1. Field of the Invention
The present invention relates to a rotary grinding mill, and to a method of grinding.
2. Description of Related Art
Conventional rotary mills include a cylindrical drum rotated about a generally horizontal axis. The rotating drum is fed with particulate material such as a slurry or powder, the rotation of the drum being at one half to three quarters of the “critical speed” (ie. the minimum speed at which material at the inner surface of the drum travels right around in contact with the mill). This causes a tumbling action as the feed and any grinding media travels part way up the inner wall of the drum then falls away to impact or grind against other particles in the feed. Size reduction of the particles is thus achieved principally by abrasion and impact.
International Patent Application WO 99/11377 discloses a grinding mill construction in which a rotary container is spun significantly above critical speed to form a compressed layer of the particulate material retained against the container inner surface, and shear members such as discs or pins contacting the layer to induce shearing in the layer. This creates stirred, high shear zones in the compressed material adjacent the shear members, providing a very effective grinding mechanism.
Where multiple shearing discs are used, these are spaced apart by a sufficient distance to produce alternate solidified and stirred zones within the grinding chamber.
The mill of WO 99/11377 is effective at small scale, but breakage rates and throughput on scale up have been found to be constrained by limitations on mobilisation of the ground material along the mill where multiple discs are employed.
Australian Patent Application AU-A-30236/00 describes adaptations of the mill of WO 99/11377, incorporating new feed arrangements.
The contents of WO 99/11377 and AU-A-30236/00 are incorporated herein by reference.
The present invention aims to provide an improved grinding mill arrangement.
In one form, the invention provides a grinding mill for particulate material, including a rotary container having an inner surface, a material feed for feeding the particulate material to the container, a first rotary drive rotating the container about a first rotational axis, and a shear inducing member contacting the particulate material in the container so as to induce shearing in said particulate material, the shear inducing member being mounted about a second axis, wherein said first rotational axis and second axis are disposed at an angular displacement relative to each other.
In a further form, the invention provides a method of grinding particulate material, including feeding the particulate material to a container which has an inner surface, rotating the container about a first rotational axis, positioning a shear inducing member within the container mounted about a second axis and so as to contact the particulate material with the shear inducing member to induce shearing in said particulate material, wherein said first rotary axis and second axis are disposed at an angular displacement relative to each other.
A further form of the invention provides a grinding mill for particulate material, including a rotary container having an inner surface, a material feed for feeding the particulate material to the container, a first rotary drive rotating the container about a first rotational axis, and a shear inducing member contacting the particulate material in the container so as to induce shearing in said layer, the shear inducing member being mounted about a second axis, and an angle adjustment mechanism for adjusting a relative angular displacement of the first rotational axis and second axis.
A further form of the invention provides a method of grinding particulate material, including feeding the particulate material to a container which has an inner surface, rotating the container about a first rotational axis, positioning a shear inducing member within the container mounted about a second axis and so as to contact the particulate material with rotating shear inducing member to induce shearing in said particulate material, wherein said first rotary axis and second axis are disposed at an adjustable angular displacement relative to each other.
Optionally, the second axis is a rotational axis of the shear inducing member, and the mill further includes a rotary drive for the shear inducing member.
Optionally also, the mill includes means for adjusting the angular displacement of the first and second axes.
Advantageously, the mill is adapted to rotate the container at above critical speed, and preferably at a speed sufficient to induces causes one or more substantially solidified zones in the particulate material layer.
Further forms of the invention include those set out in the claims.
Further preferred embodiments of the invention will now be described with reference to the accompanying drawings, in which:
With reference to
The first mounting frame supports the grinding container 106 and associated rotary drive means, including a drive motor 108, gearbox or drive pulley arrangement 110 and drive shaft 112 mounted to the frame via bearings 114.
The grinding container 106 is fixed on the end of drive shaft 112 for rotation therewith about a first rotational axis 116. It will be noted that, in this embodiment, the axis is inclined, though other orientations such as horizontal or vertical axes may be employed.
