This application claims priority from Japanese Patent Application No. 2020 088009 filed on May 20, 2020, the contents of which are relied upon and incorporated herein by reference in its entirety.
The present disclosure relates to a glass preform production apparatus, a glass preform production method, and a preform profile prediction method.
Patent Document 1 discloses monitoring a deposition surface shape of a glass particulate deposit (finally constituting part of an optical fiber preform) by a vapor-phase axial deposition (VAD) method, controlling a pulling speed to achieve a target shape, controlling at least one of a concentration or a flow rate of a gas containing a glass raw material or the like and a burner position together with controlling the pulling speed, and stopping a deposition operation of glass fine particles when deviating from the target shape.
Patent Document 1: Japanese Patent Application Laid-Open No. 2012-91965
A glass preform production apparatus according to an embodiment of the present disclosure is an apparatus that produces a glass particulate deposit by a VAD method, and includes a gas supply system, a burner, and a profile prediction system in order to achieve the above object. The gas supply system individually supplies a glass raw material gas and a gas for flame generation (fuel gas). While generating glass fine particles from the glass raw material gas in the flame obtained by combustion of the fuel gas supplied from the gas supply system, the burner blows the glass fine particles in the flame onto the glass particulate deposit. The profile prediction system outputs, at any one or more time points during a period from a start of production to an end of production of the glass particulate deposit, a prediction result of a refractive index profile of the transparent glass preform obtained by dehydrating and sintering the glass particulate deposit. Specifically, the profile prediction system includes an imaging device and a calculation unit. The imaging device images a flame blown from the burner to the glass particulate deposit or a particle flow of glass fine particles generated in the flame. The calculation unit performs an image process of extracting image data representing a state of at least a flame or a particle flow from an image obtained by the imaging device. In addition, the calculation unit regressively predicts the refractive index profile of the transparent glass preform serving as the objective variable from the explanatory variable including at least the image data.
As a result of studying the above-described conventional technique, the inventors have found the following problems. That is, in the glass preform production method disclosed in Patent Document 1, the deposition shape of a glass particulate deposit by the VAD method is monitored, but it is not possible to predict the refractive index profile of the transparent glass preform obtained by dehydrating and sintering the glass particulate deposit. In the related art, since a refractive index profile of a transparent glass preform obtained from a glass particulate deposit including a portion to be a core of an optical fiber which is a final product greatly affects optical characteristics of the optical fiber, profile measurement is performed before executing a next step.
The present disclosure has been made to solve the above-described problems, and an object of the present disclosure is to provide a glass preform production apparatus, a glass preform production method, and a preform profile prediction method capable of predicting a refractive index profile of a transparent glass preform including a portion to be a core of an optical fiber as a final product in a production stage of a glass particulate deposit before sintering.
According to various embodiments of the present disclosure, it is possible to predict the profile of the transparent glass preform over the entire length of the transparent glass preform. In addition, such profile prediction in the middle of the production of the glass particulate deposit makes it possible to change the production conditions and effectively suppress the occurrence of characteristic defects due to structural defects of the optical fiber as a final product.
First, contents of embodiments of the present disclosure will be individually listed and described.
(1) A glass preform production apparatus according to an embodiment of the present disclosure is an apparatus that produces a glass particulate deposit (including a portion to be a core of an optical fiber as a final product) by a VAD method, and includes, as an aspect thereof, a gas supply system, a burner, and a profile prediction system. The gas supply system individually supplies a glass raw material gas and a gas for flame generation (fuel gas). While generating the glass fine particles from the glass raw material gas in the flame obtained by combustion of the fuel gas supplied from the gas supply system, the burner blows the glass fine particles generated in the flame onto the glass particulate deposit. The profile prediction system outputs, at any one or more time points during a period from a start of production to an end of production of the glass particulate deposit, a prediction result of a refractive index profile of the transparent glass preform obtained by dehydrating and sintering the glass particulate deposit.
Specifically, the profile prediction system includes an imaging device and a calculation unit. The imaging device images a flame blown from the burner to the glass particulate deposit or a particle flow of glass fine particles generated in the flame. The calculation unit performs an image process of extracting image data representing a state of at least a flame or a particle flow from an image obtained by the imaging device. In addition, the calculation unit regressively predicts the refractive index profile of the transparent glass preform serving as the objective variable from the explanatory variable including the image data. Note that the image data representing the state of the particle flow includes contour information about the flame or the particle flow, luminance information about light arriving from the flame or the particle flow, and the like specified by an image obtained by imaging the flame or the particle flow.
