The present application is the US national stage of International Patent Application PCT/IB2013/058802 filed on Sep. 24, 2013which, in turn, claims priority to Italian Patent Application MI2012A001732 filed on Oct. 15, 2012.
The present invention relates to an improved getter pump comprising a plurality of getter cartridges.
Getter pumps, used alone or in combination with other types of pumps, are widely used and appreciated, and are described in various documents such as the international patent applications WO 9858173, WO 2010/105944 and WO 2009/118398 in the applicant's name.
Even though the combination of getter pumps with other types of vacuum pumps provides distinct advantages in certain applications, such as surface science systems and analyzers operating under vacuum, the use of stand-alone getter pumps is preferred when there are constraints that do not allow for such combined use, in particular when active gases such as H2, CO, CO2 are the main gas source and pumping of noble gases is not an issue.
A particular type of getter pump using a plurality of disks of getter material mounted on a central support is described in EP 0742370 and EP 0753663 both in the applicant's name, while a pump containing a plurality of such elements is described in U.S. Pat. No. 6,149,392 in the applicant's name, whose teachings and content are herein incorporated by reference.
In U.S. Pat. No. 6,149,392 it is recognized that for some applications is it more important and crucial to have a high gas sorption velocity rather than a high gas sorption capacity, a typical example being the case of particle accelerators where there are a plurality of vacuum pumps installed in different sections of the accelerator to provide an adequate vacuum level throughout the whole length.
The inventors have further investigated this problem and have found an alternate and different configuration capable of further improving the pumping speed. In a first aspect thereof the invention consists in a getter pump comprising a casing, whose shape is a solid of revolution, and a plurality of getter cartridges mounted within said getter pump casing, each cartridge comprising a linear central support and spaced getter elements mounted on said linear central support. A plane containing a linear central support and parallel to the solid of revolution axis is defined a getter cartridge “orientation plane”, a plane orthogonal to the casing axis and intersecting the midpoint of a linear central support is defined a getter cartridge “positioning plane”, the pump being characterized in that the angles formed by the positioning planes with the linear central supports are equal to or less than 30°, preferably equal to or less than 10°.
The expression “solid of revolution” is intended to comprise all those solid figures obtained by revolving a plane area about a given axis that lies in the same plane, also defined as “revolution axis”. In its common and most useful embodiment for the present invention the solid of revolution is a cylinder, while other useful shapes are cones or truncated cones or combinations thereof. Moreover for the purposes of the present invention, taking into account that the solid of revolution is an ideal shape and that the pump case is instead a real object, minor deviations from the ideal geometrical revolution shape are still within its breadth and scope.
In view of the fact that in the most preferred embodiment the solid of revolution is a cylinder, in the following examples particular reference will be made to such shape for the getter pump casing, but this is to be regarded only as a non-limiting embodiment of the wider concept of a solid of revolution as suitable geometry for the getter pump external casing.
The invention will be further illustrated with the help of the following figures, where:
In the figures, the dimensions and dimensional ratios of the elements may not be correct and in some cases, such as for example in
The getter pump according to the present invention envisions the presence of a plurality of getter cartridges, such as the one schematically represented in
As shown in
The features and characteristics of the getter cartridges will not be described in greater detail since this knowledge is in possession of a person skilled in the art, in any case some details and information are present in the already mentioned EP 0742370 and EP 0753663. In the present invention it is necessary for the shaft 11 acting as support of the getter elements to be linear, such as shown in
It should also be noted that the invention is not limited to a specific getter material, but any suitable material capable to sorb gases and to be reactivated by means of a thermal treatment may be employed and falls within the definition of getter materials for the scope and purposes of the present invention. The knowledge and characteristics of such materials are available to a person skilled in the art and may be easily retrieved from various sources, such as, for example, the above mentioned EP 0742370. Particularly advantageous are getter metals or alloys comprising at least 30% of one or more of titanium, zirconium, yttrium.
The inventors, in trying to further improve the speed of a getter pump using a plurality of getter cartridges, have found specific configurations that provide improvements with respect to the ones described in U.S. Pat. No. 6,149,392.
In particular,
The getter pump shown in
Getter cartridges whose positioning planes have a distance smaller than 1,5 cm are considered getter cartridges lying essentially in the same plane, which will be defined as a getter “subassembly plane” and is coincident with the lowest positioning plane (i.e. the one upstream with respect to the flow direction) of the getter cartridges lying in essentially the same plane.
In
With regards to the getter cartridges suitable to be used in the getter pump structure according to the present invention, those have a linear central support whose length is comprised between 4 and 30 cm, holding between 2 and 7 getter disks per cm in the disk-holding portion.
Moreover additional elements external to the getter pump such as a power supply and control elements have not been shown since they are conventional. Their purpose is typically to supply current to the linear central support of the getter cartridges so that the getter disks are reactivated by heating the support. With regards to heating, this may be alternatively provided by external sources that heat the casing of the getter pump, such sources possibly being already present in the system where the getter pump is installed, since the system often envisions the presence of baking systems that in some cases may advantageously be used also to heat up and activate the getter pump.
With regards to the casing, that is preferably cylindrical, there are two preferred embodiments. In the first one the casing is closed at one end by a metallic base, usually made with the same material of the side wall, and at the other end by a standard vacuum flange.
