Herbicidal oxadiazolidines

Abstract
Compounds of Formula (1) and processes for their preparation, their N-oxides and agriculturally suitable salts, are disclosed which are useful for controlling undesired vegetation wherein Q, X1, X2, X3, R1, R2, R6 and R7 are as defined in the disclosure. Also disclosed are novel intermediates of Formula (5), Formula (8) and Formula (20) wherein R27 is —(CR6R7)q—Q; R6, R7, q, Q, X1 and X2 are as defined in the disclosure. Also disclosed are compositions containing the compounds of Formula (1) and a method for controlling undesired vegetation which involves contacting the vegetation or its environment with an effective amount of a compound of Formula (1).
Description




BACKGROUND OF THE INVENTION




This invention relates to certain oxadiazolidines, processes for their preparation, their N-oxides, agriculturally suitable salts and compositions, and methods of their use for controlling undesirable vegetation. This invention also relates to mixtures of herbicides that have a synergistic effect on weeds or have a safening effect on crops while retaining or increasing weed control.




The control of undesired vegetation is extremely important in achieving high crop efficiency. Achievement of selective control of the growth of weeds especially in such useful crops as rice, soybean, sugar beet, corn (maize), potato, wheat, barley, tomato and plantation crops, among others, is very desirable. Unchecked weed growth in such useful crops can cause significant reduction in productivity and thereby result in increased costs to the consumer. The control of undesired vegetation in noncrop areas is also important. Many products are commercially available for these purposes, but the need continues for new compounds which are more effective, less costly, less toxic, environmentally safer or have different modes of action.


Arch. Pharm


. (1974), 307, 7-12 discloses the chemical structures of N,N-substituted 4-aryloxazolidindiones. However, it does not disclose the compounds of the present invention.




SUMMARY OF THE INVENTION




This invention is directed to compounds and processes to prepare compounds of Formula 1 including all geometric and stereoisomers, N-oxides, and agriculturally suitable salts thereof, agricultural compositions containing them and their use for controlling undesirable vegetation:











wherein




Q is H; or C


1


-C


12


alkyl, C


3


-C


10


cycloalkyl, C


6


-C


14


bicycloalkyl, C


3


-C


12


alkenyl, C


3


-C


10


cycloalkenyl, C


6


-C


14


bicycloalkenyl or C


3


-C


12


alkynyl, each optionally substituted with one or more R


21


; or




Q is a 3- to 7-membered fully saturated or 5- to 7-membered partially saturated heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)


n


, then only one X may be present and (b) when two X are present in the ring, they cannot be bonded directly to each other; or




Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R


16


; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom; or




Q is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R


16


, phenoxy and Z; or




Q is











Q is —C(R


14


)(═NOR


15


), —C(O)R


19


, —C(O)OR


19


, —C(O)SR


19


, —C(S)R


19


, —C(S)OR


19


, —C(S)SR


19


, —C(O)NR


23


R


24


, —C(S)NR


23


R


24


, —OR


19


, —NR


19


R


20


, —S(O)


n


R


19


or —S(O)


n


NR


19


R


20


;




each X is —O—, —S(O)


n


—, —N═, —NR


10


— or —Si(R


11


)


2


—;




Y is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered carbocyclic ring optionally substituted with one or more C


1


-C


4


alkyl groups; or




Y is, together, with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered heterocyclic ring which contains one or two X and is optionally substituted with one or more R


12


, provided that when said heterocyclic ring contains two X, then one X is other than O;




Z is phenyl or a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each phenyl and heterocyclic ring system is optionally substituted with one or more R


16


;




R


1


is C


1


-C


6


alkyl, C


1


-C


6


haloalkyl, C


3


-C


6


alkenyl, C


3


-C


6


haloalkenyl, C


3


-C


6


alkynyl, C


3


-C


6


haloalkynyl, C


1


-C


6


alkoxy, C


2


-C


6


alkoxyalkyl or C


2


-C


6


haloalkoxyalkyl; or R


1


is C


3


-C


7


cycloalkyl or C


3


-C


7


cycloalkenyl, each optionally substituted with one or more R


5


; or




R


1


is phenyl optionally substituted with one or more R


13


; or




R


1


is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R


16


;




R


2


is C


1


-C


6


alkyl, C


1


-C


6


haloalkyl, C


3


-C


7


cycloalkyl, C


3


-C


6


alkenyl, C


3


-C


6


haloalkenyl, C


3


-C


6


alkynyl, C


3


-C


6


haloalkynyl, C


1


-C


6


alkoxy, C


2


-C


6


alkoxyalkyl, C


2


-C


6


haloalkoxyalkyl or NR


3


R


4


; or




R


2


is











R


1


and R


2


are taken together as —CH


2


CH


2


—, —CH


2


CH


2


CH


2


—, —CH


2


CH


2


CH


2


CH


2


—, —CH


2


CH


2


CH


2


CH


2


CH


2


— or —CH


2


CH


2


OCH


2


CH


2


—;




R


3


is C


1


-C


6


alkyl, C


1


-C


6


haloalkyl, C


3


-C


6


alkenyl, C


3


-C


6


haloalkenyl, C


3


-C


6


alkynyl, C


3


-C


6


haloalkynyl; or




R


3


is C


3


-C


7


cycloalkyl or C


3


-C


7


cycloalkenyl, each optionally substituted with one or more R


5


; or




R


3


is a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing 1 to 2 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, and each heterocyclic ring is optionally substituted with one or more R


5


; or




R


3


is phenyl optionally substituted with one or more R


26


groups; or




R


1


and R


3


are taken together with the two nitrogen atoms to which they are attached to form a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing an optional third heteroatom selected from the group consisting of oxygen sulfur and nitrogen, and said heterocyclic ring is optionally substituted with one, or more R


9


; or




R


2


and R


13


, together with the two atoms to which they are attached and the atom between them, form a fully saturated 5-, 6- or 7-membered carbocyclic or heterocyclic ring containing one oxygen, one sulfur or one or two nitrogen atoms, said heterocyclic ring is optionally substituted with one or more R


12


, provided that when said heterocyclic ring contains two nitrogen atoms, they are other than bonded directly to each other;




R


4


is H or C


1


-C


4


alkyl; or




R


3


and R


4


are taken together with the nitrogen atom to which they are attached to form a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing an optional second heteroatom selected from the group consisting of oxygen, sulfur and nitrogen, and said heterocyclic ring is optionally substituted with 1-4 R


9


;




each R


5


is independently halogen, C


1


-C


4


alkyl or C


1


-C


4


alkoxy; or when two R


5


are attached to the same carbon, then said two R


5


groups are taken together as (═O);




each R


6


and R


7


are independently H or C


1


-C


4


alkyl;




R


8


is independently C


1


-C


4


alkyl, C


1


-C


4


haloalkyl or C


1


-C


4


alkoxy,




each R


9


is independently C


1


-C


4


alkyl or C


1


-C


4


alkoxy; or when two R


9


are attached to the same carbon, then said two R


9


groups are taken together as (═O);




W is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)


n


, then only one X may be present; (b) when two X are present in the ring, they cannot be bonded directly to each other; and (c) said heterocyclic ring is bonded to the group (CR


17


R


18


)


q


through other than X;




R


10


is H, C


1


-C


4


alkyl, C


1


-C


4


haloalkyl, C


3


-C


4


alkenyl, C


3


-C


4


alkynyl, C


2


-C


4


alkoxycarbonyl or C


2


-C


4


alkylcarbonyl; or R


10


is phenyl optionally substituted with C


1


-C


3


alkyl, halogen, cyano, nitro or C


2


-C


4


alkoxycarbonyl;




each R


11


is C


1


-C


4


alkyl;




each R


12


is independently halogen, C


1


-C


4


alkyl, C


1


-C


4


haloalkyl, C


1


-C


4


alkoxy, C


1


-C


4


haloalkoxy, C


1


-C


4


alkylthio, C


1


-C


4


haloalkylthio, C


1


-C


4


alkylsufinyl, C


1


-C


4


alkylsufonyl or C


2


-C


4


alkoxycarbonyl;




each R


13


is independently halogen, C


1


-C


3


alkyl, C


l


-C


3


haloalkyl, C


1


-C


3


alkoxy, C


1


-C


3


haloalkoxy, C


3


-C


6


alkenyloxy, C


3


-C


6


alkynyloxy, C


1


-C


4


alkylthio, C


1


-C


4


haloaIkylthio, C


1


-C


4


alkylsufinyl, C


1


-C


4


alkylsufonyl, cyano, amino, nitro or C


2


-C


4


alkoxycarbonyl;




R


14


is H, C


1


-C


6


alkyl, C


1


-C


6


haloalkyl or C


2


-C


6


alkoxyalkyl; or




R


14


and R


6


, together with the carbon atoms to which they are bonded, form a 5- or 6-membered saturated carbocyclic ring optionally substituted with one or more C


1


-C


4


alkyl groups;




R


15


is H, C


1


-C


6


alkyl, C


1


-C


6


haloalkyl, C


3


-C


4


alkenyl or C


3


-C


4


alkynyl;




each R


16


is independently halogen, nitro, cyano, C


1


-C


4


alkyl, C


1


-C


4


haloalkyl, C


3


-C


4


alkenyl, C


3


-C


4


alkynyl, OR


22


, NR


23


R


24


or S(O)


n


R


19


;




each R


17


and R


18


are independently H or C


1


-C


4


alkyl;




each R


19


and R


20


are independently C


1


-C


12


alkyl, C


3


-C


8


cycloalkyl, C


3


-C


12


alkenyl, C


3


-C


8


cycloalkenyl or C


3


-C


12


alkynyl, each optionally substituted with one or more R


21


;




each R


21


is halogen, C


4


-C


8


trialkylsilylalkyl, CN, NO


2


, —OR


22


, —NR


23


R


24


, —S(O)


n


R


22


, —S(O)


n


NR


23


R


24


, —C(O)R


22


, —C(S)R


22


, —C(O)OR


22


, —C(S)OR


22


, —C(S)SR


22


, —C(O)NR


23


R


24


, —C(S)NR


23


R


24


, —CHR


25


COR


22


, —CHR


25


P(O)(OR


22


)


2


, —CHR


25


P(S)(OR


22


)


2


, —CHR


25


C(O)NR


23


R


24


, —CHR


25


C(O)NH


2


, —CHR


25


CO


2


R


22


, phenyl optionally substituted with one or more R


26


groups or benzyl optionally substituted with one or more R


26


groups;




each R


22


is C


1


-C


8


alkyl, C


3


-C


8


cycloalkyl, C


3


-C


8


alkenyl, C


3


-C


8


alkynyl, C


1


-C


8


haloalkyl, C


2


-C


8


alkoxyalkyl, C


2


-C


8


alkylthioalkyl, C


2


-C


8


alkylsulfinylalkyl, C


2


-C


8


alkylsulfonylalkyl, C


4


-C


8


alkoxyalkoxyalkyl, C


4


-C


8


cycloalkylalkyl, C


4


-C


8


alkenoxyalkyl, C


4


-C


8


alkynyloxyalkyl, C


6


-C


8


cycloalkoxyalkyl, C


4


-C


8


alkenyloxyalkyl, C


4


-C


8


alkynyloxyalkyl, C


3


-C


8


haloalkoxyalkyl, C


4


-C


8


haloalkenoxyalkyl, C


4


-C


8


haloalkynyloxyalkyl, C


6


-C


8


cycloalkylthioalkyl, C


4


-C


8


alkenylthioalkyl, C


4


-C


8


alkynylthioalkyl, C


1


-C


4


alkyl substituted with phenoxy or benzyloxy, each ring optionally substituted with halogen, C


1


-C


3


alkyl or C


1


-C


3


haloalkyl, C


4


-C


8


trialkylsilylalkyl, C


3


-C


8


cyanoalkyl, C


3


-C


8


halocycloalkyl, C


3


-C


8


haloalkenyl, C


5


-C


8


alkoxyalkenyl, C


5


-C


8


haloalkoxyalkenyl, C


5


-C


8


alkylthioalkenyl, C


3


-C


8


haloalkynyl, C


5


-C


8


alkoxyalkynyl, C


5


-C


8


haloalkoxyalkynyl, C


5


-C


8


alkylthioalkynyl, C


2


-C


8


alkyl carbonyl, C


2


-C


8


alkoxy carbonyl, phenyl optionally substituted with halogen, CN, C


1


-C


2


haloalkyl and C


1


-C


2


haloalkoxy or benzyl optionally substituted with halogen, C


1


-C


3


alkyl and C


1


-C


3


haloalkyl;




each R


23


is H or C


1


-C


4


alkyl;




each R


24


is C


1


-C


4


alkyl or phenyl optionally substituted with one or more R


26


groups;




R


23


and R


24


may be taken together as —(CH


2


)


5


—, —(CH


2


)


4


— or —CH


2


CH


2


OCH


2


CH


2


—, each ring optionally substituted with C


1


-C


3


alkyl, phenyl or benzyl;




each R


25


is H or C


1


-C


4


alkyl;




each R


26


is C


1


-C


3


alkyl, C


1


-C


3


haloalkyl, C


1


-C


3


alkoxy, C


1


-C


3


haloalkoxy, C


1


-C


3


alkylthio, C


2


-C


5


alkylcarbonyl, C


2


-C


5


alkoxycarbonyl, halogen, amino, cyano or nitro;




R


28


is H or C


1


-C


4


alkyl;




X


1


and X


2


are independently O or S;




X


3


is O, S or NR


28


;




m is 0, 1, 2, 3 or 4;




each n is independently 0, 1 or 2;




p is 0 or 1;




each q is independently 0, 1 or 2; and




t is 0, 1 or 2;




provided that when Q is unsubstituted phenyl, X


1


, X


2


and X


3


are O, q is 0 and R


2


is methyl, then R


1


is other than methyl.




In the above recitations, the term “alkyl”used either alone or in compound words such as “alkylthio” or “haloalkyl” includes straight-chain or branched alkyl, such as, methyl, ethyl, n-propyl, i-propyl, or the different butyl, pentyl or hexyl isomers. The term “1-2 alkyl” indicates that one or two of the available positions for that substituent may be alkyl. “Alkenyl” includes straight-chain or branched alkenes such as 1-propenyl, 2-propenyl, and the different butenyl, pentenyl and hexenyl isomers. “Alkenyl” also includes polyenes such as 1,2-propadienyl and 2,4-hexadienyl. “Alkynyl” includes straight-chain or branched alkynes such as 1-propynyl, 2-propynyl and the different butynyl, pentynyl and hexynyl isomers. “Alkynyl” can also include moieties comprised of multiple triple bonds such as 2,5-hexadiynyl. “Alkoxy” includes, for example, methoxy, ethoxy, n-propyloxy, isopropyloxy and the different butoxy, pentoxy and hexyloxy isomers. “Alkoxyalkyl” denotes alkoxy substitution on alkyl. Examples of “alkoxyalkyl” include CH


3


OCH


2


, CH


3


OCH


2


CH


2


, CH


3


CH


2


OCH


2


, CH


3


CH


2


CH


2


CH


2


OCH


2


and CH


3


CH


2


OCH


2


CH


2


. “Alkylthio” includes branched or straight-chain alkylthio moieties such as methylthio, ethylthio, and the different propylthio, butylthio, pentylthio and hexylthio isomers. “Cycloalkyl” includes, for example, cyclopropyl, cyclobutyl, cyclopentyl and cyclohexyl. “Saturated Carbocyclic” ring denotes a ring having a backbone consisting of carbon atoms linked to one another by single bonds; unless otherwise specified, the remaining carbon valences are occupied by hydrogen atoms.




The term “halogen”either alone or in compound words such as “haloalkyl”includes fluorine, chlorine, bromine or iodine. Further, when used in compound words such as “haloalkyl”said alkyl may be partially or fully substituted with halogen atoms which may be the same or different. Examples of“haloalkyl” include F


3


C, ClCH


2


, CF


3


CH


2


and CF


3


CCl


2


. The terms “haloalkenyl”“haloalkynyl”, “haloalkoxy”and the like, are defined analogously to the term “haloalkyl”. Examples of “haloalkenyl” include (Cl)


2


C═CHCH


2


and CF


3


CH


2


CH═CHCH


2


. Examples of “haloalkynyl” include HC≡CCHCl, CF


3


C≡C, CCl


3


C≡C and FCH


2


C≡CCH


2


. Examples of “haloalkoxy” include CF


3


O, CCl


3


CH


2


O, HCF


2


CH


2


CH


2


O and CF


3


CH


2


O.




The total number of carbon atoms in a substituent group is indicated by the “C


i


-C


j


” prefix where i and j are numbers from 1 to 12. For example, C


1


-C


3


alkylsulfonyl designates methylsulfonyl through propylsulfonyl; C


2


alkoxyalkyl designates CH


3


OCH


2


; C


3


alkoxyalkyl designates, for example, CH


3


CH(OCH


3


), CH


3


OCH


2


CH


2


or CH


3


CH


2


OCH


2


; and C


4


alkoxyalkyl designates the various isomers of an alkyl group substituted with an alkoxy group containing a total of four carbon atoms, examples including CH


3


CH


2


CH


2


OCH


2


and CH


3


CH


2


OCH


2


CH


2


. In the above recitations, when a compound of Formula 1 contains a heterocyclic ring, all substituents are attached to this ring through any available carbon or nitrogen by replacement of a hydrogen on said carbon or nitrogen.




When a group contains a substituent which can be hydrogen, for example R


3


, then, when this substituent is taken as hydrogen, it is recognized that this is equivalent to said group being unsubstituted.




Compounds of this invention can exist as one or more stereoisomers. The various stereoisomers include enantiomers, diastereomers, atropisomers and geometric isomers. One skilled in the art ,will appreciate that one stereoisomer may be more active and/or may exhibit beneficial effects when enriched relative to the other stereoisomer(s) or when separated from the other stereoisomer(s). Additionally, the skilled artisan knows how to separate, enrich, and/or to selectively prepare said stereoisomers. Accordingly, the present invention comprises compounds selected from Formula 1, N-oxides and agriculturally suitable salts thereof The compounds of the invention may be present as a mixture of stereoisomers, individual stereoisomers, or as an optically active form.




One skilled in the art will appreciate that not all nitrogen containing heterocycles can form N-oxides since the nitrogen requires an available lone pair for oxidation to the oxide; one skilled in the art will recognize those nitrogen containing heterocycles which can form N-oxides. One skilled in the art will also recognize that tertiary amines can form N-oxides. Synthetic methods for the preparation of N-oxides of heterocycles and tertiary amines are very well known by one skilled in the art including the oxidation of heterocycles and tertiary amines with peroxy acids such as peracetic and m-chloroperbenzoic acid (MCPBA), hydrogen peroxide, alkyl hydroperoxides such as t-butyl hydroperoxide, sodium perborate, and dioxiranes such as dimethydioxirane. These methods for the preparation of N-oxides have been extensively described and reviewed in the literature, see for example: T. L. Gilchrist in


Comprehensive Organic Synthesis


, vol. 7, pp 748-750, S. V. Ley, Ed, Pergamon Press; M. Tisler and B. Stanovnik in


Comprehensive Heterocyclic Chemistry


, vol. 3, pp 18-20, A. J. Boulton and A. McKillop, Eds., Pergamon Press; M. R. Grimmett and B. R. T. Keene in


Advances in Heterocyclic Chemistry


, vol. 43, pp 149-161, A. R. Katritzky, Ed., Academic Press; M. Tisler and B. Stanovnik in


Advances in Heterocyclic Chemistry


, vol. 9, pp 285-291, A. R. Katritzky and A. J. Boulton, Eds., Academic Press; and G. W. H. Cheeseman and E. S. G. Werstiuk in


Advances in Heterocyclic Chemistry


, vol. 22, pp 390-392, A. CR. Katritzky and A. J. Boulton, Eds., Academic Press.




The salts of the compounds of the invention include acid-addition salts with inorganic or organic acids such as hydrobrornic, hydrochloric, nitric, phosphoric, sulfuric, acetic, butyric, fumaric, lactic, maleic, malonic, oxalic, propionic, salicylic, tartaric, 4-toluenesulfonic or valeric acids.




Preferred compounds for reasons of better activity and/or ease of synthesis are:




Preferred 1. Compounds of Formula 1 wherein




Q is H; or C


1


-C


12


alkyl, C


3


-C


8


cycloalkyl, C


3


-C


12


alkenyl, C


3


-C


8


cycloalkenyl or C


3


-C 12 alkynyl, each optionally substituted with one or more R


21


; or




Q is a 3- to 7-membered fully saturated or 5- to 7-membered partially saturated heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)


n


, then only one X may be present and (b) when two X are present in the ring, they cannot be bonded directly to each other; or




Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R


16


; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom; or




Q is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R


16


, phenoxy and Z.




Preferred 2. Compounds of Preferred 1 wherein




Q is C


1


-C


12


alkyl, C


3


-C


8


cycloalkyl, C


3


-C


12


alkenyl, C


3


-C


8


cycloalkenyl or C


3


-C


12


alkynyl, each optionally substituted with one or more R


21


.




Preferred 3. Compounds of Preferred 1 wherein




Q is a 3- to 7-membered fully saturated or 5- to 7-membered partially saturated heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)


n


, then only one X may be present and (b) when two X are present in the ring, they cannot be bonded directly to each other, or




Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R


16


; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom.




Preferred 4. Compounds of Preferred 1 wherein




Q is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R


16


, phenoxy and Z.




Preferred 5. Compounds of Preferred 2 wherein




Q is C


1


-C


6


alkyl optionally substituted with one or more R


21


, C


5


-C


7


cycloalkyl, C


3


-C


7


alkenyl or C


3


-C


6


alkynyl.




Preferred 6. Compounds of Preferred 3 wherein




Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R


16


; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom.




Preferred 7. Compounds of Preferred 4 wherein




Q is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R


16


.




Preferred 8. Compounds of Preferred 2, Preferred 3 or Preferred 4 wherein X


1


, X2 and X


3


are O.




Preferred 9. Compounds of Preferred 7 wherein




Q is phenyl with substituents on the 2-, and 6-position independently selected from the group consisting of R


16


.




Preferred 10. Compounds of Preferred 5 wherein




q is 0 or 1.




Preferred 11. Compounds of Preferred 6 wherein




q is 0 or 1.




Preferred 12. Compounds of Preferred 7 wherein




q is 0 or 1.




Preferred 13. Compounds of Preferred 1 wherein




R


1


is phenyl substituted with one or more R


13


.




Preferred 14. Compounds of Preferred 1 wherein




R


2


is C


2


-C


6


alkyl, C


2


-C


6


haloalkyl or C


2


-C


6


alkoxyalkyl.




Most preferred is the compound of Formula 1 which is selected from the group consisting of:




(a) N-(4-fluorophenyl)-N-(1-methylethyl)-4-(2-methylphenyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide;




(b) 4-(2,6-dimethylphenyl)-N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo1,2,4-oxadiazolidine-2-carboxamiide;




(c) 4-(2,6-dimethylphenyl)N-(1-methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamide;




(d) 4-cyclohexyl-N-(1-methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamide;




(e) 4-cyclohexyl-N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




(f) N,4-bis(1-methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamiide;




(g) N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-4-(cyclopropyl)-1,2,4-oxadiazolidine-2-carboxamide; and




(h) N-(4-fluorophenyl)-N,4-bis(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-carboxamide.




The oxadiazolidines of Formula 1 are useful as herbicides. The present invention also relates to processes for preparing an oxadiazolidine of Formula 1. The present processes for preparing the oxadiazolidines of Formula 1 provided herein are characterized by employing a process sequence selected from process sequences A, B, C, D or E as described below.




PROCESS SEQUENCE A




A process for preparing a compound of Formula 1











wherein Q, R


6


, R


7


, q, X


1


, X


2


, X


3


, R


1


and R


2


are as defined above, comprising:




(a) contacting a compound of Formula 5











 wherein R


27


is —(CR


6


R


7


)


q


—Q, with a compound of Formula 4






Q—(CR


6


R


7


)


q


—X


4


  4






 wherein X


4


is halogen or mesylate, in the presence of a base to provide a compound of Formula3











(b) contacting the compound of Formula 3 with a carbamoyl or thiocarbamoyl chloride of Formula 2











PROCESS SEQUENCE B




A process for preparing a compound of Formula 1











wherein Q, R


6


, R


7


, q, X


1


, X2, X


3


, R


1


and R


2


are as defined above, comprising:




(a) contacting a compound of Formula 5











 wherein R


27


is —(CR


6


R


7


)


q


—Q, with an alcohol of Formula 6






Q—(CR


6


R


7


)


q


—OH  6






 under reaction conditions involving a tertiary phosphine and an azo compound to provide a compound of Formula 3











(b) contacting the compound of Formula 3 with a carbamoyl or thiocarbamoyl chloride of Formula 2











PROCESS SEQUENCE C




A process for preparing a compound of Formula 1











wherein Q, R


6


, R


7


, q, X


1


, X


2


, X


3


, R


1


and R


2


are as defined above, comprising:




(a) contacting a compound of Formula 5











 wherein R


27


is —(CR


6


R


7


)


q


—Q, with a carbamoyl or thiocarbamoyl chloride of Formula 2











 in the presence of a base to provide the compound of Formula 1











 directly or a compound of Formula 7











(b) contacting the compound of Formula 7 with an alcohol of Formula 6






Q—(CR


6


R


7


)


q


—OH  6






 under reaction conditions involving a tertiary phosphine and an azo compound or with a compound of Formula 4






Q—(CR


6


R


7


)


q


—X


4


  4






 in the presence of a base.




PROCESS SEQUENCE D




A process for preparing a compound of Formula 1











wherein Q, R


6


, R


7


, q, X


2


, X


3


, R


1


and R


2


are as defined above, and X


1


is O, comprising:




(a) contacting a compound of Formula 19











 with phosgene or thiophosgene to provide a compound of Formula 20











(b) contacting the compound of Formula 20 with hydroxylamine, following by treatment with a base, and then an acid, to provide a compound of Formula 8











(c) contacting the compound of Formula 8 with a compound of Formula 2











PROCESS SEQUENCE E




A process for preparing a compound of Formula 1











wherein Q, R


6


, R


7


, q, X


1


, X


2


, X


3


, R


1


and R


2


are as defined above, comprising:




(a) contacting a compound of Formula 2











 with hydroxylamine in the presence of a base to provide a compound of Formula 22











(b) contacting the compound of Formula 22 with a compound of Formula 23











 in the presence of a base to provide a compound of Formula 7











(c) contacting the compound of Formula 7 with an alcohol of Formula 6






Q—(CR


6


R


7


)


q


—OH  6






 under reaction conditions involving a tertiary phosphine and an azo compound or with a compound of Formula 4






Q—(CR


6


R


7


)


q


—X


4


  4






in the presence of a base.




PROCESS SEQUENCE F




A process for preparing a compound of Formula 1











wherein Q, R


6


, R


7


, q, X


1


, X


2


, X


3


, R


1


and R


2


are as defined above, comprising contacting a compound of Formula 7











with an orthoformate of Formula 24






(R


27


O)


3


CH  24






wherein R


27


is —(CR


6


R


7


)


q


—Q, in the presence of a base.




PROCESS SEQUENCE G




A process for preparing a compound of Formula 1











wherein Q, R


6


, R


7


, q, X


1


, X


2


, X


3


, R


1


and R


2


are as defined above, comprising:




(a) contacting a compound of Formula 8











 with a compound of Formula 26











 to provide a compound of Formula 25











 or a compound of Formula 27











 in the presence of a catalyst such as hexamethylguanidinium chloride; and




(b) contacting the compound of Formula 25 or Formula 27 with an amine of Formula 13











 in the presence of a base.




The present invention also relates to an intermediate compound of Formula 5











wherein




R


27


is —(CR


6


R


7


)


q


—Q; R


6


, R


7


, q, Q, X


1


and X


2


are as defined above for Formula 1;




provided that when X


1


and X


2


are O and q is 0, then Q is other than unsubstituted benzyl. The present invention also relates to intermediate compounds of Formula 8 and Formula 20











wherein




R


6


, R


7


, q, Q and X


2


are as defined above for Formula 1; and X


1


is O;




provided that when X


2


is O and q is 0, then Q is other than unsubstituted benzyl.




The oxadiazolidines of Formula 1 can be used alone or in combination with other commercial pesticides. The present invention also relates to certain rare combinations that surprisingly give greater-than-expected or synergistic effect, or give a less-than-additive or safening effect on crops while retaining or increasing synergistically weed control. The mixtures of compounds of Formula 1 and certain sulfonylureas have now been discovered to synergistically control weeds. Also, the mixtures of compounds of Formula 1 and safeners such as dichlormid or naphthalic anhydride have now been discovered to exhibit a crop safening effect while retaining or synergistically increasing weed control.




This invention also relates to a herbicidal composition comprising a herbicidally effective amount of a compound of Formula 1 and at least one of a surfactant, a solid diluent or a liquid diluent. The preferred compositions of the present invention are those which comprise the above preferred compounds.




This invention also relates to a method for controlling the growth of undesired vegetation comprising contacting the vegetation or its environment with a herbicidally effective amount of a compound of Formula 1.




DETAILS OF THE INVENTION




Compounds of the Formula 1 can be readily prepared by one skilled in the art by using the reactions and techniques described in Scheme 1 to Scheme 10 below. In cases where a substituent of the starting material is not compatible with the reaction conditions described for any of the reaction schemes, the substituent can be converted to a protected form prior to the described reaction scheme and then deprotected after the reaction using commonly accepted protection/deprotection techniques (see Green, T. W and Wuts, P. G.,


Protecting Groups in Organic Transformations


, 2nd Edition, John Wiley and Sons, New York, 1991). Otherwise, alternative approaches known to one skilled in the art are available. The definitions of Q, X


1


, X


2


, X


3


, R


1


, R


2


, R


6


, R


7


, and q in compounds of Formulae 1-21 below are as defined in the Summary of the Invention.




As shown in Scheme 1, compounds of Formula 1 can be obtained by the reaction of oxadiazolidines of Formula 8 with carbamyl chlorides of Formula 2. The preferred solvent for the carbamoylation reaction is an inert solvent such as tetrahydrofuran, toluene, benzene or dioxane. The presence of a tertiary amine base such as triethylaamine or diisopropylethylarnine is preferable. Use of an acylation catalyst such as 4-dimethylaminopyridine or 4-pyrrolidinopyridine in a catalytic or stoichiometric amount is preferred. Other bases such as alkali hydroxide, carbonates or hydrides may also be employed. The reaction can be carried out at temperatures between 20 to 150° C.











Oxadiazolidines of Formula 8 can be prepared by methods known in the literature. Zinner reported the preparation of a wide variety of oxadiazolidines. See, for example:


Arch. Pharm


. (1965), 298, 580-587


; Arch. Pharm


. (1971), 303, 139-144, German patent application, DE 2010396 (1971). As shown in Scheme 2, a hydroxyurea or hydroxythiourea of Formula 9 is reacted with an activated carbonyl or thiocarbonyl compound of Formula 10 in the presence of a base to give compounds of Formula 8. Examples of suitable activated carbonyl compounds are ethyl chloroformate, phenyl chloroformate, carbonyl diimidazole, phosgene, diphosgene or triphosgene. Examples of suitable activated thiocarbonyl compounds are carbon disulfide, thiophosgene and thiocarbonyldiimidazole. Suitable bases include alkali carbonates, tertiary amines such as triethylamine and alkali hydroxides. The reaction can be carried out in a variety of solvents including tetrahydrofuran, toluene, dichloromethane, chloroform, acetonitrile or dioxane. The reaction may also be carried out in two-phase mixtures of water and an organic solvent such as dichloromethane, ethyl acetate or toluene. Depending on the reactivity of the carbonyl or thiocarbonyl compound, the reaction may be carried out at temperatures from 0 to 150° C.











As shown in Scheme 3, compounds of Formula 8a wherein X


1


and X


2


are O can be made via the method of Zinner,


Arch. Pharm


. (1981), 314, 294-302. The reaction of isocyanates of Formula 11 with hydroxyurethanes of Formula 12 gives compounds of Formula 8a. The cyclization can be carried out in a variety of solvents such as acetone, dichloromethane, tetrahydrofuran, dioxane, ethyl acetate, and other solvents inert to isocyanates. The presence of a base such as triethylamine or sodium hydroxide is also useful. The reaction may be carried out at temperatures from 20 to 150° C.











Carbamyl chlorides of Formula 2a (which are compounds of Formula 2 wherein X


3


is O) are well known in the literature and can be made by the reaction of amines of Formula 13 with phosgene or a phosgene equivalent such as di- or triphosgene as shown in Scheme 4. The presence of a base is useful and the use of hindered tertiary amines such as diisopropylethyl amine is preferred. The reaction can be carried out in a variety of solvents such as toluene or benzene that are inert to phosgene and its equivalents. The reaction can be carried out at temperatures from 0 to 120° C.











As shown in Scheme 5, hydroxyureas and thioureas of Formula 9 can be prepared from the reaction of hydroxylamine with isocyanates or isothiocyanates of Formula 11. The reaction is carried out in a two-phase reaction medium consisting of water and an organic solvent such as toluene, benzene, dichloroethane, dichloromethane, ethyl acetate or chlorobutane. The hydroxylamine employed can be a commercially available aqueous solution or can be prepared in situ from the reaction of an acid addition salt of hydroxylamine with an alkali hydroxide or carbonate. The reaction is generally carried out at temperatures between 0 and 40° C.











Isocyanates of Formula 11a are commercially available or can be prepared from amines of Formula 14 as shown in Scheme 6. The reaction of phosgene or its equivalents (such as di- and triphosgene) with amines or amine hydrochlorides of Formula 14 gives the isocyanates of Formula 11a. This reaction is well known in the literature and can be carried out in a variety of solvents such as toluene, benzene, ethyl acetate or dichloroethane which are inert to phosgene. Depending upon the reactivity of the amine of Formula 14, the reaction may be carried out at temperatures from 0 to 200° C.











As shown in Scheme 7, isocyanates of Formula 11a can also be formed from activated acids of Formula 15. Acid halides, anhydrides, imidazolides and the like can be reacted with various azides to provide, after a Curtius rearrangement, the isocyanates of Formula 11a. The azide used may be an alkali azide, trialkylsilyl azide or trialkylstannyl azide. The reaction may be carried out in solvents such as toluene, tetrahydrofuran, ethyl acetate, dioxane, benzene, or methyl tert-butyl ether. When an alkali azide is employed, biphasic aqueous solvents or miscible aqueous containing mixtures are preferred in the formation of the acyl azide intermediate. For further examples of Curtius rearrangements, see: March,


J. Advanced Organic Chemistry


, 3rd edition; John Wiley & Sons, 1985; pp 984-985 and 380. See also Kim, World Patent Application 98/51683 (1998) and Larock,


Comprehensive Organic Transformations


, VCH, 1989, pp 931-932.











As shown in Scheme 8, compounds of Formula 9 can also be made by the reaction of compounds of Formula 16 with hydroxylamine. The reaction may be carried out in a number of different solvents including tetrahydrofuran, dioxane, acetonitrile, dimethylformamide and dimethylsulfoxide. Temperatures from 0 to 160° C. may be employed in this transformation. Many compounds of Formula 16 are known, and can be made by the reaction of commercially available chlorofornates and chlorothioformates with compounds of Formula 14.











As shown in Scheme 9, compounds of Formula 9 can also be made by the reaction of activated hydroxylamines of Formula 17 with amines of Formula 14. The reaction may be carried out in a number of different solvents including tetrahydrofuran, dioxane, acetonitrile, dimethylformamide and dimethylsulfoxide. In some cases lower alcohols or even mixtures of water and alcohols may also be employed. Temperatures from 0 to 160° C. may be employed in this transformation. Compounds of Formula 17 are known in the literature and can be made from hydroxylamine and activated esters or thioesters (See Oesper and Broker,


J. Am. Chem. Soc


., 1925, 47, 2607; Defoin et. al.,


Helv. Chim. Acta


., 1992, 75, 109-123; and Stewart and Brooks,


J. Org. Chem


., 1992, 57, 5020-5023).











Compounds of Formula 2b (which are compounds of Formula 2 wherein X


3


is NR


23


) can be made by the chlorination of ureas of Formula 18 as shown in Scheme 10. The chlorination may be carried out with a wide variety of reagents such as phosphorus oxychloride, thionyl chloride, phosphorous pentachloride, or triphenylphosphine reagents with carbon tetrachloride or chlorine. A variety of solvents may be used including halogenated solvents such as dichloromethane, dichloroethane, or trichloroethane. A preferred solvent of the transformation is dimethylformamide. The reaction may be carried out from 0 to 150° C. Some known chloroamidine compounds and their synthesis may be found in Reid,


Chem. Ber


., 1975, 108, 2290-2299; Kuehle et al.;


Angew. Chem


.; 1969; 81; 18; and Shevchenko, V. I. et al.;


J. Gen. Chem. USSR


(Engl.Transl.); 1976;46;535-539.











Many isothiocyanates of Formula 11a are commercially available. Amines of Formula 13 are commercially available or can be prepared by methods disclosed in the literature. See the following references and references cited therein for synthesis of these materials: Kim, World Patent Application 98/51683 (1998); Dhar, World Patent Application 98/35961 (1998); Rorer, World Patent Application 98/25912 (1998); and Morita et. al., World Patent Application WO 98/11079 (1998).




Amines of Formula 14 are commercially available or can be synthesized by methods known in the art. See the following references and references cited therein for synthesis of these materials: Kim, World Patent Application 98/51683 (1998); Dhar, World Patent Application 98/35961(1998); Rorer, World Patent Application 98/25912 (1998), Goto et. al., European Patent Application EP 695748 (1996); Goto et. al., European Patent Application EP 771,797 (1997); and Goto et. al. U.S. Pat. No. 5,589,439 (1996).