As described above, the prediction of the refractive index profile of the transparent glass preform is performed at any one or more time points during the period from the start of production to the end of production of the glass particulate deposit. Therefore, the profile of the transparent glass preform can be predicted over the entire length of the transparent glass preform. In addition, such profile prediction in the middle of the production of the glass particulate deposit makes it possible to change the production conditions, and to effectively suppress characteristic defects caused by structural defects of the optical fiber as a final product.
More specifically, the glass preform production apparatus or the like of the present disclosure makes it possible to predict a refractive index profile of a main portion of an optical fiber preform finally obtained (a portion including a portion to be a core of an optical fiber), that is, a transparent glass preform obtained by dehydrating and sintering a glass particulate deposit, during the production of the glass particulate deposit. This means that the production conditions of the transparent glass preform can be adjusted before the profile measurement, so that the number of defectives of the transparent glass preform can be reduced. In addition, it is possible to make process engineers less skilled and shorten the feedback time for adjustment of production conditions.
Furthermore, according to the glass preform production apparatus and the like of the present disclosure, since the refractive index profile of the glass preform can be controlled to have a desired profile shape over the entire length of the preform, the characteristics of the obtained transparent glass preform can be stabilized to desired characteristics. In addition, by producing an optical fiber as a final product from an optical fiber preform containing such a transparent glass preform, the optical characteristics of the optical fiber can be stabilized to desired characteristics.
(2) The glass preform production method of the present disclosure is a method for producing a glass particulate deposit by a VAD method, and is realized by the above-described glass preform production apparatus. Specifically, the glass preform production method includes, as an aspect thereof, a gas supply step, a deposition step, and a prediction step. In the gas supply step, the glass raw material gas and the fuel gas are individually supplied to the burner. The deposition step includes generating the glass fine particles from the glass raw material gas in the flame obtained by the combustion of the fuel gas supplied to the burner and blowing the glass fine particles generated in the flame onto the glass particulate deposit. The prediction step includes predicting, at any one or more time points during the period from the start to the end of the deposition step, a refractive index profile of the transparent glass preform obtained by dehydration and sintering of the glass particulate deposit. Specifically, the prediction step includes an imaging step and a calculation step. The imaging step includes imaging a flame blown from the burner to the glass particulate deposit or a particle flow of glass fine particles generated in the flame. The calculation step includes extracting at least image data representing the state of the flame or the particle flow from the image obtained in the imaging step. Further, a refractive index profile of the transparent glass preform serving as an objective variable is regressively predicted from the explanatory variable including the extracted image data. The glass preform production method also achieves the effect same as that of the above-described glass preform production apparatus.
(3) The preform profile prediction method of the present disclosure is a method applicable to the above-described glass preform production apparatus and glass preform production method, and the method includes predicting, at any one or more time points during a period from the start of production to the end of production of a glass particulate deposit, a refractive index profile of a transparent glass preform obtained by dehydration and sintering of the glass particulate deposit produced by a VAD method. Specifically, the preform profile prediction method includes, as an aspect, an imaging step, an image processing step, and a calculation step. The imaging step includes imaging a flame blown from the burner to the glass particulate deposit or a particle flow of glass fine particles generated in the flame. This flame or particle flow imaging (imaging step) includes generating the glass fine particles from the glass raw material gas supplied to the burner in a flame obtained by combustion of the fuel gas supplied to the burner and performing imaging at any time points when the glass fine particles generated in the flame are blown onto the glass particulate deposit. The image processing step includes extracting image data representing the state of the flame or the particle flow from the image obtained in the imaging step. The calculation step includes regressively predicting the refractive index profile of the transparent glass preform serving as the objective variable from the explanatory variable including at least the image data extracted in the image processing step. The preform profile prediction method also achieves the effect same as that of the above-described glass preform production apparatus.