As best shown in
The front and rear halves 106b,106a of the grinding container are removably attached to each other—for example by bolting, clamping or other suitable means—to allow assembly of the container halves after attachment of the shearing member 126 to the end of its drive shaft 136 by bolts 152 or other suitable means.
In the embodiment of
As best seen in
The second mounting frame 105 supports the rotary shear member 126 and its associated rotary drive means, including a drive motor 134 and drive shaft 136 arrangement.
The motor 134 and drive shaft 136 drive rotation of the shear member 126 about a second rotational axis 138, which is disposed at an angle to the rotational axis 116 and intersects with axis 116 within the grinding chamber 120.
The motor 134, drive shaft 136 and shear member 126 are mounted to the second frame 106 via a pivot frame 140 which attaches to the frame 106 at pivot points 142 at either side of the frame to define a pivot axis 144 which passes through the centre of the spherical grinding chamber, coincident with the intersection of the rotational axes 116,138.
Pivoting of the pivot frame 140 is guided by guide pins 146 which track within arcuate guide slots 148, with a clamping mechanism 150 for fixing the angle of the pivot frame. In this way, the angle between the shear member axis 138 and the container axis 116 may be adjusted.
The drive shaft 136 is mounted to the pivot frame 140 via bearings 151.
Further details of one embodiment of the grinding container and shearing member can be seen in
In the embodiment illustrated in
The mechanism for adjusting the angle of the drive shaft 136 and shearing member 126 retains this concentric arrangement between the shearing member and the grinding chamber.
In use, the container drive arrangement drives high speed rotation of the container 106, preferably at above critical speed, and preferably much greater than critical speed, for example at a speed which imparts a force of at least 100 times gravity to material at the inner surface of the container.
Motor 134 and drive shaft 136 drive the shear member 126 to rotate relative to the container 106. The shear member rotation may be in the same direction as, or counter to, the rotation of the container 106, as discussed further below, or in some embodiments the shear member may be fixed against rotation.
The flowable particulate material to be ground—typically in the form of a slurry—is fed continuously to the grinding chamber via a stationary feed tube 158 (
The mill is adapted for autogenous grinding—i.e. where the material is ground without a separate grinding media—though if required for the particular application the mill may be fed an initial charge of an exogenous grinding media which remains in the mill.
The high speed rotation of the container causes the feed material to form a compressed, solidified layer 180 which is retained against and rotates with the inner surface 118 of the container, in a generally similar fashion to that described in WO99/11377 and AU-A-30236/00, and as schematically shown in
The relative rotation of the container 106 and shear member discs 156 causes mobilisation of the compressed charge layer in the vicinity of the discs 156, forming a stirred, high shear zone bounded by the discs 156 and the solidified layer.
In many applications it will be advantageous to have the shear member rotating counter to the rotation of the container, to maximise the grinding effect by the sides of the shear discs or other shear members contacting the material travelling around with the container shell. In other applications—such as for grinding of fine, dry material, it may be found to be advantageous to have the container and shear member rotating in the same direction but at differential speeds, to maximise the pressure in the mill due to the centrifugal action. There may be some applications in which it is desirable to keep the shear member fixed, and rely purely on the container rotation to achieve the differential rotation.
Size reduction of the particles within the shear zone is achieved primarily by shearing and attrition under pressure; assisted by compression fracturing due to the exaggerated ‘gravitational’ force. Inter-particle impact may also play some role, especially for larger size particles greater than about 5-10 μm.
The speed of rotation of the container and the shear member, and the radial position of the discharge opening—which affects the depth of the material bed—may be adjusted to vary the pressure within the material bed. For example, in many applications it will be advantageous to use very high G force, such as 100 G or more, to maximise particle fracture, while there may be applications, such as attritioning of a surface layer of the particles, where a lower G force such as 20 G may be more suitable.
