base, the arrival opening for the gas g originating from the lower part of the distributing tray 20.
According to the invention, given that the element for distribution of the gas 82 of at least one of the chimneys 80, for example of the three central chimneys as represented, partially overlaps the zone for collecting the liquid 90, the distributing tray exhibits a surface area open to the passage of the gas which is improved with respect to the gas-distributing trays according to the prior art, in particular with respect to gas-distributing trays according to the prior art having chimneys in right-angled parallelogram form without overlapping of the collecting zone. Such an improved surface area for passage to the gas makes possible better homogenization of the gas velocity downstream of the gas-distributing tray.
The surface area open to the passage of the gas can be quantified by the degree of opening to the passage of the gas, defined in the present description as the ratio of the total surface area formed by the openings for escape of the gas at the top of the chimneys 80 (i.e. at the top of the element for distribution of the gas 82 of the chimneys 80) to the total surface area of the gas-distributing tray 20, the said total surface area of the tray conventionally being that of a circle for a tray which is inscribed in a cylinder, the diameter ϕ of which is that of the gas/liquid contact column.
Further details are given below regarding the overlapping of a part of the collecting zone 90 by the element for distribution of the gas 82 of at least one chimney 80 of the gas-distributing tray.
The chimneys 80 in, preferably right-angled, parallelepiped form advantageously extend between the weirs (91, 92). They are thus extended along an axis X orthogonal to the planes formed by the weirs (91,92).
Advantageously, the length of the element for distribution of the gas 82 of at least one of the chimneys 80 is greater than the width L of the portion 21 of the upper face of the tray 20 supporting the chimneys 80. This width L of the portion 21 is defined by the distance separating the two weirs (91, 92), as clearly visible in
Advantageously, the length of the raising chamber 81 of each chimney 80 is less than or equal to the said width L of the portion 21 of the tray and is less than or equal to the length of the element for distribution of the gas 82.
Thus it is that, in the tray represented in
Preferably, the element for distribution of the gas 82 of the chimneys 80 is surmounted by a cap 84 for preventing the passage of the liquid l through the chimneys. The cap 84 is raised with respect to the top of the element for distribution of the gas 82 by a given height h4, as visible in
Preferably, the inside of the element for distribution of the gas 82 of at least one of the chimneys 80 is provided with an element which is dispersive with respect to the gas, that is to say an element which provides dispersion of the gas as it passes through the element for distribution of the gas of the chimney, thus generating a better dissemination (within the meaning of the homogenization) of the gas in this part of the chimney and thus at the outlet of the chimney. Such a rehomogenization of the gas is particularly advantageous when the length of the element for distribution of the gas 82 of the chimney is greater than that of the raising chamber 81 of the chimney. Preferably, all the chimneys of the distributing tray are provided with such a dispersive element, so as to favour a homogenization of the gas stream downstream of the distributing tray.
This dispersive element can be positioned at the base of the element for distribution of the gas 82 of the chimney, for example in the first third of the element for distribution of the gas 82 of the chimney. By thus being closer to the base of the element for distribution of the gas 82 than to its top, the dispersive element makes it possible to redistribute the gas over the whole of the surface of the chimney, while leaving a sufficient height for the stabilization of the gas which has passed through the dispersive element.
Advantageously, the dispersive element comprises a perforated plate comprising circular orifices or slits. The example of distributing tray according to the invention represented in
Random packing refers to anarchic haphazard stacks of unit elements having specific shapes, for example rings, spirals, and the like. They are generally used to perform exchanges of heat and/or of material, which are carried out within these unit elements. These unit elements can be made of metal, of ceramic, of plastic or of analogous materials. Patent Applications EP 1 478 457 and WO 2008/067031 describe two examples of random packing unit element. The random packing offers advantageous qualities in terms of efficiency of transfer, low pressure drop and simplicity of installation. The geometric area of the random packing can be between 70 and 250 m2/m3. Structured packing refers to a stack of bent or corrugated (that is to say, substantially undulating with right angles) plates or sheets arranged in an organized manner in the form of large blocks, as described in particular in Patent Applications FR 2 913 353 (US 2010/0213625), U.S. Pat. No. 3,679,537 and U.S. Pat. No. 4,296,050. They are generally used to produce exchanges of heat and/or of material, which are carried out on these plates. The structured packings have the advantage of offering a great geometric area for a given representative diameter. The geometric area of the structured packing can be between 100 and 500 m2/m3.
When a random packing or packing of structured type is concerned, the dispersive element can be disseminated inside the element for distribution of the gas 82 of the chimney or chimneys for the exclusive passage of the gas uniformly in the direction of the height of the chimney (along the axis Z) and uniformly along a plane orthogonal to the height of the chimney (along the axis X). In this way, the dispersion of the gas passing through the chimney or chimneys is as homogeneous as possible, which makes possible a gas stream at the outlet of the chimney or chimneys which is unvarying over a section corresponding to the section of the chimney or chimneys.
Still when a random packing or packing of structured type is concerned, the dispersive element can be uniformly disseminated in the element for distribution of the gas 82 of the chimney over a thickness at least equal to 5 cm in the direction of the height of the chimney. In this way, the gas particles passing through such thicknesses of dispersive material are sufficiently dispersed to provide a homogeneous gas stream at the outlet of the chimneys. The dispersive element can by also be uniformly disseminated over the entire height of the element for distribution of the gas 82 of the chimney or chimneys for the exclusive passage of the gas.