Activated carboxylic acids of Formula 10 are commercially available or can be prepared by methods disclosed in the literature. See the following references and references cited therein for the synthesis of these materials: Kim, World Patent Application 98/51683 (1998); Dhar, World Patent Application 98/35961(1998); Rorer World Patent Application 98/25912 (1998); and Goto et. al., European Patent Application EP 695748.(1996). See also Larock,


Comprehensive Organic Transformations


, VCH, 1989, p 821 for a list of comprehensive references for the synthesis and chemistry of carboxylic acids and activated derivatives.




This invention is further directed to processes for the preparation of compounds of Formula 1 using process sequences described below.




PROCESS SEQUENCE A
















Step 1 forms compounds of Formula 3 by contacting compounds of Formula 5 with compounds of Formula 4 in the presence of a suitable base either neat or in a suitable solvent.




Compounds of Formula 5 may be prepared, for example, by methods described in


Synthesis


, 1991, 265.




For Step 1, the reaction temperature is generally from −10 to 250° C., preferably from 0 to 100° C. The reaction times are generally from 0.25 to 48 h, preferably from 0.25 to 24 h. Generally, the pressure is in the range of 1.013×10


2


to 2.026×10


2


KPa, preferably ambient pressure. Suitable solvents include typical organic solvents in which the reactants can be dissolved and the process of Step 1 can proceed without interference. Examples of such reactants include aromatics such as benzene, toluene, xylene, chlorobenzene and dichlorobenzene, ethers such as dioxane and tetrahydrofuran, nitriles such as acetonitrile and propionitrile, ethyl acetate, dichloromethane, dichloroethane, and polar aprotic solvents such as dimethylformarnide and dimethylsulfoxide.




Suitable bases include organic trialkylamines such as trimethylamine, triethylamine, diisopropylethylamnine, tributylamine and the like, dimethylaniline, N,N-dimethylaminopyridine, N-methylmorpholine, 1,8-diazabicyclo[5.4.0]undec-7-ene, 1,4-diazabicyclo[2.2.2]octane and 1,5-diazabicyclo[4.3.0]non-5-ene. 1,8-Diazabicyclo[5.4.0]undec-7-ene is a particularly useful organic base for this reaction. Inorganic bases include, but are not limited to, potassium carbonate, sodium carbonate, potassium hydride, sodium hydride, lithium carbonate and cesium carbonate.




A phase transfer catalyst can accelerate the reaction in the presence of inorganic bases. Phase transfer catalysts include tetraalkylammonium halides, crown ethers, phosphonium salts, silicon analogs of crown ethers and acyclic analogs of crown ethers. Particularly useful as a base is the combination of potassium carbonate and a phase transfer catalyst.




Generally at least an equimolar amount of the Formula 4 compound is used in respect to the Formula 5 compound, and preferably at least a small molar excess of the Formula 4 compound is used. More particularly, the molar ratio of the Formula 4 compound to the Formula 5 compound is usually in the range of 1.05:1 to 10:1. In most cases, the molar ratio of the Formula 5 compound to the Formula 4 compound is preferably in the range of 1.1:1 to 1.5:1. Generally at least an equivalent of base is used in respect to the Formula 5 compound, and preferably at least a small equivalent excess of the base is used. More particularly, the ratio of the number of equivalents of base to number of moles of the Formula 5 compound is usually in the range of 1.05:1 to 10:1. In most cases, the ratio of the number of equivalents of base to number of moles of the Formula 5 compound is preferably in the range of 1.1:1 to 1.5:1. The equivalent amount of base may be similar to the molar amount of the Formula 4 compound, but this is not necessary.




The compound of Formula 4 is preferably added to the reaction mixture containing the compound of Formula 5 and a base either neat or in a solvent. The reaction temperature is maintained during and after the addition and until the reaction reaches completion.




Isolation of product of Step 1 can be accomplished by standard workup procedures or the resultant mixture can be used directly in Step 2.











Step 2 forms compounds of Formula 1 from the reaction of compounds of Formula 3 with compounds of Formula 2 in the presence of a suitable base in a suitable solvent.




For Step 2, the general and preferred reaction conditions are the same as the ones described above for Step 1.




Alternatively, the processes of Step 1 and 2 can be combined without isolating product of Step 1 and preferably, the reaction conditions (e.g. temperature, mole ratio, reaction time etc) are balanced to achieve a high yield of compound of Formula 1.




The compound of Formula 1 can be isolated by standard procedures.




PROCESS SEQUENCE B
















Step 1 forms the compounds of Formula 3 from the reaction of compounds of Formula 5 with compounds of Formula 6 under Mitsunobu reaction conditions involving a tertiary phosphine and an azo compound. One skilled in the art can find a variety of the tertiary phosphine and azo compounds as well as solvents useful for this transformation in


Synthesis


, 1981, 1 and


Org. Reactions


, 1992, 42, 335.




For the process of Step 1, the reaction temperature is generally from about −40 to 250° C., preferably from −20 to 80° C. The reaction times are generally from about 0.20 to 24 h, preferably from 0.5 to 12 h. Generally, the pressure is from 1.013×10


2


to 5.065×10


2


KPa; preferably ambient pressure.




Generally at least an equimolar amount of the Formula 5 compound is used in respect to the Formula 6 compound, and preferably at least a small molar excess of the Formula 6 compound is used. More particularly, the molar ratio of the Formula 6 compound to the Formula 5 compound is usually in the range of 1.05:1 to 10:1. In most cases, the molar ratio of the Formula 6 compound to the Formula 5 compound is preferably in the range of 1.1:1 to 1.5:1.




Isolation of product of Step 1 can be accomplished by standard workup procedures.




Step 2




Compounds of Formula 1 are then obtained by the reaction of the compounds of Formula 3 prepared in Step 1 and compounds of Formula 2 under the same reaction conditions as already described in Step 2 for Sequence A.




PROCESS SEQUENCE C
















Step 1a forms the compounds of Formula 1 by contacting compounds of Formula 5 with compounds of Formula 2 in the presence of a suitable base either neat or in a suitable solvent.




For the process of Step 1a, the general and preferred reaction conditions are the same as the ones described above for Step 1 in Process Sequence A.




A solution of compound of Formula 2 can be added to a solution/suspension of compound of Formula 5 and a base in a solvent. Reaction temperature is maintained during and after the addition and until the reaction reaches completion. Isolation of product of Step 1a can be accomplished by standard workup procedures.











Step 1b forms the compounds of Formula 7 from the reaction of compounds of Formula 5 and compounds of Formula 2 in the presence of a base either neat or in a suitable solvent.




For the process of Step 1b, the general and preferred reaction conditions are the same as the ones described above for Step 1 in Process Sequence A.




The product of Step 1b can be isolated by standard workup procedures.











Step 2a forms the compounds of Formula 1 from the reaction of compounds of Formula 7 and compounds of Formula 6 under Mitsunobu reaction conditions involving a tertiary phosphine and an azo compound. One skilled in the art can find a variety of the tertiary phosphine and azo compounds as well as solvents useful for this transformation in


Synthesis


, 1981, 1 and


Org. Reactions


, 1992, 42, 335.




For the process of Step 2a, the reaction temperature is generally from about −40 to 250° C., preferably from −20 to 80° C. The reaction times are generally from about 0.20 to 24 h, preferably from 0.5 to 12 h. Generally, the pressure is from 1.013×10


2


to 5.065×10


2


KPa; preferably ambient pressure.




Generally at least an equimolar amount of the Formula 7 compound is used in respect to the Formula 6 compound, and preferably at least a small molar excess of the Formula 6 compound is used. More particularly, the molar ratio of the Formula 6 compound to the Formula 7 compound is usually in the range of 1.05:1 to 10:1. In most cases, the molar ratio of the Formula 7 compound to the Formula 6 compound is preferably in the range of 1.1:1 to 1.5:1.




Isolation of product of Step 2a can be accomplished by standard workup procedures.











Step 2b forms compounds of Formula 1 by contacting compounds of Formula 7 with compounds of Formula 4 in the presence of a suitable base either neat or in a suitable solvent.




For the process of Step 2b, the general and preferred reaction conditions are similar to the ones described above for Step 1 in Process Sequence A.




Isolation of product of Step 2b can be accomplished by standard workup procedures.




PROCESS SEQUENCE D




Compounds of the Formula 8 can be readily prepared by one skilled in the art by using the reactions and techniques described in Steps 1 and 2. In cases where a substituent of the starting material is not compatible with the reaction conditions described for any of the reaction schemes, the substituent can be converted to a protected form prior to the described reaction scheme and then deprotected after the reaction using commonly accepted protection/deprotection techniques (see Green, T. W. and Wuts, P. G.,


Protecting Groups in Organic Transformations


, 2nd Edition, John Wiley and Sons, New York, 1991). Otherwise, alternative approaches known to one skilled in the art are available.











Step 1 forms compounds of Formula 20 from the reaction of compounds of Formula 19 with phosgene or thiophosgene in the presence of a base. For general reaction conditions for this transformation, see: U.S. Pat. No. 5,602,251. Compounds of Formula 19 are well known in the literature. See: for example,


J. Chem. Soc. Perkin I


(1997), 1041.











Step 2 forms compounds of Formula 8 in the form of a salt by treatment of compounds of Formula 20 with hydroxylamine and a base. The salt is then converted to compound of Formula 8 by treatment with an acid.




The reaction is conducted in a suitable organic solvent such as, but not limited to, tetrahydrofuran, dioxane or toluene at a temperature between −20 and 100° C. with 10-50° C. being the preferred temperature. Hydroxylamine may be generated from one of its salts by use of a suitable base such as, but not limited to, potassium carbonate, potassium hydroxide or sodium hydroxide. Alternatively, hydroxylamine in water may be used. Judicious use of an appropriate co-solvent such as water or a phase transfer catalyst may be effective in facilitating the reaction. Further amounts of the base (vide supra) can be added to scavenge the HCl formed in the reaction. Alternatively, an excess amount of hydroxylaniine can be used to achieve the same purpose.




The intermediate compound of Formula 21 is not usually isolated, but converted directly to compounds of Formula 8 by addition of further quantities of base. It is apparent to one skilled in the art that salts of compounds of Formula 8 generated from this reaction may be used directly in the preparation of compounds of Formula 1 as described in Scheme 1. To facilitate the transformation, it may be desirable to adjust the solvent composition by removal of co-solvents such as water prior to the reaction. Alternatively, compounds of Formula 8 may be isolated from their salts by addition of an appropriate mineral acid such as, but not limited to, HCl before being subjected to the reaction conditions as described in Scheme 1 to produce compounds of Formula 1.




PROCESS SEQUENCE E




Compounds of the Formula 7 can be readily prepared by one skilled in the art by using the reactions and techniques described in Steps 1 and 2. Since hydroxylamine is unstable upon heating, this sequence allows a safe and efficient route to the compounds of the Formula 7 under mild conditions.











Step 1 forms the compounds of Formula 22 by contacting a compound of Formula 2 with hydroxylamine in the presence of a suitable base in a suitable solvent. Hydroxylamine may be generated from one of its salts or hydroxylamine in water may be used.




For Step 1, the reaction temperature is generally from −10 to 150° C., preferably from 0 to 100° C. The reaction times are generally from 0.10 to 24 h, preferably from 0.10 to 2 h. Generally, the pressure is in the range of 1.013×10


2


to 2.026×10


2


KPa; preferably ambient pressure. Suitable solvents include typical organic solvents in which the reactants can be dissolved and the process of Step 1 can proceed without interference. Examples of such solvents include aromatics such as benzene, toluene, xylene, chlorobenzene and dichlorobenzene, ethers such as dioxane and tetrahydrofuran, nitriles such as acetonitrile and propionitrile, ethyl acetate, dichloromethane, dichloroethane, and polar aprotic solvents such as dimethylformamide and dimethylsulfoxide. Judicious use of an appropriate co-solvent such as water or a phase transfer catalyst may be effective in facilitating the reaction.




Suitable bases include organic trialkylamines such as trimethylamine, triethylamine, diisopropylethylamine, tributylamine and the like, dimethylaniline, N,N-dimethylaminopyridine, N-methylmorpholine, 1,8-diazabicyclo[5.4.0]undec-7-ene, 1,4 diazabicyclo[2.2.2]octane and 1,5-diazabicyclo[4.3.0]non-5-ene. Trialkylamines is a particularly useful organic base for this reaction. When an excess quantity of hydroxylamine is employed, the excess hydroxylamine can also serve as a base. Inorganic bases include, but are not limited to, potassium hydroxide, sodium hydroxide, potassium carbonate, sodium carbonate, lithium carbonate and cesium carbonate.




Generally at least an equimolar amount of the Formula 2 compound is used in respect to hydroxylamine, and preferably at least a small molar excess of hydroxylamine is used. More particularly, the molar ratio of the Formula 2 compound to hydroxylamine is usually in the range of 1:1.05 to 1:10. In most cases, the molar ratio of the Formula 2 compound to hydroxylamine is preferably in the range of 1:1.1 to 1:1.5. Generally at least an equivalent of base is used in respect to the Formula 2 compound, and preferably at least a small equivalent excess of the base is used. More particularly, the ratio of the number of equivalents of base to number of moles of the Formula 2 compound is usually in the range of 1.05:1 to 10:1. In most cases, the ratio of the number of equivalents of base to number of moles of the Formula 2 compound is preferably in the range of 1.1:1 to 1.5:1. The equivalent amount of base may be similar to the molar amount of the Formula 2 compound, but this is not necessary.




Isolation of product of Step 1 can be accomplished by standard workup procedures. In the scenario that the reaction is carried our in an aqueous solution, a filtration can be employed to collect compounds of Formula 22.











Compounds of Formula 7 are synthesized by contacting compounds of Formula 22 with chlorocarbonyl isocyanate (X


1


and X


2


are O) or chlorocarbonyl isothiocyanate (X


1


is O and X


2


is S) or chlorothiocarbonyl isocyanate (X


1


is S and X


2


is O) or chlorothiocarbonyl isothiocyanate (X


1


and X


2


are S) in the presence of a base to scavange the HCl byproduct. Similar examples of such reactions using N-alkyl-N-hydroxylamine and chlorocarbonyl isocyanate have been reported in


Syn


., 1982, 781-2 and in WO 9741097 but there is no example of compound like 22 and chlorocarbonyl isocyanate in the literature.




Compounds of Formula 23 are either commercially available or may be prepared by one skilled in the art using methods known in the art (or slight modification of these methods); for example, see:


Chem. Ber


. 1981, 114, 1746-51


, Chem. Ber


. 1973, 106, 1487-95, and


Chem. Ber


. 1966, 99,3572-81.




For Step 2, the reaction temperature is generally from −10 to 150° C., preferably from 0 to 100° C. The reaction times are generally from 0.10 to 24 h, preferably from 0.10 to 2 h. Generally, the pressure is in the range of 1.013×10


2


to 2.026×10


2


KPa; preferably ambient pressure. Suitable solvents include typical organic solvents in which the reactants can be dissolved and the process of Step 1 can proceed without interference. Examples of such reactants include aromatics such as benzene, toluene, xylene, chlorobenzene and dichlorobenzene, ethers such as dioxane and tetrahydrofuran, nitriles such as acetonitrile and propionitrile, ethyl acetate, dichloromethane, dichloroethane, and polar aprotic solvents such as dimethylformamide and dimethylsulfoxide.




Suitable bases for Step 2 are similar to the ones described above for Step 1.




Generally at least an equimolar amount of the Formula 22 compound is used in respect to the Formula 23 compound, and preferably at least a small molar excess of the Formula 23 compound is used. More particularly, the molar ratio of the Formula 22 compound to the Formula 23 compound is usually in the range of 1:1.05 to 1:10. In most cases, the molar ratio of the Formula 22 compound to the Formula 23 compound is preferably in the range of 1:1.1 to 1:1.5. Generally at least an equivalent of base is used in respect to the Formula 22 compound, and preferably at least a small equivalent excess of the base is used. More particularly, the ratio of the number of equivalents of base to number of moles of the Formula 22 compound is usually in the range of 1.05:1 to 10:1. In most cases, the ratio of the number of equivalents of base to number of moles of the Formula 22 compound is preferably in the range of 1.1:1 to 1.5:1. The equivalent amount of base may be similar to the molar amount of the Formula 22 compound, but this is not necessary.




Isolation of product of Step 2 can be accomplished by standard workup procedures.




Compounds 7 can be readily converted into alkali salts when treated with potassium carbonate or sodium carbonate in water. The salts may be useful in alkylation reactions.




Compounds of Formula 1 are then obtained by the reaction of compounds of Formula 7 under the same reaction conditions as already described in Step 2a/2b in Sequence C.




PROCESS SEQUENCE F




Compounds of the Formula 1 can be readily prepared by one skilled in the art by using the reactions and techniques described in the scheme below.











The compounds of Formula 1 are formed by contacting a compound of Formula 7 with an orthoformate of Formula 24 either neat or in the presence of a suitable solvent.




The reaction temperature is generally from −10 to 150° C., preferably from 0 to 100° C. The reaction times are generally from 0.10 to 24 h, preferably from 0.10 to 2 h. Generally, the pressure is in the range of 1.013×10


2


to 2.026×10


2


KPa; preferably ambient pressure. Suitable solvents include typical organic solvents in which the reactants can be dissolved and the process can proceed without interference. Examples of such reactants include aromatics such as benzene, toluene, xylene, chlorobenzene and dichlorobenzene, ethers such as dioxane and tetrahydrofuran, nitriles such as acetonitrile and propionitrile, ethyl acetate, dichloromethane, dichloroethane, and polar aprotic solvents such as dimethylformamide and dimethylsulfoxide.




Generally at least an equimolar amount of the Formula 24 compound is used in respect to the Formula 7 compound, and preferably at least a small molar excess of Formula 24 compound is used. More particularly, the molar ratio of the Formula 7 compound to the Formula 24 compound is usually in the range of 1:1.05 to 1:10. In most cases, the molar ratio of the Formula 7 compound to the Formula 24 compound is preferably in the range of 1:1.1 to 1:1.5.




PROCESS SEQUENCE G




Compounds of the Formula 1 can be readily prepared by one skilled in the art by using the reactions and techniques described in Steps 1 and 2.











Step 1 forms the compounds of Formula 25 by contacting a compound of Formula 8 with a compound of Formula 26 either neat or in a suitable solvent.




For Step 1, the reaction temperature is generally from −10 to 150° C., preferably from 0 to 100° C. The reaction times are generally from 0.10 to 24 h, preferably from 0.10 to 2 h. Generally, the pressure is in the range of 1.013×10


2


to 2.026×10


2


KPa; preferably ambient pressure. Suitable solvents include typical organic solvents in which the reactants can be dissolved and the process of Step 1 can proceed without interference. Examples of such reactants include aromatics such as benzene, toluene, xylene, chlorobenzene and dichlorobenzene, ethers such as dioxane and tetraydrofuran, nitriles such as acetonitrile and propionitrile, ethyl acetate, dichloromethane and dichloroethane.




Generally at least an equimolar amount of the Formula 26 compound is used in respect to the Formula 8 compound, and preferably at least a small molar excess of the Formula 26 compound is used. More particularly, the molar ratio of the Formula 8 compound to the Formula 26 compound is usually in the range of 1:1.05 to 1:10. In most cases, the molar ratio of the Formula 8 compound to the Formula 26 compound is preferably in the range of 1:1.1 to 1:1.5.




In the presence of a catalyst such as hexamethylguanidinium chloride, the reaction of compounds of Formula 8 and compounds of Formula 26 produces compounds of Formula 27. For general and preferred conditions, see


Tet. Lett


. 1987, 5823-5826.




Isolation of product of Step 1 can be accomplished by standard workup procedures.











Compounds of Formula 1 are synthesized by contacting compounds of either Formula 25 or Formula 27 with amines of Formula 13 in the presence of a suitable base in a suitable solvent.




For Step 2, the general and preferred reaction conditions are the same as the ones described above for Step 1 in Process Sequence A.




One skilled in the art will recognize that, in some cases, after the introduction of a given reagent as it is depicted in any individual scheme, it may be necessary to perform additional routine synthetic steps not described in detail to complete the synthesis of compounds of Formula 1. One skilled in the art will also recognize that it may be necessary to perform a combination of the steps illustrated in the above schemes in an order other than that implied by the particular sequence presented to prepare the compounds of Formula 1.




One skilled in the art will also recognize that compounds of Formula 1 and the intermediates described herein can be subjected to various electrophilic, nucleophilic, radical, organometallic, oxidation, and reduction reactions to add substituents or modify existing substituents.




Without further elaboration, it is believed that one skilled in the art using the preceding description can utilize the present invention to its fullest extent The following Examples are, therefore, to be construed as merely illustrative, and not limiting of the disclosure in any way whatsoever. Percentages are by weight except for chromatographic solvent mixtures or where otherwise indicated. Parts and percentages for chromatographic solvent mixtures are by volume unless otherwise indicated.


1


H NMR spectra are reported in ppm downfield from tetramethylsilane; s=singlet, d=doublet, t=triplet, q=quartet, m=multiplet, dd=doublet of doublets, dt=doublet of triplets, br s=broad singlet.











EXAMPLE 1




Step A: Preparation of N-(2,4-Dichlorophenyl)-N′-hydroxyurea




A solution of 14.2 g (75 mmol) of 2,4-dichlorophenylisocyanate in 50 mL of toluene was added to a mixture of 8.26 g (120 mmol) of hydroxylamine hydrochloride and 4.8 g (120 mmol) of sodium hydroxide in a two-phase solvent mixture consisting of 50 mL of water and 50 mL of toluene. The resulting mixture was stirred at 25° C. for 30 minutes and filtered. The solid thus obtained was washed with water and then dissolved in 200 mL of ethyl acetate. The solution was dried over magnesium sulfate and the solvent was removed under reduced pressure to yield 12.7 g of the title compound of Step A as a white solid melting at 157-158° C. It was used directly in the next step without further purification.




Step B: Preparation of 4-(2,4-Dichlorophenyl)-1,2,4-oxadiazolidine-3,5-dione




A solution of 4.2 g (19 mmol) of the compound of step A in tetrahydrofuran (20 mL) was treated with carbonyldiimidazole (3.2 g, 19 mmol). The mixture was stirred at 25° C. for 16 h. Some precipitated imidazole was filtered off and the filtrate was concentrated under reduced pressure. The residue was partitioned between 1N HCl (20 mL) and ethyl acetate (50 mL). The organic layer was dried over magnesium sulfate and concentrated to an oil which solidified to give 3.8 g of the title compound of Step B as a solid melting at 104-107° C. It was used directly for the next step without further purification.




Step C: Preparation of 4-Fluoro-N-Propylbenzenamine




A 3 L three neck round bottom flask equipped with a nitrogen inlet, a thermometer, an overhead stirrer and a solid addition funnel was charged with 250 mL acetic acid, 50 mL absolute ethanol and 29.5 g (0.27 mol) of 4-fluoroaniline. To this mixture was added acetone (23 mL, 6.31 mol) in one portion followed by the portion-wise addition of sodium acetate trihydrate over 5 min. This vigorously stirred mixture was cooled to 0° C. (dry-ice/acetone) and 4.5 g of sodium borohydride (1.2 mol) was added portion-wise via a solid addition funnel over 50 min while keeping the internal temperature below 10° C. During this addition, acetic acid (100 mL) and absolute ethanol (50 mL) were added to facilitate stirring. After the addition, the mixture was allowed to warm to room temperature, and then stirred at ambient temperature for 12 h. Sufficient ammonium hydroxide (30% aqueous) was added to adjust the pH to ˜8 while maintaining the internal temperature below 30° C. using an ice/water bath. The mixture was extracted with ether (4×400 mL). The combined organic layers were washed with brine, dried over MgSO


4


, filtered, then concentrated under reduced pressure to give the desired product as a black/brown oil (38 g).






1


H NMR: (300 MHz, CDCl


3


) δ 6.8-6.9 (t, 2H), 6.5 (m, 2H), 3.5 (m, 1H), 1.2 (d, 6H).




Step D: Preparation of 4-(Fluorophenyl)propylcarbamic Chloride




A 1 L three neck round bottom flask equipped with a nitrogen inlet, a thermometer and two addition funnels was charged with 600 mL of toluene and 36.0 g (0.22 mol) of the compound of Step C. This stirred mixture was cooled to 3° C., and then 116 mL (0.22 mol) of a 20% solution of phosgene in toluene was added dropwise over 15 min while maintaining the temperature below 10° C. Ten min after the addition, diisopropyl ethylamine (39 mL, 0.22 mol) was added dropwise over 15 min while maintaining the temperature below 7° C. The reaction mixture was allowed to warm to room temperature and stirred for 14 hours. The resulting brown solution was flooded with CH


2


Cl


2


(700 mL), and then saturated NaHCO


3


solution. The organic layer was separated and washed with saturated NaHCO


3


solution (3×500 mL), dried over MgSO


4


, and filtered. The solvent was removed under reduced pressure, then in vacuo, during which time the resulting oil slowly crystallized. This solid was triturated with hexanes to give 36 g (78%) of a gray solid melting at 50-55° C.






1


H NMR: (300 MHz, CDCl


3


) δ 7.1-7.2 (m, 4H), 4.68 (m, 1H), 1.1-1.2 (d, 6H).




Step E: Preparation of 4-(2,4-Dichlorophenyl)-N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A solution of 0.6 g (2.4 mmol) of the compound of Step B in toluene (25 mL) was treated with 0.42 g (1.9 mmol) of the compound of Step D and 0.35 g (2.9 mmol) of 4-dimethylaminopyridine. The resulting mixture was heated at 80° C. for 1 hour, and subsequently diluted with 1N hydrochloric acid (20 mL) and ethyl acetate (50 mL). The organic layer was separated and washed with saturated brine solution (30 mL). It was then dried over magnesium sulfate and concentrated under reduced pressure. The residue was subjected to column chromatography on silica gel with 85:15 hexanes-ethyl acetate as eluent. Appropriate fractions were combined and concentrated to give 0.32 g of the title compound of Step E, a compound of this invention, as an oil which solidified on standing to give a solid melting at 57-60° C.






1


H NMR (CDCl


3


) δ 1.22 (m, 6H), 4.7 (m, 1H), 7.04-7.17 (m, 2H), 7.2-7.3 (m, 3H), 7.39 (d, 1H), 7.58 (s, 1H).




EXAMPLE 2




Step A: Preparation of N-(2,6-Dimethylphenyl)-N′-hydroxylurea




A 500 mL side arm flask equipped with a thermometer and an addition funnel with a nitrogen inlet was charged with 100 mL of toluene and 2.00 g (0.10 mol) of 50% hydroxylamine in water. A solution of 4.41 g of 2,6-dimethylphenyl isocyanate (0.03 mol) dissolved in 50 mL of toluene was added dropwise over 15 min. External cooling was used to maintain the, internal reaction temperature below 25° C. Stirring was continued at room temp for 18 h. The solvent was removed under reduced pressure to give a white solid. The residual solvent was further co-evaporated twice with toluene, then oven dried overnight to give the desired product (5.25 g) as a white solid melting at 192-193° C.






1


H NMR: (300 MHz, DMSO-d


6


) δ 8.85 (d, 1H), 8.58 (s, 1H), 8.14 (s, 1H), 7.00-7.08 (m, 3H), 2.15 (s, 6H).




Step B: Preparation of 4-(2,6-Dimethylphenyl)-1,2,4-oxadiazolidine-3,5-dione




A 300 mL flask with side arm equipped with a nitrogen inlet and a thermometer was charged with 25 mL of tetrahydrofuran followed by 5.00 g (0.0277 mol) of 2,6-dimethylphenyl hydroxyurea. To this stirred suspension was added portion-wise 4.41 g (0.0277 mol) of carbonyl diimidazole over 5 min. While stirring at room temperature, the suspension turned into a solution before precipitate started to form slowly. After 18 h, the mixture was quenched with 50 mL of 1N HCl which caused the suspension to turn into a solution. It was partitioned between ethyl acetate (250 mL) and 1N HCl (50 mL). The organic layer was separated and washed with brine, then dried over MgSO


4


and filtered. The solvent was removed under reduced pressure to give the title compound as a red oil (5.20 g) which slowly crystallized upon standing at room temperature to give a solid melting at 90-100° C.






1


H NMR: (300 MHz, CDCl


3


) δ 7.30 (t, 1H), 7.20 (d, 2H), 2.24 (s, 6H).




Step C: Preparation of 4-(2,6-Dimethylphenyl)-N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




To a 500 mL two neck round bottom flask equipped with a thermometer and a reflux condenser with nitrogen inlet was charged sequentially 30 mL of toluene, 1.50 g (0.0072 mol) of the compound of Step B, 1.60 g (0.0074 mol) of the compound of Step D in Example 1, and lastly 0.90 g of 4-dimethylaminopyridine (0.072 mol). The reaction became homogeneous upon heating to 85° C. Heating was continued at 85° C. for 2 h during which time a precipitate was formed. The reaction mixture was then cooled to room temperature, filtered and the solid was washed with toluene (2×25 mL). The toluene was removed under reduced pressure to give a tan solid. The product was washed with cool isopropyl alcohol (2×10 mL) to give 2.16 g of the title compound, a compound of the invention, as a white solid melting at 134-136° C.






1


H NMR: (300 MHz, DMSO-d


6


) δ 7.20-7.47 (m, 7H), 4.52-4.65 (m, 1H), 2.03 (s, 6H).




EXAMPLE 3




Step A: Preparation of 4-(2-Propenyl)-1,2,4-oxadiazolidine-3,5-dione




To a 500 mL round-bottom flask were added acetone (300 mL), allyl isocyanate (12.0 g, 0.145 mol), N-hydroxyurethane (6.1 g, 0.058 mol) and triethylamine (11.7 g, 0.116 mol) respectively at room temperature under nitrogen with efficient stirring. The reaction mixture was allowed to stir at room temperature for 6 d. The solvent was removed under reduced pressure. The residue was suspended in 100 mL of 1N HCl, extracted with ethyl acetate (3×150 mL). The organic solution was washed with water, brine, dried over MgSO


4


and concentrated to a clear yellow oil. The crude product was dried under high vacuum for 4 h to give the title compound as an oil (13.1 g) which was used in the next step without further purification.






1


H NMR: (300 MHz, CDCl


3


) δ: 5.87 (m, 1H), 5.27 (m, 2H), 4.17 (m, 1H), 3.82 (bs, 1H).




Step B: Preparation of N-(4-Fluoroyhenyl)-N-(1-methylethyl)-3,5-dioxo-4-(2-propenyl)-1,2,4-oxadiazolidine-2-carboxamide




A dry 100 mL round-bottom flask was changed with dry tetrahydrofuran (20 mL), the compound of step A (1.0 g, 7.0 mmol), the compound of Step D in Example 1 (1.5 g, 7.0 mmol), triethylamine (1.0 g, 10.0 mmol) and 4-dimethylaminopyridine (0.2 g, 1.6 mmol) respectively at room temperature under nitrogen atmosphere with stirring. The reaction mixture was heated at reflux for 1.5 h during which time a white solid precipitated out. The reaction mixture was cooled to room temperature and diluted with 150 mL of ethyl acetate. The organic layer was washed with 1N HCl, water, brine, and dried over MgSO


4


. Upon concentration, a yellow syrup (1.8 g) was obtained. The crude product was purified by flash chromatography on silica gel with ethyl acetate/hexanes 1:9 as eluent to provide 1.22 g of the title compound, a compound of the invention, as a white solid melting at 65-66° C.






1


H NMR: (300 MHz, CDCl


3


) δ 7.22 (m, 2H), 7.11 (m, 2H), 5.78 (m, 1H), 5.26 (m, 2H), 4.42 (m, 1H), 4.07 (d, 2H), 1.20 (d, 6H).




EXAMPLE 4




Step A: Preparation of Phenylhydroxycarbamate




To a stirred solution of NaHCO


3


(60.5 g) in water (200 mL) in a 2 L beaker was added portion-wise over 15 min 27.5 g of hydroxylamine hydrochloride. Once the bubbling subsided, dichloromethane (200 mL) was added to the reaction mixture and cooled to 5° C. Phenyl chloroformate (50 g) was then added at a steady rate to the reaction mixture. The reaction mixture was allowed to warm to room temperature and stirred for 1 h. Ethyl acetate (100 mL) was employed to bring the reaction mixture to a transparent solution. The organic layer was separated, washed with brine (200 mL) and dried over MgSO


4


. The organic solvent was removed under reduced pressure to give the title compound (38.20 g) as a white solid melting at 104-107° C.




Step B: Preparation of N-Hydroxy-2,2-dimethylhydrazinecarboxamide




To a solution of 37.3 g of the compound of Step A in tetrahydrofuran (200 mL) at room temperature under nitrogen was added 22 mL of 1,1-dimethylhydrazine. The reaction mixture was then heated at reflux overnight. The solvent was removed under reduced pressure to afford an oil which was purified by column chromatography with 9:1 ethyl acetate-methanol as eluent to give a semi-solid. Triturating of the residue with dichloromethane gave the title compound (7.25 g) as a white solid melting at 115-118° C.






1


H NMR (DMSO-d


6


) δ 8.5 (brs, 1H), 8.27 (brs, 1H), 7.4 (brs, 1H), 2.4 (s, 6H).




Step C: Preparation of 4-(Dimethylamino)-1,2,4-oxadiazolinedine-3,5-dione




The compound of Step B (4.25 g, 29 mmol) was suspended in tetrahydrofuran (25 mL) at 5° C. under nitrogen. To the mixture was added portion-wise 1,1′-carbonyldiimidazole (5.78 g, 29 mmol) while maintaining the reaction temperature under 10° C. The reaction was partitioned between ethyl acetate (125 mL) and 1N HCl (60 mL). The organic layer was separated. The aqueous layer was further extracted with ethyl acetate (2×100 mL). The combined organic layers were dried over MgSO


4


and concentrated under reduced pressure to afford the title compound as an oil (2.9 g).






1


H NMR (CDCl


3


) δ 5.1 (br s, 1H), 2.9 (s, 6H).




Step D: Preparation of 4-(Dimethylamino)-N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




The compound of Step D, Example 1 (1.48 g, 6.9 mmol), 4-dimethylaminopyridine (0.84 g, 6.9 mmol), and the compound of Step C (1.00 g, 6.9 mmol) were combined in toluene (25 mL) at room temperature. The reaction mixture was heated to 80° C. for 3 h. Acetonitrile (20 mL) and silica gel (5 g) were added and the solvent was removed under reduced pressure. After column chromatography with 8:2 hexanes-ethyl acetate as eluent, the title compound, a compound of the invention, was isolated as a white solid (1.23 g) melting at 69-71° C.






1


H NMR (CDCl


3


) δ 7.2 (m, 2H), 7.1 (m, 2H), 4.6 (m, 1H), 2.9 (s, 6H), 1.2 (d, 6H).




EXAMPLE 5




Step A: Preparation of 4-[(2-Methylphenyl)methyl]-3-phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one




A 50 mL round bottom flask equipped with a thermometer, a stirrer, and a nitrogen inlet was charged with 3-(phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one (


Synthesis


, (1991), 265 0.5 g, 2.6 mmol), potassium carbonate (0.5 g, 3.6 mmol), tetrabutylammonium bromide (0.022 g, 0.1 mmol), 2-methylbenzyl bromide (0.6 g, 3.2 mmol) and acetonitrile (10 mL). The reaction mixture was stirred at room temperature for 18 h. The reaction mixture was poured into water (25 mL) and extracted with dichloromethane (3×20 mL), dried over MgSO


4


and concentrated under reduced pressure to provide a solid. The solid was further purified by flashichromatography on silica gel using 9:1 hexane-ethyl acetate to provide 0.3 g (40%) of the title compound as a white solid melting at 77-78° C.






1


H NMR (CDCl


3


): δ 7.39 (m, 3H), 7.27 (m, 3H), 7.17 (m, 3H), 5.26 (s, 2H), 4.69 (s, 2H), 2.31 (s, 3H).




Step B: Preparation of N-(4-Chlorophenyl)-N-(1-methylethyl)-4-[(2-methylphenyl)methyl]-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A 50 mL round bottom flask equipped with a stirrer, a thermometer, and a nitrogen inlet was charged with the compound of Step A (0.6 g, 2.05 mmol), (4-chlorophenyl)(1-methylethyl)carbamic chloride (0.5 g, 2.155 mmol), N,N′-dimethylaminopyridine (0.26 g, 2.13 mmol) and tetrahydrofuran (20 mL). The mixture was heated to reflux for 3 hours, then cooled to room temperature and poured into 1N HCl (50 mL). The mixture was extracted with diethyl ether (3×25 mL). The organic layer was dried over MgSO


4


and concentrated under reduced pressure to provide a thick oil. The oil was purified by flash chromatography on silica gel using 9:1 hexane-ethyl acetate to provide 0.22 g (28%) of the title compound as a white solid melting at 90-91° C.






1


H NMR (CDCl


3


): δ 7.5-7.0 (m, 8H), 4.63 (s, 2H), 4.6 (m, 1H), 2.36 (s, 3H), 1.18 (d, 6H).




EXAMPLE 6




Step A: Preparation of 4-Methyl-3-(phenylmethoxy)-1,2-oxadiazol-5(4H)-one




A 50 mL round bottom flask equipped with a thermometer, a stirrer and a nitrogen inlet was charged with 3-(phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one (1 g, 5.2 mmol), iodomethane (0.916 g, 6.5 mmol), 1,8-diazabicyclo[5.4.0]undec-7-ene (1 g, 6.5 mmol) and acetonitrile (10 mL). The mixture was stirred at room temperature for 18 h. The entire reaction mixture was flash chromatographed (silica gel, 8:2 hexane-ethyl acetate) to provide 1 g (37.5%) of the title compound as a white solid melting at 80-83° C.






1


H NMR (CDCl


3


): δ 7.43 (m, 5H), 5.32 (s, 2H), 3.09 (s, 3H).




