The invention relates to a gas pressure measuring cell configuration according to the preamble of Patent Claim 1.
It is known to employ gas pressure measuring cells that are implemented as thermal conduction measuring cells, for example according to Pirani. In such measuring cells a heating element, conventionally a measuring filament or measuring wire, is heated electrically, and from the filament power the pressure of the gas is determined via the pressure-dependence of the thermal conductivity of the gas. In this manner the pressure can be measured in a range between approximately 10−4 mbar and a few 100 mbar. However, above a few 10 mbar the convective heat transfer predominates such that the measurement of gas flow is affected and becomes highly position-dependent. In addition, measurement according to this method is gas-type dependent. Analysis of the measuring signal with electronic measuring circuitry is relatively complex if precise results over a broad range are to be attained. This is especially the case toward higher pressures starting at approximately 10 mbar since at this pressure the measuring curve, filament power as a function of gas pressure, levels out at constant heating filament temperature. One reason inter alia is also the fact that in this pressure range, as previously indicated, the effect of the flow regime of the gas increases. As is known, the measuring circuitry utilized for this purpose is realized with a Wheatstone-bridge configuration in which one of the four bridge resistances is determined by the measuring filament. Regulation of the measuring filament temperature and analysis of the signal voltage output by the bridge is carried out using measuring electronics, conventionally in analog circuit technology, which, in known manner, comprises for example operational amplifiers and/or comparators. Due to the high temperature sensitivity of the measuring configuration, the temperature of the measuring configuration must additionally be acquired as a reference and also be taken into consideration with the measuring electronics. Such Pirani type gas pressure measuring cells are sensitive and therefore relatively complex and expensive in their realization. However, they are currently in wide use. An overview of this measuring technique is described for example in M. Wutz et al. “Theorie and Praxis der Vakuumtechnik”, F. Vieweg & Sohn, Braunschweig, 1982, 2nd Edition, pp. 366-373.
Such a product has been distributed worldwide for many years with great success by INFICON GmbH, FL-9496 Balzers, Liechtenstein under the product identification Series PSG 50X.
To expand the pressure range to be measured it has also been proposed to combine such a Pirani measuring cell with at least one further different measuring principle. Herewith the pressure range to be measured can be expanded in the lower range as well as the upper range such that it becomes feasible, for example, to realize a combination measuring cell which can measure pressures in the range of 10−8 mbar up to a few bar. Such a combination measuring cell is described, for example, in EP 0 658 755 B1 which combines on a common measuring head a Pirani sensor with an ionization sensor. This document also describes the manner in which the overlapping regions can be handled in terms of signal technology in order to ensure a continuous and linear transition in the signal analysis.
EP 1 097 361 B1 describes a further combination measuring cell in which a Pirani sensor is combined with a capacitive membrane sensor (CDG). In this document directions are also provided for improving the manner in which the problems of temperature control, always inherent in the Pirani measuring principle, can be improved through measures on the sensor head.
Known is also the use of piezoresistive pressure sensors based on semiconductors for acquiring the pressures, especially in the range from 1.0 mbar to 1.0 bar, or even a few bar up to approximately 3.0 bar. Such pressure sensors are suitable for the upper pressure range. Such a pressure sensor is for example described in M. Wutz et al. “Theorie and Praxis der Vakuumtechnik”, F Vieweg & Sohn, Braunschweig, 2010, 10th Edition, pp. 513-514. In such sensors onto a semiconductor membrane are for example applied doped, low-ohmic conductor tracks which form resistances. The resistances are connected such that they form a bridge. For reading out the signal the bridge terminals are carried to the outside. A change of the gas pressure on the membrane causes a deformation of the semiconductor membrane and, from the resistance change resulting therefrom, to the detuning of the bridge. Silicon is especially suitable as the semiconductor material since it is highly flexible. In such semiconductor resistances a pressure change in the material causes a resistance change which is analyzed as pressure mass. Semiconductor materials are especially suitable since not only the resistance changes in them due to the change of the geometric dimensions but additionally its specific resistance whereby additionally the piezoresistive effect is also reinforced. Moreover, the conventional four resistances can be disposed on the membrane such that all effect a signal change in the desired direction during the membrane flexure. This leads to good signal levels. In addition, this configuration also enables integrating, as desired, directly further active components, such as amplifiers or digital elements. Suitable piezoresistive pressure sensors based on silicon are distributed, for example, by Measurement Specialities, 1000 Lucas Way, Hampton, Va. 23666, USA.