Again when a random packing or packing of structured type is concerned, this dispersive element is preferably more capacitive than the packing used as gas/liquid contactor positioned higher in the column for exchange of material and/or of heat between a gas and a liquid.
The invention also relates to a column for exchange of material and/or of heat between a gas and a liquid, in which the two fluids are brought into contact by means of at least one gas/liquid contactor. Such a gas/liquid contactor is preferably a bed of structured or random packing, as are defined above. It can also be any other means for bringing into gas/liquid contact which makes possible an exchange of material and/or of heat, such as trays.
The gas and the liquid flow in the column countercurrentwise, in particular with an ascending gas stream and a descending liquid stream.
The column according to the invention can be a column as described in connection with
The column according to the invention is characterized in that it comprises a single gas-distributing tray 20, as described above, positioned at the bottom of the column upstream of any gas/liquid contactor in order to uniformly distribute the gas at the base of the said gas/contactor.
According to one embodiment of the present invention, the column comprises several sections, each section comprising a gas/liquid contactor, preferably a bed of structured or random packing.
The column according to the invention can be used in a process for the treatment of gas, in particular a process for the removal of acid compounds present in a gas by means of a liquid solution based on amine(s), for example for treating natural gas, or in a process for capturing CO2, which is typically a process for the treatment of the gas by means of a liquid solution based on amine(s), for example in order to treat combustion flue gases. The column according to the invention can also be advantageously used in a process for the dehydration of a gas targeted at removing the water (“to dry”) present in a gaseous effluent, such as natural gas, by bringing the gas into contact with liquid solvent, such as glycol, or again be used in a process of the distillation of liquids. Other types of solvents can be used in these processes where a column according to the invention can be used.
Without further elaboration, it is believed that one skilled in the art can, using the preceding description, utilize the present invention to its fullest extent. The preceding preferred specific embodiments are, therefore, to be construed as merely illustrative, and not limitative of the remainder of the disclosure in any way whatsoever.
In the foregoing and in the examples, all temperatures are set forth uncorrected in degrees Celsius and, all parts and percentages are by weight, unless otherwise indicated.
The entire disclosures of all applications, patents and publications, cited herein and of corresponding application No. FR 1761469, filed Nov. 30, 2017 are incorporated by reference herein.
The following example illustrates certain advantages of the present invention, on comparing the results obtained using a gas-distributing tray according to the invention and a gas-distributing tray according to the prior art, in the context of a process for the reactive absorption of acid compounds by washing with amines of the capturing of CO2 type, in order to achieve a target specification of CO2 content at the outlet of the absorber. The column and the process for capturing CO2 exhibit the following main characteristics:
The exemplified distributing tray according to the invention is in accordance with that represented in
The gas-distributing tray according to the prior art tested differs from the present example of gas-distributing tray according to the invention in that the chimneys of right-angled parallelepiped form are extended along an axis parallel to the weirs, without possible overlapping of the collecting zone by the chimneys. It comprises 7 chimneys. Other differences relate to the dimensions of the collecting zone (and in particular the height h1 of the weirs). The tray according to the prior art and the tray according to the invention have different dimensions of the collecting zone but an identical volume (0.0908 m3) of the collecting zone. Other geometric characteristics of the tray according to the invention are summarized below in Table 1.
In this example, the tray according to the invention is designed so as to obtain at least the same performance qualities as those obtained with the exemplified tray according to the prior art.
Certain parameters of the gas-distributing trays tested are compared in Table 1 below.
In Table 1:
It is noted that a high value of the degree of opening to the passage of the gas S, as is the case for the exemplified gas-distributing tray according to the invention, makes possible a better quality of distribution.
A value of approximately 1 of the ratio V/VSG, as is the case with the exemplified gas-distributing tray according to the invention, reflects a good quality of distribution of the gas, makes it possible to reduce the height of homogenization of the streams H between the gas-distributing tray and the bed of packing positioned above the said tray, and thus to reduce the bulkiness.
A low value of the total height of the gas-distributing tray Htotal, as is the case for the exemplified gas-distributing tray according to the invention, makes possible a more compact and less expensive design. A low value of Htotal also makes it possible to reduce the total height of the absorption column.
In comparison with the gas-distributing tray according to the prior art without overlapping of the collecting zone by the chimneys, the gas-distributing tray and liquid collector according to the invention make it possible to provide a better degree of opening to the passage of the gas, thus contributing to better homogenization of the gas velocity downstream of the gas-distributing tray, while exhibiting a reduced bulkiness with a gain of 27% with respect to the distributor according to the prior art, making it possible to advantageously reduce the height of the column.
The preceding examples can be repeated with similar success by substituting the generically or specifically described reactants and/or operating conditions of this invention for those used in the preceding examples.
From the foregoing description, one skilled in the art can easily ascertain the essential characteristics of this invention and, without departing from the spirit and scope thereof, can make various changes and modifications of the invention to adapt it to various usages and conditions.
| Number | Date | Country | Kind |
|---|---|---|---|
| 1761469 | Nov 2017 | FR | national |