Step B: Preparation of N-(4-Fluorophenyl)-4-methyl-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A 50 mL round bottom flask equipped with a thermometer, a stirrer and a nitrogen inlet was charged with 4-methyl-3-(phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one (0.55 g, 2.66 mmol), (4-fluorophenyl)(1-methylethyl)carbamic chloride (0.581 g, 2.7 mmol), N,N′-dimethylaminopyridine (0.329 g, 2.7 mmol) and acetonitrile (10 mL). The reaction mixture was heated to reflux 2 h, and allowed to cool to room temperature. The entire mixture was flash chromatographed (silica gel, 9: 1, then 8:2 hexane-ethyl acetate) to provide 0.6 g (76%) of the title compound as a white solid melting at 135-136° C.






1


H NMR (CDCl


3


) δ 7.29 (m, 2H), 7.11 (m, 2H), 4.64 (m, 1H), 3.05 (s, 3H), 1.18 (d, 6H).




EXAMPLE 7




Step A: Preparation of N-(4-Chlorophenyl)-4-methyl-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A 50 mL round bottom flask, equipped with a thermometer, a stirrer and nitrogen inlet was charged with 3-(phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one (0.5 g, 2.6 mmol), 1,8-diazabicyclo[5.4.0]unded-7-ene (0.5 g, 3.28 mmol), iodomethane (0.5 g, 3.54 mmol) and acetonitrile (5 mL). The mixture was stirred at room temperature for 18 h. To the mixture was added (4-chlorophenyl)(1-methylethyl)carbamic chloride (0.7 g, 3 mmol) and N,N′-dimethylamino-pyridine (0.367 g, 3 mmol), and the resulting mixture was heated to reflux for 2 h. It was then cooled to room temperature and flash chromatographed (silica gel, 9:1 hexane-ethyl acetate) to provide 150 mg (18%) of the title compound as a white solid melting at 121-123° C.






1


H NMR (CDCl


3


): δ 7.36 (m, 2H), 7.2 (m, 2H), 4.6 (m, 1H), 3.05 (s, 3H), 1.21 (d, 6H).




EXAMPLE 8




Step A: Preparation of 4-(2-Methylproyl)-3-(phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one




A 50 mL round bottom flask equipped with a thermometer, a stirrer, addition funnel and nitrogen inlet was charged with 3-(phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one (1 g, 5.2 mmol), 2-methyl propanol (0.45 g, 6 mmol), triphenylphosphine (1.57 g, 6 mmol) and tetrahydrofuran (5 mL). The mixture was cooled to 0° C. and a solution of diethyl azodicarboxylate (1.04 g, 6 mmol) in tetrahydrofuran (2 mL) was added dropwise over a period of 10 min. The reaction mixture was allowed to warm to room temperature, and stirred for 18 h. The entire mixture was flash chromatographed (silica gel, 8:2 hexane-ethyl acetate) to provide 1.1 g (84%) of the title compound as a white solid melting at 53-60° C.






1


H NMR (CDCl


3


): δ 7.42 (m, 5H), 5.31 (s, 2H), 3.34 (d, 2H), 2.01 (m, 1H), 0.89 (d, 6H).




Step B: Preparation of N-(4-Fluororhenyl)-N-(1-methylethyl)-4-(2-methylpropyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A 50 mL round bottom flask equipped with a stirrer, a thermometer and a nitrogen inlet was charged with 4-(2-methylpropyl)-3-(phenylmethoxy)-1,2,4-oxadiazol-5(4H)-one (0.25 g, 1 mmol), (4-fluorophenyl)(1-methylethyl)carbamic chloride (0.24 g, 1.1 mmol), N,N′-dimethylaminopyridine (0.14 g, 1.1 mmol) and acetonitrile (10 mL). The mixture was heated to reflux; for 2 h and allowed to cool to room temperature. The entire mixture was flashed chromatographed (silica gel, 9:1 hexane-ethyl acetate) to provide 0.18 (53%) of the title compound as a white solid melting at 80-81° C.






1


H NMR (CDCl


3


): δ 7.24 (m, 2H), 7.11 (m, 2H), 4.65 (m, 1H), 3.29 (d, 2H), 2.0 (m, 1H), 1.2 (d, 6H), 0.89 (d, 6H).




EXAMPLE 9




Step A: Preparation of N-(4-Fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-4-(phenylmethyl)-1,2,4-oxadiazolidine-2-carboxamide




A 50 mL round bottom flask equipped with a thermometer, a stirrer and a nitrogen inlet was charged with 3-(phenyhnethoxy)-1,2,4-oxadiazol-5(4H)-one (0.5 g, 2.6 mmol), (4-fluorophenyl)(1-methylethyl)carbamic chloride (0.58 g, 27 mmol), N,N′-dimethylaminopyridine (0.33 g, 2.7 mmol) and acetonitrile (5 mL). The mixture was heated to reflux for 3 h and allowed to cool to room temperature. The mixture was flash chromatographed (silica gel, 9:1 hexane-ethyl acetate) to provide 0.24 g (25%) of the title compound as a white solid melting at 95-96° C.






1


H NMR (CDCl


3


): δ 7.22 (s, 5H), 7.2 (m, 2H), 7.06 (m, 2H), 4.6 (m, 1H), 4.59 (s, 2H), 1.17 (d, 6H).




EXAMPLE 10




Step A: Preparation of N-(4-Fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide and N-(4-fluorophenyl)-4-methyl-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A 50 mL round bottom flask equipped with a thermometer, a stirrer and nitrogen inlet was charged with 3-methoxy-1,2,4-oxadiazol-5(4H)-one (1.16 g, 0.01 m), (4-fluorophenyl)(1-methylethy)carbamic chloride (2.4 g, 0.011 m), N,N′-dimethylaminopyridine (1.35 g, 0.011 m) and acetonitrile (20 mL). The mixture was heated to reflux for 18 h. The mixture was allowed to cool to room temperature, poured into 1N HCl (20 mL) and extracted with ethyl acetate (3×25 mL). The organic phase was dried over MgSO


4


and concentrated under reduced pressure to provide a thick oil. The oil was flash chromatographed (silica gel, 7:3 dichloromethane-ethyl acetate) to provide two fractions. Fraction A contained 0.42 g (15%) of N-(4-fluorophenyl)-4-methyl-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide as a white solid melting at 135-136° C.


1


H NMR (CDCl


3


): δ 7.26 (m, 2H), 7.11 (m, 2H), 4.6 (m, 1H), 3.05 (s, 3H), 1.17 (m, 6H). Fraction B contained 1.1 g (40%) of N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide as a solid melting at 55-60° C.




1H NMR (CDCl


3


): δ 7.24 (m, 2H), 7.19 (m, 2H), 4.6 (m, 1H), 1.2 (d, 6H). IR (CH


2


Cl


2


); 3200, 3300, 1776, 1715 cm


−1


. MS (M+1): 281, 257.




Step B: Preparation of N-(4-Fluorophenyl)-N-(1-methylethyl)-4-(2-methylpropyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A 50 mL round bottom flask equipped with a thermometer, a stirrer, an addition funnel, and a nitrogen inlet was charged with N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide (5.5 g, 0.019 m), 2-methyl-1-propanol (3 g, 0.04 mol), triphenylphosphine (6.3 g, 0.021 mol) and tetrahydrofuran (60 mL). The reaction solution was cooled to 15° C. and diethyl azodicarboxylate (4.2 g, 0.024 mol) in tetrahydrofuran (10 mL) was added dropwise over a period of 10 min. The reaction mixture was stirred at room temperature for 18 h. The solvent was removed under reduced pressure and the residue was flash chromatographed (silica gel, 9:1 hexane-ethyl acetate) to provide the title compound as a white solid (5.6 g, 88%). The solid has a melting range of 80-81° C., and was identical to the material prepared in Example 8, Step B.




EXAMPLE 11




Step A: Preparation of Methyl (Chlorocarbonyl)(2,6-dimethylphenyl)carbamate




A mixture of toluene (150 mL), biphenyl (0.2 g) and sodium methoxide in methanol (23.76 g, 0.11 mol, 25% by weight) was heated at reflux, and the methanol-toluene azeotrope was removed. The mixture was allowed to cool to 80° C., and toluene (80 mL) was added. To the resulting mixture was added in five portions methyl (2,6-dimethylphenyl)carbamate (17.9 g, 0.1 mol). The methanol formed in the reaction was removed as the above azeotrope. When most of the methanol had been removed, ethylene glycol dimethyl ether (8 mL) was added, and the mixture was distilled until the head temperature reached 110° C. The mixture was allowed to cool to 25° C., and ethylene glycol dimethyl ether (3 mL) was added. The mixture was then added to phosgene in toluene (22.5 g, 0.56 mol, 25% by weight). When the addition was complete, excess phosgene was removed by distillation. The mixture was allowed to cool to 25° C., and then washed with sodium bicarbonate solution (40 mL, saturated). The organic layer was dried and the volatiles removed by evaporation to give 17.21 g (64.5%) of the title compound as a solid. An analytical sample was prepared by column chromatography on silica gel using 1:3 ethyl acetate-hexanes as the eluent.




M.P. 84.5-86° C.; IR (Nujol): 1814, 1437, 1252, 1229, 1209, 1182, 1013, 982, 845 cm


−1


; 1H NMR (CDCl


3


): δ 7.28-7.12 (m, 3H), 3.82 (s, 3H), 2.23 (s, 6H).




Step B: Preparation of 4-(2,6-Dimethylphenyl)-2-methyl-1,2,4-oxadiazolidine-3,5-dione




A portion of the compound from Step A (3.72 g, 15.4 mmol) in dioxane (15 mL) was added to a mixture of aqueous hydroxylainie (2.03 g, 30.7 mmol, 50% by weight) in dioxane (1 5 mL). When the addition was complete, a solution of potassium hydroxide (2.22 g, 33.6 mmol, 85%) in water (5 mL) was added dropwise to the mixture so that the temperature did, not rise beyond 30° C. When the addition was complete, the solvent was removed until the volume was reduced to about 5 mL. The mixture was poured into water (100 mL), and the aqueous mixture was extracted with ethyl acetate (2×50 mL). The aqueous mixture was acidified with HCl and further extracted with ethyl acetate (2×50 mL). The combined organic extracts from the second extraction were dried and evaporated to give the title compound as a solid (2.34 g, 73.7%). The solid has a melting point range of 92-93.5° C. after crystallization from ether/hexanes, and was identical to material prepared in Example 2, Step B.




EXAMPLE 12




Step A: Preparation of N′-Hydroxy-N-(1-methylethyl)-N-phenylurea




A solution, of 50% aqueous hydroxylamine (16.8 g, 0.25 mol) was added dropwise to a solution of (1-methylethyl)phenylcarbamic chloride (20.0 g, 0.1 mol) in 200 mL of THF in an ice bath so that the reaction temperature was kept below 30° C. Precipitate began to form halfway through the addition. The resulting slurry was stirred overnight. The mixture was filtered, and the solids collected were first washed with water and then with hexane/ether. After air-drying, 14.56 g of the title compound was obtained. Its structure was confirmed by an analysis of the NMR spectra. The filtrate was stripped down to afford a residue which was washed sequentially with 1N HCl, water and hexane/ether to yield a second crop of the title compound (5.38 g) melting at 165-166° C. The combined yield was 100%.






1


H NMR.(300 MHz, DMSO-d


6


): δ 8.10 (br s, 1H), 7.74 (s, 1H), 7.38 (m, 3H), 7.12 (m, 2H), 4.55 (m, 1H), 0.97 (d, 6H)




Step B: Preparation of N-(1-Methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamide




A solution of chlorocarbonyl isocyanate (5.0 g, 0.047 mol) was added dropwise to a slurry of the title compound of Step A (9.2 g, 0.047 mol) and triethylamine (5.3 g, 0.052 mol) in 200 mL of THF while maintaining the reaction temperature below 30° C. using an ice bath. After 2 hours, TLC showed the presence of starting material. Another 0.5 g of chlorocarbonyl isocyanate was added, and the reaction mixture was stirred for another hour. At that point, TLC showed still the presence of starting material. The reaction mixture was filtered to, remove solids, and the filtrate was stripped to dryness and then extracted with 1N HCl and ether. Upon evaporation of volatiles, a gummy product was obtained which was taken into methylene chloride and potassium carbonate solution. Solids were collected by a filtration, washed with methylene chloride and air dried. The solids (5.3 g) were found to be the potassium salt of the title compound. The basic aqueous filtrate was acidified with concentrated HCl and extracted with methylene chloride to afford 4 g of the title compound, an intermediate useful for the preparation of the compounds of the present invention, melting at 116-7° C. From the methylene chloride used to wash the solids, 2.6 g of the title compound of Step A was recovered. This represented a 71.7% conversion. The combined yield was therefore 96% based on the 71.7% conversion.






1


H NMR (300 MHz, DMSO-d


6


): δ 9.60 (brs, 1H), 7.37 (m, 3H), 7.23 (m, 2H), 4.60 (m, 1H), 1.19 (d, 6H).




EXAMPLE 13




Step A: Preparation of N-(4-Fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A 1 L three neck round bottom flask equipped with nitrogen inlet, thermometer and water condenser was charged with dioxanes (400 mL), 1,2,4-oxadiazole-3,5-dione (30 g 0.29 moles, prepared according to Srivastava, P. and Robins, R.,


J. Med. Chem


. 1981, 24, 1172-1177), 4-dimethylaminopyridine (36 g, 0.29 mole), and N-isopropyl-4-flourophenylcarbamoyl chloride (63 g, 0.29 moles) at room temperature. The yellow mixture was heated at reflux for 4 hours. When no starting material was detected by thin layer chromatography, heat was tuned off and mixture was cooled to room temperature. The solvent was removed under reduced pressure and the resulting solids were suspended in ethyl acetate. The mixture was washed with 1N HCl, and the aqueous layer was extracted twice with ethyl acetate. The combined organic solutions were washed with brine, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure. The product was crystallized from chlorobutane and hexanes, and filtered to give 47 g (57%) of the title compound as a white solid melting at 94-95° C.






1


H NMR: (300 MHz, CDCl


3


) δ 7.24 (m, 2H), 7.09 (m, 2H), 4.63 (m, 1H), 1.18 (d, 6H).




Step B: Preparation of N-(4-Fluorophenyl)-N,4-bis(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




A solution of the compound of Step A (1.0 g, 3.6 mmol) in 20 mL of triisopropylorthoformate was heated at 145° C. for 2 h and then allowed to stir at ambient temperature overnight. The volatiles were removed under reduced pressure, and the residue recrystallized from methanol to give 0.99 g (86%) of the title compound, a compound of this invention, as a solid melting at 78-80° C.






1


H NMR (300 MHz, CDCl


3


): δ 7.26(m, 2H), 7.11(m, 2H), 4.62(m, 1H), 4.18(m, 1H), 1.40(d, 6H), 1.20 (d, 6H).




EXAMPLE 14




Step A: Preparation of 2,2′-Carbonylbis[4-(1-methylethyl)-1,2,4-oxadiazolidine-3,5-dione




To a solution of 4-(1-methylethyl)-1,2,4-oxadiazolidine-3,5-dione (20 g, 139 mmol) and hexamethylguanidinium chloride (0.25 g, 1.39 mmol) in 150 mL of toluene was added phosgene (6.88 g, 69 mmol, 20% by weight in toluene). The resulting mixture was heated at reflux for 1.5 h with the use of a dry ice/acetone condenser. The volatiles were removed under reduced pressure, and the residue recrystallized from 150 mL of n-BuCl to give 14 g (64%) of the title compound as a white solid melting at 150° C.






1


H NMR (300 MHz, CDCl


3


): δ 1.52 (d, 6H), 4.36 (m, 1H).




Step B: Preparation of N,4-bis(1-Methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamide




A solution of the compound of Step A (0.5 g, 1.6 mmol), N-phenyl-N-(2-methylethyl)amine (0.215 g, 1.6 mmol) and 4-dimethylaminopyridine (0.19 g, 1.6 mmol) in 10 mL of acetonitrile was heated at reflux under a nitrogen atmosphere. The resulting mixture was allowed to cool to ambient temperature and poured into 25 mL of water. It was then extracted with ethylacetate (4×25 mL). Condensation gave an oil which was purified by flash chromatography using 1:3 EtOAc-Hexanes as the eluant to give the title compound, a compound of this invention, as a white solid melting at 83-84° C.






1


H NMR (300 MHz, CDCl


3


): δ 1.20 (d, 6H), 1.38 (d, 6H), 4.16 (m, 1H), 4.63 (m, 1H), 7.26 (m, 2H), 7.39 (m, 3H).




EXAMPLE 15




Step A: N-(4-Fluorophenyl)-4-(methoxymethyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide




To a solution of 308 uL of bromomethyl methyl ether (1 eq, 90% tech.) in 8 mL dry acetonitrile was added 995 mg of the title compound of Step A in Example 13. To this mixture was then added 508 uL (1 eq) of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU). The resulting solution was heated at reflux under a nitrogen atmosphere for 3 h. The reaction mixture was allowed to cool to room temperature and the volatiles removed under reduced pressure. The residue was dissolved in 1 mL of dichloromethane and loaded onto a 70 mL solid phase extraction (SPE) cartridge containing 10 g of silica gel (230-400 mesh). The title compound (260 mg), a compound of this invention, was obtained after elution using a 20% ethyl acetate/hexane solution.






1


H NMR (300 MHz, CDCl


3


): δ 7.22(m, 2H), 7.09 (m, 2H), 4.89 (s, 2H), 4.65 (m, 1H), 3.39 (s, 3H), 1.2 (d, 6H).




By the procedures described herein together with methods known in the art, the following compounds of Tables 1 to 3 can be prepared. The following notations have been used in Tables.





















Q-1




Ph







Q-2




2-Cl—Ph







Q-3




3-Cl—Ph







Q-4




4-Cl—Ph







Q-5




2-Br—Ph







Q-6




2-F—Ph







Q-76




2,4-di-F—Ph







Q-8




2,6-di-F—Ph







Q-9




2,3-di-Cl—Ph







Q-10




2,4-di-Cl—Ph







Q-11




2,6-di-Cl—Ph







Q-12




2,6-di-Et-Ph







Q-13




2,6-di-OMe







Q-14




2-Cl-4-F—Ph







Q-15




2-Cl-6-F—Ph







Q-16




2-Me-Ph







Q-17




3-Me-Ph







Q-18




4-Me-Ph







Q-19




2-Et-Ph







Q-20




2-Pr—Ph







Q-21




2,5-di-Me-Ph







Q-22




4-OMe-Ph







Q-23




2-Cl-6-Me-Ph







Q-24




2,6-di-Me-Ph







Q-25




2,4-Me-Ph







Q-26




2,5-di-Me-Ph







Q-27




2,3-di-Me-Ph







Q-28




2-Me-6-Et-Ph







Q-29




2-CF


3


—Ph







Q-30




4-CF


3


—Ph







Q-31




2-OCF


2


H—Ph







Q-32




2-OCF


3


—Ph







Q-33




2,4,6-tri-Me-Ph







Q-34




4-Cl-2,6-di-Me-Ph







Q-35




2-OPh—Ph







Q-36




2-SCH


3


—Ph







Q-37




2-Me-6-(i-Pr)—Ph







Q-38




2-Cl-4-Me-Ph







Q-39




2-CN-Ph







Q-40




4-Cl-2-Me-Ph







Q-41




2-Cl-6-Me-Ph







Q-42




2-Me-5-Cl—Ph







Q-43




2-Cl-5-Me-Ph







Q-44




2-Cl-3-Me-Ph







Q-45




2-NO


2


—Ph







Q-46




1-tetrahydronaphthyl







Q-47




4-(2,3-dihydro-1H-indene)







Q-48




7-(2,3-diH-2,2-di-Me-7-benzofuran)







Q-49




2-Vinyl-Ph







Q-50




2-Ph—Ph







Q-51




1-(2-Me-tetrahydronaphthyl)







Q-52




3-(2-Cl-Pyridine)







Q-53




4,6-di-Me-Pyrimidin-5-yl







Q-54




4,6-di-OMe-Pyrimidin-5-yl







Q-55




PhCH


2










Q-56




PhC(CH


3


)—







Q-57




(2-Cl—Ph)CH


2










Q-58




(2,6-di-Cl—Ph)CH


2










Q-59




(2,3-di-Cl—Ph)CH


2










Q-60




(2-Me-Ph)CH


2










Q-61




(2-OCH


3


—Ph)CH


2










Q-62




(2,4-di-Cl—Ph)CH


2










Q-63




(2-CF


3


—Ph)CH


2










Q-64




(2-OCF


3


—Ph)CH


2










Q-65




(2-CN-Ph)CH


2










Q-66




(2-Cl—Ph)CH(CH


3


)—







Q-67




(2-Me-Ph)CH(CH


3


)—







Q-68




PhCH


2


CH


2










Q-69




(2-Cl—Ph)CH


2


CH


2










Q-70




(2-Me-Ph)CH


2


CH


2




























































Q-71




Q-72


















































Q-73




Q-74


















































Q-75




Q-76


















































Q-77




Q-78


















































Q-79




Q-80


















































Q-81




Q-82


















































Q-83




Q-84


















































Q-85




Q-86


















































Q-87




Q-88


















































Q-89




Q-90


















































Q-91




Q-92


















































Q-93




Q-94






















Q-95




n-Pr







Q-96




n-Bu







Q-97




i-Bu







Q-98




n-hex







Q-99




c-Pr







Q-100




Allyl







Q-101




Propargyl







Q-102




3-(2-Cl-Propenyl)







Q-103




Cyclohexyl







Q-104




1-cyclohexenyl







Q-105




2-Me-1-cyclohexenyl







Q-106




MeOCH


2


CH


2










Q-107




MeOCH


2










Q-108




3-Cl—Pr







Q-109




4-(1,1-di-F-butenyl)







Q-110




3-(1,1-di-Cl-propenyl)







Q-111




i-Pr







Q-112




2-OMe-Ph







Q-113




2-Me-6-OMe-Ph







Q-114




2-Cl-Et







Q-115




3-(2-Me-Propenyl)







Q-116




t-Bu







Q-117




MeC(═NOMe)CH


2










Q-118




2-Me-(c-Hex)







Q-119




Et







Q-120




c-Pentyl







Q-121




c-Butyl







Q-122




EtC(Me)


2










Q-123




CF


3


CH


2










Q-124




4-(1-Butenyl)







Q-125




3-Me-Propargyl







Q-126




1-(3-Me-1-Propenyl)







Q-127




NCCH


2










Q-128




(i-C


3


H


7


)O—







Q-129




(Allyl)O—







Q-130




(Me)


2


N—







Q-131




1-piperidino







Q-132




MeO


2


S—







Q-133




MeSCH


2


CH


2










Q-134




Me2NS(O)


2










Q-135




O


2


NCH


2










Q-136




MeC(═O)—







Q-137




(i-Pr)OC(═O)—







Q-138




EtOC(═O)—







Q-139




Me


2


NC(═O)—







Q-140




EtOC(═O)CH


2










Q-141




(MeO)


2


P(═O)CH


2










Q-142




Me


2


NC(═O)CH


2










Q-143




2-(Tetrahydropyranyl)







Q-144




(Oxirane)-CH


2




























































Q-145




Q-146


















































Q-147




Q-148


















































Q-149




Q-150


















































Q-151




Q-152


















































Q-153




Q-154


















































Q-155




Q-156














Q-157




Me


2


NCH


2


CH


2










Q-158




Me


2


NCH


2










Q-159




Me


3


SiCH


2










Q-160




Me


2


NC(═S)—







Q-161




3-oxetanyl







Q-162




NCCH


2


CH


2









Q-163




MeOC(═O)CH(CH


3


)—







Q-164




MeOC(═O)CH(i-Pr)—







Q-165




MeNH







Q-166




2-(NMe


2


)—Ph







Q-167




2-(SF


5


)—Ph







Q-168




1-(Morpholino)







Q-169




EtCH(Me)—







Q-170




Me


3


CCH


2









Q-171




(Et)


2


N—







Q-172




MeS—







Q-173




MeSC(═S)—







Q-174




4-(2-Butynyl)