The disadvantages of prior art with respect to a Pirani measuring cell and of combination measuring cells when reduced to practice are entailed in the complexity of the configuration with its large number of necessary components. Such a measuring cell requires a vacuum lead-through which separates the vacuum with the sensor cleanly and over long periods of time at high quality during different applications and temperature conditions against atmosphere toward the electronic measuring circuitry. Such vacuum lead-throughs always represent a temperature barrier which hinders the necessary measures for temperature measurements and temperature compensations and thus make them complicated. This also affects negatively the overall size, and smaller measuring cells are only conditionally realizable and the production costs cannot be further reduced.
The present invention addresses the elimination of the disadvantages of prior art. In particular, the present invention addresses the problem of significantly simplifying the structure of a Pirani gas pressure measuring cell configuration while simultaneously attaining a smaller overall size at an increase of the economy of production. This is to be attained without decreasing the measuring quality compared to known measuring cells. This quality is preferably to be improved further. An additional task comprises enabling the expansion of the measuring range of the Pirani measuring cell without the necessity for major additional expenditures.
This problem is resolved in the generic gas pressure measuring cell configuration according to the characterizing features of patent claim 1. The dependent patent claims refer to advantageous further embodiments of the invention.
The gas pressure measuring cell configuration according to the invention comprises a thermal conduction vacuum cell after Pirani comprising a measuring chamber housing which encloses a measuring chamber and which conducts the gas pressure to be measured into the measuring chamber using a measuring connection. In the measuring chamber is disposed a heatable measuring filament connected to an electronic measuring circuitry, with the electronic measuring circuitry being disposed in thermal contact on one side of an insulating carrier plate, preferably comprised of ceramics, and this carrier plate on the opposite side being a portion of the measuring chamber housing. The measuring filament is supplied in series with a measuring resistance directly in feedback by the electronic measuring circuitry and the electronic measuring circuitry determines directly the resistance of the measuring filament.
For measuring the voltages required for this purpose they are supplied to an analog/digital converter ADC and treated in a digital processor for their processing according to specified algorithms. The processor, in turn, conducts necessary signals out via a digital/analog converter DAC for driving and heating the measuring filament of the Pirani configuration which closes the feedback control circuit. The processed signal, in addition, is conducted out by the processor via an I/O interface for further utilization. This interface is preferably implemented as a serial interface. If it is desired to make other types of signals available, such as in parallel or even analog, this is feasible in simple manner using additional electronic circuitry integrated on the carrier plate. Omitting the conventional lead-through and employing the previously described carrier plate, which is preferably comprised of ceramics, as a substrate yields unexpected advantages in the overall temperature behaviour of the gas pressure measuring cell configuration and also unexpectedly novel mounting options for further structural component parts.
For the expansion of the measurable pressure range it is especially advantageous to tie directly into the electronic measuring circuitry on the carrier plate a piezoresistive semiconductor pressure sensor which thereby is also thermally coupled directly with the carrier plate. The present construction also enables connecting in simple manner the piezoresistive pressure sensor directly via a small port in the carrier plate such that it communicates with the measuring chamber in which the measuring filament is also disposed. Such a piezoresistive pressure sensor can advantageously not only be used for pressure measurements alone but also simultaneously for temperature measurements.
The processor based electronic circuitry also entails the significant advantage that it is feasible to work with lower total voltages since there is no longer a need for a bridge circuit. It is also not necessary to select the measuring resistance in the same dimension as the measuring filament. The utilized feed voltage can now be in the low range of approximately 2.0 to 5.0 V and it is even feasible to work pulse-free. In this case the temperature of the measuring filament can now be selected in broad ranges and also be set such that it is variable as a function of pressure in order to circumvent selectively, for example, contamination-sensitive regions or alternatively be better able to manage them. This combined gas pressure measuring cell configuration is extremely simple and cost-effectively realizable at high measuring accuracy and service life. The measuring range to be covered that is feasible and advantageous therewith extends from vacuum to atmosphere pressure, from approximately 10−4 mbar to 3,000 bar, preferably from 10−3 mbar to 2,000 bar at a resolution of better than 30%, preferably better than 15%, in particular better than 5% of the particular measured measurement value.
The invention will be described below schematically and by example in conjunction with Figures.