(4) As an aspect of the present disclosure, the explanatory variable preferably includes contour data of at least a flame or a particle flow in the flame. As will be described later as an example, this is because a high correlation can be confirmed between the contour data of the particle flow and the shape of the refractive index profile of the transparent glass preform by the basic analysis (the same applies to the contour data of the flame). Furthermore, as an aspect of the present disclosure, it is preferable that the explanatory variables further include at least any one of luminance distribution data of the flame or the particle flow, data obtained by quantifying an installation position and an installation angle of the burner, flow rate data of the glass raw material gas to be introduced into the burner, flow rate data of the fuel gas, a temperature (sintering temperature) in a heating furnace during the dehydration and sintering, and a gas flow rate to be supplied into the heating furnace during the dehydration and sintering. Since the data can confirm a high correlation with the refractive index profile of the transparent glass preform, it is possible to perform profile prediction with higher accuracy by including the data as explanatory variables.
(5) As an aspect of the present disclosure, the objective variable preferably includes a refractive index profile of the transparent glass preform or one or more types of data characterizing the refractive index profile of the transparent glass preform. Note that this refractive index profile is a distribution of the relative refractive index difference along the radial direction (direction orthogonal to the preform center axis) of the transparent glass preform. In this case, it is possible to visually display the prediction result.
(6) As an aspect of the present disclosure, in the calculation unit or the calculation step, a refractive index profile or one or more types of data characterizing the refractive index profile is set as an objective variable, a learning model is constructed in advance using a regression analysis including at least one of decision tree regression, random forest (RF), gradient boosting, multiple regression, and Lasso regression for each objective variable, and the objective variable is predicted using the constructed learning model (regression prediction). This learning model is a prediction model in which a correlation between an explanatory variable and an objective variable is constructed using known data. As described above, as the regression prediction, a regression analysis including at least one or more of decision tree regression, random forest, gradient boosting, multiple regression, and Lasso regression is preferably executed for each objective variable. The profile can be predicted with high accuracy by applying the regression analysis suitable for prediction for each objective variable.
(7) As an aspect of the present disclosure, the glass preform production apparatus having the above-described structure may further include a filter disposed between the imaging device and a space sandwiched between the glass particulate deposit and the burner. This filter transmits light with a predetermined wavelength from a flame or particle flow. For example, in the case of imaging thermal radiation light from a flame or a particle flow, the load of an image process is reduced by removing light with an unnecessary wavelength.
As described above, each aspect listed in the section of [Description of the embodiment of the present disclosure] is applicable to each of all the remaining aspects or to all combinations of these remaining aspects.
Hereinafter, specific structures of the glass preform production apparatus, the glass preform production method, and the preform profile prediction method of the present disclosure will be described in detail with reference to the accompanying drawings. Note that the present invention is not limited to these exemplifications, is shown by the claims, and is intended to include all modifications within the meaning and scope equivalent to the claims. Note that in the description of the drawings, the same elements are denoted by the same reference numerals, and duplicate explanation is omitted.
The glass preform production apparatus 10 according to the present embodiment includes a reactor 11 for producing the glass particulate deposit 14. The reactor 11 includes an exhaust duct 29, and the core burner 17, the cladding burner 18, and part of a support rod 12 having one end to which a starting glass rod for depositing glass fine particles is attached are located in the reactor 11. As an example, a glass rod comprised of silica glass having a diameter of 25 mm and a length of 400 mm is applied as the starting glass rod.
The other end of the support rod 12 is supported by a lifting and lowering rotation device 15, and the lifting and lowering rotation device 15 rotates the support rod 12 along an arrow S1 in
In the example of
SiCl4+2H2O→SiO2+4HCl
GeCl4+O2→GeO2+2Cl2
Note that the structure of the cladding burner 18 is substantially similar to the structure of the core burner 17 described above, but the type of the raw material of the refractive index adjusting dopant contained in the glass raw material gas supplied from the gas supply system 19 is different. For example, when fluorine (F) is added to the cladding portion as a refractive index adjusting dopant, the glass raw material gas contains CF4 together with SiCl4. However, in a case where the refractive index of the cladding portion is not adjusted, the glass raw material gas may not contain the raw material of the refractive index adjusting dopant.