Q-175




F


3


CS—



















































































B-1




B-2




B-3




B-4










































































B-5




B-6




B-7




B-8







































i-C


3


H


7


B-11




C


2


H


5


B-12















B-9




B-10










































































B-13




B-14




B-15




B-16















Allyl




Propargyl







B-17




B-18























TABLE 1




























R


2


is i-C


3


H


7


, R


13


is 4-F



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175














R


2


is i-C


3


H


7


, R


13


is 2,4-di-F



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175














R


2


is i-C


3


H


7


, R


13


is 4-Cl



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175














R


2


is i-C


3


H


7


, R


13


is H



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175






















Q




R


2






R


13






Q




R


2






R


13






Q




R


2






R


13











Q-2




CH


3






4-F




Q-2




CH


3






2,4-di-F




Q-2




CH


3






4-Cl






Q-16




CH


3






4-F




Q-16




CH


3






2,4-di-F




Q-16




CH


3






4-Cl






Q-24




CH


3






4-F




Q-24




CH


3






2,4-di-F




Q-24




CH


3






4-Cl






Q-29




CH


3






4-F




Q-29




CH


3






2,4-di-F




Q-29




CH


3






4-Cl






Q-57




CH


3






4-F




Q-57




CH


3






2,4-di-F




Q-57




CH


3






4-Cl






Q-71




CH


3






4-F




Q-71




CH


3






2,4-di-F




Q-71




CH


3






4-Cl






Q-100




CH


3






4-F




Q-100




CH


3






2,4-di-F




Q-100




CH


3






4-Cl






Q-119




CH


3






4-F




Q-119




CH


3






2,4-di-F




Q-119




CH


3






4-Cl






Q-120




CH


3






4-F




Q-120




CH


3






2,4-di-F




Q-120




CH


3






4-Cl






Q-126




CH


3






4-F




Q-126




CH


3






2,4-di-F




Q-126




CH


3






4-Cl






Q-130




CH


3






4-F




Q-130




CH


3






2,4-di-F




Q-130




CH


3






4-Cl






Q-144




CH


3






4-F




Q-144




CH


3






2,4-di-F




Q-144




CH


3






4-Cl






Q-162




CH


3






4-F




Q-162




CH


3






2,4-di-F




Q-162




CH


3






4-Cl






Q-169




CH


3






4-F




Q-169




CH


3






2,4-di-F




Q-169




CH


3






4-Cl






Q-2




C


2


H


5






4-F




Q-2




C


2


H


5






2,4-di-F




Q-2




C


2


H


5






4-Cl






Q-16




C


2


H


5






4-F




Q-16




C


2


H


5






2,4-di-F




Q-16




C


2


H


5






4-Cl






Q-24




C


2


H


5






4-F




Q-24




C


2


H


5






2,4-di-F




Q-24




C


2


H


5






4-Cl






Q-29




C


2


H


5






4-F




Q-29




C


2


H


5






2,4-di-F




Q-29




C


2


H


5






4-Cl






Q-57




C


2


H


5






4-F




Q-57




C


2


H


5






2,4-di-F




Q-57




C


2


H


5






4-Cl






Q-71




C


2


H


5






4-F




Q-71




C


2


H


5






2,4-di-F




Q-71




C


2


H


5






4-Cl






Q-100




C


2


H


5






4-F




Q-100




C


2


H


5






2,4-di-F




Q-100




C


2


H


5






4-Cl






Q-119




C


2


H


5






4-F




Q-119




C


2


H


5






2,4-di-F




Q-119




C


2


H


5






4-Cl






Q-120




C


2


H


5






4-F




Q-120




C


2


H


5






2,4-di-F




Q-120




C


2


H


5






4-Cl






Q-126




C


2


H


5






4-F




Q-126




C


2


H


5






2,4-di-F




Q-126




C


2


H


5






4-Cl






Q-130




C


2


H


5






4-F




Q-130




C


2


H


5






2,4-di-F




Q-130




C


2


H


5






4-Cl






Q-144




C


2


H


5






4-F




Q-144




C


2


H


5






2,4-di-F




Q-144




C


2


H


5






4-Cl






Q-162




C


2


H


5






4-F




Q-162




C


2


H


5






2,4-di-F




Q-162




C


2


H


5






4-Cl






Q-169




C


2


H


5






4-F




Q-169




C


2


H


5






2,4-di-F




Q-169




C


2


H


5






4-Cl






Q-2




i-C


4


H


9






4-F




Q-2




i-C


4


H


9






2,4-di-F




Q-2




i-C


4


H


9






4-Cl






Q-16




i-C


4


H


9






4-F




Q-16




i-C


4


H


9






2,4-di-F




Q-16




i-C


4


H


9






4-Cl






Q-24




i-C


4


H


9






4-F




Q-24




i-C


4


H


9






2,4-di-F




Q-24




i-C


4


H


9






4-Cl






Q-29




i-C


4


H


9






4-F




Q-29




i-C


4


H


9






2,4-di-F




Q-29




i-C


4


H


9






4-Cl






Q-57




i-C


4


H


9






4-F




Q-57




i-C


4


H


9






2,4-di-F




Q-57




i-C


4


H


9






4-Cl






Q-71




i-C


4


H


9






4-F




Q-71




i-C


4


H


9






2,4-di-F




Q-71




i-C


4


H


9






4-Cl






Q-100




i-C


4


H


9






4-F




Q-100




i-C


4


H


9






2,4-di-F




Q-100




i-C


4


H


9






4-Cl






Q-119




i-C


4


H


9






4-F




Q-119




i-C


4


H


9






2,4-di-F




Q-119




i-C


4


H


9






4-Cl






Q-120




i-C


4


H


9






4-F




Q-120




i-C


4


H


9






2,4-di-F




Q-120




i-C


4


H


9






4-Cl






Q-126




i-C


4


H


9






4-F




Q-126




i-C


4


H


9






2,4-di-F




Q-126




i-C


4


H


9






4-Cl






Q-130




i-C


4


H


9






4-F




Q-130




i-C


4


H


9






2,4-di-F




Q-130




i-C


4


H


9






4-Cl






Q-144




i-C


4


H


9






4-F




Q-144




i-C


4


H


9






2,4-di-F




Q-144




i-C


4


H


9






4-Cl






Q-162




i-C


4


H


9






4-F




Q-162




i-C


4


H


9






2,4-di-F




Q-162




i-C


4


H


9






4-Cl






Q-169




i-C


4


H


9






4-F




Q-169




i-C


4


H


9






2,4-di-F




Q-169




i-C


4


H


9






4-Cl






Q-2




n-C


3


H


7






4-F




Q-2




n-C


3


H


7






2,4-di-F




Q-2




n-C


3


H


7






4-Cl






Q-16




n-C


3


H


7






4-F




Q-16




n-C


3


H


7






2,4-di-F




Q-16




n-C


3


H


7






4-Cl






Q-24




n-C


3


H


7






4-F




Q-24




n-C


3


H


7






2,4-di-F




Q-24




nC


3


H


7






4-Cl






Q-29




n-C


3


H


7






4-F




Q-29




n-C


3


H


7






2,4-di-F




Q-29




n-C


3


H


7






4-Cl






Q-57




n-C


3


H


7






4-F




Q-57




n-C


3


H


7






2,4-di-F




Q-57




n-C


3


H


7






4-Cl






Q-71




n-C


3


H


7






4-F




Q-71




n-C


3


H


7






2,4-di-F




Q-71




n-C


3


H


7






4-Cl






Q-100




n-C


3


H


7






4-F




Q-100




n-C


3


H


7






2,4-di-F




Q-100




n-C


3


H


7






4-Cl






Q-119




n-C


3


H


7






4-F




Q-119




n-C


3


H


7






4-F




Q-119




n-C


3


H


7






4-F






Q-120




n-C


3


H


7






4-F




Q-120




n-C


3


H


7






4-F




Q-120




n-C


3


H


7






4-F






Q-126




n-C


3


H


7






4-F




Q-126




n-C


3


H


7






4-F




Q-126




n-C


3


H


7






4-F






Q-130




n-C


3


H


7






4-F




Q-130




n-C


3


H


7






4-F




Q-130




n-C


3


H


7






4-F






Q-144




n-C


3


H


7






4-F




Q-144




n-C


3


H


7






4-F




Q-144




n-C


3


H


7






4-F






Q-162




n-C


3


H


7






4-F




Q-162




n-C


3


H


7






4-F




Q-162




n-C


3


H


7






4-F






Q-169




n-C


3


H


7






4-F




Q-169




n-C


3


H


7






4-F




Q-169




n-C


3


H


7






4-F






Q-2




Cyclopropyl




4-F




Q-2




Cyclopropyl




2,4-di-F




Q-2




Cyclopropyl




4-Cl






Q-16




Cyclopropyl




4-F




Q-16




Cyclopropyl




2,4-di-F




Q-16




Cyclopropyl




4-Cl






Q-24




Cyclopropyl




4-F




Q-24




Cyclopropyl




2,4-di-F




Q-24




Cyclopropyl




4-Cl






Q-29




Cyclopropyl




4-F




Q-29




Cyclopropyl




2,4-di-F




Q-29




Cyclopropyl




4-Cl






Q-57




Cyclopropyl




4-F




Q-57




Cyclopropyl




2,4-di-F




Q-57




Cyclopropyl




4-Cl






Q-71




Cyclopropyl




4-F




Q-71




Cyclopropyl




2,4-di-F




Q-71




Cyclopropyl




4-Cl






Q-100




Cyclopropyl




4-F




Q-100




Cyclopropyl




2,4-di-F




Q-100




Cyclopropyl




4-Cl






Q-119




Cyclopropyl




4-F




Q-119




Cyclopropyl




2,4-di-F




Q-119




Cyclopropyl




4-Cl






Q-120




Cyclopropyl




4-F




Q-120




Cyclopropyl




2,4-di-F




Q-120




Cyclopropyl




4-Cl






Q-126




Cyclopropyl




4-F




Q-126




Cyclopropyl




2,4-di-F




Q-126




Cyclopropyl




4-Cl






Q-130




Cyclopropyl




4-F




Q-130




Cyclopropyl




2,4-di-F




Q-130




Cyclopropyl




4-Cl






Q-144




Cyclopropyl




4-F




Q-144




Cyclopropyl




2,4-di-F




Q-144




Cyclopropyl




4-Cl






Q-162




Cyclopropyl




4-F




Q-162




Cyclopropyl




2,4-di-F




Q-162




Cyclopropyl




4-Cl






Q-169




Cyclopropyl




4-F




Q-169




Cyclopropyl




2,4-di-F




Q-169




Cyclopropyl




4-Cl






















Q




R


2






R


13






Q




R


2






R


13






Q




R


2






R


13











Q-2




i-C


3


H


7






4-OCF


3






Q-2




i-C


3


H


7






4-COOCH


3






Q-2




i-C


3


H


7






3,5-di-F






Q-16




i-C


3


H


7






4-OCF


3






Q-16




i-C


3


H


7






4-COOCH


3






Q-16




i-C


3


H


7






3,5-di-F






Q-24




i-C


3


H


7






4-OCF


3






Q-24




i-C


3


H


7






4-COOCH


3






Q-24




i-C


3


H


7






3,5-di-F






Q-29




i-C


3


H


7






4-OCF


3






Q-29




i-C


3


H


7






4-COOCH


3






Q-29




i-C


3


H


7






3,5-di-F






Q-57




i-C


3


H


7






4-OCF


3






Q-57




i-C


3


H


7






4-COOCH


3






Q-57




i-C


3


H


7






3,5-di-F






Q-71




i-C


3


H


7






4-OCF


3






Q-71




i-C


3


H


7






4-COOCH


3






Q-71




i-C


3


H


7






3,5-di-F






Q-100




i-C


3


H


7






4-OCF


3






Q-100




i-C


3


H


7






4-COOCH


3






Q-100




i-C


3


H


7






3,5-di-F






Q-119




i-C


3


H


7






4-OCF


3






Q-119




i-C


3


H


7






4-COOCH


3






Q-119




i-C


3


H


7






3,5-di-F






Q-120




i-C


3


H


7






4-OCF


3






Q-120




i-C


3


H


7






4-COOCH


3






Q-120




i-C


3


H


7






3,5-di-F






Q-126




i-C


3


H


7






4-OCF


3






Q-126




i-C


3


H


7






4-COOCH


3






Q-126




i-C


3


H


7






3,5-di-F






Q-130




i-C


3


H


7






4-OCF


3






Q-130




i-C


3


H


7






4-COOCH


3






Q-130




i-C


3


H


7






3,5-di-F






Q-144




i-C


3


H


7






4-OCF


3






Q-144




i-C


3


H


7






4-COOCH


3






Q-144




i-C


3


H


7






3,5-di-F






Q-162




i-C


3


H


7






4-OCF


3






Q-162




i-C


3


H


7






4-COOCH


3






Q-162




i-C


3


H


7






3,5-di-F






Q-169




i-C


3


H


7






4-OCF


3






Q-169




i-C


3


H


7






4-COOCH


3






Q-169




i-C


3


H


7






3,5-di-F






Q-2




i-C


3


H


7






4-CF


3






Q-2




i-C


3


H


7






4-CH


3






Q-2




i-C


3


H


7






2,4,6-tri-F






Q-16




i-C


3


H


7






4-CF


3






Q-16




i-C


3


H


7






4-CH


3






Q-16




i-C


3


H


7






2,4,6-tri-F






Q-24




i-C


3


H


7






4-CF


3






Q-24




i-C


3


H


7






4-CH


3






Q-24




i-C


3


H


7






2,4,6-tri-F






Q-29




i-C


3


H


7






4-CF


3






Q-29




i-C


3


H


7






4-CH


3






Q-29




i-C


3


H


7






2,4,6-tri-F






Q-57




i-C


3


H


7






4-CF


3






Q-57




i-C


3


H


7






4-CH


3






Q-57




i-C


3


H


7






2,4,6-tri-F






Q-71




i-C


3


H


7






4-CF


3






Q-71




i-C


3


H


7






4-CH


3






Q-71




i-C


3


H


7






2,4,6-tri-F






Q-100




i-C


3


H


7






4-CF


3






Q-100




i-C


3


H


7






4-CH


3






Q-100




i-C


3


H


7






2,4,6-tri-F






Q-119




i-C


3


H


7






4-CF


3






Q-119




i-C


3


H


7






4-CH


3






Q-119




i-C


3


H


7






2,4,6-tri-F






Q-120




i-C


3


H


7






4-CF


3






Q-120




i-C


3


H


7






4-CH


3






Q-120




i-C


3


H


7






2,4,6-tri-F






Q-126




i-C


3


H


7






4-CF


3






Q-126




i-C


3


H


7






4-CH


3






Q-126




i-C


3


H


7






2,4,6-tri-F






Q-130




i-C


3


H


7






4-CF


3






Q-130




i-C


3


H


7






4-CH


3






Q-130




i-C


3


H


7






2,4,6-tri-F






Q-144




i-C


3


H


7






4-CF


3






Q-144




i-C


3


H


7






4-CH


3






Q-144




i-C


3


H


7






2,4,6-tri-F






Q-162




i-C


3


H


7






4-CF


3






Q-162




i-C


3


H


7






4-CH


3






Q-162




i-C


3


H


7






2,4,6-tri-F






Q-169




i-C


3


H


7






4-CF


3






Q-169




i-C


3


H


7






4-CH


3






Q-169




i-C


3


H


7






2,4,6-tri-F






Q-2




i-C


3


H


7






4-OCH


3






Q-2




i-C


3


H


7






2,4-di-Cl




Q-2




i-C


3


H


7






2,5-di-F






Q-16




i-C


3


H


7






4-OCH


3






Q-16




i-C


3


H


7






2,4-di-Cl




Q-16




i-C


3


H


7






2,5-di-F






Q-24




i-C


3


H


7






4-OCH


3






Q-24




i-C


3


H


7






2,4-di-Cl




Q-24




i-C


3


H


7






2,5-di-F






Q-29




i-C


3


H


7






4-OCH


3






Q-29




i-C


4


H


9






2,4-di-Cl




Q-29




i-C


3


H


7






2,5-di-F






Q-57




i-C


3


H


7






4-OCH


3






Q-57




i-C


3


H


7






2,4-di-Cl




Q-57




i-C


3


H


7






2,5-di-F






Q-71




i-C


3


H


7






4-OCH


3






Q-71




i-C


3


H


7






2,4-di-Cl




Q-71




i-C


3


H


7






2,5-di-F






Q-100




i-C


3


H


7






4-OCH


3






Q-100




i-C


3


H


7






2,4-di-Cl




Q-100




i-C


3


H


7






2,5-di-F






Q-119




i-C


3


H


7






4-OCH


3






Q-119




i-C


3


H


7






2,4-di-Cl




Q-119




i-C


3


H


7






2,5-di-F






Q-120




i-C


3


H


7






4-OCH


3






Q-120




i-C


3


H


7






2,4-di-Cl




Q-120




i-C


3


H


7






2,5-di-F






Q-126




i-C


3


H


7






4-OCH


3






Q-126




i-C


3


H


7






2,4-di-Cl




Q-126




i-C


3


H


7






2,5-di-F






Q-130




i-C


3


H


7






4-OCH


3






Q-130




i-C


4


H


9






2,4-di-Cl




Q-130




i-C


3


H


7






2,5-di-F






Q-144




i-C


3


H


7






4-OCH


3






Q-144




i-C


3


H


7






2,4-di-Cl




Q-144




i-C


3


H


7






2,5-di-F






Q-162




i-C


3


H


7






4-OCH


3






Q-162




i-C


3


H


7






2,4-di-Cl




Q-162




i-C


3


H


7






2,5-di-F






Q-169




i-C


3


H


7






4-OCH


3






Q-169




i-C


3


H


7






2,4-di-Cl




Q-169




i-C


3


H


7






2,5-di-F






Q-2




i-C


3


H


7






4-CN




Q-2




i-C


3


H


7






2-F, 4-Cl




Q-2




i-C


3


H


7






4-OCF


2


H






Q-16




i-C


3


H


7






4-CN




Q-16




i-C


3


H


7






2-F, 4-Cl




Q-16




i-C


3


H


7






4-OCF


2


H






Q-24




i-C


3


H


7






4-CN




Q-24




i-C


3


H


7






2-F, 4-Cl




Q-24




i-C


3


H


7






4-OCF


2


H






Q-29




i-C


3


H


7






4-CN




Q-29




i-C


3


H


7






2-F, 4-Cl




Q-29




i-C


3


H


7






4-OCF


2


H






Q-57




i-C


3


H


7






4-CN




Q-57




i-C


3


H


7






2-F, 4-Cl




Q-57




i-C


3


H


7






4-OCF


2


H






Q-71




i-C


3


H


7






4-CN




Q-71




i-C


3


H


7






2-F, 4-Cl




Q-71




i-C


3


H


7






4-OCF


2


H






Q-100




i-C


3


H


7






4-CN




Q-100




i-C


3


H


7






2-F, 4-Cl




Q-100




i-C


3


H


7






4-OCF


2


H






Q-119




i-C


3


H


7






4-CN




Q-119




i-C


3


H


7






2-F, 4-Cl




Q-119




i-C


3


H


7






4-OCF


2


H






Q-120




i-C


3


H


7






4-CN




Q-120




i-C


3


H


7






2-F, 4-Cl




Q-120




i-C


3


H


7






4-OCF


2


H






Q-126




i-C


3


H


7






4-CN




Q-126




i-C


3


H


7






2-F, 4-Cl




Q-126




i-C


3


H


7






4-OCF


2


H






Q-130




i-C


3


H


7






4-CN




Q-130




i-C


3


H


7






2-F, 4-Cl




Q-130




i-C


3


H


7






4-OCF


2


H






Q-144




i-C


3


H


7






4-CN




Q-144




i-C


3


H


7






2-F,4-Cl




Q-144




i-C


3


H


7






4-OCF


2


H






Q-162




i-C


3


H


7






4-CN




Q-162




i-C


3


H


7






2-F, 4-Cl




Q-162




i-C


3


H


7






4-OCF


2


H






Q-169




i-C


3


H


7






4-CN




Q-169




i-C


3


H


7






2-F, 4-Cl




Q-169




i-C


3


H


7






4-OCF


2


H






Q-2




i-C


3


H


7






4-NO


2






Q-2




i-C


3


H


7






3,4-di-F




Q-2




i-C


3


H


7






4-SCH


3








Q-16




i-C


3


H


7






4-NO


2






Q-16




i-C


3


H


7






3,4-di-F




Q-16




i-C


3


H


7






4-SCH


3








Q-24




i-C


3


H


7






4-NO


2






Q-24




i-C


3


H


7






3,4-di-F




Q-24




i-C


3


H


7






4-SCH


3








Q-29




i-C


3


H


7






4-NO


2






Q-29




i-C


3


H


7






3,4-di-F




Q-29




i-C


3


H


7






4-SCH


3








Q-57




i-C


3


H


7






4-NO


2






Q-57




i-C


3


H


7






3,4-di-F




Q-57




i-C


3


H


7






4-SCH


3








Q-71




i-C


3


H


7






4-NO


2






Q-71




i-C


3


H


7






3,4-di-F




Q-71




i-C


3


H


7






4-SCH


3








Q-100




i-C


3


H


7






4-NO


2






Q-100




i-C


3


H


7






3,4-di-F




Q-100




i-C


3


H


7






4-SCH


3








Q-119




i-C


3


H


7






4-NO


2






Q-119




i-C


3


H


7






3,4-di-F




Q-119




i-C


3


H


7






4-SCH


3








Q-120




i-C


3


H


7






4-NO


2






Q-120




i-C


3


H


7






3,4-di-F




Q-120




i-C


3


H


7






4-SCH


3








Q-126




i-C


3


H


7






4-NO


2






Q-126




i-C


3


H


7






3,4-di-F




Q-126




i-C


3


H


7






4-SCH


3








Q-130




i-C


3


H


7






4-NO


2






Q-130




i-C


3


H


7






3,4-di-F




Q-130




i-C


3


H


7






4-SCH


3








Q-144




i-C


3


H


7






4-NO


2






Q-144




i-C


3


H


7






3,4-di-F




Q-144




1-C


3


H


7






4-SCH


3








Q-162




i-C


3


H


7






4-NO


2






Q-162




i-C


3


H


7






3,4-di-F




Q-162




i-C


3


H


7






4-SCH


3








Q-169




i-C


3


H


7






4-NO


2






Q-169




i-C


3


H


7






3,4-di-F




Q-169




i-C


3


H


7






4-SCH


3
























Q




R


2






R


13






Q




R


2






R


13






Q




R


2






R


13











Q-2




Allyl




4-F




Q-2




Allyl




2,4-di-F




Q-2




Allyl




4-Cl






Q-16




Allyl




4-F




Q-16




Allyl




2,4-di-F




Q-16




Allyl




4-Cl






Q-24




Allyl




4-F




Q-24




Allyl




2,4-di-F




Q-24




Allyl




4-Cl






Q-29




Allyl




4-F




Q-29




Allyl




2,4-di-F




Q-29




Allyl




4-Cl






Q-57




Allyl




4-F




Q-57




Allyl




2,4-di-F




Q-57




Allyl




4-Cl






Q-71




Allyl




4-F




Q-71




Allyl




2,4-di-F




Q-71




Allyl




4-Cl






Q-100




Allyl




4-F




Q-100




Allyl




2,4-di-F




Q-100




Allyl




4-Cl






Q-119




Allyl




4-F




Q-119




Allyl




2,4-di-F




Q-119




Allyl




4-Cl






Q-120




Allyl




4-F




Q-120




Allyl




2,4-di-F




Q-120




Allyl




4-Cl






Q-126




Allyl




4-F




Q-126




Allyl




2,4-di-F




Q-126




Allyl




4-Cl






Q-130




Allyl




4-F




Q-130




Allyl




2,4-di-F




Q-130




Allyl




4-Cl






Q-144




Allyl




4-F




Q-144




Allyl




2,4-di-F




Q-144




Allyl




4-Cl






Q-162




Allyl




4-F




Q-162




Allyl




2,4-di-F




Q-162




Allyl




4-Cl






Q-169




Allyl




4-F




Q-169




Allyl




2,4-di-F




Q-169




Allyl




4-Cl






Q-2




OCH


3






4-F




Q-2




OCH


3






2,4-di-F




Q-2




OCH


3






4-Cl






Q-16




OCH


3






4-F




Q-16




OCH


3






2,4-di-F




Q-16




OCH


3






4-Cl






Q-24




OCH


3






4-F




Q-24




OCH


3






2,4-di-F




Q-24




OCH


3






4-Cl






Q-29




OCH


3






4-F




Q-29




OCH


3






2,4-di-F




Q-29




OCH


3






4-Cl






Q-57




OCH


3






4-F




Q-57




OCH


3






2,4-di-F




Q-57




OCH


3






4-Cl






Q-71




OCH


3






4-F




Q-71




OCH


3






2,4-di-F




Q-71




OCH


3






4-Cl






Q-100




OCH


3






4-F




Q-100




OCH


3






2,4-di-F




Q-100




OCH


3






4-Cl






Q-119




OCH


3






4-F




Q-119




OCH


3






2,4-di-F




Q-119




OCH


3






4-Cl






Q-120




OCH


3






4-F




Q-120




OCH


3






2,4-di-F




Q-120




OCH


3






4-Cl






Q-126




OCH


3






4-F




Q-126




OCH


3






2,4-di-F




Q-126




OCH


3






4-Cl






Q-130




OCH


3






4-F




Q-130




OCH


3






2,4-di-F




Q-130




OCH


3






4-Cl






Q-144




OCH


3






4-F




Q-144




OCH


3






2,4-di-F




Q-144




OCH


3






4-Cl






Q-162




OCH


3






4-F




Q-162




OCH


3






2,4-di-F




Q-162




OCH


3






4-Cl






Q-169




OCH


3






4-F




Q-169




OCH


3






2,4-di-F




Q-169




OCH


3






4-Cl






Q-2




N(CH


3


)


2






4-F




Q-2




N(CH


3


)


2






2,4-di-F




Q-2




N(CH


3


)


2






4-Cl






Q-16




N(CH


3


)


2






4-F




Q-16




N(CH


3


)


2






2,4-di-F




Q-16




N(CH


3


)


2






4-Cl






Q-24




N(CH


3


)


2






4-F




Q-24




N(CH


3


)


2






2,4-di-F




Q-24




N(CH


3


)


2






4-Cl






Q-29




N(CH


3


)


2






4-F




Q-29




N(CH


3


)


2






2,4-di-F




Q-29




N(CH


3


)


2






4-Cl






Q-57




N(CH


3


)


2






4-F




Q-57




N(CH


3


)


2






2,4-di-F




Q-57




N(CH


3


)


2






4-Cl






Q-71




N(CH


3


)


2






4-F




Q-71




N(CH


3


)


2






2,4-di-F




Q-71




N(CH


3


)


2






4-Cl






Q-100




N(CH


3


)


2






4-F




Q-100




N(CH


3


)


2






2,4-di-F




Q-100




N(CH


3


)


2






4-Cl






Q-119




N(CH


3


)


2






4-F




Q-119




N(CH


3


)


2






2,4-di-F




Q-119




N(CH


3


)


2






4-Cl






Q-120




N(CH


3


)


2






4-F




Q-120




N(CH


3


)


2






2,4-di-F




Q-120




N(CH


3


)


2






4-Cl






Q-126




N(CH


3


)


2






4-F




Q-126




N(CH


3


)


2






2,4-di-F




Q-126




N(CH


3


)


2






4-Cl






Q-130




N(CH


3


)


2






4-F




Q-130




N(CH


3


)


2






2,4-di-F




Q-130




N(CH


3


)


2






4-Cl






Q-144




N(CH


3


)


2






4-F




Q-144




N(CH


3


)


2






2,4-di-F




Q-144




N(CH


3


)


2






4-Cl






Q-162




N(CH


3


)


2






4-F




Q-162




N(CH


3


)


2






2,4-di-F




Q-162




N(CH


3


)


2






4-Cl






Q-169




N(CH


3


)


2






4-F




Q-169




N(CH


3


)


2






2,4-di-F




Q-169




N(CH


3


)