In the drawing depict:
a schematically and in cross section a gas pressure measuring configuration of the type of thermal conduction vacuum meter after Pirani according to prior art;
b schematically and in cross section an enlarged detail A of a portion of the measuring cell according to
A known measuring cell configuration of the type of thermal conduction vacuum cell after Pirani is shown schematically and in cross section in
With the electronic measuring circuitry disposed on the printed circuit board PCB the Pirani measuring principle is operated. In this case the measuring filament 1, as a component of a Wheatstone bridge R1′, R2, PTC, is maintained at constant temperature as is depicted schematically in
In a branch of the Wheatstone bridge in known manner a temperature sensor is installed, such as for example a PTC or an NTC, to acquire the ambient temperature and to reference to it. The measuring configuration is highly temperature sensitive and varying ambient temperatures affect the measurement and would generate measuring errors unless they are compensated. Good temperature measurement and compensation is therefore very important in Pirani thermal conduction measuring cells. The temperature sensor must therefore also be disposed at a suitable location in order to be able to acquire the critical temperature changes as characteristically as possible. A disposition of such a temperature sensor 32 in practice is depicted in
For measuring higher gas pressures in the vacuum range of approximately 1.0 mbar to 1.0 bar measuring sensors 20 have also become known which operate according to the piezoresistive principle, such as has previously been explained above. Such a sensor is depicted for example schematically and in cross section in
A gas pressure measuring cell configuration with a thermal conduction vacuum cell after Pirani according to the present invention is depicted schematically and in cross section in
The carrier plate 10 can advantageously be implemented as a separate structural unit and be mounted vacuum-tight with a seal 15, 15′ on the measuring chamber housing 3. This seal can be, for example, an elastomer seal and be implemented as an O-ring 15 or as a flat seal 15′ or it can also be implemented as a metal seal. In certain cases, however, it can also be fixedly mounted on the measuring chamber housing 3, for example through sintering, soldering, etc. However, it is especially advantageous if the carrier plate 10 is simply adhered vacuum-tight onto the measuring chamber housing 3. The present novel construction according to the invention enables the use of robust low-outgassing adhesives since the involved components now have similar thermal coefficients which prevents stress micro-fractures from forming.
The carrier plate 10 is advantageously formed in the shape of a disk. Through the mentioned disposition the lead-through and the sensor retainer (measuring filament) are now combined in a single element and simultaneously the electronic measuring circuitry is also integrated.
The measuring filament 1 comprises at both ends support pin-like filament connections 5, 5′. On the carrier plate two inlet ports 14, 14′ are provided which receive the support pins 5, 5′ and which pins are connected with the electronic circuit 11 on the other side of the carrier plate 10. For this purpose the inlet ports 14, 14′ are advantageously contacted-through in a way similar to that known from printed circuit boards. However, this type of through-contacting must also be capable of withstanding higher temperatures and must be vacuum capable and thus tight. This requires a sintering process in the production. The configuration can be structured highly compactly. It is herein advantageous if the measuring filament is disposed approximately parallel to the surface of the carrier plate 10 as is shown in the example of
The electronic measuring circuitry is applied directly on the insulating carrier plate 10. The conductor tracks are in direct contact with the surface of the carrier plate 10 on which the electronic components 13 are also integrated and/or disposed. The disposition of the conductor tracks 12 with the electronic components 13 takes place using techniques known per se such as are employed, for example, for printed circuits (PCB), thin film circuits or also thick film circuits. The thick film circuit technique is herein especially suitable. This is also compatible with the preferred ceramic as the carrier plate 10. It is also of advantage if the surface roughness of the carrier plate is lower than 0.6 μm. In thick film technique the conductor tracks 12 and any insulating layers are applied using screen printing and subsequently burnt-in or sintered. The electronic components are subsequently mounted, for example by soldering or bonding. The circuit can also be implemented in known manner as a hybrid circuit. In such circuits, for example, resistances are implemented as a component of the conductor track 12 and further structural elements 13, such as active structural elements, are mounted on the conductor tracks 12. The structural elements 13 mounted on the conductor tracks 12 are preferably and at least to some extent implemented using surface mounted device (SMD) techniques.
The carrier plate 10 can have a thickness in the range of 0.5 mm to 5.0 mm, preferably in the range of 0.6 mm to 2.0 mm. This is especially advantageous if aluminum oxide ceramic is utilized as the material for the carrier. The diameter of the carrier plate 10 is herein within a range of 10.0 mm to 50.0 mm, preferably in a range of 15 mm to 35 mm. The measuring filament 1 is implemented as a metal coil, preferably of tungsten or nickel, and has a filament length from pin 5 to pin 5′ in the range of 10.0 mm to 40.0 mm, preferably in the range of 12.0 mm to 25 mm.