In the glass preform production apparatus 10, the deposition surface shape of a portion (specifically, a periphery of a portion to be a core of the optical fiber) of the glass particulate deposit 14 is monitored by a measuring camera (CCD camera) 21. A signal processing unit (image processing unit) 22 outputs video data generated based on the electrical signal from the measuring camera 21 to an image analysis unit (deposition shape measurement unit) 23 constituting part of the control unit 16. The image analysis unit 23 divides the video data (moving image) into two-dimensional images (still images), and extracts the deposition surface shape from the obtained two-dimensional images (still images). Then, the image analysis unit 23 performs drive control on the driving unit 20 so that the extracted deposition surface shape is a target shape (outputs a corrected drive control signal to the driving unit 20). Further, the image analysis unit 23 calculates the correction amount of the concentration and the flow rate of the gas containing the glass raw material and the like and the correction amount of the burner position so that the deposition surface shape is the target shape. The control unit 16 controls the gas supply system 19, the core burner stage 24, and the cladding burner stage 25 according to the correction amount obtained by the image analysis unit 23.
The glass preform production apparatus 10 according to the present embodiment further includes a profile prediction system configured to output, at any one or more time points during a period from a start of production to an end of production of the glass particulate deposit 14, a prediction result of a refractive index profile of the transparent glass preform 140 (see
As illustrated in
Furthermore, in the profile prediction system, the calculation unit 105 performs the image process of extracting image data representing a state of at least the flame or the particle flow from a two-dimensional image obtained by the imaging device. As an example, the image process in the calculation unit 105 is performed using image analysis software, and specifically, the contour of the flame or the particle flow is clarified after the two-dimensional image from the signal processing unit 104 is adjusted in luminance. In addition, the calculation unit 105 regressively predicts a refractive index profile of the transparent glass preform 140, serving as an objective variable, from the explanatory variable including data obtained by coordinating the contour of at least the flame or the particle flow. More specifically, contour data of the flame or the particle flow, a burner installation position (burner installation position and burner installation angle along the burner X-axis), a flow rate of a glass raw material gas (including a raw material of a refractive index adjusting dopant), a flow rate of a fuel gas (H2), a flow rate of a combustible assist gas (O2), conditions of dehydration and sintering when the glass particulate deposit 14 is made into transparent glass (temperature, gas flow rate), and the like are set as explanatory variables, and data characterizing a refractive index profile is set as an objective variable. Incidentally, the dehydration and sintering step is a step of transparently vitrifying the glass particulate deposit 14 in a heating furnace, and is a step of heating the glass particulate deposit 14 by a heater disposed outside a core tube while supplying at least one kind of gas selected from, for example, nitrogen, argon, helium, chlorine or the like into the core tube housing the glass particulate deposit 14, thereby dehydrating and sintering (making transparent) the glass particulate deposit 14. The “gas flow rate” as a condition for dehydration and sintering means a flow rate of the gas to be supplied into the core tube in the dehydration and sintering step. After determining the explanatory variable and the objective variable, the calculation unit 105 models in advance the correlation between the contour of the flame or the particle flow and the refractive index profile by using decision tree regression, random forest (RF), gradient boosting, multiple regression, lasso regression, or the like. During the production of the glass particulate deposit 14, the calculation unit 105 predicts the refractive index profile of the transparent glass preform 140 using the learning model (prediction model) constructed in this manner Note that the image data representing the state of the flame or the particle flow includes contour data of the flame or the particle flow or luminance information about thermal radiation light from the particles, which is specified by a two-dimensional image obtained by imaging the particle flow.
In
The right column of the pattern 2 shows a chevron type refractive index profile as a schematic shape of a refractive index profile of the transparent glass preform 140 obtained after dehydration and sintering. In the pattern 2, as shown in the left column, the core burner 17 is disposed such that the burner center axis AX2 of the core burner 17 is shifted downward (a position farther from the starting glass rod 13 than the origin X0) with respect to the origin X0 of the burner X-axis. By disposing the core burner 17 at such a position with respect to the glass particulate deposit 14, it is easy to obtain a chevron type refractive index profile having a refractive index peak at the center of the core coinciding with the center axis AX0 of the transparent glass preform 140 after dehydration and sintering.
The right column of the pattern 3 shows a trapezoid type refractive index profile as a schematic shape of a refractive index profile of the transparent glass preform 140 obtained after dehydration and sintering. In the pattern 3, as shown in the left column, the core burner 17 is disposed such that the burner center axis AX2 of the core burner 17 intersects the origin X0 of the burner X-axis. By disposing the core burner 17 at such a position with respect to the glass particulate deposit 14, it is easy to obtain a trapezoid type refractive index profile having a small refractive index variation in a peripheral region around the center axis AX0 of the transparent glass preform 140 after dehydration and sintering.