2






4-Cl






Q-2




CH


2


OCH


3






4-F




Q-2




CH


2


OCH


3






2,4-di-F




Q-2




CH


2


OCH


3






4-Cl






Q-16




CH


2


OCH


3






4-F




Q-16




CH


2


OCH


3






2,4-di-F




Q-16




CH


2


OCH


3






4-Cl






Q-24




CH


2


OCH


3






4-F




Q-24




CH


2


OCH


3






2,4-di-F




Q-24




CH


2


OCH


3






4-Cl






Q-29




CH


2


OCH


3






4-F




Q-29




CH


2


OCH


3






2,4-di-F




Q-29




CH


2


OCH


3






4-Cl






Q-57




CH


2


OCH


3






4-F




Q-57




CH


2


OCH


3






2,4-di-F




Q-57




CH


2


OCH


3






4-Cl






Q-71




CH


2


OCH


3






4-F




Q-71




CH


2


OCH


3






2,4-di-F




Q-71




CH


2


OCH


3






4-Cl






Q-100




CH


2


OCH


3






4-F




Q-100




CH


2


OCH


3






2,4-di-F




Q-100




CH


2


OCH


3






4-Cl






Q-119




CH


2


OCH


3






4-F




Q-119




CH


2


OCH


3






2,4-di-F




Q-119




CH


2


OCH


3






4-Cl






Q-120




CH


2


OCH


3






4-F




Q-120




CH


2


OCH


3






2,4-di-F




Q-120




CH


2


OCH


3






4-Cl






Q-126




CH


2


OCH


3






4-F




Q-126




CH


2


OCH


3






2,4-di-F




Q-126




CH


2


OCH


3






4-Cl






Q-130




CH


2


OCH


3






4-F




Q-130




CH


2


OCH


3






2,4-di-F




Q-130




CH


2


OCH


3






4-Cl






Q-144




CH


2


OCH


3






4-F




Q-144




CH


2


OCH


3






2,4-di-F




Q-144




CH


2


OCH


3






4-Cl






Q-162




CH


2


OCH


3






4-F




Q-162




CH


2


OCH


3






2,4-di-F




Q-162




CH


2


OCH


3






4-Cl






Q-169




CH


2


OCH


3






4-F




Q-169




CH


2


OCH


3






2,4-di-F




Q-169




CH


2


OCH


3






4-Cl






Q-2




CH


2


CF


3






4-F




Q-2




CH


2


CF


3






2,4-di-F




Q-2




CH


2


CF


3






4-Cl






Q-16




CH


2


CF


3






4-F




Q-16




CH


2


CF


3






2,4-di-F




Q-16




CH


2


CF


3






4-Cl






Q-24




CH


2


CF


3






4-F




Q-24




CH


2


CF


3






2,4-di-F




Q-24




CH


2


CF


3






4-Cl






Q-29




CH


2


CF


3






4-F




Q-29




CH


2


CF


3






2,4-di-F




Q-29




CH


2


CF


3






4-Cl






Q-57




CH


2


CF


3






4-F




Q-57




CH


2


CF


3






2,4-di-F




Q-57




CH


2


CF


3






4-Cl






Q-71




CH


2


CF


3






4-F




Q-71




CH


2


CF


3






2,4-di-F




Q-71




CH


2


CF


3






4-Cl






Q-100




CH


2


CF


3






4-F




Q-100




CH


2


CF


3






2,4-di-F




Q-100




CH


2


CF


3






4-Cl






Q-119




CH


2


CF


3






4-F




Q-119




CH


2


CF


3






2,4-di-F




Q-119




CH


2


CF


3






4-Cl






Q-120




CH


2


CF


3






4-F




Q-120




CH


2


CF


3






2,4-di-F




Q-120




CH


2


CF


3






4-Cl






Q-126




CH


2


CF


3






4-F




Q-126




CH


2


CF


3






2,4-di-F




Q-126




CH


2


CF


3






4-Cl






Q-130




CH


2


CF


3






4-F




Q-130




CH


2


CF


3






2,4-di-F




Q-130




CH


2


CF


3






4-Cl






Q-144




CH


2


CF


3






4-F




Q-144




CH


2


CF


3






2,4-di-F




Q-144




CH


2


CF


3






4-Cl






Q-162




CH


2


CF


3






4-F




Q-162




CH


2


CF


3






2,4-di-F




Q-162




CH


2


CF


3






4-Cl






Q-169




CH


2


CF


3






4-F




Q-169




CH


2


CF


3






2,4-di-F




Q-169




CH


2


CF


3






4-Cl






















TABLE 2




























R


1


is C


2


H


5


, R


2


is B-1



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175














R


1


is i-C


3


H


7


, R


2


is B-4



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175














R


1


is C


2


H


5


, R


2


is B-4



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175














R


1


is C


2


H


5


, R


2


is B-10



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175














R


1


i-C


3


H


7


, R


2


is B-10



















Q




Q




Q




Q




Q




Q




Q




Q




Q









Q-1




Q-2




Q-3




Q-4




Q-5




Q-6




Q-7




Q-8




Q-9






Q-10




Q-11




Q-12




Q-13




Q-14




Q-15




Q-16




Q-17




Q-18






Q-19




Q-20




Q-21




Q-22




Q-23




Q-24




Q-25




Q-26




Q-27






Q-28




Q-29




Q-30




Q-31




Q-32




Q-33




Q-34




Q-35




Q-36






Q-37




Q-38




Q-39




Q-40




Q-41




Q-42




Q-43




Q-44




Q-45






Q-46




Q-47




Q-48




Q-49




Q-50




Q-51




Q-52




Q-53




Q-54






Q-55




Q-56




Q-57




Q-58




Q-59




Q-60




Q-61




Q-62




Q-63






Q-64




Q-65




Q-66




Q-67




Q-68




Q-69




Q-70




Q-71




Q-72






Q-73




Q-74




Q-75




Q-76




Q-77




Q-78




Q-79




Q-80




Q-81






Q-82




Q-83




Q-84




Q-85




Q-86




Q-87




Q-88




Q-89




Q-90






Q-91




Q-92




Q-93




Q-94




Q-95




Q-96




Q-97




Q-98




Q-99






Q-100




Q-101




Q-102




Q-103




Q-104




Q-105




Q-106




Q-107




Q-108






Q-109




Q-110




Q-111




Q-112




Q-113




Q-114




Q-115




Q-116




Q-117






Q-118




Q-119




Q-120




Q-121




Q-122




Q-123




Q-124




Q-125




Q-126






Q-127




Q-128




Q-129




Q-130




Q-131




Q-132




Q-133




Q-134




Q-135






Q-136




Q-137




Q-138




Q-139




Q-140




Q-141




Q-142




Q-143




Q-144






Q-145




Q-146




Q-147




Q-148




Q-149




Q-150




Q-151




Q-152




Q-153






Q-154




Q-155




Q-156




Q-157




Q-158




Q-159




Q-160




Q-161




Q-162






Q-163




Q-164




Q-165




Q-166




Q-167




Q-168




Q-169




Q-170




Q-171






Q-172




Q-173




Q-174




Q-175






















Q




R


1






R


2






Q




R


1






R


2






Q




R


1






R


2











Q-2




Cyclopropyl




B-10




Q-2




Allyl




B-4




Q-2




Cyclohexyl




B-18






Q-16




Cyclopropyl




B-10




Q-16




Allyl




B-4




Q-16




Cyclohexyl




B-18






Q-24




Cyclopropyl




B-10




Q-24




Allyl




B-4




Q-24




Cyclohexyl




B-18






Q-29




Cyclopropyl




B-10




Q-29




Allyl




B-4




Q-29




Cyclohexyl




B-18






Q-57




Cyclopropyl




B-10




Q-57




Allyl




B-4




Q-57




Cyclohexyl




B-18






Q-71




Cyclopropyl




B-10




Q-71




Allyl




B-4




Q-71




Cyclohexyl




B-18






Q-100




Cyclopropyl




B-10




Q-100




Allyl




B-4




Q- 100




Cyclohexyl




B-18






Q-119




Cyclopropyl




B-10




Q-119




Allyl




B-4




Q-119




Cyclohexyl




B-18






Q-120




Cyclopropyl




B-10




Q-120




Allyl




B-4




Q-120




Cyclohexyl




B-18






Q-126




Cyclopropyl




B-10




Q-126




Allyl




B-4




Q-126




Cyclohexyl




B-18






Q-130




Cyclopropyl




B-10




Q-130




Allyl




B-4




Q-130




Cyclohexyl




B-18






Q-144




Cyclopropyl




B-10




Q-144




Allyl




B-4




Q-144




Cyclohexyl




B-18






Q-162




Cyclopropyl




B-10




Q-162




Allyl




B-4




Q-162




Cyclohexyl




B-18






Q-169




Cyclopropyl




B-10




Q-169




Allyl




B-4




Q-169




Cyclohexyl




B-18






Q-2




n-C


4


H


9






B-10




Q-2




Cyclopropyl




B-4




Q-2




i-C


3


H


7






B-18






Q-16




n-C


4


H


9






B-10




Q-16




Cyclopropyl




B-4




Q-16




i-C


3


H


7






B-18






Q-24




n-C


4


H


9






B-10




Q-24




Cyclopropyl




B-4




Q-24




i-C


3


H


7






B-18






Q-29




n-C


4


H


9






B-10




Q-29




Cyclopropyl




B-4




Q-29




i-C


3


H


7






B-18






Q-57




n-C


4


H


9






B-10




Q-57




Cyclopropyl




B-4




Q-57




i-C


3


H


7






B-18






Q-71




n-C


4


H


9






B-10




Q-71




Cyclopropyl




B-4




Q-71




i-C


3


H


7






B-18






Q-100




n-C


4


H


9






B-10




Q-100




Cyclopropyl




B-4




Q-100




i-C


3


H


7






B-18






Q-119




n-C


4


H


9






B-10




Q-119




Cyclopropyl




B-4




Q-119




i-C


3


H


7






B-18






Q-120




n-C


4


H


9






B-10




Q-120




Cyclopropyl




B-4




Q-120




i-C


3


H


7






B-18






Q-126




n-C


4


H


9






B-10




Q-126




Cyclopropyl




B-4




Q-126




i-C


3


H


7






B-18






Q-130




n-C


4


H


9






B-10




Q-130




Cyclopropyl




B-4




Q-130




i-C


3


H


7






B-18






Q-144




n-C


4


H


9






B-10




Q-144




Cyclopropyl




B-4




Q-144




i-C


3


H


7






B-18






Q-162




n-C


4


H


9






B-10




Q-162




Cyclopropyl




B-4




Q-162




i-C


3


H


7






B-18






Q-169




n-C


4


H


9






B-10




Q-169




Cyclopropyl




B-4




Q-169




i-C


3


H


7






B-18






Q-2




CH


2


CH


2


OCH


3






B-10




Q-2




CH


3






B-4




Q-2




Cyclohexyl




B-17






Q-16




CH


2


CH


2


OCH


3






B-10




Q-16




CH


3






B-4




Q-16




Cyclohexyl




B-17






Q-24




CH


2


CH


2


OCH


3






B-10




Q-24




CH


3






B-4




Q-24




Cyclohexyl




B-17






Q-29




CH


2


CH


2


OCH


3






B-10




Q-29




CH


3






B-4




Q-29




Cyclohexyl




B-17






Q-57




CH


2


CH


2


OCH


3






B-10




Q-57




CH


3






B-4




Q-57




Cyclohexyl




B-17






Q-71




CH


2


CH


2


OCH


3






B-10




Q-71




CH


3






B-4




Q-71




Cyclohexyl




B-17






Q-100




CH


2


CH


2


OCH


3






B-10




Q-100




CH


3






B-4




Q-100




Cyclohexyl




B-17






Q-119




CH


2


CH


2


OCH


3






B-10




Q-119




CH


3






B-4




Q-119




Cyclobexyl




B-17






Q-120




CH


2


CH


2


CCH


3






B-10




Q-120




CH


3






B-4




Q-120




Cyclohexyl




B-17






Q-126




CH


2


CH


2


OCH


3






B-10




Q-126




CH


3






B-4




Q-126




Cyclohexyl




B-17






Q-130




CH


2


CH


2


OCH


3






B-10




Q-130




CH


3






B-4




Q-130




Cyclohexyl




B-17






Q-144




CH


2


CH


2


OCH


3






B-10




Q-144




CH


3






B-4




Q-144




Cyclohexyl




B-17






Q-162




CH


2


CH


2


OCH


3






B-10




Q-162




CH


3






B-4




Q-162




Cyclohexyl




B-17






Q-169




CH


2


CH


2


OCH


3






B-10




Q-169




CH


3






B-4




Q-169




Cyclohexyl




B-17






Q-2




CH


3






B-10




Q-2




CH


3






B-4




Q-2




C


2


H


5






B-17






Q-16




CH


3






B-10




Q-16




CH


3






B-4




Q-16




C


2


H


5






B-17






Q-24




CH


3






B-10




Q-24




CH


3






B-4




Q-24




C


2


H


5






B-17






Q-29




CH


3






B-10




Q-29




CH


3






B-4




Q-29




C


2


H


5






B-17






Q-57




CH


3






B-10




Q-57




CH


3






B-4




Q-57




C


2


H


5






B-17






Q-71




CH


3






B-10




Q-71




CH


3






B-4




Q-71




C


2


H


5






B-17






Q-100




CH


3






B-10




Q-100




CH


3






B-4




Q-100




C


2


H


5






B-17






Q-119




CH


3






B-10




Q-119




CH


3






B-4




Q-119




C


2


H


5






B-17






Q-120




CH


3






B-10




Q-120




CH


3






B-4




Q-120




C


2


H


5






B-17






Q-126




CH


3






B-10




Q-126




CH


3






B-4




Q-126




C


2


H


5






B-17






Q-130




CH


3






B-10




Q-130




CH


3






B-4




Q-130




C


2


H


5






B-17






Q-144




CH


3






B-10




Q-144




CH


3






B-4




Q-144




C


2


H


5






B-17






Q-162




CH


3






B-10




Q-162




CH


3






B-4




Q-162




C


2


H


5






B-17






Q-169




CH


3






B-10




Q-169




CH


3






B-4




Q-169




C


2


H


5






B-17






Q-2




n-C


6


H


13






B-10




Q-2




CH


2


CF


3






B-4




Q-2




n-C


3


H


7






B-6






Q-16




n-C


6


H


13






B-10




Q-16




CH


2


CF


3






B-4




Q-16




n-C


3


H


7






B-6






Q-24




n-C


6


H


13






B-10




Q-24




CH


2


CF


3






B-4




Q-24




n-C


3


H


7






B-6






Q-29




n-C


6


H


13






B-10




Q-29




CH


2


CF


3






B-4




Q-29




n-C


3


H


7






B-6






Q-57




n-C


6


H


13






B-10




Q-57




CH


2


CF


3






B-4




Q-57




n-C


3


H


7






B-6






Q-71




n-C


6


H


13






B-10




Q-71




CH


2


CF


3






B-4




Q-71




n-C


3


H


7






B-6






Q-100




n-C


6


H


13






B-10




Q-100




CH


2


CF


3






B-4




Q-100




n-C


3


H


7






B-6






Q-119




n-C


6


H


13






B-10




Q-119




CH


2


CF


3






B-4




Q-119




n-C


3


H


7






B-6






Q-120




n-C


6


H


13






B-10




Q-120




CH


2


CF


3






B-4




Q-120




n-C


3


H


7






B-6






Q-126




n-C


6


H


13






B-10




Q-126




CH


2


CF


3






B-4




Q-126




n-C


3


H


7






B-6






Q-130




n-C


6


H


13






B-10




Q-130




CH


2


CF


3






B-4




Q-130




n-C


3


H


7






B-6






Q-144




n-C


6


H


13






B-10




Q-144




CH


2


CF


3






B-4




Q-144




n-C


3


H


7






B-6






Q-162




n-C


6


H


13






B-10




Q-162




CH


2


CF


3






B-4




Q-162




n-C


3


H


7






B-6






Q-169




n-C


6


H


13






B-10




Q-169




CH


2


CF


3






B-4




Q-169




n-C


3


H


7






B-6






















Q




R


1






R


2






Q




R


1






R


2






Q




R


1






R


2











Q-2




C


2


H


5






B-2




Q-2




C


2


H


5






B-5




Q-2




C


2


H


5






B-8






Q-16




C


2


H


5






B-2




Q-16




C


2


H


5






B-5




Q-16




C


2


H


5






B-8






Q-24




C


2


H


5






B-2




Q-24




C


2


H


5






B-5




Q-24




C


2


H


5






B-8






Q-29




C


2


H


5






B-2




Q-29




C


2


H


5






B-5




Q-29




C


2


H


5






B-8






Q-57




C


2


H


5






B-2




Q-57




C


2


H


5






B-5




Q-57




C


2


H


5






B-8






Q-71




C


2


H


5






B-2




Q-71




C


2


H


5






B-5




Q-71




C


2


H


5






B-8






Q-100




C


2


H


5






B-2




Q-100




C


2


H


5






B-5




Q-100




C


2


H


5






B-8






Q-119




C


2


H


5






B-2




Q-119




C


2


H


5






B-5




Q-119




C


2


H


5






B-8






Q-120




C


2


H


5






B-2




Q-120




C


2


H


5






B-5




Q-120




C


2


H


5






B-8






Q-126




C


2


H


5






B-2




Q-126




C


2


H


5






B-5




Q-126




C


2


H


5






B-8






Q-130




C


2


H


5






B-2




Q-130




C


2


H


5






B-5




Q-130




C


2


H


5






B-8






Q-144




C


2


H


5






B-2




Q-144




C


2


H


5






B-5




Q-144




C


2


H


5






B-8






Q-162




C


2


H


5






B-2




Q-162




C


2


H


5






B-5




Q-162




C


2


H


5






B-8






Q-169




C


2


H


5






B-2




Q-169




C


2


H


5






B-5




Q-169




C


2


H


5






B-8






Q-2




C


3


H


7






B-2




Q-2




i-C


3


H


7






B-6




Q-2




Cyclopropyl




B-8






Q-16




C


3


H


7






B-2




Q-16




i-C


3


H


7






B-6




Q-16




Cyclopropyl




B-8






Q-24




C


3


H


7






B-2




Q-24




i-C


3


H


7






B-6




Q-24




Cyclopropyl




B-8






Q-29




C


3


H


7






B-2




Q-29




i-C


3


H


7






B-6




Q-29




Cyclopropyl




B-8






Q-57




C


3


H


7






B-2




Q-57




i-C


3


H


7






B-6




Q-57




Cyclopropyl




B-8






Q-71




C


3


H


7






B-2




Q-71




i-C


3


H


7






B-6




Q-71




Cyclopropyl




B-8






Q-100




C


3


H


7






B-2




Q-100




i-C


3


H


7






B-6




Q-100




Cyclopropyl




B-8






Q-119




C


3


H


7






B-2




Q-119




i-C


3


H


7






B-6




Q-119




Cyclopropyl




B-8






Q-120




C


3


H


7






B-2




Q-120




i-C


3


H


7






B-6




Q-120




Cyclopropyl




B-8






Q-126




C


3


H


7






B-2




Q-126




i-C


3


H


7






B-6




Q-126




Cyclopropyl




B-8






Q-130




C


3


H


7






B-2




Q-130




i-C


3


H


7






B-6




Q-130




Cyclopropyl




B-8






Q-144




C


3


H


7






B-2




Q-144




i-C


3


H


7






B-6




Q-144




Cyclopropyl




B-8






Q-162




C


3


H


7






B-2




Q-162




i-C


3


H


7






B-6




Q-162




Cyclopropyl




B-8






Q-169




C


3


H


7






B-2




Q-169




i-C


3


H


7






B-6




Q-169




Cyclopropyl




B-8






Q-2




C


2


H


5






B-3




Q-2




C


2


H


5






B-6




Q-2




C


2


H


5






B-9






Q-16




C


2


H


5






B-3




Q-16




C


2


H


5






B-6




Q-16




C


2


H


5






B-9






Q-24




C


2


H


5






B-3




Q-24




C


2


H


5






B-6




Q-24




C


2


H


5






B-9






Q-29




C


2


H


5






B-3




Q-29




C


2


H


5






B-6




Q-29




C


2


H


5






B-9






Q-57




C


2


H


5






B-3




Q-57




C


2


H


5






B-6




Q-57




C


2


H


5






B-9






Q-71




C


2


H


5






B-3




Q-71




C


2


H


5






B-6




Q-71




C


2


H


5






B-9






Q-100




C


2


H


5






B-3




Q-100




C


2


H


5






B-6




Q-100




C


2


H


5






B-9






Q-119




C


2


H


5






B-3




Q-119




C


2


H


5






B-6




Q-119




C


2


H


5






B-9






Q-120




C


2


H


5






B-3




Q-120




C


2


H


5






B-6




Q-120




C


2


H


5






B-9






Q-126




C


2


H


5






B-3




Q-126




C


2


H


5






B-6




Q-126




C


2


H


5






B-9






Q-130




C


2


H


5






B-3




Q-130




C


2


H


5






B-6




Q-130




C


2


H


5






B-9






Q-144




C


2


H


5






B-3




Q-144




C


2


H


5






B-6




Q-144




C


2


H


5






B-9






Q-162




C


2


H


5






B-3




Q-162




C


2


H


5






B-6




Q-162




C


2


H


5






B-9






Q-169




C


2


H


5






B-3




Q-169




C


2


H


5






B-6




Q-169




C


2


H


5






B-9






Q-2




i-C


3


H


7






B-3




Q-2




C


2


H


5






B-7




Q-2




i-C


3


H


7






B-9






Q-16




i-C


3


H


7






B-3




Q-16




C


2


H


5






B-7




Q-16




i-C


3


H


7






B-9






Q-24




i-C


3


H


7






B-3




Q-24




C


2


H


5






B-7




Q-24




i-C


3


H


7






B-9






Q-29




i-C


3


H


7






B-3




Q-29




C


2


H


5






B-7




Q-29




I-C


3


H


7






B-9






Q-57




i-C


3


H


7






B-3




Q-57




C


2


H


5






B-7




Q-57




i-C


3


H


7






B-9






Q-71




i-C


3


H


7






B-3




Q-71




C


2


H


5






B-7




Q-71




i-C


3


H


7






B-9






Q-100




i-C


3


H


7






B-3




Q-100




C


2


H


5






B-7




Q-100




i-C


3


H


7






B-9






Q-119




i-C


3


H


7






B-3




Q-119




C


2


H


5






B-7




Q-119




i-C


3


H


7






B-9






Q-120




i-C


3


H


7






B-3




Q-120




C


2


H


5






B-7




Q-120




i-C


3


H


7






B-9






Q-126




i-C


3


H


7






B-3




Q-126




C


2


H


5






B-7




Q-126




i-C


3


H


7






B-9






Q-130




i-C


3


H


7






B-3




Q-130




C


2


H


5






B-7




Q-130




i-C


3


H


7






B-9






Q-144




i-C


3


H


7






B-3




Q-144




C


2


H


5






B-7




Q-144




i-C


3


H


7






B-9






Q-162




i-C


3


H


7






B-3




Q-162




C


2


H


5






B-7




Q-162




i-C


3


H


7






B-9






Q-169




i-C


3


H


7






B-3




Q-169




C


2


H


5






B-7




Q-169




i-C


3


H


7






B-9






Q-2




C


2


H


5






B-4




Q-2




i-C


3


H


7






B-7




Q-2




C


2


H


5






B-11






Q-16




C


2


H


5






B-4




Q-16




i-C


3


H


7






B-7




Q-16




C


2


H


5






B-11






B-24




C


2


H


5






B-4




Q-24




i-C


3


H


7






B-7




Q-24




C


2


H


5






B-11






Q-29




C


2


H


5






B-4




Q-29




i-C


3


H


7






B-7




Q-29




C


2


H


5






B-11






Q-57




C


2


H


5






B-4




Q-57




i-C


3


H


7






B-7




Q-57




C


2


H


5






B-11






Q-71




C


2


H


5






B-4




Q-71




i-C


3


H


7






B-7




Q-71




C


2


H


5






B-11






Q-100




C


2


H


5






B-4




Q-100




i-C


3


H


7






B-7




Q-100




C


2


H


5






B-11






Q-119




C


2


H


5






B-4




Q-119




i-C


3


H


7






B-7




Q-119




C


2


H


5






B-11






Q-120




C


2


H


5






B-4




Q-120




i-C


3


H


7






B-7




Q-120




C


2


H


5






B-11






Q-126




C


2


H


5






B-4




Q-126




i-C


3


H


7






B-7




Q-126




C


2


H


5






B-11






Q-130




C


2


H


5






B-4




Q-130




i-C


3


H


7






B-7




Q-130




C


2


H


5






B-11






Q-144




C


2


H


5






B-4




Q-144




i-C


3


H


7






B-7




Q-144




C


2


H


5






B-11






Q-162




C


2


H


5






B-4




Q-162




i-C


3


H


7






B-7




Q-162




C


2


H


5






B-11






Q-169




C


2


H


5






B-4




Q-169




i-C


3


H


7






B-7




Q-169




C


2


H


5






B-11






















Q




R


1






R


2






Q




R


1






R


2






Q




R


1






R


2











Q-2




Cyclopropyl




B-11




Q-2




C


2


H


5






B-14




Q-2




i-C


3


H


7






B-16






Q-16




Cyclopropyl




B-11




Q-16




C


2


H


5






B-14




Q-16




i-C


3


H


7






B-16






Q-24




Cyclopropyl




B-11




Q-24




C


2


H


5






B-14




Q-24




i-C


3


H


7






B-16






Q-29




Cyclopropyl




B-11




Q-29




C


2


H


5






B-14




Q-29




i-C


3


H


7






B-16






Q-57




Cyclopropyl




B-11




Q-57




C


2


H


5






B-14




Q-57




i-C


3


H


7






B-16






Q-71




Cyclopropyl




B-11




Q-71




C


2


H


5






B-14




Q-71




i-C


3


H


7






B-16






Q-100




Cyclopropyl




B-11




Q-100




C


2


H


5






B-14




Q-100




i-C


3


H


7






B-16






Q-119




Cyclopropyl




B-11




Q-119




C


2


H


5






B-14




Q-119




i-C


3


H


7






B-16






Q-120




Cyclopropyl




B-11




Q-120




C


2


H


5






B-14




Q-120




i-C


3


H


7






B-16






Q-126




Cyclopropyl




B-11




Q-126




C


2


H


5






B-14




Q-126




i-C


3


H


7






B-16






Q-130




Cyclopropyl




B-11




Q-130




C


2


H


5






B-14




Q-130




i-C


3


H


7






B-16






Q-144




Cyclopropyl




B-11




Q-144




C


2


H


5






B-14




Q-144




i-C


3


H


7






B-16






Q-162




Cyclopropyl




B-11




Q-162




C


2


H


5






B-14




Q-162




i-C


3


H


7






B-16






Q-169




Cyclopropyl




B-11




Q-169




C


2


H


5






B-14




Q-169




i-C


3


H


7






B-16






Q-2




C


2


H


5






B-12




Q-2




i-C


3


H


7






B-14




Q-2




t-C


4


H


9






B-10






Q-16




C


2


H


5






B-12




Q-16




i-C


3


H


7






B-14




Q-16




t-C


4


H


9






B-10






Q-24




C


2


H


5






B-12




Q-24




i-C


3


H


7






B-14




B-24




t-C


4


H


9






B-10






Q-29




C


2


H


5






B-12




Q-29




i-C


3


H


7






B-14




B-29




t-C


4


H


9






B-10






Q-57




C


2


H


5






B-12




Q-57




i-C


3


H


7






B-14




Q-57




t-C


4


H


9






B-10






Q-71




C


2


H


5






B-12




Q-71




i-C


3


H


7






B-14




Q-71




t-C


4


H


9






B-10






Q-100




C


2


H


5






B-12




Q-100




i-C


3


H


7






B-14




Q-100




t-C


4


H


9






B-10






Q-119




C


2


H


5






B-12




Q-119




i-C


3


H


7






B-14




Q-119




t-C


4


H


9






B-10






Q-120




C


2


H


5






B-12




Q-120




i-C


3


H


7






B-14




Q-120




t-C


4


H


9






B-10






Q-126




C


2


H


5






B-12




Q-126




i-C


3


H


7






B-14




Q-126




t-C


4


H


9






B-10






Q-130




C


2


H


5






B-12




Q-130




i-C


3


H


7






B-14




Q-130




t-C


4


H


9






B-10






Q-144




C


2


H


5






B-12




Q-144




i-C


3


H


7






B-14




Q-144




t-C


4


H


9






B-10






Q-162




C


2


H


5






B-12




Q-162




i-C


3


H


7






B-14




Q-162




t-C


4


H


9






B-10






Q-169




C


2


H


5






B-12




Q-169




i-C


3


H


7






B-14




Q-169




t-C


4


H


9






B-10






Q-2




i-C


3


H


7






B-12




Q-2




C


2


H


5






B-15




Q-2




i-C


4


H


9






B-10






Q-16




i-C


3


H


7






B-12




Q-16




C


2


H


5






B-15




Q-16




i-C


4


H


9






B-10






Q-24




i-C


3


H


7






B-12




Q-24




C


2


H


5






B-15




Q-24




i-C


4


H


9






B-10






Q-29




i-C


3


H


7






B-12




Q-29




C


2


H


5






B-15




Q-29




i-C


4


H


9






B-10






Q-57




i-C


3


H


7






B-12




Q-57




C


2


H


5






B-15




Q-57




i-C


4


H


9






B-10






Q-71




i-C


3


H


7






B-12




Q-71




C


2


H


5






B-15




Q-71




i-C


4


H


9






B-10






Q-100




i-C


3


H


7






B-12




Q-100




C


2


H


5






B-15




Q-100




i-C


4


H


9






B-10






Q-119




i-C


3


H


7






B-12




Q-119




C


2


H


5






B-15




Q-119




i-C


4


H


9






B-10






Q-120




i-C


3


H


7






B-12




Q-120




C


2


H


5






B-15




Q-120




i-C


4


H


9






B-10






Q-126




i-C


3


H


7






B-12




Q-126




C


2


H


5






B-15




Q-126




i-C


4


H


9






B-10






Q-130




i-C


3


H


7






B-12




Q-130




C


2


H


5






B-15




Q-130




i-C


4


H


9






B-10






Q-144




i-C


3


H


7






B-12




Q-144




C


2


H


5






B-15




Q-144




i-C


4


H


9






B-10






Q-162




i-C


3


H


7






B-12




Q-162




C


2


H


5






B-15




Q-162




i-C


4


H


9






B-10






Q-169




i-C


3


H


7






B-12




Q-169




C


2


H


5






B-15




Q-169




i-C


4


H


9






B-10






Q-2




C


2


H


5






B-13




Q-2




i-C


3


H


7






B-15




Q-2




CH


2


CF


3






B-10






Q-16




C


2


H


5






B-13




Q-16




i-C


3


H


7






B-15




Q-16




CH


2


CF


3






B-10






Q-24




C


2


H


5






B-13




Q-24




i-C


3


H


7






B-15




Q-24




CH


2


CF


3






B-10






Q-29




C


2


H


5






B-13




Q-29




i-C


3


H


7






B-15




Q-29




CH


2


CF


3






B-10






Q-57




C


2


H


5






B-13




Q-57




i-C


3


H


7






B-15




Q-57




CH


2


CF


3






B-10






Q-71




C


2


H


5






B-13




Q-71




i-C


3


H


7






B-15




Q-71




CH


2


CF


3






B-10






Q-100




C


2


H


5






B-13




Q-100




i-C


3


H


7






B-15




Q-100




CH


2


CF


3






B-10






Q-119




C


2


H


5






B-13




Q-119




i-C


3


H


7






B-15




Q-119




CH


2


CF


3






B-10






Q-120




C


2


H


5






B-13




Q-120




i-C


3


H


7






B-15




Q-120




CH


2


CF


3






B-10






Q-126




C


2


H


5






B-13




Q-126




i-C


3


H


7






B-15




Q-126




CH


2


CF


3






B-10






Q-130




C


2


H


5






B-13




Q-130




i-C


3


H


7






B-15




Q-130




CH


2


CF


3






B-10






Q-144




C


2


H


5






B-13




Q-144




i-C


3


H


7






B-15




Q-144




CH


2


CF


3






B-10






Q-162




C


2


H


5






B-13




Q-162




i-C


3


H


7






B-15




Q-162




CH


2


CF


3






B-10






Q-169




C


2


H


5






B-13




Q-169




i-C


3


H


7






B-15




Q-169




CH


2


CF


3






B-10






Q-2




i-C


3


H


7






B-13




Q-2




C


2


H


5






B-16




Q-2




n-C


3


H


7






B-10






Q-16




i-C


3


H


7






B-13




Q-16




C


2


H


5






B-16




Q-16




n-C


3


H


7






B-10






Q-24




i-C


3


H


7






B-13




Q-24




C


2


H


5






B-16




Q-24




n-C


3


H


7






B-10






Q-29




i-C


3


H


7






B-13




Q-29




C


2


H


5






B-16




Q-29




n-C


3


H


7






B-10






Q-57




i-C


3


H


7






B-13




Q-57




C


2


H


5






B-16




Q-57




n-C


3


H


7






B-10






Q-71




i-C


3


H


7






B-13




Q-71




C


2


H


5






B-16




Q-71




n-C


3


H


7






B-10






Q-100




i-C


3


H


7






B-13




Q-100




C


2


H


5






B-16




Q-100




n-C


3


H


7






B-10






Q-119




i-C


3


H


7






B-13




Q-119




C


2


H


5






B-16




Q-119




n-C


3


H


7






B-10






Q-120




i-C


3


H


7






B-13




Q-120




C


2


H


5






B-16




Q-120




n-C


3


H


7






B-10






Q-126




i-C


3


H


7






B-13




Q-126




C


2


H


5






B-16




Q-126




n-C


3


H


7






B-10






Q-130




i-C


3


H


7






B-13




Q-130




C


2


H


5






B-16




Q-130




n-C


3


H


7






B-10






Q-144




i-C


3


H


7






B-13




Q-144




C


2


H


5






B-16




Q-144




n-C


3


H


7






B-10






Q-162




i-C


3


H


7






B-13




Q-162




C


2


H


5






B-16




Q-162




n-C


3


H


7






B-10






Q-169




i-C


3


H


7






B-13




Q-169




C


2


H


5






B-16




Q-169




n-C


3


H


7






B-10






















TABLE 3










































Q




X


1






X


2






X


3






R


1






R


2











i-Pr




S




O




O




i-Pr




4-F-Phenyl






i-Pr




O




S




O




i-Pr




4-F-Phenyl






i-Pr




O




O




S




i-Pr




4-F-Phenyl






i-Pr




NMe




O




O




i-Pr




4-F-Phenyl






i-Pr




O




NMe




O




i-Pr




4-F-Phenyl






i-Pr




O




O




NMe




i-Pr




4-F-Phenyl






i-Pr




NCN




O




O




i-Pr




4-F-Phenyl






i-Pr




O




NCN




O




i-Pr




4-F-Phenyl






i-Pr




O




O




NCN




i-Pr




4-F-Phenyl






i-Pr




S




S




O




i-Pr




4-F-Phenyl






i-Pr




S




O




S




i-Pr




4-F-Phenyl






i-Pr




O




S




S




i-Pr




4-F-Phenyl






i-Pr




S




S




S




i-Pr




4-F-Phenyl






c-Pr




S




O




O




i-Pr




4-F-Phenyl






c-Pr




O




S




O




i-Pr




4-F-Phenyl






c-Pr




O




O




S




i-Pr




4-F-Phenyl






c-Pr




NMe




O




O




i-Pr




4-F-Phcnyl






c-Pr




O




NMe




O




i-Pr




4-F-Phenyl






c-Pr




O




O




NMe




i-Pr




4-F-Phenyl






c-Pr




NCN




O




O




i-Pr




4-F-Phenyl






c-Pr




O




NCN




O




i-Pr




4-F-Phenyl






c-Pr




O




O




NCN




i-Pr




4-F-Phenyl






c-Pr




S




S




O




i-Pr




4-F-Phenyl






c-Pr




S




O




S




i-Pr




4-F-Phenyl






c-Pr




O




S




S




i-Pr




4-F-Phenyl






c-Pr




S




S




S




i-Pr




4-F-Phenyl






i-Pr




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






i-Pr




O




O




O




i-Pr




2-F-Pyridin-5-yl






i-Pr




O




O




O




i-Pr




2-Br-Pyridin-5-yl






i-Pr




O




O




O




i-Pr




2-Me-Pyridin-5-yl






i-Pr




O




O




O




i-Pr




2-CF


3


-Pyridin-5-yl






i-Pr




O




O




O




i-Pr




2-Cl-Pyrimidin-5-yl






i-Pr




O




O




O




i-Pr




2-F-Pyrimidin-5-yl






i-Pr




O




O




O




i-Pr




2-Br-Pyrimidin-5-yl






i-Pr




O




O




O




i-Pr




2-Me-Pyrimidin-5-yl






i-Pr




O




O




O




i-Pr




2-CF


3


-Pyrimidin-5-yl






i-Pr




O




O




O




i-Pr




2-Cl-Thien-5-yl






i-Pr




O




O




O




i-Pr




2-F-Thien-5-yl






i-Pr




O




O




O




i-Pr




2-Me-Thien-5-yl






i-Pr




O




O




O




i-Pr




Thien-2-yl






i-Pr




O




O




O




i-Pr




Pyrimidin-5-yl






i-Pr




O




O




O




i-Pr




2-Cl-Pyridazin-5-yl






i-Pr




O




O




O




i-Pr




2-Cl-1,3,4-Thiadiazol-5-yl






i-Pr




O




O




O




i-Pr




2-CF


3


-1,3,4-Thiadiazol-5-yl






i-Pr




O




O




O




i-Pr




2-Cl-Thiazol-5-yl






i-Pr




O




O




O




i-Pr




5-Cl-Thiazol-2-yl






c-Pr




O




O




O




i-Pr




Thien-2-yl






Et




O




O




O




i-Pr




Thien-2-yl






n-Pr




O




O




O




i-Pr




Thien-2-yl






Me




O




O




O




i-Pr




Thien-2-yl






i-Bu




O




O




O




i-Pr




Thien-2-yl






Allyl




O




O




O




i-Pr




Thien-2-yl






c-Hexyl




O




O




O




i-Pr




Thien-2-yl






c-Pr




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






Et




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






n-Pr




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






Me




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






i-Bu




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






Allyl




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






c-Hexyl




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






s-Bu




O




O




O




i-Pr




2-Cl-Pyridin-5-yl






s-Bu




O




O




O




i-Pr




Thien-2-yl














Formulation/Utility




Compounds of this invention will generally be used as a formulation or composition with an agriculturally suitable carrier comprising at least one of a liquid diluent, a solid diluent or a surfactant. The formulation or composition ingredients are selected to be consistent with the physical properties of the active ingredient, mode of application and environmental factors such as soil type, moisture and temperature. Useful formulations include liquids such as solutions (including emulsifiable concentrates), suspensions, emulsions (including microemulsions and/or suspoemulsions) and the like which optionally can be thickened into gels. Useful formulations further include solids such as dusts, powders, granules, pellets, tablets, films, and the like which can be water-dispersible (“wettable”) or water-soluble. Active ingredient can be (micro)encapsulated and further formed into a suspension or solid formulation; alternatively the entire formulation of active ingredient can be encapsulated (or “overcoated”). Encapsulation can control or delay release of the active ingredient. Sprayable formulations can be extended in suitable media and used at spray volumes from about one to several hundred liters per hectare. High-strength compositions are primarily used as intermediates for further formulation.




The formulations will typically contain effective amounts of active ingredient, diluent and surfactant within the following approximate ranges which add up to 100 percent by weight.


















Weight Percent















Active









Ingredient




Diluent




Surfactant


















Water-Dispersible and




 5-90




 0-94




 1-15






Water-soluble Granules,






Tablets and Powders.






Suspensions, Emulsions, Solutions




 5-50




40-95




 0-15






(including Emulsifiable






Concentrates)






Dusts




 1-25




70-99




0-5






Granules and Pellets




0.01-99  




   5-99.99




 0-15






High Strength Compositions




90-99




 0-10




0-2














Typical solid diluents are described in Watkins, et al.,


Handbook of Insecticide Dust Diluents and Carrers


, 2nd Ed., Dorland Books, Caldwell, N.J. Typical liquid diluents are described in Marsden,


Solvents Guide


, 2nd Ed., Interscience, New York, 1950


. McCutcheon's Detergents and Emulsifiers Annual


, Allured Publ. Corp., Ridgewood, N.J., as well as Sisely and Wood,


Encyclopedia of Surface Active Agents


, Chemical Publ. Co., Inc., New York, 1964, list surfactants and recommended uses. All formulations can contain minor amounts of additives to reduce foam, caking, corrosion, microbiological growth and the like, or thickeners to increase viscosity.




Surfactants include, for example, polyethoxylated alcohols, polyethoxylated alkylphenols, polyethoxylated sorbitan fatty acid esters, dialkyl sulfosuccinates, alkyl sulfates, alkylbenzene sulfonates, organosilicones, N,N-dialkyltaurates, lignin sulfonates, naphthalene sulfonate formaldehyde condensates, polycarboxylates, and polyoxyethylene/polyoxypropylene block copolymers. Solid diluents include, for example, clays such as bentonite, montmorillonite, attapulgite and kaolin, starch, sugar, silica, talc, diatomaceous earth, urea, calcium carbonate, sodium carbonate and bicarbonate, and sodium sulfate. Liquid diluents include, for example, water, N,N-dimethylformamide, dimethyl sulfoxide, N-alkylpyrrolidone, ethylene glycol, polypropylene glycol, paraffins, alkylbenzenes, alkylnaphthalenes, oils of olive, castor, linseed, tung, sesame, corn, peanut, cotton-seed, soybean, rape-seed and coconut, fatty acid esters, ketones such as cyclohexanone, 2-heptanone, isophorone and 4-hydroxy-4-methyl-2-pentanone, and alcohols such as methanol, cyclohexanol, decanol and tetrahydrofIrfuryl alcohol.




Solutions, including emulsifiable concentrates, can be prepared by simply mixing the ingredients. Dusts and powders can be prepared by blending and, usually, grinding as in a hammer mill or fluid-energy mill. Suspensions are usually prepared by wet-milling; see, for example, U.S. Pat. No. 3,060,084. Granules and pellets can be prepared by spraying the active material upon performed granular carriers or by agglomeration techniques. See Browning, “Agglomeration”,


Chemical Engineering


, Dec. 4, 1967, pp 147-48


, Perry's Chemical Engineer's Handbook


, 4th Ed., McGraw-Hill, New York, 1963, pages 8-57 and following, and WO 91/13546. Pellets can be prepared as described in U.S. Pat. No. 4,172,714. Water-dispersible and water-soluble granules can be prepared as taught in U.S. Pat. No. 4,144,050, U.S. Pat. No. 3,920,442 and DE 3,246,493. Tablets can be prepared as taught in U.S. Pat. No. 5,180,587, U.S. Pat. No. 5,232,701 and U.S. Pat. No. 5,208,030. Films can be prepared as taught in GB 2,095,558 and U.S. Pat. No. 3,299,566.




For further information regarding the art of formulation, see U.S. Pat. No. 3,235,361, Col. 6, line 16 through Col. 7, line 19 and Examples 10-41; U.S. Pat. No. 3,309,192, Col. 5, line 43 through Col. 7, line 62 and Examples 8, 12, 15, 39, 41, 52, 53, 58, 132, 138-140, 162-164, 166, 167 and 169-182; U.S. Pat. No. 2,891,855, Col. 3, line 66 through Col. 5, line 17 and Examples 1-4; Klingman,


Weed Control as a Science


, John Wiley and Sons, Inc., New York, 1961, pp 81-96; and Hance et al.,


Weed Control Handbook


, 8th Ed., Blackwell Scientific Publications, Oxford, 1989.




In the following Examples, all percentages are by weight and all formulations are prepared in conventional ways. Compound numbers refer to compounds in Index Tables A-D below.

















Example A














High Strength Concentrate








Compound 2




98.5%







silica aerogel




0.5%







synthetic amorphous fine silica




1.0%.











Example B














Wettable Powder








Compound 2




65.0%







dodecylphenol polyethylene glycol ether




2.0%







sodium ligninsulfonate




4.0%







sodium silicoaluminate




6.0%







montmorillonite (calcined)




23.0%.











Example C














Granule








Compound 2




10.0%







attapulgite granules (low volatile matter,







0.71/0.30 mm; U.S.S. No. 25-50 sieves)




90.0%.











Example D














Extruded Pellet








Compound 2




25.0%







anhydrous sodium sulfate




10.0%







crude calcium ligninsulfonate




5.0%







sodium alkylnaphthalenesulfonate




1.0%







calcium/magnesium bentonite




59.00%.















Test results indicate that the compounds of the present invention are highly active preemergent and postemergent herbicides or plant growth regulants. Many of them have utility for broad-spectrum pre- and/or postemergence weed control in areas where complete control of all vegetation is desired such as around fuel storage tanks, industrial storage areas, parking lots, drive-in theaters, air fields, river banks, irrigation and other waterways, around billboards and highway and railroad structures. Some of the compounds are useful for the control of selected grass and broadleaf weeds with tolerance to important agronomic crops which include but are not limited to alfalfa, barley, cotton, wheat, rape, sugar beets, corn (maize), sorghum, soybeans, rice, oats, peanuts, vegetables, tomato, potato, perennial plantation crops including coffee, cocoa, oil palm, rubber, sugarcane, citrus, grapes, fruit trees, nut trees, banana, plantain, pineapple, hops, tea and forests such as eucalyptus and conifers (e.g., loblolly pine), and turf species (e.g., Kentucky bluegrass, St. Augustine grass, Kentucky fescue and Bermuda grass). Those skilled in the art will appreciate that not all compounds are equally effective against all weeds. Alternatively, the subject compounds are useful to modify plant growth.




A herbicidally effective amount of the compounds of this invention is determined by a number of factors. These factors include: formulation selected, method of application, amount and type of vegetation present, growing conditions, etc. In general, a herbicidally effective amount of compounds of this invention is 0.001 to 20 kg/ha with a preferred range of 0.004 to 1.0 kg/ha. One skilled in the art can easily determine the herbicidally effective amount necessary for the desired level of weed control.




Compounds of this invention can be used alone or in combination with other commercial herbicides, insecticides or fungicides. Compounds of this invention can also be used in combination with commercial herbicide safeners such as benoxacor, dichlormid and furilazole to increase safety to certain crops. A mixture of one or more of the following herbicides with a compound of this invention may be particularly useful for weed control: acetochlor, acifluorfen and its sodium salt, aclonifen, acrolein (2-propenal), alachlor, ametryn, amidosulfuron, amitrole, ammonium sulfamate, anilofos, asulam, atrazine, azafenidin, azimsulfuron, benazolin, benazolin-ethyl, benfluralin, benfuresate, bensulfuron-methyl, bensulide, bentazone, bifenox, bispyribac and its sodium salt, bromacil, bromoxynil, bromoxynil octanoate, butachlor, butralin, butroxydim (ICIA0500), butylate, caloxydim (BAS 620H), carfentrazone-ethyl, chlomethoxyfen, chloramben, chlorbromuron, chloridazon, chlorimuron-ethyl, chlornitrofen, chlorotoluron, chlorpropham, chlorsulfuron, chlorthal-dimethyl, cinmethylin, cinosulfuron, clethodim, clomazone, clopyralid, clopyralid-olamine, cyanazine, cycloate, cyclosulfamuron, 2,4-D and its butotyl, butyl, isoctyl and isopropyl esters and its dimethylammonium, diolamine and trolamine salts, daimuron, dalapon, dalapon-sodium, dazomet, 2,4-DB and its dimethylammonium, potassium and sodium salts, desmedipham, desmetryn, dicamba and its diglycolammonium, dimethylammonium, potassium and sodium salts, dichlobenil, dichlorprop, diclofop-methyl, 2-[4,5-dihydro4 methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-methyl-3-pyridinecarboxylic acid (AC 263,222), difenzoquat metilsulfate, diflufenican, dimepiperate, dimethenamid, dimethylarsinic acid and its sodium salt, dinitramine, diphenamid, diquat dibromide, dithiopyr, diuron, DNOC, endothal, EPTC, esprocarb, ethalfluralin, ethametsulfuron-methyl, ethofumesate, ethoxysulfuron, fenoxaprop-ethyl, fenoxaprop-P-ethyl, fenuron, fenuron-TCA, flamprop-methyl, flamprop-M-isopropyl, flamprop-M-methyl, flazasulfuron, fluazifop-butyl, fluazifop-P-butyl, fluchloralin, flufenacet, flumetsulam, flumiclorac-pentyl, flumioxazin, fluometuron, fluoroglycofen-ethyl, flupoxam, flupyrsulfuron-methyl and its sodium salt, fluridone, flurochloridone, fluroxypyr, fluthiacet-methyl, fomesafen, fosamine-ammonium, glufosinate, glufosinate-ammonium, glyphosate, glyphosate-isopropylammonium, glyphosate-sesquisodium, glyphosate-trimesium, halosulfuron-methyl, haloxyfop-etotyl, haloxyfop-methyl, hexazinone, imazamethabenz-methyl, imazamox, imazapyr, imazaquin, imazaquin-ammonium, imazethapyr, imazethapyr-ammonium, imazosulfuron, ioxynil, ioxynil octanoate, ioxynil-sodium, isoproturon, isouron, isoxaben, isoxaflutole, lactofen, lenacil, linuron, maleic hydrazide, MCPA and its dimethylammonium, potassium and sodium salts, MCPA-isoctyl, mecoprop, mecoprop-P, mefenacet, mefluidide, metam-sodium, methabenzthiazuron, methylarsonic acid and its calcium, monoammonium, monosodium and disodium salts, methyl [[[1-[5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrophenyl]-2-methoxyethylidene]amino]oxy]acetate (AKH-7088), methyl 5-[[[[(4,6-dimethyl-2-pyrimidinyl)amino]carbonyl]amino]sulfonyl]-1-(2-pyridin)-1H-pyrazole-4-carboxylate (NC-330), metobenzuron, metolachlor, metosulam, metoxuron, metribuzin, metsulfuron-methyl, molinate, monolinuron, napropamide, naptalam, neburon, nicosulfuron, norflurazon, oryzalin, oxadiazon, oxasulfuron, oxyfluorfen, paraquat dichloride, pebulate, pendimethalin, pentoxazone (KPP-314), perfluidone, phenmediphali, picloram, picloram-potassium, pretilachlor, primisulfuron-methyl, prometon, prometryn, propachlor, propanil, propaquizafop, propazine, propham, propyzamide, prosulfuron, pyrazolynate, pyrazosulfuron-ethyl, pyridate, pyriminobac-methyl, pyrithiobac, pyrithiobac-sodium, quinclorac, quizalofop-ethyl, quizalofop-P-ethyl, quizalofop-P-tefuryl, rimsulfuron, sethoxydim, siduron, simazine, sulcotrione (ICIA0051), sulfentrazone, sulfometuron-methyl, TCA, TCA-sodium, tebuthiuron, terbacil, terbuthylazine, terbutryn, thenylchlor, thiafluamide (BAY 11390), thifensulfuron-methyl, thiobencarb, tralkoxydim, tri-allate, triasulfuron, triaziflam, tribenuron-methyl, triclopyr, triclopyr-butotyl, triclopyr-triethylammonium, tridiphane, trifluralin, triflusulfuron-methyl, and vernolate.




In certain instances, combinations with other herbicides having a similar spectrum of control but a different mode of action will be particularly advantageous for preventing the development of resistant weeds. Certain combinations of compounds of this invention with other herbicides may provide synergistic herbicidal effects on weeds or may provide enhanced crop safety.




Preferred for better control of undesired vegetation in corn (e.g., lower use rate, broader spectrum of weeds controlled, or enhanced crop safety) or for preventing the development of resistant weeds in corn are mixtures of a compound of this invention with one or more of the herbicides selected from the group rimsulfuron, nicosulfuron, thifensulfuron, prosulfuron, halosulfuron, naphthalic anhydride, flurazole, dichlormid, fenchlorazole ethyl, naphthalic anhydride, MG-191 (2-dichloromethyl)-2-methyl-1,3-dioxolane), dicyclonon, benoxacor, cyometrinil, furilazole, oxabetrinil, cloquintocet mexyl, fluxofenim, fenclorim, menfenpyr diethyl, and R-29148 (3-(dichloroacetyl)-2,2,5-trimethyloxazolidine).




Specifically preferred mixtures for use in corn are selected from the group consisting of:




a) Compound 113 (Index Table C, mixture partner A, generally applied at a rate of 10 to 1000 g/ha, preferably applied at a rate of 50 to 500 g/ha) in combination with:
















Combination







Number




Mixture partner B











1




rimsulfuron






2




nicosulfuron






3




dichlormid






4




benoxacor






5




naphthalic anhydride






6




rimsulfuron (B1) in combination with dichlormid (B2)






7




nicosulfuron (B3) in combination with dichlormid (B4)














Combination 1 is generally used in a ratio of A to B of 3:1 to 50:1, preferably 5:1 to 30:1, with B being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha. Combination 2 is generally used in a ratio of A to B of 2:1 to 20:1, preferably 4:1 to 10:1, with B being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha. Combination 3 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 2:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 4 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 4:1, with B being applied at a rate of 1 to 1000 g/ha, preferably 20 to 5:00 g/ha. Combination 5 is generally used in a ratio of A to B of 1:500 to 50:1, preferably 1:20 to 10:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 6 is generally used in a ratio of A to B1 of 3:1 to 50:1, preferably 5:1 to 30:1, and a ratio of A to B2 of 1:10 to 10:1, preferably 1:2 to 2:1, with B1 being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha, and B2 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 7 is generally used in a ratio of A to B3 of 2:1 to 20:1, preferably 4:1 to 10:1, and a ratio of A to B4 of 1:10 to 10:1, preferably 1:2 to 2:1, with B3 being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha, and B4 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha.




b) Compound 131 (Index Table C, mixture partner A, generally applied at a rate of 10 to 1000 g/ha, preferably applied at a rate of 50 to 500 g/ha) in combination with:
















Combination







Number




Mixture partner B











1




rimsulfuron






2




nicosulfuron






3




dichlormid






4




benoxacor






5




naphthalic anhydride






6




rimsulfuron (B1) in combination with dichlormid (B2)






7




nicosulfuron (B3) in combination with dichlormid (B4)














Combination 1 is generally used in a ratio of A to B of 3:1 to 50:1, preferably 5:1 to 30:1, with B being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha Combination 2 is generally used in a ratio of A to B of 2:1 to 20:1, preferably 4:1 to 10:1, with B being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha. Combination 3 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 2:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 4 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 4:1, with B being applied at a rate of 1 to 1000 g/ha, preferably 20 to 500 g/ha. Combination 5 is generally used in a ratio of A to B of 1:500 to 50:1, preferably 1:20 to 10:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 6 is generally used in a ratio of A to B1 of 3:1 to 50:1, preferably 5:1 to 30:1, and a ratio of A to B2 of 1:10 to 10:1, preferably 1:2 to 2:1, with B1 being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha, and B2 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 7 is generally used in a ratio of A to B3 of 2:1 to 20:1, preferably 4:1 to 10:1, and a ratio of A to B4 of 1:10 to 10:1, preferably 1:2 to 2:1, with B3 being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha, and B4 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha




c) Compound 242 (Index Table C, mixture partner A, generally applied at a rate of 10 to 1000 g/ha, preferably applied at a rate of 50 to 500 g/ha) in combination with:
















Combination







Number




Mixture partner B











1




Rimsulfuron






2




Nicosulfuron






3




Dichlormid






4




Benoxacor






5




naphthalic anhydride






6




rimsulfuron (B1) in combination with dichlormid (B2)






7




nicosulfuron (B3) in combination with dichlormid (B4)














Combination 1 is generally used in a ratio of A to B of 3:1 to 50:1, preferably 5:1 to 30:1, with B being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha. Combination 2 is generally used in a ratio of A to B of 2:1 to 20:1, preferably 4:1 to 10:1, with B being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha. Combination 3 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 2:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 4 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 4:1, with B being applied at a rate of 1 to 1000 g/ha, preferably 20 to 500 g/ha. Combination 5 is generally used in a ratio of A to B of 1:500 to 50:1, preferably 1:20 to 10:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 6 is generally used in a ratio of A to B1 of 3:1 to 50:1, preferably 5:1 to 30:1, and a ratio of A to B2 of 1:10 to 10:1, preferably 1:2 to 2:1, with B1 being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha, and B2 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 7 is generally used in a ratio of A to B3 of 2:1 to 20:1, preferably 4:1 to 10:1, and a ratio of A to B4 of 1:10 to 10:1, preferably 1:2 to 2:1, with B3 being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha, and B4 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha.




d) Compound 146 (Index Table C, mixture partner A, generally applied at a rate of 10 to 1000 g/ha, preferably applied at a rate of 50 to 500 g/ha) in combination with:
















Combination







Number




Mixture partner B











1




Rimsulfuron






2




Nicosulfuron






3




Dichlormid






4




Benoxacor






5




naphthalic anhydride






6




rimsulfuron (B1) in combination with dichlormid (B2)






7




nicosulfuron (B3) in combination with dichlormid (B4)














Combination 1 is generally used in a ratio of A to B of 3:1 to 50:1, preferably 5:1 to 30:1, with B being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha. Combination 2 is generally used in a ratio of A to B of 2:1 to 20:1, preferably 4:1 to 10:1, with B being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha. Combination 3 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 2:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 4 is generally used in a ratio of A to B of 1:10 to 10:1, preferably 1:2 to 4:1, with B being applied at a rate of 1 to 1000 g/ha, preferably 20 to 500 g/ha. Combination 5 is generally used in a ratio of A to B of 1:500 to 50:1, preferably 1:20 to 10:1, with B being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 6 is generally used in a ratio of A to B 1 of 3:1 to 50:1, preferably 5:1 to 30:1, and a ratio of A to B2 of 1:I0 to 10:1, preferably 1:2 to 2:1, with B1 being applied at a rate of 1 to 100 g/ha, preferably 5 to 50 g/ha, and B2 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha. Combination 7 is generally used in a ratio of A to B3 of 2:1 to 20:1, preferably 4:1 to 10:1, and a ratio of A to B4 of1:10 to 10:1, preferably 1:2 to 2:1, with B3 being applied at a rate of 1 to 100 g/ha, preferably 20 to 70 g/ha, and B4 being applied at a rate of 10 to 1000 g/ha, preferably 50 to 500 g/ha.




The following Tests demonstrate the control efficacy of the compounds of this invention against specific weeds. The weed control afforded by the compounds is not limited, however, to these species. See Index Tables A-D for compound descriptions. The abbreviation “dec” indicates that the compound appeared to decompose on melting. The abbreviation “Ex.” stands for “Example” and is followed by a number indicating in which example the compound is prepared.












INDEX TABLE A









































Cmpd










No.




R


1






R


2






R


16






MP (° C.)