The entire measuring cell can therewith be built very small with a diameter in the range of only 14 mm to 54 mm, preferably 19 mm to 39 mm, with the height without cable tap being in the range of 15 mm to 40 mm. The connection flange can be implemented, for example, as threading, such as for example with ⅛″ threading.
The electronic measuring circuitry includes a processor (μC) for the digital processing of the measured signals and control of the measuring filament 1 as is shown in the circuit diagram of
The measuring resistor Rm is connected in series with the measuring filament 1 and is disposed between the driver T1 and the measuring filament 1. The signal at the measuring resistor Rm and at the measuring filament 1 is tapped and supplied across one analog/digital converter (ADC1, 2) to the processor (μC) for further processing. Hereby the feedback circuit is formed across which the filament power is controlled and/or regulated according to the programmed specifications. According to the programmed specified algorithms the gas pressure to be measured is determined with the processor and transmitted to the I/O interface for further analysis or further processing to the periphery. In addition, with a temperature sensor Tr disposed in the circuit configuration on the carrier plate 10, the reference temperature at this site is determined and its signal is also supplied to the processor across an analog/digital converter (ADC3) such that the programmed processor can determine the suitable correction measures and include them. The configuration with the direct measurement and regulation via a processor also enables the temperature of the measuring filament 1 as a function of the measured conditions to be now freely selectable and settable.
The above concept can be readily equipped with further additional electronic components should this be required and desired. It is, for example, especially advantageous for the circuit configuration on the carrier plate to be supplemented by a further electronic component, that is to say by a piezoresistive pressure sensor 20 on semiconductor base, as is shown schematically and in cross section in
The piezoresistive semiconductor pressure sensor 20 comprises preferably a silicon membrane 24. In the carrier plate 10 a port is provided as a connection duct 26 which connects the measuring chamber 2 with the piezoresistive pressure sensor 20 such that they communicate. The piezoresistive pressure sensor 20 is consequently oriented on the carrier plate such that its access port 22 is connected as the measuring port directly with the connection duct 26 located in the carrier plate 10 such that they communicate and thereby the connection to the measuring chamber 2 is established in which the measuring filament 1 is also disposed. The signal output of the piezoresistive pressure sensor 20 is connected across a further ADC (ADC4) with the processor for its direct signal analysis as is shown in the circuit diagrams in
A further advantageous feasibility of acquiring the reference temperature comprises measuring the temperature coefficient of the piezoresistive pressure sensor 20 directly and acquiring it, for example, via a resistor R5 connected between terminal d of the bridge and Gnd, as is shown by example in
A further, still more advantageous feasibility for measuring the reference temperature comprises utilizing the temperature coefficient of the internal diode D1 of the semiconductor junction of the piezoresistive pressure sensor 20. The terminal of diode D1 is led out at point a and connected to Gnd across a resistor R6 as is depicted by example in
With the introduced combined gas pressure measuring cell configuration the two measuring principles, a Pirani thermal conduction manometer and a piezoresistive pressure sensor, are according to the present invention optimally combined with one another. The measuring ranges of the two measuring principles overlap and with the introduced electronic signal analysis a large pressure range to be measured for gas pressures can now be covered continuously and with high measuring precision. The Pirani configuration Pi can preferably cover a range from 10−3 mbar to a few 100 mbar and the piezoresistive pressure sensor 20 a range of 1 mbar to 2.0 bar. Consequently, the entire preferably coverable measuring range lies at gas pressures in the range from 10−3 mbar to 2.0 bar at sufficiently high precision. In certain cases it is also feasible to utilize piezoresistive pressure sensors which expand the range further up to approximately three bar. In such a case with a single gas pressure measuring cell configuration a range from vacuum up to overpressure of a few bar can be covered. A further advantage of the introduced gas pressure measuring cell configuration lies in its calibration. Both sensor types must be calibrated and this can be carried out more simply in the present configuration since the temperature behaviour in the present configuration has high synchronization characteristics of the involved components and the configuration is compact. For this reason it is now also feasible to realize a permanent field calibration, for example by acquiring value sets of pressure-temperature which can subsequently be compared automatically.
Number | Date | Country | Kind |
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577/11 | Mar 2011 | CH | national |
Filing Document | Filing Date | Country | Kind | 371c Date |
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PCT/CH2012/000038 | 2/10/2012 | WO | 00 | 9/11/2013 |