In a second preferred embodiment the casing is defined only by the side wall, in this configuration the getter pump has an open-ended casing, so that gas molecules can travel across the getter pump. This configuration is useful when the pump may be directly integrated, for example co-axially, in systems rather than being an additional element, as for example in the case of wall sections of particle accelerators that may be substituted with getter pumps according to the present invention, with a casing made according to the second preferred embodiment. This getter pump configuration allows distributing large sorption velocity and capacity inside the main section of particle accelerator without interfering with any particle or electron beam moving through it.
Even though the getter pumps according to the present invention are most suitably used as stand-alone pumps, they can also be used in pumping systems coupled with other types of pumps, such as for example turbomolecular pumps, Sputter Ion Pumps (SIP), cryogenic pumps, or other NEG (Non Evaporable Getter) pumps.
A top plan view of a getter pump with getter cartridges that are in a same getter subassembly plane is shown in
It is to be remarked that
An interesting variation of the embodiment shown in
By comparing systems using the same number of cartridges, this will result in a reduced capacity and speed with respect to standard cartridges. But the advantages lies in the fact that there is more flexibility in terms of placing of the getter cartridges, allowing to take into account case or geometries constraints, and therefore allowing to place in the pump a higher number of cartridges, resulting at the end in an overall improvement in the pump technical characteristics.
In a getter pump according to the present invention it is particularly useful to have a plurality of cartridges in a plurality of getter subassembly planes. The number of getter subassembly planes is determined by the length of the getter pump casing, such number being preferably comprised between 40 and 80 per meter, scaling accordingly for casings whose length is less than 1 meter.
Each subassembly plane may have a different number of getter cartridges arranged according to different configurations. In this case it is preferred that the adjacent polygon apexes in different getter subassembly planes are not aligned parallel to the revolution axis, but rather that the lines connecting adjacent polygon apexes lying in different subassembly planes form with the subassembly planes themselves (which are parallel to each other) angles equal to or less than 80°, preferably less than 60°.
The invention will be further illustrated with the help of the following non-limiting examples.
A set of getter cartridges is prepared, each cartridge comprising 39 disks with a 1,3 mm spacing. The getter material used for the disks is a Zr (82 wt %)—V (14,8 wt %)—Fe (3,2 wt %) alloy, marketed by the applicant under the trade name “St 172”. The disks have a 1 mm thickness and a diameter of 25,4 mm. At the terminal parts of the cartridges 24,8 mm are free of getter elements, whereby the overall length of the linear support is 140 mm.
The evaluation of the pumping speed of a pump according to the present invention is made, the pump consisting of a cylindrical casing with a height of 140 mm and a diameter of 160 mm , closed at one end by a base and at the opposite end by a vacuum flange. Six cartridges are arranged into two distinct subassembly planes with a 3 cm distance therebetween, the getter cartridges orientation planes for the cartridges in a same subassembly plane forming an equilateral triangle, while the angle formed by the lines connecting the adjacent polygon apexes lying in different getter subassembly planes is about 23°. The result of the evaluation gives a pumping speed higher than 2500 l/s.
Other getter cartridges from the same set of example 1 are used to evaluate the pumping speed of a getter pump according to the prior art. The closed getter pump casing has the same diameter and height as in example 1, but with the cartridges mounted in such a way that the angles formed by the positioning planes with the linear central supports are 90°, i.e. the linear supports are parallel to the walls of the casing, and the cartridges are disposed around the perimeter of the casing and equally spaced among each other. In this case the result of the evaluation provides a pumping speed lower than 2200 l/s.
Number | Date | Country | Kind |
---|---|---|---|
MI2012A1732 | Oct 2012 | IT | national |
Filing Document | Filing Date | Country | Kind |
---|---|---|---|
PCT/IB2013/058802 | 9/24/2013 | WO | 00 |
Publishing Document | Publishing Date | Country | Kind |
---|---|---|---|
WO2014/060879 | 4/24/2014 | WO | A |
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6309184 | Moraja | Oct 2001 | B1 |
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Number | Date | Country |
---|---|---|
0753663 | Jan 1996 | EP |
0742370 | Nov 1996 | EP |
2013165293 | Aug 2013 | JP |
9402957 | Feb 1994 | WO |
9858173 | Dec 1998 | WO |
9858173 | Dec 1998 | WO |
2009118398 | Oct 2009 | WO |
2010105944 | Sep 2010 | WO |
2014060879 | Apr 2014 | WO |
Entry |
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PCT International Search Report mailed on Feb. 5, 2014 for PCT/IB2013/058802 filed on Sep. 24, 2013 in the name of SAES GETTERS S.P.A. |
International Search Report for PCT/IB2015/052174 filed Mar. 25, 2015 on behalf of SAES GETTERS S.P.A. Mail Date: Jun. 23, 2015. 4 pages. |
Written Opinion for PCT/IB2015/052174 filed Mar. 25, 2015 on behalf of SAES GETTERS S.P.A. Mail Date: Jun. 23, 2015. 5 pages. |
Non-Final Office Action for U.S. Appl. No. 14/786,138, filed Oct. 21, 2015 on behalf of Antonio Bonucci. Mail Date: Apr. 15, 2016. 10 pages. |
Notice of Allowance for U.S. Appl. No. 14/786,138, filed Oct. 21, 2015 on behalf of Antonio Bonucci. Mail Date: Oct. 11, 2016. 8 pages. |
Written Opinion for PCT/IB2013/058802 filed Sep. 24, 2013 on behalf of SAES GETTERS S.P.A. Mail Date: Feb. 5, 2014. 4 pages. |
Number | Date | Country | |
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20140369856 A1 | Dec 2014 | US |