 1




Et




Et




4-OCH


3






113-116






 2




Et




Et




2,6-dimethyl




90-93






 3




Et




Et




4-F




71-76






 4




i-Pr




4-F-Phenyl




2-CH


3






122-124






 5




i-Pr




4-F-Phenyl




4-OCH


3






145-148






 6




i-Pr




3,6-dihydro-2H-pyran




4-OCH


3






 98-100






 7




i-Pr




4-F-Phenyl




2,4-di-Cl




57-60






(Ex. 1)






 8




i-Pr




4-F-Phenyl




2-Cl




80-83






 9




i-Pr




3,6-dihydro-2H-pyran




3,5-di-Cl




137-139






10




i-Pr




3,6-dihydro-2H-pyran




2-CH


3






143-145






11




Et




Et




3,5-di-Cl




oil*






12




Et




Et




4-OCF


3






oil*






13




i-Pr




3,6-dihydro-2H-pyran




4-OCF


3






oil*






14




i-Pr




4-F-Phenyl




2-OCF


3






129-131






15




i-Pr




4-F-Phenyl




2-CF


3






131-134






16




i-Pr




4-F-Phenyl




2, 5-di-Cl




120-122






17




i-Pr




4-F-Phenyl




1, 4-di-Me




154-156






18




i-Pr




4-F-Phenyl




2,6-di-Me




103-105






19




i-Pr




4-F-Phenyl




2,6-di-Cl




130-132






20




i-Pr




4-F-Phenyl




4-Cl-2-CF


3






128-131






21




i-Pr




4-F-Phenyl




3-Cl-2-Me




170-172






22




i-Pr




2,4-di-F-Phenyl




2,4-di-F




108-110






23




Et




c-Hex




2,4-di-F




oil*






24




i-Pr




2,4-di-F-Phenyl




2,4-di-Me




103-106






25




i-Pr




2,4-di-F-Phenyl




2-Me




85-89






26




Et




c-Hex




2,4-di-Me




118-120






27




Et




c-Hex




2,6-di-Me




120-122






28




i-Pr




2,4-di-F-Phenyl




2,6-di-Me




129-131






29




Et




c-Hex




2-OMe




111-114






30




i-Pr




4-F-Phenyl




2-OMe




109-111






31




i-Pr




2,4-di-F-Phenyl




2-OMe




55-60






32




i-Pr




2,4-di-F-Phenyl




2,4-di-OMe




134-137






33




i-Pr




4-F-Phenyl




2,4-di-OMe




175-177






34




i-Pr




4-F-Phenyl




2-Et




94-97






35




i-Pr




4-F-Phenyl




2-Me-4-OMe




112-115






36




i-Pr




Phenyl




2-Me




148-150






37




c-Pr




4-F-Phenyl




2-Me




oil*






38




i-Pr




4-F-Phenyl




H




oil*






39




i-Pr




4-CF


3


-Phenyl




2-Me




 85






40




i-Pr




4-Me-Phenyl




2-Me




128






41




i-Pr




4-Cl-Phenyl




2-Me




139-141






42




i-Pr




2,4-di-Cl-5-O-i-Pr-Phenyl




2-Me




68-70






43




i-Pr




4-F-Phenyl




2,4-di-Cl-5-




148-150









O-i-Pr






44




i-Pr




4-NO


2


-Phenyl




2-Me




148






45




i-Pr




2,4-di-F-Phenyl




2-Et




93-97






46




i-Pr




Phenyl




2,6-di-Me




146-148






(Ex. 2)






47




i-Pr




4-Cl-Phenyl




2,6-di-Me




143-147






48




i-Pr




3,4-di-F-Phenyl




2-Me




124






49




i-Pr




4-OMe-Phenyl




2-Me




 95






50




c-Pr




2,4-diF-Phenyl




2-Me




oil*






51




i-Pr




4-CN-Phenyl




2-Me




205






52




i-Pr




4-F-Phenyl




2-Et-6-Me




oil*






53




i-Pr




4-F-Phenyl




2-Cl-6-Me




oil*






54




i-Pr




4-Cl-Phenyl




2-Cl-6-Me




oil*






55




i-Pr




Pyrrolidinyl




2,4-di-Cl




120-122






56




i-Pr




Pyrrolidinyl




2-OCF


3






oil*






57




i-Pr




Pyrrolidinyl




2-CF


3






120-122






58




i-Pr




Pyrrolidinyl




2, 5-di-Cl




139-140






59




i-Pr




Pyrrolidinyl




2-Me




103-106






60




i-Pr




4-F-Phenyl




2,4, 6-tri-Me




181-183






61




i-Pr




4-Cl-Phenyl




2,4, 6-tri-Me




121-122






62




i-Pr




4-F-Phenyl




2-Me-6-OMe




100-102






63




Et




c-Hex




2,4, 6-tri-Me




122-123






64




i-Pr




4-Cl-Phenyl




2-i-Pr, 6-Me




oil*






65




i-Pr




4-F-Phenyl




2-i-Pr, 6-Me




oil*






66




i-Pr




Phenyl




2-i-Pr, 6-Me




oil*






67




i-Pr




3,5-di-F




2-Me




120






68




i-Pr




2, 5-di-F




2-Me




 98






69




i-Pr




Benzyl




2,6-di-Me




oil*






70




Et




Benzyl




2,6-di-Me




oil*






71




Et




Benzyl




2-Me




oil*






72




i-Pr




Benzyl




2-Me




oil*






73




i-Pr




Phenyl




2-OMe, 6-Me




132-134






74




i-Pr




2,4-di-F-Phenyl




2-OMe, 6-Me




107-109











*see Index Table B for


1


H NMR data.






















INDEX TABLE B









Cmpd







No.






1


H NMR Data (CDCl


3


solution unless indicated otherwise)


a













11




δ 1.25(t, 6H), 3.40(m, 4H), 6.96(s, 1H), 7.55(s, 1H),







8.59(s, 1H).






12




δ 1.26(t, 6H), 3.58(m, 4H), 7.36(d, 2H), 7.61(d, 2H).






13




δ 1.33(d, 6H) 2.3-2.4(m, 2H), 3.86(t, 2H), 4.2-4.3(m, 2H),







4.38-4.45(m, 1H), 5.83-5.90 7.38(m, 2H), 7.60(m, 2H).






23




δ 7.5-7.4(m, 1H), 7.1(t, 2H), 4.2-3.8(m, 1H), 3.5-3.2(m, 2H),







2.0-1.8(m, 3H), 1.8-1.0(m






37




δ 7.3-7.4(m, 6H), 7.0-7.1(t, 2H), 3.4(m, 1H), 2.21(s, 3H),







0.9(m, 2H), 0.7-0.8(m, 2H).






38




δ 7.4-7.6(m, 4H), 7.3(m, 1H), 7.0-7.2(m, 2H), 4.7(m, 1H),







1.2(d, 6H).






50




δ 7.3-7.4(m, 4H), 7.2(d, 1H), 6.8-7.0(q, 2H), 3.4(m, 1H),







2.2(s, 3H), 0.9(d, 2H), 0.8(d,






52




δ 7.2-7.4(m, 3H), 7.0-7.2(m, 4H), 4.7(m, 1H), 2.3-2.4(q, 2H),







2.1(s, 3H), 1.2(d, 6H), 1. (t, 3H).






53




δ 7.3(m, 3H), 7.2(m, 2H), 7.1(t, 2H), 4.6-4.7(m, 1H), 2.19(s,







3H), 1.2(d, 6H).






54




δ 7.3-7.4(q, 4H), 7.2(m, 3H), 4.6-4.7(m, 1H), 2.198(s, 3H),







1.2(d, 6H).






69




δ 7.4-7.1(m, 8H), 4.68(s, 2H), 4.5(bs, 1H), 2.23(s, 6H),







1.27(d, 6H).






70




δ 7.4-7.1(m, 8H), 4.74(s, 2H), 3.6-3.4(bs, 2H), 2.26(s, 6H),







1.2(m, 3H).






71




δ 7.5-7.3(m, 9H), 4.74(m, 2H), 3.6-3.4(bm, 2H), 2.30(s, 3H),







1.2(bt, 3H).






72




δ 7.5-7.1(m, 9H), 4.67(s, 2H), 4.5(bs, 1H), 2.27(s, 3H),







1.28(d, 6H).













a1


H NMR data are in ppm downfield from tetramethylsilane. Couplings are designated by (s)-singlet, (d)-doublet, (t)-triplet, (q)-quartet, (m)-multiplet, (dd)-doublet of doublets, (dt)-doublet of triplets, (br s)-broad singlet.





















INDEX TABLE C









































Cmpd.




Q




R


1






R


2






MP ° C.









 75




1,3,5-Trimethylpyrazol-4-yl




i-Pr




4-F-Phenyl




152-154






 76




1,3,5-Trimethylpyrazol-4-yl




i-Pr




2,4-diF-Phenyl




45-50






 77




2-Thienylmethyl




Et




Et




oil*






 78




Benzyl




i-Pr




4-F-Phenyl




95-96






(Ex. 9)






 79




Benzyl




i-Pr




2,4-diF-Phenyl




93-95






 80




2-Thienylmethyl




i-Pr




4-F-Phenyl




oil*






 81




2-Thienylmethyl




i-Pr




2-Dihydropyranyl




oil*






 82




2-Thienylmethyl




Et




c-Hexyl




oil*






 83




2-Thienylmethyl




Me




Phenyl




oil*






 84




2-Methylbenzyl




Et




Et




oil*






 85




2-Methylbenzyl




Me




Ph




oil*






 86




2-Thienylmethyl




i-Pr




2,4-diF-Ph




77-80






 87




2-Methylbenzyl




i-Pr




2,4-diF-Phenyl




oil*






 88




2-Methylbenzyl




i-Pr




4-F-Phenyl




118-120






 89




5-Tetrahydronaphthyl




Et




Et




oil*






 90




5-Tetrahydronaphthyl




i-Pr




4-F-Phenyl




oil*






 91




n-Propyl




i-Pr




4-F-Phenyl




oil*






 92




n-Propyl




i-Pr




Phenyl




oil*






 93




Allyl




i-Pr




Phenyl




68-70






 94




Benzyl




i-Pr




Phenyl




90-94






 95




1,3-Dimethyl-5-chloropyrazol-4-yl




i-Pr




4-F-Phenyl




109-112






 96




1,3-Dimethyl-5-chloropyrazol-4-yl




i-Pr




2,4-diF-Phenyl




55-59






 97




1-Methyl-5-chloropyrazol-4-yl




i-Pr




4-F-Phenyl




55-60






 98




1-Methylpyrazol-4-yl




i-Pr




4-F-Phenyl




145-146






 99




2-Trifluoromethylcyclohexyl




i-Pr




4-F-Phenyl




oil*






100




3-Phenyl-5-methylisoxazol-4-yl




i-Pr




4-F-Phenyl




206-209






101




3-Ethyl-5-methylisoxazol-4-yl




i-Pr




4-F-Phenyl




oil*






102




3-Ethyl-5-ethylisoxazol-4-yl




i-Pr




4-F-Phenyl




74-77






103




2-Thienylmethyl




i-Pr




Phenyl




90-95






104




2-Methoxybenzyl




i-Pr




Phenyl




115-117






105




Allyl




i-Pr




4-Cl-Phenyl




oil*






106




Benzyl




i-Pr




4-Cl-Phenyl




oil*






107




Ethyl




i-Pr




4-F-Phenyl




78-81






108




Ethyl




i-Pr




4-Cl-Phenyl




83-86






109




Isopropyl




i-Pr




2,4-diF-Phenyl




82-85






110




c-Hexyl




i-Pr




4-F-Phenyl




128-131






111




c-Hexyl




i-Pr




4-Cl-Phenyl




126-130






112




c-Hexyl




i-Pr




Phenyl




136-139






113




Isopropyl




i-Pr




Phenyl




82-86






 (Ex. 14)






114




Isopropyl




i-Pr




4-Cl-Phenyl




76-80






115




c-Hexyl




i-Pr




2,4-diF-Phenyl




88-90






116




Ethyl




i-Pr




2,4-diF-Phenyl




75-77






117




Ethyl




i-Pr




Phenyl




74-76






118




t-Bu




i-Pr




4-Cl-Phenyl




88-90






119




n-Pr




i-Pr




4-Cl-Phenyl




oil*






120




1,3,5-Trimethylpyrazol-4-yl




i-Pr




Phenyl




48-52






121




1,3-Dimethyl-5-chloropyrazol-4-yl




i-Pr




Phenyl




54-56






122




1-Methyl-5-chloropyrazol-4-yl




i-Pr




Phenyl




94-97






123




1-Methylpyrazol-4-yl




i-Pr




Phenyl




111-112






124




1-Methylpyrazol-5-yl




i-Pr




4-F-Phenyl




52-59






125




1,4-Dimethylpyrazol-5-yl




i-Pr




4-F-Phenyl




45-49






126




3,5-di-Me-isoxazol-4-yl




i-Pr




2-Dihydropyranyl




oil*






127




Allyl




c-Pr




2,4-F-Phenyl




oil*






128




CH


2


CO


2


Et




i-Pr




4-F-Phenyl




oil*






129




t-Bu




i-Pr




Phenyl




oil*






130




n-Pr




i-Pr




2,4-diF-Phenyl




oil*






131




i-Pr




i-Pr




4-F-Phenyl




78-80






 (Ex. 13)






132




i-Pr




i-Pr




4-Me-Phenyl




68-71






133




α-Me-Benzyl




i-Pr




4-Cl-Phenyl




oil*






134




α-Me-Benzyl




i-Pr




4-F-Phenyl




oil*






135




3,5-Diisopropylisoxazol-4-yl




i-Pr




4-F-Phenyl




oil*






136




2-Methylbenzyl




i-Pr




4-Cl-Phenyl




oil*






(Ex. 5)






137




Methyl




i-Pr




4-Cl-Phenyl




121-123






(Ex. 7)






138




Methyl




i-Pr




4-F-Phenyl




135-136






(Ex. 6)






139




2-Methylallyl




i-Pr




4-F-Phenyl




oil*






140




2-Chlorobenzyl




i-Pr




4-F-Phenyl




oil*






141




2-Chlorobenzyl




i-Pr




Pyrrolidinyl




oil*






142




2-Methoxybenzyl




i-Pr




Pyrrolidinyl




oil*






143




2-Methoxybenzyl




i-Pr




4-F-Phenyl




104-106






144




2-Chlorobenzyl




i-Pr




2-Dihydropyrinyl




oil*






145




2-Chlorobenzyl




i-Pr




c-Hexenyl




oil*






146




Allyl




i-Pr




4-F-Phenyl




65-66






(Ex. 3)






147




Allyl




i-Pr




2-Dihydropyranyl




oil*






148




2-Chloroethyl




i-Pr




4-F-Phenyl




oil*






149




2-Chloroethyl




i-Pr




2-Dihydropyranyl




oil*






150




Allyl




Et




Pyrrolidinyl




oil*






151




Allyl




i-Pr




2,4-diF-Phenyl




oil*






152




Benzyl




Et




Et




oil*






153




Benzyl




Me




Phenyl




oil*






154




Allyl




c-Pr




4-F-Phenyl




oil*






155




3,5-Dimethylisoxazol-4-yl




i-Pr




4-F-Phenyl




133-136






156




3,5-Dimethylisoxazol-4-yl




i-Pr




2,4-diF-Phenyl




175-178






157




3,5-Dimethylisothiazol-4-yl




i-Pr




4-F-Phenyl




oil*






158




3,5-Dimethylisothiazol-4-yl




i-Pr




2,4-di-F-Phenyl




158-161






159




3,5-Dimethylisothiazol-4-yl




i-Pr




4-Cl-Phenyl




124-127






160




2, 5-Dichlorothiazoly-4-yl




i-Pr




4-F-Phenyl




oil*






161




2-Me-c-Hex




i-Pr




4-F-Phenyl




78-81






162




2-Me-c-Hex




i-Pr




Phenyl




oil*






163




CF


3


CH


2






i-Pr




4-F-Phenyl




122-124






164




H




i-Pr




4-F-Phenyl




55-60






165




i-Pr




i-Pr




Benzyl




oil*






166




i-Pr




Et




Benzyl




oil*






167




α-Me-Benzyl (S)




i-Pr




4-F-Phenyl




oil*






168




α-Me-Benzyl (S)




i-Pr




Phenyl




oil*






169




i-Bu




i-Pr




4-F-Phenyl




80-81






(Ex. 8)






170




NMe2




i-Pr




4-F-Phenyl




69-71






(Ex. 4)






171




2-Methylphenyl




i-Pr




2, 3-DiF-Phenyl




88






172




2-Methyl-c-hexyl




i-Pr




2,4-DiF-Phenyl




oil*






173




α-Methylbenzyl (S)




i-Pr




Phenyl




72-74






174




α-Methylbenzyl (S)




i-Pr




4-Cl-Phenyl




oil*






175




2-Methylphenyl




i-Pr




4-Br-Phenyl




117






176




2-Methylphenyl




i-Pr




2,6-di-F-Phenyl




 91






177




Phenyl (Me)N




i-Pr




4-F-Phenyl




62-64






178




α-Methylbenzyl (R)




i-Pr




4-Cl-Phenyl




oil*






179




α-Methylbenzyl (R)




i-Pr




4-F-Phenyl




64-67






180




2,6-DiMe-Phenyl




i-Pr




4, 6-Dimethoxy-1,3,5-Triazine-2-yl




oil*






181




2-Me-Phenyl




i-Pr




4, 6-Dimethoxy-1,3,5-Triazine-2-yl




oil*






182




i-Propyl




i-Pr




4, 6-Dimethoxy-1,3,5-Triazine-2-yl




oil*






183




Phenyl (Me)N




Et




c-Hexyl




oil*






184




3-Trifluoromethylcyclohexyl




i-Pr




4-F-Phenyl




oil*






185




2-Methylphenyl




i-Pr




2,4-DiCl-Phenyl




 54






186




2-Methylphenyl




i-Pr




2-Cl, 4-F-Phenyl




48-51






187




2-Methylphenyl




i-Pr




4-Ph-Phenyl




 63






188




Oxiranylmethyl




i-Pr




4-F-Phenyl




oil*






189




i-Propyl




Et




4-Pyridylmethyl




oil*






190




i-Propyl




Et




1,3,4-Thiadiazol-2-yl




oil*






191




(2,4-Dimethylthiazol-5-yl)methyl




i-Pr




4-Cl-Phenyl




oil*






192




(2,4-Dimethylthiazol-5-yl)methyl




i-Pr




4-F-Phenyl




oil*






193




2-Methylphenyl




3-Pentyl




4-F-Phenyl




142-145






194




Allyl




c-Bu




4-F-Phenyl




61-63






195




2-Methylphenyl




i-Pr




4-Cl, 2-F-Phenyl




 50






196




2,4-Dimethylthiazol-5-yl




i-Pr




4-Cl-Phenyl




oil*






197




2,4-Dimethylthiazol-5-yl




i-Pr




Phenyl




oil*






198




2,4-Dimethylthiazol-5-yl




i-Pr




4-F-Phenyl




oil*






199




1-(3-Methyl-3-Butenyl)




i-Pr




4-F-Phenyl




77-78






200




2-Methylphenyl




c-Bu




4-F-Phenyl




108-110






201




2-Et-6-Me-Phenyl




i-Pr




4-F-Phenyl




oil*






202




4-Trifluoromethoxyphenyl




i-Pr




4-F-Phenyl




88-92






203




2-Methylphenyl




i-Pr




4-Methylsulfonylphenyl




153






204




2-Methylphenyl




i-Pr




2-F-Phenyl




 42






205




2-Methylphenyl




i-Pr




4-Methylthiophenyl




104






206




2-Furanylmethyl




i-Pr




4-Cl-Phenyl




oil*






207




2-Furanylmethyl




i-Pr




4-F-Phenyl




oil*






208




2-Furanylmethyl




i-Pr




2,4-diF-Phenyl




oil*






209




2-Furanylmethyl




i-Pr




Phenyl




67-70






210




Cinnamyl




i-Pr




4-F-Phenyl




oil*






211




4-Acetoxybutyl




i-Pr




4-F-Phenyl




93-95






212




Propargyl




i-Pr




4-F-Phenyl




74-75






213




3-Trimethylsilylpropargyl




i-Pr




4-F-Phenyl




oil*






214




1-(3-Ethoxycarbonyl-2-Propenyl)




i-Pr




4-F-Phenyl




oil*






215




MeO


2


CCH


2






i-Pr




4-F-Phenyl




oil*






216




t-BuCOCH


2






i-Pr




4-F-Phenyl




oil*






217




MeCOCH


2






i-Pr




4-F-Phenyl




oil*






218




1-(3,4,4-Trifluoro-3-Butenyl)




i-Pr




4-F-Phenyl




oil*






219




2-(1,3-Dioxolan-2-yl)ethyl




i-Pr




4-F-Phenyl




94-96






220




CH


3


OCH


2


CH


2


OCH


2






i-Pr




4-F-Phenyl




oil*






221




n-Butyl




i-Pr




4-F-Phenyl




oil*






222




2,4-DiMe-6-OMe-Phenyl




i-Pr




4-F-Phenyl




oil*






223




2,4-DiMe-6-OMe-Phenyl




i-Pr




2,4-diF-Phenyl




oil*






224




2-Br-4, 6-diMe-Phenyl




i-Pr




4-F-Phenyl




141-144






225




Me


2


N




i-Pr




Phenyl




oil*






226




3-Methyl-3-oxetanylmethyl




i-Pr




4-F-Phenyl




65-77






227




1-(3,3,3-Trifluoro-2-methoximino)propyl




i-Pr




4-F-Phenyl




 80-105






228




Methyl




Et




c-Hex




65-74






229




2-Methylphenyl




i-Pr




4-n-Bu-Phenyl




oil*






230




2-Methylphenyl




i-Pr




4-Et-Phenyl




oil*






231




2-Methylphenyl




i-Pr




4-i-Pr-Phenyl




 94






232




(2,4-DiMe-Thiazol-5-yl)methyl




i-Pr




4-F-Phenyl




oil*






233




(2,4-DiMe-Thiazol-5-yl)methyl




i-Pr




2,4-diF-Phenyl




oil*






234




3-Pyridyl




i-Pr




4-F-Phenyl




109-112






235




3-Pyridyl




i-Pr




Phenyl




116-118






236




2-Methylphenyl




i-Pr




2-Me-Phenyl




oil*






237




2-Methylphenyl




i-Pr




4-Dimethylamino-Phenyl




115






238




α-Me-Benzyl (R)




i-Pr




2,4-diF-Phenyl




oil*






239




2-Methylphenyl




s-Bu




4-F-Phenyl




79-82






240




2-Methylphenyl




1-c-Pr-ethyl




4-F-Phenyl




90-93






241




c-Propyl




i-Pr




4-Cl-Phenyl




oil*






242




c-Propyl




i-Pr




4-F-Phenyl




65-67






243




c-Propyl




i-Pr




Phenyl




70-74






244




2,6-DiMe-Phenyl




1-Ethoxycarbonylethyl




4-F-Phenyl




97-99






245




D


3


C




i-Pr




4-F-Phenyl




141-143






246




Neopentyl




i-Pr




4-F-Phenyl




106-108






247




2-Methylphenyl




1-Ethoxycarbonylethyl




4-F-Phenyl




97-99






248




Ethyl




1-Ethoxycarbonylethyl




4-F-Phenyl




oil*






249




Allyl




c-Heptyl




4-F-Phenyl




72-79






250




2-Phenethyl




i-Pr




4-F-Phenyl




95-96






251




c-Propylmethyl




i-Pr




4-F-Phenyl




oil*






252




CH


3


CH


2


C(O)CH


2






i-Pr




4-F-Phenyl




oil*






253




n-C


19


H


39






i-Pr




4-F-Phenyl




oil*






254




1-(2-Octynyl)




i-Pr




4-F-Phenyl




oil*






255




2-(1,3-Dioxan-2-yl)ethyl




i-Pr




4-F-Phenyl




82-83






256




1-(2-Trimethylsilylmethyl-2-propenyl)




i-Pr




4-F-Phenyl




oil*






257




2-Cyclohexylethyl




i-Pr




4-F-Phenyl




oil*






258




CH


3


OCH


2


CH


2


OCH


2






i-Pr




4-F-Phenyl




119-120






259




(3,5-dimethylisoxazol-4-yl)methyl




i-Pr




4-F-Phenyl




oil*






260




PhC(O)CH(Me)




i-Pr




4-F-Phenyl




oil*






261




PhCH


2


OCH


2






i-Pr




4-F-Phenyl




110-112






262




Geranyl




i-Pr




4-F-Phenyl




oil*






263




1-(3-Methoxycarbonyl-2-Propenyl)




i-Pr




4-F-Phenyl




oil*






264




Et


2


NC(O)CH


2






i-Pr




4-F-Phenyl




oil*






265




t-BuO


2


CCH


2






i-Pr




4-F-Phenyl




oil*






266




MeO


2


CCH


2


CH


2


CH


2






i-Pr




4-F-Phenyl




oil*






267




2-Pyridylmethyl




i-Pr




4-F-Phenyl




oil*






268




2-Methylphenyl




i-Pr




4-Phenoxy-Phenyl




 51






269




2-Methylphenyl




i-Pr




3-F-Phenyl




128






270




2-Methylphenyl




i-Pr




4-t-Bu-Phenyl




oil*






271




c-Pentyl




i-Pr




4-F-Phenyl




79-80






272




3-Thienyl




i-Pr




4-F-Phenyl




125-128






273




2,6-DiMe-Phenyl




i-Pr




2-Cyclohexenyl




105-112






274




Me


2


N




Et




c-Hex




oil*






275




Neopentyl




Et




c-Hex




oil*






276




Neopentyl




i-Pr




Phenyl




116-118






277




Neopentyl




i-Pr




2,4-DiF-Phenyl




oil*






278




2-Methylphenyl




i-Pr




5-Indanyl




115






279




Allyl




1-Ethoxycarbonylethyl




4-F-Phenyl




oil*






280




c-Hexyl




1-Ethoxycarbonylethyl




4-F-Phenyl




oil*






281




2, 3-Dihydro-2-Me-benzofuran-7-yl




i-Pr




4-F-Phenyl




148-150






282




c-Pentyl




i-Pr




4-Cl-Phenyl




104-106






283




c-Pentyl




i-Pr




Phenyl




oil*






284




c-Pentyl




i-Pr




2,4-DiF-Phenyl




oil*






285




1-(3-Chlorobutenyl)




i-Pr




4-F-Phenyl




oil*






286




1-(2-Pentenyl)




i-Pr




4-F-Phenyl




oil*






287




3-Fluoropropyl




i-Pr




4-F-Phenyl




oil*






288




1-(3-Methyl-2-butenyl)




i-Pr




4-F-Phenyl




oil*






289




1-(4-Fluorobutyl)




i-Pr




4-F-Phenyl




oil*






290




n-Pentyl




i-Pr




4-F-Phenyl




oil*






291




1-(4-Pentenyl)




i-Pr




4-F-Phenyl




oil*






292




Acetoxymethyl




i-Pr




4-F-Phenyl




oil*






293




Methoxymethyl




i-Pr




4-F-Phenyl




oil*






 (Ex. 15)






294




Trimethylsilylmethyl




i-Pr




4-F-Phenyl




oil*






295




Ethoxymethyl




i-Pr




4-F-Phenyl




oil*






296




i-Propyl




i-Pr




2-Pyrazinyl




oil*






297




c-Propyl




Et




Et




oil*






298




c-Propyl




Et




c-Hex




oil*






299




c-Propyl




i-Pr




2,4-DiF-Phenyl




83-85






300




2-Methylphenyl




i-Pr




4-CF


3


O-Phenyl




109






301




2-Methylphenyl




i-Pr




4-Pyridinyl




152-154






302




i-Propyl




1-Ethoxycarbonylethyl




4-F-Phenyl




oil*






303




2-t-Bu-6-Me-Phenyl




i-Pr




Phenyl




oil*






304




2,6-DiEt-Phenyl




i-Pr




4-F-Phenyl




oil*






305




2,6-DiEt-Phenyl




i-Pr




Phenyl




77-83






306




2-Methylphenyl




i-Pr




2-Naphthyl




 49






307




Allyl




Et




c-Hex




62-65






308




c-Hexyl




Et




c-Hex




oil*






309




i-Propyl




Et




c-Hex




oil*






310




4-Tetrahydropyranyl




i-Pr




4-F-Phenyl




101-103






311




2-Tetrahydropyranyl




i-Pr




4-F-Phenyl




103-105






312




2-Furanylmethyl




Et




c-Hex




oil*






313




2-Biphenylylmethyl




i-Pr




4-F-Phenyl




113-126






314




1-(2-Methylthioethyl)




i-Pr




4-F-Phenyl




101-106






315




2,6-DiMe-Phenyl




i-Pr




2-Dihydropyrinyl




122-124






316




2-(3-Methylbutyl)




i-Pr




4-F-Phenyl




62-64






317




1-(2,2-Dimethoxyethyl)




i-Pr




4-F-Phenyl




oil*






318




2,6-DiMe-Phenyl




c-Bu




2,4-DiCl-Phenyl




127-131






319




i-Propyl




c-Bu




2,4-DiCl-Phenyl




103-106






320




(5-Cl-1,2,3-thiadiazol-4-yl)methyl




i-Pr




2,4-DiF-Phenyl




103-108






321




(5-Cl-1,2,3-thiadiazol-4-yl)methyl




i-Pr




Phenyl




128-131






322




Cyclopentylmethyl




i-Pr




4-F-Phenyl




83-90






323




1-(3-Dimethylaminopropyl)




i-Pr




4-F-Phenyl




oil*






324




2-Methylphenyl




2-(3-OMe-propyl)




4-F-Phenyl




115-121






325




Allyl




1-c-Pr-ethyl




4-Cl-Phenyl




oil*






326




[2.2.1]-Bicyclohept-2-yl




i-Pr




2,4-DiF-Phenyl




103-105






327




[2.2.1]-Bicyclohept-2-yl




i-Pr




4-F-Phenyl




90-94






328




[2.2.1]-Bicyclohept-2-yl




i-Pr




Phenyl




90-91






329




2-Naphthyl




i-Pr




4-F-Phenyl




150-151






330




2-Methylphenyl




1-c-Pr-ethyl




4-Cl-Phenyl




111-115






331




2-MeO-6-Me-Phenyl




1-Ethoxycarbonylethyl




4-F-Phenyl




oil*






332




2-Naphthyl




i-Pr




Phenyl




134-135






333




2-Naphthyl




i-Pr




4-Cl-Phenyl




142-143






334




2-Naphthyl




i-Pr




4-Me-Phenyl




172-173






335




2-Naphthyl




i-Pr




2,4-DiF-Phenyl




oil*






336




1-Me-2-Naphthyl




i-Pr




4-Cl-Phenyl




oil*






337




1-Me-2-Naphthyl




i-Pr




2,4-DiF-Phenyl




oil*






338




1-Me-2-Naphthyl




i-Pr




4-F-Phenyl




oil*






339




c-Heptyl




i-Pr




4-Cl-Phenyl




125-135






340




c-Heptyl




i-Pr




4-F-Phenyl




104-105






341




c-Heptyl




i-Pr




Phenyl




100-102






342




c-Heptyl




i-Pr




2,4-DiF-Phenyl




87-90






343




2-Tetrahydrofuranylmethyl




i-Pr




4-F-Phenyl




95-96






344




1-Me-2-Naphthyl




i-Pr




Phenyl




oil*






345




2-Tetrahydrofuranyl




i-Pr




4-F-Phenyl




oil*






346




(3,5-Dimethylpyrazol-1-yl)methyl




i-Pr




Phenyl




138-148






347




(3,5-Dimethylpyrazol-1-yl)methyl




i-Pr




4-F-Phenyl




140-144






348




c-Butyl




i-Pr




Phenyl




70-72






349




c-Butyl




i-Pr




4-Cl-Phenyl




64-68






350




c-Butyl




i-Pr




4-F-Phenyl




 97-100






351




c-Butyl




i-Pr




2,4-diF-Phenyl




65-67






352




MeOCH


2


CH(Me)




i-Pr




2,4-diF-Phenyl




oil*






353




3-Pentyl




i-Pr




2,4-diF-Phenyl




72-75






354




3-Pentyl




i-Pr




Phenyl




oil*






355




2-(3-Methylbutyl)




i-Pr




Phenyl




oil*






356




2-(3-Methylbutyl)




i-Pr




2,4-diF-Phenyl




oil*






357




MeOCH


2


CH(Me)




i-Pr




2,4-diF-Phenyl




81-85






358




3-Pentyl




i-Pr




4-F-Phenyl




oil*






359




2-t-Bu-6-Me-Phenyl




i-Pr




4-F-Phenyl




oil*






360




1-(1-Me-c-propyl)




i-Pr




Phenyl




82-83






361




1-(1-Me-c-propyl)




i-Pr




4-Cl-Phenyl




oil*






362




1-(1-Me-c-propyl)




i-Pr




4-F-Phenyl




oil*






363




1-(1-Me-c-propyl)




i-Pr




2,4-diF-Phenyl




oil*






364




2-Methylphenyl




Et




Et




oil*






365




Methyl




1-Ethoxycarbonylethyl




4-F-Phenyl




oil*






366




3-Pyridylmethyl




i-Pr




4-F-Phenyl




oil*






367




2-(3-Chloropropyl)




i-Pr




4-F-Phenyl




oil*






368




Methyl




i-Pr




2,4-diF-Phenyl




oil*






369




1-(2-Me-c-propyl)




i-Pr




4-Cl-Phenyl




oil*






370




1-(2-Me-c-propyl)




i-Pr




Phenyl




oil*






371




1-(2-Me-c-propyl)




i-Pr




4-F-Phenyl




95-97






372




1-(2-Me-c-propyl)




i-Pr




2,4-diF-Phenyl




oil*






373




(5-Cl-3-Me-isothiazol-4-yl)methyl




i-Pr




4-F-Phenyl




126-129






374




(5-Cl-3-Me-isothiazol-4-yl)methyl




i-Pr




Phenyl




133-136






375




3-Tetrahydrofurylmethyl




i-Pr




4-F-Phenyl




84-86






376




Chloromethyl




i-Pr




4-F-Phenyl




83-86






377




H




i-Pr




4-Cl-Phenyl




137-138






378




(4-Methyl-1,2,3-thiadiazol-5-yl)methyl




i-Pr




Phenyl




109-113






379




(2-Ethoxy-4-CF


3


-thiazol-5-yl)methyl




i-Pr




Phenyl




oil*






380




(4-Methyl-1,2,3-thiadiazol-5-yl)methyl




i-Pr




4-F-Phenyl




54-55






381




(2-Ethoxy-4-CF


3


-thiazol-5-yl)methyl




i-Pr




4-F-Phenyl




oil*






382




1-(2,6-Dimethylpiperidine)




i-Pr




4-F-Phenyl




 97-100






383




1-(2,6-Dimethylpiperidine)




i-Pr




2,4-diF-Phenyl




81-84






384




4-(Morpholino)




i-Pr




2,4-diF-Phenyl




62-68






385




4-(Morpholino)




i-Pr




4-F-Phenyl




173-175






386




H




i-Pr




Phenyl




116-117






387




2-(2-Cyanoethyl)




i-Pr




4-F-Phenyl




oil*






388




1-(2-Cyanoethyl)




i-Pr




4-F-Phenyl




125-128






389




n-Hexyl




i-Pr




4-F-Phenyl




oil*






390




2-(1,3-Difluoropropyl)




i-Pr




4-F-Phenyl




 99-101






391




H




i-Pr




2,4-diF-Phenyl




110-112






392




Trans-1-(2-Me-c-propyl)




i-Pr




4-F-Phenyl




90-91






393




1-(1-Chloroethyl)




i-Pr




4-F-Phenyl




70-73






394




i-Butyl




i-Pr




2,4-diF-Phenyl




oil*






395




Cyanomethyl




i-Pr




4-F-Phenyl




120-123






396




1-(2-Ethoxy-3-ethoxycarbonyl-2-propenyl)




i-Pr




4-F-Phenyl




112-114






397




1-(3,3,3-trifluoropropyl)




i-Pr




4-F-Phenyl




 99-100






398




1-(4,4,4-trifluorobutyl)




i-Pr




4-F-Phenyl




71-72






399




1-(3,4,4, 4-Tetrafluoro-3-trifluoromethylbutyl)




i-Pr




4-F-Phenyl




oil*






400




CH


3


C(O)CH(CH


3


)




i-Pr




4-F-Phenyl




oil*






401




1-(2-Cl-4-Me-thiazol-5-yl)ethyl




i-Pr




4-F-Phenyl




oil*






402




2-Methyl-c-propylmethyl




i-Pr




4-F-Phenyl




81-83






403




c-Butylmethyl




i-Pr




4-F-Phenyl




74-76






404




1-(c-Propylethyl)




i-Pr




4-F-Phenyl




97-99






405




1-(2-Cl-4-Me-thiazol-5-yl)ethyl




i-Pr




2,4-F-Phenyl




122-125






406




1-(2-Cl-4-Me-thiazol-5-yl)ethyl




i-Pr




4-Cl-Phenyl




128-131






407




1-(2-Cl-4-Me-thiazol-5-yl)ethyl




i-Pr




Phenyl




128-131






408




2-(3-Chloropropyl)




i-Pr




2,4-diF-Phenyl




oil*






409




Methyl




i-Pr




Phenyl




105-114






410




i-Butyl




i-Pr




Phenyl




55-67






411




2-(3-Chloropropyl)




i-Pr




Phenyl




 95-105






412




1-(2-Butenyl)




i-Pr




4-F-Phenyl




oil*






413




2-(3-Butenyl)




i-Pr




4-F-Phenyl




oil*






414




Allyldimethylsilylmethyl




i-Pr




4-Cl-Phenyl




oil*






415




1-(2-Bromoethyl)




i-Pr




Phenyl




90-92






416




4-Tetrahydropyranyl




i-Pr




Phenyl




80-93






417




i-Butyl




i-Pr




4-Cl-Phenyl




oil*






418




1-(3-Methyl-3-Butenyl)




i-Pr




Phenyl




oil*






419




1-(2-Methylthioethyl)




i-Pr




Phenyl




oil*






420




(3-Methyl-3-oxetanyl)methyl




i-Pr




Phenyl




oil*






421




2-(1,3-difluoropropyl)




i-Pr




Phenyl




 95-107






422




Chloromethyl




i-Pr




4-Cl-Phenyl




75-77






423




Chloromethyl




i-Pr




Phenyl




75-77






424




Phenyldimethylsilylmethyl




i-Pr




4-Cl-Phenyl




oil*






425




Vinyldimethylsilylmethyl




i-Pr




4-Cl-Phenyl




oil*






426




Allyldimethylsilylmethyl




i-Pr




4-F-Phenyl




oil*






427




c-Heptyl




i-Pr




3, 6-dihydro-2H-pyran




oil*






428




c-Heptyl




i-Pr




1-Cyclohexenyl




oil*






429




c-Heptyl




Et




c-Hexyl




oil*






430




(5,6-Dihydro-1,2-Oxazin-3-yl)methyl




i-Pr




Phenyl




95-97






431




Cyanomethyl




i-Pr




2,4-diF-Phenyl




123-126






432




1-(1-Cyanoethyl)




i-Pr




2,4-diF-Phenyl




oil*






433




1-(2-Cyanoethyl)




i-Pr




2,4-diF-Phenyl




112-114






434




Cyanomethyl




i-Pr




Phenyl




90-91






435




1-(1-Cyanoethyl)




i-Pr




Phenyl




oil*






436




1-(2-Cyanoethyl)




i-Pr




Phenyl




74-77






437




Chloromethyl




i-Pr




2,4-diF-Phenyl




69-71






438




1-(1-Chloroethyl)




i-Pr




Phenyl




73-75






439




1-(1-Methoxyethyl)




i-Pr




4-F-Phenyl




77-79






440




Me


2


NC(O)CH


2






i-Pr




2,4-diF-Phenyl




111






441




1-(1-Methoxyethyl)




i-Pr




Phenyl




oil*






442




1-(2,4-Dimethylthiazol-5-yl)ethyl




i-Pr




Phenyl




oil*






443




1-(2,4-Dimethylthiazol-5-yl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






444




1-(2-Cyanoethyl)




i-Pr




4-Cl-Phenyl




139-142






445




PhCONHCH


2






i-Pr




4-F-Phenyl




161-163






446




1-(1,2-Dimethoxyethyl)




i-Pr




4-F-Phenyl




oil*






447




(EtO)