The angular displacement between the rotational axes 116,138 of the container 106 and shear member 126 causes the discs 156 to track along the container surface as the container and discs rotate, so that instead of simply forming a groove in the solidified layer as in WO 99/11377 and AU-A-30236/00, the relative rotation of the container and shear member in the present embodiment additionally causes mobilisation longitudinally along the grinding chamber, assisting passage of the ground material through the mill.
As a result of this longitudinal tracking of the discs along the container surface, the solidified zone is retained at the container inner surface but the charge is mobilised within the body of the mill, achieving a large active volume for grinding.
Adjustment of the angle of the shear member axis relative to the container, by adjusting the angle of pivot frame 140, allows this longitudinal mobilisation, and hence mill residence time and throughput, to be adjusted to suit the particular grinding application.
The grinding container and feed arrangements are similar to those described with reference to the embodiment of
The shear member 164 is ball-shaped, and has its axis 138′ offset to one side of the grinding chamber so that the gap between the shear member and the inner surface of the grinding container is “X” on one side and a smaller distance, “Y”, at the other side.
The rotation of the container delivers the material into the smaller gap Y, with the relative rotation of the shear member and container acting, in effect, as mortar and pestle arrangement, causing shearing of the particulate material between the shear member and the rotating, solidified layer described above.
As in the embodiments of
The ball-shaped shear member may have a smooth surface, as shown, or may have grooves, ridges or other formations to enhance the grinding.
Each blade has a central mounting aperture 172 which may be non-circular, such as square/rectangular (as shown) or keyed, for mounting to a correspondingly shaped portion of the mounting shaft 136.
The blades may configured for mounting on the shaft with the notches aligned or circumferentially offset, providing that the blade configuration is adapted for balanced rotation of the shear member about its rotational axis.
The shear member configuration of
Reference numerals in
The grinding container 206 with its drive mechanism—including motor 208, gearbox or drive pulley (omitted for clarity), bearings 214 and drive shaft 212—are mounted on a first mounting frame 204 fixed to the base 202.
The shear member and its drive mechanism—motor 234, gearbox or drive pulley (omitted for clarity), bearings 251 and drive shaft 236—are mounted to the basis via a pivot frame 240. The pivot frame pivots horizontally about pivot point 242 directly below the centre of the grinding chamber, with alignment holes 266 on the base 202 and pivot frame 240 allowing fixing of the angle to a plurality of predetermined angles.
The general operation of the mill of
The optimal angular displacement between the container rotational axis and the shear member axis may vary depending on the material to be ground, the mill diameter and rotational velocities of the container and shear inducing member. In general, larger diameter mills will require a smaller angular displacement as the greater diameter will result in a greater longitudinal travel of the shear member relative to the container surface for a given angle. For example, an angle of about 5° may be employed for a mill of diameter of 250 mm while an angle of only 2.5° may be required for a larger mill of 2.5 m diameter.
Typical angular displacements may vary between 0.2 to 20°, more typically from 0.5 to 15°, and more preferably from about 1 to 10°.
In addition, while the illustrated embodiments provide an adjustable angle between the axes, it will appreciated that a fixed angle may be used. For example, an adjustable angle mill may be used in test work to determine the optimal angle for a particular application, and then a fixed angle mill constructed to that angle.
In this specification, the word “comprising” is to be understood in its “open” sense, that is, in the sense of “including”, and thus not limited to its “closed” sense, that is the sense of “consisting only of”. A corresponding meaning is to be attributed to the corresponding words “comprise, comprised and comprises where they appear.
While particular embodiments of this invention have been described, it will be evident to those skilled in the art that the present invention may be embodied in other specific forms without departing from the essential characteristics thereof. The present embodiments and examples are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. It will further be understood that any reference herein to known prior art does not, unless the contrary indication appears, constitute an admission that such prior art is commonly known by those skilled in the art to which the invention relates.
Number | Date | Country | Kind |
---|---|---|---|
2007904870 | Sep 2007 | AU | national |
Filing Document | Filing Date | Country | Kind | 371c Date |
---|---|---|---|---|
PCT/AU2008/001307 | 9/3/2008 | WO | 00 | 6/8/2011 |