The calculation unit 105 constructs a correlation between the explanatory variable and the objective variable by the learning model by utilizing the explanatory variable and the objective variable obtained in the past manufacturing, has a memory storing the constructed learning model, and performs regression prediction using the learning model. In the regression prediction, arbitrarily selected regression analysis (In the example of
In general, the random forest is an analysis method in which the process of randomly selecting learning data and constructing a decision tree is performed a plurality of times, and classification and regression are performed by a majority decision or an average value of estimation results of each decision tree. Specifically, the random forest is referred to as ensemble learning because a plurality of learning models (decision trees) is used.
The gradient boosting is an analysis method in which a decision tree analysis is first performed, and a process of constructing a decision tree for an error between a prediction value and a true value of a constructed decision tree model is repeated a plurality of times. Like the random forest, it is ensemble learning, but random forest creates decision trees in parallel, whereas gradient boosting configures decision trees in series.
The multiple regression analysis is an analysis method for predicting one objective variable with a plurality of explanatory variables (numerical values). For example, when one objective variable is represented by y and n (n is an integer of 1 or more) explanatory variables are represented by xi (i is an integer from 1 to n), the multiple regression analysis is given by the following Formula (1).
y=a1×x1+a2×x2+ . . . +an×xn+b (1)
where ai (i is an integer from 1 to n) is a regression coefficient, and b is an intercept. A learning model is constructed by determining the regression coefficient ai and the intercept b using a plurality of pieces of learning data in which the objective variable y and the explanatory variable xi are known.
The Lasso regression analysis is an analysis model in which “L1 regularization” is added to linear regression as in the above-described multiple regression analysis. In the Lasso regression analysis, since the regression coefficient for data that is less likely to affect prediction is brought close to zero, only substantially important explanatory variables are selected for the regression analysis.
In the present embodiment, the objective variable obtained by the regression prediction is a refractive index profile of the transparent glass preform 140 or data characterizing the refractive index profile. The output unit 106 includes a monitor or the like that reproduces a refractive index profile predicted by regression.
The calculation unit 105 takes in video data (moving image) outputted from the signal processing unit 104, divides the data into n (an integer of 1 or more) two-dimensional still images Gi (i is an integer from 1 to n), and extracts contour data (image data) of a particle flow in flame blown from the core burner 17 to the glass particulate deposit 14 for each two-dimensional still image. Specifically, as illustrated in the upper part of
In the graph illustrated in the lower part of
Furthermore, in the image process in the calculation unit 105 described above, as illustrated in
As in the contour data extraction operation described above, the calculation unit 105 takes in the video data (moving image) outputted from the signal processing unit 104, divides the data into n (an integer of 1 or more) two-dimensional still images Gi (i is an integer of 1 to n), and extracts, for each two-dimensional still image, the luminance distribution of the particle flow generated in the flame blown from the core burner 17 to the glass particulate deposit 14. Specifically, as illustrated in the upper part of
The obtained average luminance ABT (CPx) indicates an average luminance distribution at a total of 70 locations of CP1 to CP 70 on the line segment FL. Further, the luminance distribution data prepared as the explanatory variable is configured by, for example, the average luminance ABT (CPx) at 40 locations arbitrarily selected from the CP1 to the CP 70. Note that the number of luminance measurement points selected from the luminance measurement points on the line segment FL is not limited to 40, and for example, the number of optimal luminance distribution data configurations (the number of luminance measurement points) may be determined by evaluating each luminance distribution configured at 5, 10, 20, and 40 locations.
Four types of data characterizing the refractive index profile will be described with reference to
RMSE: root-mean-square error ((1/n)×Σ(true value−prediction value)2)½
n: number of data
In
As illustrated in
As can be seen from
10 glass preform production apparatus
11 reactor
12 support rod
13 starting glass rod
14 glass particulate deposit
15 lifting and lowering rotation device
16 control unit
17 core burner
18 cladding burner
19 gas supply system
20 driving unit
21 measuring camera
22 signal processing unit
23 image analysis unit
24
a,
25
a angle adjustment mechanism
24, 25 stage
29 exhaust duct
RA imaging area
102 filter
103 CCD camera (imaging device)
104 signal processing unit
105 calculation unit
106 output unit
110 Personal computer (PC).
Number | Date | Country | Kind |
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2020-088009 | May 2020 | JP | national |
Filing Document | Filing Date | Country | Kind |
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PCT/JP2021/018678 | 5/17/2021 | WO |