2


P(O)CH


2






i-Pr




Phenyl




oil*






448




(EtO)


2


P(O)CH(CH


3


)




i-Pr




Phenyl




oil*






449




1-(2-Ethyl-4-methylthiazol-5-yl)ethyl




i-Pr




4-F-Phenyl




106-109






450




(5,6-Dihydro-1,2-Oxazin-3-yl)methyl




i-Pr




4-Cl-Phenyl




105-108






451




1-(1-Cyanoethyl)




i-Pr




4-Cl-Phenyl




117-127






452




1-(1-Methoxy-2-propenyl)




i-Pr




4-F-Phenyl




oil*






453




1-(2-Methylsulfonylethyl)




i-Pr




4-F-Phenyl




oil*






454




1-(2-Pentenyl)




i-Pr




Phenyl




oil*






455




3-(4-Pentenyl)




i-Pr




Phenyl




oil*






456




2-(3-Chloropropyl)




i-Pr




4-Cl-Phenyl




oil*






457




Hydroxymethyl




i-Pr




4-Cl-Phenyl




oil*






458




1-(2-Chloro-1-methoxyethyl)




i-Pr




4-Cl-Phenyl




oil*






459




Ethyldimethylsilylmethyl




i-Pr




4-F-Phenyl




54-55






460




Ethyldimethylsilylmethyl




i-Pr




4-Cl-Phenyl




68-71






461




1-(3-Trimethylsilylpropyl)




i-Pr




4-F-Phenyl




oil*






462




t-BuC(O)OCH


2






i-Pr




4-F-Phenyl




87-90






463




CH


3


O


2


CCH(CH


3


)




i-Pr




2,4-diF-Phenyl




oil*






464




CH


3


O


2


CCH(CH


3


)




i-Pr




Phenyl




oil*






465




EtO


2


CCH


2


CH(CO


2


Et)




i-Pr




2,4-diF-Phenyl




oil*






466




(3,4-Dihydroisoxazol-3-yl)methyl




i-Pr




4-F-Phenyl




93-95






467




Me


3


SiCH


2


CH


2


OCH


2






i-Pr




4-Cl-Phenyl




oil*






468




2-(1,3-Difluoropropyl)




i-Pr




4-Cl-Phenyl




93-96






469




1-(2-Chloroethyl)




i-Pr




Phenyl




80-83






470




Hydroxymethyl




i-Pr




4-F-Phenyl




89-95






471




2-(3, 3-Dimethoxypropyl)




i-Pr




4-F-Phenyl




60-63






472




2-(3, 3-Dimethoxypropyl)




i-Pr




2,4-diF-Phenyl




oil*






473




MeCONHCH


2






i-Pr




4-F-Phenyl




150-168






474




1-(2-Chloroethyl)




i-Pr




4-Cl-Phenyl




100-101






475




1-(2-Chloroethyl)




i-Pr




2,4-diF-Phenyl




70-72






476




Cyanomethyl




i-Pr




4-Cl-Phenyl




173-179






477




Me


2


NC(O)CH


2






i-Pr




4-Cl-Phenyl




152-153






478




Me


2


NC(O)CH(CH


3


)




i-Pr




4-F-Phenyl




oil*






479




Me


2


NC(O)CH(CH


3


)




i-Pr




Phenyl




oil*






480




Me


2


NC(O)CH(CH


3


)




i-Pr




4-Cl-Phenyl




102






481




Me


2


NC(O)CH(CH


3


)




i-Pr




2,4-diF-Phenyl




oil*






482




(2-Chlorothiazol-5-yl)methyl




i-Pr




4-F-Phenyl




69-70






483




1-(2-nitroethyl)




i-Pr




4-Cl-Phenyl




119-122






484




i-PrC(CO)CH


2






i-Pr




4-F-Phenyl




79-81






485




i-PrC(CO)CH


2






i-Pr




Phenyl




oil*






486




i-PrC(CO)CH


2






i-Pr




2,4-diF-Phenyl




oil*






487




i-PrC(CO)CH


2






i-Pr




4-Cl-Phenyl




oil*






488




c-PrC(CO)CH


2






i-Pr




4-F-Phenyl




oil*






489




c-PrC(CO)CH


2






i-Pr




Phenyl




87-89






490




c-PrC(CO)CH


2






i-Pr




2,4-diF-Phenyl




oil*






491




HC(O)CH


2






i-Pr




4-F-Phenyl




oil*






492




ClCH


2


C(O)NHCH


2


CH


2






i-Pr




Phenyl




oil*






493




ClCH


2


C(O)NHCH


2


CH


2


CH


2






i-Pr




Phenyl




oil*






494




(5,6-Dihydro-1,3-oxazin-2-yl)methyl




i-Pr




Phenyl




oil*






495




(3,4-Dihydrooxazol-2-yl)methyl




i-Pr




Phenyl




oil*






496




(1-Cyclohexenyl)methyl




i-Pr




Phenyl




oil*






497




(1-Methyl-1,2,5,6-tetrahydropyridin-3-yl)methyl




i-Pr




Phenyl




oil*






498




1-(2-(3-Pyridyl)-2-propenyl)




i-Pr




Phenyl




oil*






499




1-(2-Ethyl-4-methylthiazol-5-yl)methyl




i-Pr




4-Cl-Phenyl




103-104






500




1-(3-Fluoropropyl)




i-Pr




2,4-diF-Phenyl




oil*






501




2-(1,3-Dioxolan-2-yl)methyl




i-Pr




2,4-diF-Phenyl




oil*






502




2-(1,3-Dioxan-2-yl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






503




Methoxymethyl




i-Pr




2,4-diF-Phenyl




oil*






504




Ethoxymethyl




i-Pr




2,4-diF-Phenyl




oil*






505




CH


3


OCH


2


CH


2


OCH


2






i-Pr




2,4-diF-Phenyl




oil*






506




1-(4-Acetoxybutyl)




i-Pr




2,4-diF-Phenyl




oil*






507




1-(3,4,4-Trifluoro-3-butenyl)




i-Pr




2,4-diF-Phenyl




oil*






508




1-(2-Phenylethyl)




i-Pr




2,4-diF-Phenyl




oil*






509




Cyclopropylmethyl




i-Pr




2,4-diF-Phenyl




oil*






510




(3,5-Dimethyloxazol-4-yl)methyl




i-Pr




2,4-diF-Phenyl




oil*






511




PhCOCH(CH


3


)




i-Pr




2,4-diF-Phenyl




oil*






512




Et


2


NC(O)CH


2






i-Pr




2,4-diF-Phenyl




oil*






513




MeO


2


CCH


2


CH


2


CH


2






i-Pr




2,4-diF-Phenyl




oil*






514




1-(3-Chloro-2-butenyl)




i-Pr




2,4-diF-Phenyl




oil*






515




1-(3-Methyl-2-butenyl)




i-Pr




2,4-diF-Phenyl




oil*






516




1-(4-Pentenyl)




i-Pr




2,4-diF-Phenyl




oil*






517




CH


3


C(O)CH(CH


3


)




i-Pr




2,4-diF-Phenyl




oil*






518




Trimethylsilylmethyl




i-Pr




2,4-diF-Phenyl




oil*






519




1-(2-Ethoxy-3-ethoxycarbonyl-2-propenyl)




i-Pr




2,4-diF-Phenyl




oil*






520




PhCH


2


OCH


2






i-Pr




2,4-diF-Phenyl




oil*






521




Cyclobutylmethyl




i-Pr




2,4-diF-Phenyl




oil*






522




1-(4-Fluorobutyl)




i-Pr




2,4-diF-Phenyl




oil*






523




1-(2-Pentenyl)




i-Pr




2,4-diF-Phenyl




oil*






524




CH


3


CH


2


C(O)CH


2






i-Pr




2,4-diF-Phenyl




oil*






525




1-(3,3,3-Trifluoropropyl)




i-Pr




2,4-diF-Phenyl




oil*






526




1-(4,4,4-Trifluorobutyl)




i-Pr




2,4-diF-Phenyl




oil*






527




n-Butyl




i-Pr




4-Cl-Phenyl




oil*






528




n-Pentyl




i-Pr




4-Cl-Phenyl




oil*






529




n-Hexyl




i-Pr




4-Cl-Phenyl




oil*






530




1-(3-Fluoropropyl)




i-Pr




4-Cl-Phenyl




oil*






531




2-(1,3-Dioxolan-2-yl)ethyl




i-Pr




4-Cl-Phenyl




oil*






532




2-(1,3-Dioxan-2-yl)ethyl




i-Pr




4-Cl-Phenyl




oil*






533




Methoxymethyl




i-Pr




4-Cl-Phenyl




oil*






534




Ethoxymethyl




i-Pr




4-Cl-Phenyl




oil*






535




CH


3


OCH


2


CH


2


OCH


2






i-Pr




4-Cl-Phenyl




oil*






536




1-(4-Acetoxybutyl)




i-Pr




4-Cl-Phenyl




oil*






537




1-(3,4,4-Trifluoro-3-butenyl)




i-Pr




4-Cl-Phenyl




oil*






538




1-(2-Phenylethyl)




i-Pr




4-Cl-Phenyl




oil*






539




Cyclopropylmethyl




i-Pr




4-Cl-Phenyl




oil*






540




(3,5-Dimethyloxazol-4-yl)methyl




i-Pr




4-Cl-Phenyl




oil*






541




PhCOCH(CH


3


)




i-Pr




4-Cl-Phenyl




oil*






542




Et


2


NC(O)CH


2






i-Pr




4-Cl-Phenyl




oil*






543




MeO


2


CCH


2


CH


2


CH


2






i-Pr




4-Cl-Phenyl




oil*






544




1-(3-Chloro-2-butenyl)




i-Pr




4-Cl-Phenyl




oil*






545




1-(3-Methyl-2-butenyl)




i-Pr




4-Cl-Phenyl




oil*






546




1-(4-Pentenyl)




i-Pr




4-Cl-Phenyl




oil*






547




CH


3


C(O)CH(CH


3


)




i-Pr




4-Cl-Phenyl




oil*






548




Trimethylsilylmethyl




i-Pr




4-Cl-Phenyl




oil*






549




1-(2-Ethoxy-3-ethoxycarbonyl-2-propenyl)




i-Pr




4-Cl-Phenyl




oil*






550




Cyclobutylmethyl




i-Pr




4-Cl-Phenyl




oil*






551




1-(4-Fluorobutyl)




i-Pr




4-Cl-Phenyl




oil*






552




1-(2-Pentenyl)




i-Pr




4-Cl-Phenyl




oil*






553




CH


3


CH


2


C(O)CH


2






i-Pr




4-Cl-Phenyl




oil*






554




1-(3,3,3-Trifluoropropyl)




i-Pr




4-Cl-Phenyl




oil*






555




1-(4,4,4-Trifluorobutyl)




i-Pr




4-Cl-Phenyl




oil*






556




n-Butyl




i-Pr




Phenyl




oil*






557




n-Pentyl




i-Pr




Phenyl




oil*






558




n-Hexyl




i-Pr




Phenyl




oil*






559




1-(3-Fluoropropyl)




i-Pr




Phenyl




oil*






560




2-(1,3-Dioxolan-2-yl)ethyl




i-Pr




Phenyl




oil*






561




2-(1,3-Dioxan-2-yl)ethyl




i-Pr




Phenyl




oil*






562




Methoxymethyl




i-Pr




Phenyl




oil*






563




Ethoxymethyl




i-Pr




Phenyl




oil*






564




CH


3


OCH


2


CH


2


OCH


2






i-Pr




Phenyl




oil*






565




1-(4-Acetoxybutyl)




i-Pr




Phenyl




oil*






566




1-(3,4,4-Trifluoro-3-butenyl)




i-Pr




Phenyl




oil*






567




1-(2-Phenylethyl)




i-Pr




Phenyl




oil*






568




Cyclopropylmethyl




i-Pr




Phenyl




oil*






569




(3,5-Dimethyloxazol-4-yl)methyl




i-Pr




Phenyl




oil*






570




PhCOCH(CH


3


)




i-Pr




Phenyl




oil*






571




Et


2


NC(O)CH


2






i-Pr




Phenyl




oil*






572




MeO


2


CCH


2


CH


2


CH


2






i-Pr




Phenyl




oil*






573




1-(3-Chloro-2-butenyl)




i-Pr




Phenyl




oil*






574




1-(3-Methyl-2-butenyl)




i-Pr




Phenyl




oil*






575




1-(4-Pentenyl)




i-Pr




Phenyl




oil*






576




CH


3


C(O)CH(CH


3


)




i-Pr




Phenyl




oil*






577




Trimethylsilylmethyl




i-Pr




Phenyl




oil*






578




1-(2-Ethoxy-3-ethoxycarbonyl-2-propenyl)




i-Pr




Phenyl




oil*






579




PhCH


2


OCH


2






i-Pr




Phenyl




oil*






580




Cyclobutylmethyl




i-Pr




Phenyl




oil*






581




1-(4-Fluorobutyl)




i-Pr




Phenyl




oil*






582




1-(2-Pentenyl)




i-Pr




Phenyl




oil*






583




CH


3


CH


2


C(O)CH


2






i-Pr




Phenyl




oil*






584




1-(3,3,3-Trifluoropropyl)




i-Pr




Phenyl




oil*






585




1-(4,4,4-Trifluorobutyl)




i-Pr




Phenyl




oil*






586




Me


2


NC(O)CH


2






i-pr




4-F-Phenyl




117






587




(EtO)


2


P(O)CH


2






i-Pr




4-F-Phenyl




oil*






588




Me


2


NC(O)CH


2






i-Pr




Phenyl




152






589




1-(2-Ethyl-4-methylthiazol-5-yl)ethyl




i-Pr




2,4-diF-Phenyl




87-90






590




1-(2-Ethyl-4-methylthiazol-5-yl)ethyl




i-Pr




4-Cl-Phenyl




93-97






591




1-(2-Nitroethyl)




i-Pr




2,4-diF-Phenyl




92-98






592




1-(1-Methoxyethyl)




i-Pr




4-Cl-Phenyl




oil*






593




1-(1-Methoxyethyl)




i-Pr




2,4-diF-Phenyl




oil*






594




2-(3-Bromopropyl)




i-Pr




2,4-diF-Phenyl




oil*






595




2-(1,3-Difluoropropyl)




i-Pr




2,4-diF-Phenyl




91-96






596




2-(3-Acetoxy-1-chloropropyl)




i-Pr




4-F-Phenyl




oil*






597




F


3


CC(O)CH


2






i-Pr




4-Cl-Phenyl




oil*






598




F


3


CC(O)CH


2






i-Pr




2,4-diF-Phenyl




oil*






599




(EtO)


2


P(O)CH


2






i-Pr




4-Cl-Phenyl




oil*






600




Allyl




2-(3-OMe-propyl)




2,6-DiMe-Phenyl




oil*






601




(5,6-Dihydro-1,2-Oxazin-3-yl)methyl




i-Pr




4-F-Phenyl




108-112






602




(5,6-Dihydro-1,2-Oxazin-3-yl)methyl




i-Pr




2,4-diF-Phenyl




87-95






603




1-(2-Nitropropyl)




i-Pr




2,4-diF-Phenyl




oil*






604




1-(2-Nitropropyl)




i-Pr




Phenyl




oil*






605




1-(2-(6-Chloro-2-pyridyl)-2-propenyl)




i-Pr




Phenyl




oil*






606




1-(2-(4-Fluorophenyl)-2-propenyl)




i-Pr




Phenyl




oil*






607




1-(2-Methyl-2-propenyl)




i-Pr




Phenyl




oil*






608




1-(2-Chlorol-2-propenyl)




i-Pr




Phenyl




oil*






609




2-(3-Butynyl)




i-Pr




Phenyl




oil*






610




s-Butyl (R)




i-Pr




Phenyl




53-55






611




s-Butyl (S)




i-Pr




Phenyl




55-57






612




s-Butyl (S)




i-Pr




Phenyl




41-43






613




s-Butyl (R)




i-Pr




4-F-Phenyl




41-43






614




EtO


2


CCH


2


CH(CO


2


Et)




i-Pr




Phenyl




oil*






615




EtO


2


CCH


2


CH(CO


2


Et)




i-Pr




4-F-Phenyl




oil*






616




MeO


2


CCH(CH


3


)




i-Pr




4-F-Phenyl




oil*






617




(EtO)


2


P(O)CH(CH


3


)




i-Pr




4-F-Phenyl




oil*






618




Thiocyanatomethyl




i-Pr




4-F-Phenyl




125-127






619




PhC(O)NHCH


2






i-Pr




2,4-diF-Phenyl




120-123






620




PhC(O)NHCH


2






i-Pr




Phenyl




145-146






621




MeC(O)NHCH


2






i-Pr




Phenyl




122-126






622




MeC(O)NHCH


2






i-Pr




2,4-diF-Phenyl




173-175






623




MeO


2


CCH(CH


3


)




i-Pr




4-Cl-Phenyl




oil*






624




(2-Tetrahydropyranyl)methyl




i-Pr




4-F-Phenyl




80-82






625




CH


3


C(O)N(CH


3


)CH


2


CH


2






i-Pr




4-F-Phenyl




112-126






626




1-(2-Fluoroethyl)




i-Pr




4-F-Phenyl




95-96






627




1-(2-Methoxyethyl)




i-Pr




4-F-Phenyl




oil*






628




1-(2-Methoxyethyl)




i-Pr




2,4-diF-Phenyl




94-97






629




1-(2,2-Diethoxyethyl)




i-Pr




4-F-Phenyl




oil*






630




1-(2,2-Diethoxyethyl)




i-Pr




2,4-diF-Phenyl




84-88






631




1-(2-Methoxyethyl)




i-Pr




Phenyl




oil*






632




1-(2,2-Diethoxyethyl)




i-Pr




Phenyl




oil*






633




1-(2,2-Diethoxyethyl)




i-Pr




4-Cl-Phenyl




73-75






634




1-(2-Chloro-2-propenyl)




i-Pr




2,4-diF-Phenyl




oil*






635




n-Butyl




i-Pr




2,4-diF-Phenyl




oil*






636




n-Pentyl




i-Pr




2,4-diF-Phenyl




oil*






637




n-Hexyl




i-Pr




2,4-diF-Phenyl




oil*






638




Me


2


NC(O)CH


2


CH


2






i-Pr




4-F-Phenyl




100






639




c-PrC(O)CH


2






i-Pr




4-Cl-Phenyl




oil*






640




c-BuC(O)CH


2






i-Pr




4-F-Phenyl




oil*






641




c-BuC(O)CH


2






i-Pr




Phenyl




115-117






642




c-BuC(O)CH


2






i-Pr




2,4-diF-Phenyl




oil*






643




c-BuC(O)CH


2






i-Pr




4-Cl-Phenyl




oil*






644




(EtO)


2


P(O)CH(CH


3


)




i-Pr




4-Cl-Phenyl




oil*






645




(2-Chloro-1,3,4-thiadiazol-5-yl)methyl




i-Pr




2,4-diF-Phenyl




106-109






646




(2-Chloro-1,3,4-thiadiazol-5-yl)methyl




i-Pr




4-F-Phenyl




110-112






647




1-(3-Cyanopropyl)




i-Pr




4-F-Phenyl




oil*






648




1-(2-t-Butyl-2-propenyl)




i-Pr




Phenyl




oil*






649




1-(2-i-Propyl-2-propenyl)




i-Pr




Phenyl




oil*






650




1-(2-Benzyl-2-propenyl)




i-Pr




Phenyl




oil*






651




2-(3-Carbomethoxy-3-butenyl)




i-Pr




Phenyl




oil*






652




1-(1-Ethynyl-3-methyl-2-butenyl)




i-Pr




Phenyl




oil*






653




(2-Chloro-1,3,4-thiadiazol-5-yl)methyl




i-Pr




4-Cl-Phenyl




oil*






654




(2-Chloro-1,3,4-thiadiazol-5-yl)methyl




i-Pr




Phenyl




oil*






655




2-(4-Ethynyl-2-methyl-3-butenyl)




i-Pr




Phenyl




oil*






656




2-(5,6-Dihydro-1,2-Oxazin-3-yl)ethyl




i-Pr




4-F-Phenyl




oil*






657




2-(3-Butynyl)




i-Pr




2,4-diF-Phenyl




oil*






658




2-(3-Butynyl)




i-Pr




4-Cl-Phenyl




oil*






659




(2-Tetrahydropyranyl)methyl




i-Pr




Phenyl




 97-100






660




(2-Tetrahydropyranyl)methyl




i-Pr




4-Cl-Phenyl




82-84






661




(3,4-Dihydroisoxazol-3-yl)methyl




i-Pr




4-Cl-Phenyl




105-107






662




(MeO)


2


P(O)CH


2


CH


2






i-Pr




4-F-Phenyl




79-85






663




i-Propyl




i-Pr




4-Pyridyl




85-89






664




s-Butyl (S)




i-Pr




4-Cl-Phenyl




53-56






665




s-Butyl (R)




i-Pr




4-Cl-Phenyl




54-56






666




s-Butyl (S)




i-Pr




2,4-diF-Phenyl




59-61






667




s-Butyl (R)




i-Pr




2,4-diF-Phenyl




58-60






668




1-(2-Fluoroethyl)




i-Pr




4-Cl-Phenyl




120-121






669




1-(2-Fluoroethyl)




i-Pr




Phenyl




88-89






670




1-(2-Fluoroethyl)




i-Pr




2,4-diF-Phenyl




90-91






671




Me


2


NC(O)CH


2


CH


2






i-Pr




Phenyl




 91






672




2-(1,3-Dichloropropyl)




i-Pr




4-F-Phenyl




oil*






673




1-(2,2-Dichloroethyl)




i-Pr




2,4-diF-Phenyl




121-122






674




1-(3-Cyanopropyl)




i-Pr




Phenyl




89-92






675




1-(3-Cyanopropyl)




i-Pr




2,4-diF-Phenyl




oil*






676




(3,4-Dihydroisoxazol-3-yl)methyl




i-Pr




2,4-diF-Phenyl




66-68






677




PhCH(CO


2


Me)




i-Pr




4-F-Phenyl




oil*






678




HOCH


2


CH


2


CH(CO


2


Me)




i-Pr




Phenyl




120-123






679




HOCH


2


CH


2


CH(CO


2


Me)




i-Pr




4-Cl-Phenyl




107-110






680




HOCH


2


CH


2


CH(CO


2


Me)




i-Pr




4-F-Phenyl




102-106






681




EtO


2


CCH


2


CH(CO


2


Et)




i-Pr




4-Cl-Phenyl




oil*






682




(1-Ethyl-5-Chloropyrazol-4-yl)methyl




i-Pr




2,4-diF-Phenyl




oil*






683




(1-Ethyl-5-Chloropyrazol-4-yl)methyl




i-Pr




Phenyl




oil*






684




(1-Ethyl-5-Chloropyrazol-4-yl)methyl




i-Pr




4-Cl-Phenyl




oil*






685




(1-Ethyl-5-Chloropyrazol-4-yl)methyl




i-Pr




4-F-Phenyl




oil*






686




(1-Ethyl-5-Chloropyrazol-4-yl)methyl




i-Pr




4-F-Phenyl




oil*






687




Me


2


NC(O)CH


2


CH


2






i-Pr




2,4-diF-Phenyl




oil*






688




i-Propyl




s-Butyl (S)




4-F-Phenyl




59-61






689




i-Propyl




s-Butyl




4-F-Phenyl




74-75






690




i-Propyl




s-Butyl (R)




4-F-Phenyl




64-65






691




i-Propyl




i-Pr




4-Br-Phenyl




75-76






692




3-Cyclohexenyl




i-Pr




4-F-Phenyl




80-82






693




HC(O)CH(CH


3


)




i-Pr




Phenyl




oil*






694




3-Cyclohexenyl




i-Pr




2,4-diF-Phenyl




oil*






695




3-Cyclohexenyl




i-Pr




4-Cl-Phenyl




87-89






696




3-Cyclohexenyl




i-Pr




Phenyl




oil*






697




(MeO)


2


P(O)CH


2


CH


2






i-Pr




Phenyl




oil*






698




(MeO)


2


P(O)CH


2


CH


2






i-Pr




4-Cl-Phenyl




oil*






699




1-(Cyclopropyl)ethyl




i-Pr




Phenyl




65-67






700




1-(Cyclopropyl)ethyl




i-Pr




4-Cl-Phenyl




52-54






701




1-(Cyclobutyl)ethyl




i-Pr




4-Cl-Phenyl




oil*






702




1-(Cyclobutyl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






703




1-(Morpholinocarbonyl)ethyl




i-Pr




4-Cl-Phenyl




163






704




Me


2


NC(S)CH(CH


3


)




i-Pr




Phenyl




141






705




1-(Morpholinocarbonyl)ethyl




i-Pr




4-F-Phenyl




oil*






706




(3,4-Dihydroisoxazol-3-yl)methyl




i-Pr




Phenyl




oil*






707




2-(1-Chloro-3-fluoropropyl)




i-Pr




4-F-Phenyl




85-86






708




2-(1-Acetoxy-3-chloropropyl)




i-Pr




2,4-diF-Phenyl




oil*






709




Fluoromethyl




i-Pr




4-F-Phenyl




126-127






710




2,2-Difluoroethyl




i-Pr




4-F-Phenyl




94-96






711




2,2-Difluoroethyl




i-Pr




2,4-diF-Phenyl




105-108






712




1-(4-Chlorobutyl)




i-Pr




4-F-Phenyl




oil*






713




1-(3-Chloropropyl)




i-Pr




4-F-Phenyl




oil*






714




1-(2-Chloropropyl) (S)




i-Pr




2,4-diF-Phenyl




oil*






715




(2-Tetrahydropyranyl)methyl




i-Pr




2,4-diF-Phenyl




oil*






716




(2-Phenyl-1,3,4-oxadiazol-5-yl)methyl




i-Pr




Phenyl




130-132






717




1-(Cyclobutyl)ethyl




i-Pr




Phenyl




oil*






718




1-(Cyclobutyl)ethyl




i-Pr




4-F-Phenyl




oil*






719




Me


2


NC(O)CH


2


CH


2






i-Pr




4-Cl-Phenyl




82-83






720




1-(Cyclopropyl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






721




1-(3,4-Dihydroisoxazol-3-yl)ethyl




i-Pr




4-F-Phenyl




oil*






722




(5-Phenyl-1, 2, 5-oxadiazol-2-yl)methyl




i-Pr




Phenyl




120-121






723




PhCH(CO


2


Me)




i-Pr




Phenyl




oil*






724




PhCH(CO


2


Me)




i-Pr




4-Cl-Phenyl




oil*






725




1-(2-Chloro-1-methoxyethyl)




i-Pr




4-Cl-Phenyl




oil*






726




1-(1,2-Dimethoxyethyl)




i-Pr




4-Cl-Phenyl




oil*






727




CH


3


C(O)NHCH


2


CH


2






i-Pr




4-F-Phenyl




oil*






728




Me


2


NC(S)CH(CH


3


)




i-Pr




4-F-Phenyl




130






729




1-(3,4-Dihydroisoxazol-3-yl)ethyl




i-Pr




Phenyl




oil*






730




1-(3,4-Dihydroisoxazol-3-yl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






731




1-(2-(6-Chloro-2-pyridyl)-2-propenyl)




i-Pr




Phenyl




oil*






732




1-(2-Carbomethoxy-2-propenyl)




i-Pr




4-F-Phenyl




oil*






733




Me


2


NC(S)CH(CH


3


)




i-Pr




4-Cl-Phenyl




136






734




1-(1,2-Dimethoxyethyl)




i-Pr




Phenyl




oil*






735




1-(2-Chloro-1-methoxyethyl)




i-Pr




Phenyl




oil*






736




(EtO)


2


P(O)CH


2






i-Pr




2,4-diF-Phenyl




113-115






737




1-(2-Chloro-1-methoxyethyl)




i-Pr




2,4-diF-Phenyl




oil*






738




1-(1,2-Dimethoxyethyl)




i-Pr




2,4-diF-Phenyl




oil*






739




Me


2


NC(S)CH(CH


3


)




i-Pr




2,4-diF-Phenyl




107






740




(5,6-Dihydro-1,2,4-Dioxazin-3-yl)methyl




i-Pr




4-Cl-Phenyl




107






741




PhCON(CH


3


)CH


2


CH


2






i-Pr




4-F-Phenyl




141-146






742




1-(1-Ethoxypropyl)




i-Pr




4-F-Phenyl




oil*






743




Propargyl




i-Pr




4-F-Phenyl




oil*






744




1-(3-Butynyl)




i-Pr




2,4-diF-Phenyl




oil*






745




2,2-Difluoroethyl




i-Pr




4-Cl-Phenyl




104-107






746




2,2-Difluoroethyl




i-Pr




Phenyl




oil*






747




1-(2-Chloropropyl) (S)




i-Pr




Phenyl




oil*






748




1-(2-Chloropropyl) (S)




i-Pr




4-Cl-Phenyl




oil*






749




1-(3-Chloropropyl)




i-Pr




4-Cl-Phenyl




68-72






750




1-(3-Chloropropyl)




i-Pr




Phenyl




oil*






751




s-Butyl




i-Pr




4-F-Phenyl




42-44






752




1-(3-Bromo-2-methylpropyl)




i-Pr




4-F-Phenyl




 96-100






753




3-(4-Pentynyl)




i-Pr




4-F-Phenyl




oil*






754




Propargyl




i-Pr




Phenyl




75-76






755




Bromomethyl




i-Pr




Phenyl




82-84






756




1-(4,5-Dimethylthiazol-2-yl)ethyl




i-Pr




Phenyl




101-104






757




1-(4,5-Dimethylthiazol-2-yl)ethyl




i-Pr




4-F-Phenyl




103-105






758




(5,6-Dihydro-1,2,4-Dioxzain-3-yl)methyl




i-Pr




2,4-diF-Phenyl




oil*






759




1-(3,4-Dihydroisoxazol-3-yl)ethyl




i-Pr




4-Cl-Phenyl




oil*






760




(5,6-Dihydro-6-OMe-1,2-oxazin-3-yl)methyl




i-Pr




4-Cl-Phenyl




107-109






761




PhCON(CH


3


)CH


2


CH


2






i-Pr




Phenyl




124-127






762




PhCON(CH


3


)CH


2


CH


2






i-Pr




2,4-diF-Phenyl




106-108






763




2-(3-Butynyl)




i-Pr




4-F-Phenyl




oil*






764




Propargyl




i-Pr




2,4-diF-Phenyl




oil*






765




(5,6-Dihydro-1,2,4-Dioxazin-3-yl)methyl




i-Pr




4-F-Phenyl




oil*






766




(Dihydro-6-OMe-1,2-oxazin-3-yl)methyl




i-Pr




4-F-Phenyl




oil*






767




1-(3-Butynyl)




i-Pr




4-F-Phenyl




oil*






768




1-(3-Butynyl)




i-Pr




Phenyl




oil*






769




(5-i-Propyl-1, 2, 5-oxadiazol-2-yl)methyl




i-Pr




Phenyl




oil*






770




(5-c-Hexyl-1, 2, 5-oxadiazol-2-yl)methyl




i-Pr




Phenyl




106-108






771




i-Propyl




i-Pr




2-Cl-5-Pyridiyl




oil*






772




1-(1-Ethoxypropyl)




i-Pr




4-Cl-Phenyl




oil*






773




1-(1-Ethoxypropyl)




i-Pr




Phenyl




oil*






774




1-(1-Ethoxypropyl)




i-Pr




2,4-diF-Phenyl




oil*






775




CH


3


O


2


CN(CH


3


)CH


2


CH


2






i-Pr




Phenyl




oil*






776




(EtO)


2


P(O)CH(CH


3


)




i-Pr




2,4-diF-Phenyl




oil*






777




(CH


3


O)


2


P(O)CH


2


CH


2






i-Pr




2,4-diF-Phenyl




oil*






778




CH


3


O


2


CN(CH


3


CH


2


CH


2






i-Pr




2,4-diF-Phenyl




oil*






779




CH


3


O


2


CN(CH


3


CH


2


CH


2






i-Pr




4-Cl-Phenyl




oil*






780




i-Propyl




i-Pr




4-OMe-Phenyl




93-94






781




1-(3-Methyl-3-nitropropyl)




i-Pr




2,4-diF-Phenyl




118-120






782




1-(3, 3-Dichloro-2-propenyl)




i-Pr




4-F-Phenyl




oil*






783




3-(4-Pentynyl)




i-Pr




2,4-diF-Phenyl




oil*






784




Propargyl




i-Pr




4-Cl-Phenyl




oil*






785




1-(4,5-Dimethylthiazol-2-yl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






786




Pyrrolidinothiocarbonylmethyl




i-Pr




2,4-diF-Phenyl




 68






787




Pyrrolidinothiocarbonylmethyl




i-Pr




4-Cl-Phenyl




144






788




Pyrrolidinothiocarbonylmethyl




i-Pr




Phenyl




117






789




Pyrrolidinothiocarbonylmethyl




i-Pr




4-F-Phenyl




142






790




2-(3-Methoximinopropyl)




i-Pr




Phenyl




82-87






791




1-(4-Chlorobutyl)




i-Pr




4-Cl-Phenyl




103-109






792




1-(4-Chlorobutyl)




i-Pr




Phenyl




oil*






793




4-Cyclohexenyl




i-Pr




4-F-Phenyl




107-108






794




1-(2-Bromoethyl)




i-Pr




4-F-Phenyl




105-106






795




1-(2-Bromoethyl)




i-Pr




2,4-diF-Phenyl




77-80






796




1-(2-Bromoethyl)




i-Pr




4-Cl-Phenyl




85-87






797




(Pinenyl)methyl




i-Pr




Phenyl




oil*






798




i-Propyl




i-Pr




(3,5-Dimethylisoxazol-4-yl)methyl




oil*






799




1-(2,2-Dimethylcyclopropyl)




i-Pr




4-F-Phenyl




69-72






800




1-(2,2-Dimethylcyclopropyl)




i-Pr




Phenyl




oil*






801




1-(2,2-Dimethylcyclopropyl)




i-Pr




4-Cl-Phenyl




oil*






802




1-(2,2-Dimethylcyclopropyl)




i-Pr




2,4-diF-Phenyl




oil*






803




3-(4-Pentynyl)




i-Pr




Phenyl




oil*






804




1-(3-Butynyl)




i-Pr




4-Cl-Phenyl




oil*






805




2-(1,3-Dibromopropyl)




i-Pr




4-F-Phenyl




oil*






806




1-(3-Bromo-2,2-dimethylpropyl)




i-Pr




4-F-Phenyl




122-126






807




(5,6-Dihydro-6-methoxy-,2-oxazin-3-yl)methyl




i-Pr




2,4-diF-Phenyl




110-115






808




3-(4-Pentynyl)




i-Pr




4-Cl-Phenyl




oil*






809




(5,6-Dihydro-6-methoxy-1,2-oxazin-3-yl)methyl




i-Pr




Phenyl




96-98






810




1-(4,5-Dihydro-5-methoxyisoxazol-3-yl)ethyl




i-Pr




4-F-Phenyl




oil*






811




1-(4,5-Dihydroisoxazol-5-yl)ethyl




i-Pr




4-F-Phenyl




oil*






812




1-(4,5-Dihydro-5-methoxyisoxazol-3-yl)ethyl




i-Pr




Phenyl




oil*






813




i-Pr




c-PrCH


2






4-F-Phenyl




76-77






814




1-(4,5-Dihydroisoxazol-5-yl)ethyl




i-Pr




4-Cl-Phenyl




oil*






815




1-(4,5-Dihydroisoxazol-5-yl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






816




1-(4,5-Dihydroisoxazol-5-yl)ethyl




i-Pr




Phenyl




oil*






817




2-(1,1,1-Trifluoropropyl)




i-Pr




2,4-diF-Phenyl




oil*






818




3-(1-Trimethylsilylpropyl)




i-Pr




4-F-Phenyl




oil 






819




1-(2,3-Epoxy-2-methylpropyl) (R)




i-Pr




4-F-Phenyl




oil*






820




1-(2,3-Epoxy-2-methylpropyl) (S)




i-Pr




4-F-Phenyl




78-80






821




(MeO


2


C)


2


CH




i-Pr




Phenyl




oil 






822




1-(3-Chloropropyl)




i-Pr




2,4-diF-Phenyl




oil*






823




1-(4-Chlorobutyl)




i-Pr




2,4-diF-Phenyl




oil*






824




2-(3-Chloro-3-methoxypropyl)




i-Pr




Phenyl




oil*






825




2-(3-Chloro-3-methoxypropyl)




i-Pr




4-F-Phenyl




oil*






826




1-(2,2-Dichloroethyl)




i-Pr




4-F-Phenyl




95-98






827




1-(2-Butynyl)




i-Pr




2,4-diF-Phenyl




131-132






828




1-(2-Butynyl)




i-Pr




4-F-Phenyl




  115-116.5






829




i-Pr




i-Pr




(5-t-Butyl-1,2,4-oxadiazol-3-yl)methyl




oil*






830




1-(2-Butynyl)




i-Pr




4-Cl-Phenyl




24-25






831




1-(2-Cyclopropylethyl)




i-Pr




4-F-Phenyl




70-72






832




1-(2-Cyclopropylethyl)




i-Pr




Phenyl




70-72






833




1-(2-Butynyl)




i-Pr




Phenyl




90.5-92  






834




1-(1,3-Dioxolan-2-yl)ethyl




i-Pr




4-F-Phenyl




104-107






835




1-(1,3-Dioxan-2-yl)ethyl




i-Pr




4-F-Phenyl




94-96






836




1-(5,5-Dimethyl-1,3-dioxan-2-yl)ethyl




i-Pr




4-F-Phenyl




90-93






837




1-(1,3-Dioxepin-5-en-2-yl)ethyl




i-Pr




4-F-Phenyl




oil*






838




i-Pr




i-Pr




2,6-DiF-Phenyl




80-83






839




i-Pr




i-Pr




2,3-DiF-Phenyl




oil*






840




i-Pr




Et




4-F-Phenyl




oil*






841




2-(3-Butenyl)




i-Pr




4-Cl-Phenyl




oil*






842




2-(3-Butenyl)




i-Pr




2,4-diF-Phenyl




oil*






843




2-(3-Butenyl)




i-Pr




Phenyl




oil*






844




1-(3-Methylenecyclobutane)




i-Pr




4-F-Phenyl




60-61






845




1-(3-Methylenecyclobutane)




i-Pr




2,4-diF-Phenyl




oil*






846




1-(3-Methylenecyclobutane)




i-Pr




Phenyl




oil*






847




1-(3-Methylenecyclobutane)




i-Pr




4-Cl-Phenyl




81-84






848




3-Cyclopentene




i-Pr




4-F-Phenyl




71-74






849




HC(O)CH(CH


3


)




i-Pr




4-Cl-Phenyl




oil*






850




HC(O)CH(CH


3


)




i-Pr




Phenyl




oil*






851




(3-Chloro-1-methylpyrazol-4-yl)methyl




i-Pr




4-F-Phenyl




105-107






852




(3-Chloro-1-methylpyrazol-4-yl)methyl




i-Pr




4-Cl-Phenyl




oil*






853




(3-Chloro-1-methylpyrazol-4-yl)methyl




i-Pr




Phenyl




oil*






854




(3-Chloro-1-methylpyrazol-4-yl)methyl




i-Pr




2,4-diF-Phenyl




oil*






855




(1-Methyl-5-chloro-3-trifluoromethylpyrazol-4-yl)methyl




i-Pr




Phenyl




152-154






856




(1-Methyl-5-chloro-3-trifluoromethylpyrazol-4-yl)methyl




i-Pr




4-F-Phenyl




148-149






857




(1-Methyl-5-chloro-3-trifluoromethylpyrazol-4-yl)methyl




i-Pr




2,4-diF-Phenyl




112-114






858




(1-Methyl-5-chloro-3-trifluoromethylpyrazol-4-yl)methyl




i-Pr




4-Cl-Phenyl




132-136






859




(1-Methyl-4-bromopyrazol-3-yl)methyl




i-Pr




Phenyl




161-165






860




(1-Methyl-4-bromopyrazol-3-yl)methyl




i-Pr




4-F-Phenyl




124-132






861




1-(1-Methyl-4-bromopyrazol-3-yl)ethyl




i-Pr




Phenyl




123-124






862




1-(1-Methyl-4-bromopyrazol-3-yl)ethyl




i-Pr




4-F-Phenyl




122-124






863




(1-Methyl-4-bromopyrazol-3-yl)methyl




i-Pr




4-Cl-Phenyl




147-150






864




1-(1-Methyl-4-bromopyrazol-3-yl)ethyl




i-Pr




4-Cl-Phenyl




119-121






865




(1-Methyl-4-bromopyrazol-3-yl)methyl




i-Pr




2,4-diF-Phenyl




116-117






866




1-(1-Methyl-4-bromopyrazol-3-yl)ethyl




i-Pr




2,4-diF-Phenyl




oil*






867




Cyclooctyl




i-Pr




4-F-Phenyl




81-84






868




i-Pr




2-(3-MeO-propyl)




Phenyl




73-77






869




i-Pr




2-(3-MeO-propyl)




4-F-Phenyl




119-125






870




i-Pr




2-(3-MeO-propyl)




4-Cl-Phenyl




76-81






871




2-(3-Chloro-3-methoxypropyl)




i-Pr




4-Cl-Phenyl




oil*






872




2-(3-Chloro-3-methoxypropyl)




i-Pr




2,4-diF-Phenyl




oil*






873




1-(2,2-Dichloroethyl)




i-Pr




4-Cl-Phenyl




80-88






874




1-(2,2-Dichloroethyl)




i-Pr




Phenyl




95-96






875




1-(2-Chloropropyl) (S)




i-Pr




4-F-Phenyl




55-60






876




2-(1,1,1-Trifluoropropyl)




i-Pr




4-Cl-Phenyl











877




Cyclooctyl




i-Pr




Phenyl




50-58






878




i-Pr




Allyl




Phenyl




58-60






879




Cyclooctyl




i-Pr




4-Cl-Phenyl




 99-103






880




Cyclooctyl




i-Pr




2,4-diF-Phenyl




89-93






881




Me


2


NC(O)OCH


2


CH


2






i-Pr




4-F-Phenyl




94-96






882




3-(1-Hexynyl)




i-Pr




Phenyl




oil*






883




i-Pr




(CD


3


)


2


CH




4-F-Phenyl




66-68






884




1-(3-Allyloxy-2-methoximinopropyl)




i-Pr




4-F-Phenyl




oil*






885




1-(3-Allyloxy-2-methoximinopropyl)




i-Pr




Phenyl




oil*






886




1-(3-Allyloxy-2-methoximinopropyl)




i-Pr




2,4-diF-Phenyl




oil*






887




1-(3-Allyloxy-2-methoximinopropyl)




i-Pr




4-Cl-Phenyl




oil*






888




i-Pr




2-(1-Chloropropyl)




4-Cl-Phenyl




oil*






889




(1,3-Dioxolan-4-yl)methyl




i-Pr




4-F-Phenyl




75-78






890




(2,2-Dimethyl-1,3-dioxolan-4-yl)methyl




i-Pr




4-F-Phenyl




110-113






891




(1,3-Dioxolan-4-yl)methyl




i-Pr




Phenyl




91-96






892




2-Methoxymethylpyrrolidin-1-yl




i-Pr




4-F-Phenyl




oil*






893




1-(3-Methylbutyl)




i-Pr




Phenyl




63-65






894




1-(3-Methylbutyl)




i-Pr




4-Cl-Phenyl




64-66






895




1-(3-Methylbutyl)




i-Pr




4-F-Phenyl




88-91






896




1-(3-Methylbutyl)




i-Pr




2,4-diF-Phenyl




54-56






897




3-(1-Hexynyl)




i-Pr




2,4-diF-Phenyl




63-64






898




1-(1,3-Dioxepin-2-yl)ethyl




i-Pr




4-F-Phenyl




oil*






899




(1,3-Dioxolan-2-yl)methyl




i-Pr




4-F-Phenyl




84-87






900




1-(3-Benzyloxy-2-methoximinopropyl)




i-Pr




4-F-Phenyl




oil*






901




1-(3-Benzyloxy-2-methoximinopropyl)




i-Pr




Phenyl




oil*






902




1-(3-Methoxy-2-methoximinopropyl)




i-Pr




4-F-Phenyl




oil*






903




1-(3-Methoxy-2-methoximinopropyl)




i-Pr




Phenyl




oil*






904




1-(3-Methoxy-2-methoximinopropyl)




i-Pr




Phenyl




oil*






905




i-Pr




2-(1,1-Dimethoxypropyl)




4-Cl-Phenyl




oil*






906




i-Pr




2-(1-Chloropropyl)




Phenyl




92-94






907




i-Pr




2-(1-Chloropropyl)




4-F-Phenyl




95-97






908




i-Pr




2-(3-Chloropropyl)




Phenyl




oil*






909




i-Pr




2-(3-Chloropropyl)




4-F-Phenyl




oil*






910




i-Pr




n-Bu




4-F-Phenyl




72-73






911




i-Pr




n-Pr




4-F-Phenyl




63-64






912




i-Pr




i-Bu




4-F-Phenyl




66-67






913




CH


3


C(O)CH


2


CH


2






i-Pr




Phenyl




oil*






914




HC(O)CH


2


CH


2






i-Pr




4-F-Phenyl




oil*






915




CH


3


C(O)CH


2


CH


2


CH


2






i-Pr




2,4-diF-Phenyl




oil*






916




CH


3


C(O)CH


2


CH


2


CH


2






i-Pr




4-Cl-Phenyl




oil*






917




3-(1-Hexynyl)




i-Pr




4-Cl-Phenyl




oil*






918




i-Pr




2-(1,1,1-Trifluoropropyl)




Phenyl




92-94






919




i-Pr




2-(1,1-Dimethoxypropyl)




Phenyl




oil*






920




i-Pr




2-(1,1-Dimethoxypropyl)




4-F-Phenyl




oil*






921




i-Pr




1-(1-Cyanoethyl)




4-F-Phenyl




80-82






922




1-(3-Methoxy-2-methoximinopropyl)




i-Pr




4-Cl-Phenyl




oil*






923




1-(3-Methoxy-2-methoximinopropyl)




i-Pr




2,4-diF-Phenyl




oil*






924




i-Pr




Allyl




4-F-Phenyl




57-59






925




i-Pr




c-Hexyl




4-F-Phenyl




126-131






926




i-Pr




c-Pentyl




4-F-Phenyl




93-95






927




3-(Cyclopentene)




i-Pr




2,4-diF-Phenyl




oil*






928




3-(Cyclopentene)




i-Pr




4-Cl-Phenyl




100-103






929




3-(Cyclopentene)




i-Pr




Phenyl




oil*






930




1-(3-Oxocyclobutyl)




i-Pr




4-F-Phenyl




oil*






931




1-(3-Oxocyclobutyl)




i-Pr




2,4-diF-Phenyl




95-97






932




1-(3-Oxocyclobutyl)




i-Pr




Phenyl




148-150






933




1-(3-Oxocyclobutyl)




i-Pr




4-Cl-Phenyl




120-122






934




CH


3


C(O)CH


2


CH


2






i-Pr




4-F-Phenyl




94-95






935




CH


3


C(O)CH


2


CH


2






i-Pr




2,4-diF-Phenyl




oil*






936




CH


3


C(O)CH


2


CH


2






i-Pr




4-Cl-Phenyl




111-113






937




1-(3-Butenyl)




i-Pr




4-F-Phenyl




40-42






938




1-(3-Butenyl)




i-Pr




2,4-diF-Phenyl




58-60






939




1-(3-Butenyl)




i-Pr




Phenyl




43-45






940




1-(3-Butenyl)




i-Pr




4-Cl-Phenyl




50-51






941




i-Pr




Neopentyl




4-F-Phenyl




88-89






942




i-Pr




(CH


3


)


3


CCH


2


CH


2






4-F-Phenyl




79-80






943




2-(1-Chloro-3-Fluoropropyl)




i-Pr




4-Cl-Phenyl




87-90






944




2-(1,3-Dichloropropyl)




i-Pr




4-Cl-Phenyl




79-82






945




4-(2,3,5,6-Tetrahydrothiopyranyl)




i-Pr




4-F-Phenyl




163-165






946




4-(2,3,5,6-Tetrahydrothiopyranyl)




i-Pr




Phenyl




145-148






947




4-(2,3,5,6-Tetrahydrothiopyranyl)




i-Pr




2,4-diF-Phenyl




oil*






948




4-(2,3,5,6-Tetrahydrothiopyranyl)




i-Pr




4-Cl-Phenyl




153-157






949




3-(2,3,4,5-Tetrahydrothienyl)




i-Pr




4-F-Phenyl




67-70






950




2-(1-Chloro-3-Fluoropropyl)




i-Pr




Phenyl




100-103






951




i-Pr




3-(2,3,4,5-




4-F-Phenyl




114-117








Tetrahydrothienyl)






952




i-Pr




N═CHMe




Phenyl




oil*






953




i-Pr




N═CMe


2






Phenyl




oil*






954




PyrrolidinoC(O)OCH


2


CH


2






i-Pr




Phenyl




100-104






955




i-Pr




2-(1,3-DiCl-propyl)




Phenyl




oil*






956




i-Pr




(2-(1,3-DiCl-propyl)




4-F-Phenyl




oil*






957




i-Pr




3-(2-Me-butyl)




4-F-Phenyl




109-110






958




c-Pr




(CD


3


)


2


CH




4-F-Phenyl




69-70






959




3-(2-Methyl-4-pentynyl)




i-Pr




Phenyl




oil*






960




EtOC(O)OCH


2


CH


2






i-Pr




4-F-Phenyl




105-108






961




i-Pr




3-Pentyl




4-F-Phenyl




55-57






962




CH


3


C(O)CH


2


CH


2


CH


2






i-Pr




4-F-Phenyl




oil*






963




CH


3


C(O)CH


2


CH


2


CH


2






i-Pr




Phenyl




oil*






964




HC(O)CH


2


CH


2






i-Pr




2,4-diF-Phenyl




oil*






965




HC(O)CH


2


CH


2






i-Pr




Phenyl




oil*






966




HC(O)CH


2


CH


2






i-Pr




4-Cl-Phenyl




 98-100






967




4-(1-Hexynyl)




i-Pr




4-F-Phenyl




oil*











*see Index Table D for


1


H NMR data.
























INDEX TABLE D











Cmpd






1


H NMR Data (CDCl


3


solution unless







No.




indicated otherwise)


a















 77




δ 7.30(d, 1H), 7.20(d, 1H), 6.99(m, 1H), 4.89(s, 2H),








3.50(q, 4H), 1.24(t, 6H).







 80




δ 7.22(m, 4H), 7.09(m, 2H), 6.96(m, 1H), 4.78(s, 2H),








4.42(m, 1H), 1.20(d, 6H).







 82




δ 7.32(d, 1H), 7.20(d, 1H), 7.00(m, 1H), 4.90(s, 2H),








3.95(m, 1H), 3.40(m, 2H), 1.82(m, 4H), 1.70-1.50(m,








2H), 1.40-1.20(m, 7H).







 83




δ 7.3(d, 1H), 7.19(d, 1H), 6.96(m, 1H), 4.88(s, 2H),








4.38(m, 1H), 4.20(s,2H), 3.80(t, 2H) 2.30(br.s, 2H),








1.28(d, 6H).







 84




δ 7.41(d, 1H), 7.10(m, 4H), 4.75(s, 2H), 3.50(q, 4H),








3.45(s, 3H), 1.24(t, 6H).







 85




δ 7.41-7.14(m, 9H), 4.66(s, 2H), 3.44(s, 3H), 2.37








(s, 3H).







 87




δ 7.38(m, 1H), 7.10(m, 4H), 6.92(m, 2H), 4.64(m, 3H),








2.36(s, 3H), 1.10(m, 6H).







 90




δ 7.10(m, 8H), 5.20(m, 1H), 4.60(m, 1H), 2.80(m, 3H),








2.20(m, 2H) 1.20(d, 6H).







 91




δ 7.22(m, 2H), 7.08(m, 2H), 4.62(m, 1H), 3.42(t, 2H),








1.62(m, 2H), 1.20(d, 6H), 0.90(t, 3H).







 92




δ 7.40(m, 2H), 7.12(m, 2H), 4.64(m, 1H), 3.42(t, 2H),








1.62(m, 2H), 1.20(d, 6H), 0.90(t, 3H).







 99




δ 7.3(m, 2H), 7.1(m, 2H), 4.7(m, 1H), 4.1(m, 1H),








2.4-2.7(m, 2H), 2.2(m, 1H), 2.0(m, 1H), 1.3-1.8








(m, 5H), 1.2(d, 6H).







101




δ 6.87(t, 2H), 6.52(dd, 2H), 3.57(m, 1H), 2.91(q,








2H), 2.70(s, 3H), 1.32(t, 3H), 1.19(d, 6H).







105




δ 7.40(d, 2H), 7.20(d, 2H), 5.80(m, 1H), 5.30(m, 2H),








4.04(d, 2H), 1.20(d, 6H).







106




δ 7.40-7.08(m, 9H), 4.40(m, 3H), 1.20(d, 6H).







115




δ 7.40(d, 2H), 7.10(d, 2H), 4.62(m, 1H), 3.42(t, 2H),








1.64(q, 2H), 1.20(d, 6H), 0.92(t, 3H).







126




δ 5.87(br m, 1H), 4.41(m, 1H), 4.27(m, 2H), 3.86(t, 2H),








2.41(s, 3H), 2.35(br m, 2H), 2.25(s, 3H), 1.32(d, 6H).







127




δ 7.3(m, 1H), 6.8-7.0(m, 2H), 5.7-5.9(m, 1H),








5.2-5.4(t, 2H), 4.1(d, 2H), 3.3(m, 1H), 1.3(m, 2H), 0.7








(d, 2H).







128




δ 7.2-7.4(m, 4H), 7.1(t, 2H), 4.8(m, 1H), 4.2(g, 4H),








4.0(s, 2H), 1.3(t, 6H), 1.1(d, 6H).







129




δ 7.40-7.20(m, 5H), 4.62(m, 1H), 3.42(t, 2H), 1.58(s,








9H), 1.20(d, 6H).







130




δ 7.38(m, 1H), 6.94(m, 2H), 4.64(m, 1H), 3.43(t, 2H),








1.62(m, 2H), 1.20(m, 6H), 0.90(t, 3H).







133




δ 7.40-7.18(m, 9H), 5.18(q, 1H), 4.40(m, 1H), 1.80(d,








3H), 1.18(d, 6H).







134




δ 7.40-7.10(m, 9H), 5.18(q, 1H), 4.42(m, 1H), 1.80(d,








3H), 1.18(d, 6H).







135




δ 7.27(m, 2H), 7.11(t, 2H), 4.69(m, 1H), 2.92(m, 1H),








2.76(m, 1H), 1.32-1.14(m, 18H).







144




δ 7.40-7.27(m, 8H), 5.80(s, 1H), 4.86(s, 2H), 4.40(m,








1H), 4.22(s, 2H), 3.80(t, 2H), 2.30(s, 2H), 1.28(d, 6H).







145




δ 7.40-7.27(m, 4H), 5.80(br.s, 1H), 4.86(s, 2H), 4.30








(m, 1H), 2.38(m, 1H), 2.16(m, 4H), 1.90(m, 1H),








1.70(m, 2H), 1.26(d, 6H).







147




δ 5.8(m, 2H), 5.38(m, 2H), 4.4(m, 1H), 4.22(s, 2H),








4.08(m, 2H), 3.83(t, 2H), 2.30(br.s, 2H), 1.26(d, 6H).







148




δ 7.22(m, 2H), 7.10(m, 2H), 4.40(m, 1H), 3.80-3.50(m,








4H), 1.21(d, 6H).







149




δ 5.72(s, 1H), 4.40(m, 1H), 4.28(s, 2H), 4.16(m, 2H),








7.10(m, 2H), 4.40(m, 1H), 3.80-3.50(m, 4H),








1.21(d, 6H).







150




δ 5.82(s, 1H), 5.38(m, 2H), 4.18(d, 2H), 3.72(br.s, 2H),








3.54(br.s, 2H), 1.96(br.s, 4H).







151




δ 7.30(m, 1H), 6.92(m, 2H), 5.80(m, 1H), 5.26(m, 2H),








4.42(m, 1H), 4.06(d, 2H), 1.2(m, 6H).







152




δ 7.40(m, 5H), 4.71(s, 2H), 3.50(q, 4H), 1.24(t, 6H).







153




δ 7.31(m, 10H), 4.61(s, 2H), 3.43(s, 3H).







172




δ 7.40(m, 1H), 6.94(m, 2H), 4.62(m, 1H), 4.02(m, 1H),








3.40(m, 1H), 1.20(m, 6H), 0.78(d, 3H).







174




δ 7.20-7.40(m, 4H), 5.02(m, 1H), 4.62(m, 1H), 1.80(d,








3H), 1.18(d, 6H).







178




δ 7.40-7.20(m, 4H), 4.62(m, 1H), 3.40(m, 1H), 1.20(d,








6H), 0.78(d, 3H).







180




δ 7.3(m, 1H), 7.2-7.1(d, 2H), 5.1-5.0(m, 1H), 3.99(s,








6H), 2.22(s, 6H), 1.46(d, 6H).







181




δ 7.5-7.1(m, 4H), 5.1-5.0(m, 1H), 4.00(s, 6H), 2.26(s,








3H), 1.5(d, 6H).







182




δ 5.0(m, 1H), 4.3(m, 1H), 3.97(s, 6H), 1.5-1.4(m, 12H).







183




δ 7.3(m, 2H), 7.0(m, 1H), 6.8(m, 2H), 3.9(m, 1H),








3.4(m, 5H), 1.9-1.1(m, 13H).







184




δ 7.2(m, 2H), 7.1(m, 2H), 4.6(m, 1H), 4.1-3.8(m, 1H),








2.2-1.7(m, 9H), 1.2(d, 6H).







188




δ 7.25(m, 2H), 7.10(m, 2H), 4.65(m, 1H), 3.65(m, 2H),








3.20(m, 1H), 2.80(t, 1H), 2.62(m, 1H), 1.21(d, 6H).







189




δ 8.6(m, 2H), 7.2(m, 2H), 4.69(s, 2H), 4.3(m, 1H),








3.5(bm, 2H), 1.50(d, 6H), 1.22(t, 3H).







190




δ 8.97(s, 1H), 4.6(q, 2H), 4.4(m, 1H), 1.5(m, 9H).







191




δ 7.37(d, 2H), 7.19(d, 2H), 4.70(s, 2H), 4.55-4.67(m,








1H), 2.61(s, 3H), 2.42(s, 3H), 1.20(d, 6H).







192




δ 7.20-7.25(m, 2H), 7.04-7.10(m, 2H), 4.70(s, 2H),








4.58-4.67(m, 1H), 2.61(s, 3H), 2.42(s, 3H), 1.19(d, 6H).







196




δ 7.38-7.41(m, 2H), 7.20-7.23(m, 2H), 4.62-4.71








(m, 1H), 2.66(s, 3H), 2.21(s, 3H), 1.23(d, 6H).







197




δ 7.41-7.43(m, 3H), 7.25-7.28(m, 2H), 4.61-4.74








(m, 1H), 2.65(s, 3H), 2.19(s, 3H), 1.24(d, 6H).







198




δ 7.25-7.28(m, 2H), 7.11(t, 2H), 4.61-4.74(m, 1H),








2.66(s, 3H), 2.21(s, 3H), 1.23(d, 6H).







201




δ 7.4(m, 3H), 7.2-7.25(m, 3H), 7.1-7.2(t, 2H),








4.6-4.8(m, 1H), 2.3-2.4(q, 2H), 2.07(s, 3H), 1.2(d, 6H),








1.0(t, 3H).







206




δ 7.40-7.20(m, 5H), 6.40(m, 1H), 6.36(m, 1H), 4.60(m,








3H), 1.20(d, 6H).







207




δ 7.40(s, 1H) 7.20(m, 2H), 7.18(m, 2H), 4.60(m, 3H),








1.20(d, 6H).







208




δ 7.40(m, 2H), 6.94(t, 2H), 6.38(m, 1H), 6.36(m, 1H),








4.62(m, 3H), 1.20(d, 6H).







210




δ 7.29(m, 7H), 7.17(m, 2H), 6.65(d, 1H), 6.1(m, 1H),








4.65(m, 1H), 4.22(d, 2H), 1.2(d, 6H).







213




δ 7.23(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 4.24(s, 2H),








1.2(d, 6H), 0.14(s, 9H).







214




δ 7.24(m, 2H), 7.1(m, 2H), 6.75(m, 1H), 5.92(m, 1H),








4.65(m, 1H), 4.2(m, 4H), 1.28(t, 3H), 1.2(d, 6H).







215




δ 7.23(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 4.21(s, 2H),








3.77(s, 3H), 1.2(d, 6H).







216




δ 7.27(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 4.38(s, 2H),








1.21(m, 15H).







217




δ 7.2(m, 2H), 7.1(m, 2H), 4.65(m, 1H), 4.25(s, 2H),








2.22(s, 3H), 1.2(d, 6H).







218




δ 7.23(m, 2H), 7.11(m, 2H), 4.65(m, 1H), 3.7(t, 2H),








2.65(m, 2H), 1.2(d, 6H).







220




δ 7.23(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 3.68(m, 4H),








3.55(m, 2H), 3.44(m, 2H), 3.31(s, 3H), 1.2(d, 6H).







221




δ 7.22(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 3.47(t, 2H),








1.6(m, 2H), 1.3(m, 2H), 1.2(d, 6H), 0.9(t, 3H).







222




δ 7.40(m, 1H), 6.90(m, 2H), 4.70(m, 1H), 3.71(s, 3H),








2.31(s, 3H), 2.10(s, 3H), 1.20(m, 6H).







223




δ 7.26(m, 2H), 7.15(m, 4H), 6.70(m, 1H), 2.33(s, 3H),








2.15(s, 3H), 1.20(m, 6H).







225




δ 7.40(m, 3H), 7.30(m, 2H), 4.65(m, 1H), 2.80(s, 6H),








1.20(s, 6H).







229




δ 7.20(m, 8H), 4.66(m, 1H), 2.64(t, 2H), 2.13(s, 3H),








1.59(m, 2H), 1.35(m, 2H), 1.23(m, 6H), 0.94(t, 3H).







230




δ 7.40-7.13(m, 8H), 4.68(m, 1H), 2.69(q, 2H), 2.14








(s, 3H), 1.26(m, 9H).







232




δ 7.37(m, 3H), 7.20-7.30(m, 2H), 4.68(s, 2H), 4.61








(m, 1H), 2.61(s, 3H), 2.41(s, 3H), 1.20(d, 6H).







233




δ 7.37(dd, 1H), 6.92(dd, 1H), 4.69(s, 2H), 4.61(m, 1H),








2.61(s, 3H), 2.41(s, 3H), 1.21(d, 6H).







236




δ 7.28(m, 8H), 4.53(m, 1H), 2.33(s, 3H), 2.20(s, 1.5H),








2.07(s, 1.5H), 1.44(d, 3H), 1.16(d, 3H).







238




δ 7.40(m, 3H), 5.05(m, 1H), 4.60(m, 1H), 1.80(d, 3H),








1.20(m, 6H).







241




δ 7.37(d, 2H), 7.19(d, 2H), 4.61(m, 1H), 2.65(m, 1H),








1.119(d, 6H), 0.97(m, 4H).







248




δ 7.40(m, 2H), 7.05(m, 2H), 4.80(q, 1H), 4.25(q, 2H),








3.55(q, 2H), 1.43(d, 3H), 1.30(m, 12H).







251




δ 7.23(m, 2H), 7.11(m, 2H), 4.65(m, 1H), 3.34(d, 2H),








1.22(m, 7H), 0.55(m, 2H), 0.35(m, 2H).







252




δ 7.22(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 4.25(s, 2H),








2.48(q, 2H), 1.19(d, 6H), 1.1(t, 3H).







253




δ 7.22(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 3.4(m, 4H),








1.9-1.19(m, 34H), 0.88(m, 7H).







254




δ 7.23(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 4.22(m, 2H),








2.13(m, 2H), 1.45(m, 2H), 1.29(m, 4H), 10.88(m, 3H).







256




δ 7.2(m, 2H), 7.04(m, 2H), 4.61(m, 3H), 3.88(s, 2H),








1.43(s, 2H), 0.04(m, 9H).







257




δ 7.23(m, 2H), 7.1(m, 2H), 4.65(m, 1H), 3.46(m, 3H),








1.67-0.9(m, 18H).







258




δ 7.23(m, 2H), 7.08(m, 2H), 4.98(s, 2H), 4.65(m, 1H),








3.71(m, 2H), 3.45(m, 2H), 3.28(s, 3H), 1.2(d, 6H).







260




δ 7.75(d, 2H), 7.6(t, 1H), 7.45(t, 2H), 7.2(m, 2H),








7.05(m, 2H), 5.38(q, 1H), 4.65(m, 1H), 1.73(d, 3H),








1.19(d, 6H).







262




δ 7.23(m, 2H), 7.08(m, 2H), 5.17(m, 1H), 5.02(m, 1H),








4.65(m, 1H), 4.06(d, 2H), 2.02(m, 4H), 11.65(s, 3H),








1.57(s, 3H), 1.19(d, 6H).







263




δ 7.22(m, 2H), 7.1(m, 2H), 6.75(m, 1H), 6.92(m, 1H),








4.65(m, 1H), 4.22(m, 2H), 3.74(s, 3H), 1.2(d, 6H).







264




δ 7.22(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 4.07(s, 2H),








3.38(m, 4H), 1.24-1.14(m, 12H).







265




δ 7.23(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 4.09(s, 2H),








1.43(s, 9H), 1.19(d, 6H).







266




δ 7.21(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 3.66(s, 3H),








3.55(t, 2H), 2.33(t, 2H), 1.96(m, 2H), 1.2(







267




δ 8.53(m, 1H), 7.76(m, 1H), 7.25(m, 6H), 7.08(t, 2H),








4.76(s, 2H), 4.66(m, 1H), 1.19(d, 6H).







274




δ 3.90(m, 1H), 3.40(q, 2H), 2.97(s, 6H), 1.50(m, 15H).







275




δ 3.90(m, 1H), 3.45(m, 4H), 1.70(m, 10H), 1.00(s, 9H),







277




δ 7.30(m, 1H), 6.90(m, 2H), 4.70(m, 1H), 3.20(s, 2H),








1.20(m, 6H), 0.90(s, 9H).







279




δ 7.4(m, 2H), 7.05(m, 2H), 5.80(m, 1H), 5.30(m, 1H),








5.25(m, 1H), 4.80(q, 1H), 4.25(m, 2H), 4.6(m, 2H),








1.42(d, 3H), 1.30(m, 6H).







280




δ 7.4(m, 2H), 7.05(m, 2H), 4.80(q, 1H), 4.25(q, 2H),








3.75(m, 1H), 1.00-2.00(m, 19H).







283




δ 7.40-7.20(m, 5H), 4.6(m, 1H), 4.10(m, 1H), 1.80(m,








8H), 1.20(d, 6H).







284




δ 7.40(m, 1H), 6.80(m, 2H), 4.6(m, 1H), 4.10(m, 1H),








1.80(m, 8H), 1.20(d, 6H).







285




δ 7.23(m, 2H), 7.08(m, 2H), 5.5(t, 1H), 4.65(m, 1H),








4.2(d, 2H), 2.12(s, 3H), 1.2(d, 6H).







286




δ 7.23(m, 2H), 7.11(m, 2H), 5.8(m, 1H), 5.4(m, 1H),








4.65(m, 1H), 4.0(d, 2H), 2.05(m, 2H), 1.2(d, 6H), 0.96








(t, 3H).







287




δ 7.21(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 4.54(t, 1H),








4.38(t, 1H), 3.65(t, 2H), 2.05(m, 2H), 1.2(d, 6H).







288




δ 7.21(m, 2H), 7.08(m, 2H), 5.2(m, 1H), 4.65(m, 1H),








4.05(d, 2H), 1.73(d, 6H), 1.2(d, 6H).







289




δ 7.23(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 4.52(t, 1H),








4.36(t, 1H), 3.53(t, 1H), 1.8-1.6(m, 4H), 1.2(d, 6H).







290




δ 7.23(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 3.46(t, 2H),








1.6(m, 2H), 1.3(m, 4H), 1.19(d, 6H), 0.87(t, 3H).







291




δ 7.22(m, 2H), 7.09(m, 2H), 5.72(m, 1H), 4.99(m, 2H),








4.65(m, 1H), 3.48(t, 2H), 2.05(q, 2H), 1.7 1.2(d, 6H).







292




δ 7.38-7.35(m, 2H), 7.21-7.18(m, 2H), 4.65(m,








1H), 2.93(s, 2H), 1.2(d, 6H), 0.08(s, 9H).







293




δ 7.22(m, 2H), 7.09(m, 2H), 4.89(s, 2H), 4.65(m, 1H),








3.39(s, 3H), 1.2(d, 6H).







294




δ 7.23(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 2.93(s, 2H),








1.2(d, 6H), 0.08(s, 9H).







295




δ 7.23(m, 2H), 7.09(m, 2H), 4.92(s, 2H), 4.65(m, 1H),








3.58(q, 2H), 1.2(m, 9H).







296




δ 8.59(s, 1H), 8.51(s, 2H), 4.7(m, 1H), 4.2-4.1(m,








1H), 1.4-1.3(m, 12H).







297




δ 3.49(m, 1H), 2.77(m, 1H), 1.25(,6H), 1.05(m, 4H).







298




δ 3.9(m, 1H), 3.41(q, 2H), 2.79(m, 1H), 2-1(m, 17H).







302




δ 7.4(m, 2H), 7.1(m, 2H), 4.8(m, 1H), 4.3(m, 3H),








1.5-1.2(m, 12H).







303




δ 7.4(m, 4H), 7.2-7.3(m, 1H), 7.1-7.2(m, 2H),








4.7-4.8(m, 1H), 2.306(s, 3H), 1.3-1.4(m, 9H), 1.2(m,








3H), 1.1(m, 3H).







304




δ 7.40(t, 1H), 7.26(m, 1H), 7.15(d, 2H), 7.10(m, 2H),








4.70(m, 1H), 2.38(q, 4H), 1.20(d, 6H), 1.10(t, 6H).







308




δ 3.95(m, 1H), 3.40(m, 1H), 2.10(m, 1H), 1.80(m,








3H), 1.70-1.20(m, 6H).







309




δ 4.28(m, 1H), 3.80(m, 1H), 3.40(m, 2H), 1.8(m, 2H)








1.25(d, 6H), 1.20(t, 3H).







312




δ 7.40(m, 1H), 6.42(s, 1H), 6.40(s, 1H), 4.74(s, 2H),








3.84(M, 1H), 3.40(m, 2H), 1.80(4H), 1.20(t, 3H).







317




δ 7.20(m, 2H), 7.10(m, 2H), 4.70(m, 1H), 3.50(d, 2H),








3.30(s, 6H), 1.20(d, 6H).







323




δ 7.22(m, 2H), 7.07(m, 2H), 4.6(m, 1H), 3.55(t, 2H),








2.26(t, 2H), 2.11(s, 6H), 1.8(t, 2H), 1.2(d, 6H)







325




δ 7.4(m, 2H), 7.3(m, 2H), 5.9-5.7(m, 1H), 5.3-5.2(m,








2H), 4.1(d, 2H), 3.7(q, 1H), 1.3(d, 3H), 0.7-0.4(m,








4H), 0.3(m, 1H).







331




δ 7.4(m, 2H), 7.30(t, 1H), 7.05(t, 2H), 6.95(d, 1H),








6.90(d, 1H), 4.80(q, 1H), 4.25(q, 2H), 3.75(s, 3H), 2.12








(s, 3H), 1.45(s, 3H), 1.30(t, 6H).







335




δ 8.18(d, 1H), 8.08(d, 1H), 7.82(d, 1H), 7.62-








7.44(m, 6H), 7.20(m, 1H), 4.60(m, 1H), 1.20(br.s,








6H) (In DMSO).







336




δ 8.18-8.00(m, 2H), 7.60-7.43(m, 8H), 4.62(m,








1H), 2.24(s, 3H), 1.20(m, 6H) (in DMSO).







337




δ 8.14-8.00(m, 2H), 7.60-7.20(m, 7H), 4.62(m,








1H), 2.20(s, 3H), 1.20(s, 6H) (in DMSO).







338




δ 8.12-8.00(m, 2H), 7.60-7.22(m, 8H), 4.60(m,








1H), 2.24(s, 3H), 1.19(d, 6H) (in DMSO).







344




δ 8.10-8.00(m, 2H), 7.6-7.22(m, 9H), 4.62(m,








1H), 2.22(s, 3H), 1.20(m, 6H) (in DMSO).







345




δ 7.40-7.20(m, 4H), 5.60(m, 1H), 5.02(m, 1H),








4.60(m, 1H), 4.00(m, 1H), 3.60(m, 1H), 3.40(m, 1H),








1.20(d, 6H).







352




δ 7.30(m, 1H), 6.90(m, 2H), 4.65(m, 1H), 4.20(m, 1H),








3.75(t, 1H), 3.40(q, 1H), 3.20(s, 3H), 1.30(d, 3H), 1.20








(m, 6H).







354




δ







355




δ 7.30(m, 1H), 6.90(m, 2H), 4.70(m, 1H), 3.60(m, 1H),








2.20(m, 1H), 1.35(s, 3H), 1.20(m, 6H), 0.90(d, 3H), 0.80








(d, 3H).







356




δ 7.40(m, 3H), 7.28(m, 2H), 4.70(m, 1H), 3.60(m, 1H),








2.20(m, 1H), 1.35(s, 3H), 1.20(d, 6H), 0.90(d, 3H), 0.80








(d, 3H).







358




δ 7.20(m, 2H), 7.10(m, 2H), 4.70(m, 1H), 1.90(m, 2H),








1.70(m, 2H), 1.20(d, 6H), 0.80(t, 6H).







359




δ 7.2-7.4(m, 2H), 7.15(m, 2H), 7.0-7.1(t, 3H),








4.7-4.8(m, 1H), 2.308(s, 3H), 1.3-1.4(m, 12H),








1.16(s, 3H).







361




δ 7.37(d, 2H), 7.18(d, 2H), 4.64(m, 1H), 1.39(s, 3H),








1.19(d, 6H), 1.02(m, 2H), 0.86(m, 2H).







362




δ 7.24(d, 2H), 7.18(d, 2H), 4.64(m, 1H), 1.39(s, 3H),








1.19(d, 6H), 1.02(m, 2H), 0.86(m, 2H).







363




δ 7.37(d, 1H), 6.92(m, 2H), 4.64(m, 1H), 1,39(s, 3H),








1.19(d, 6H), 1.02(m, 2H), 0.86(m, 2H).







364




δ 7.40(m, 3H), 7.28(m, 2H), 4.70(m, 1H), 3.60(m, 1H),








1.90(m, 2H), 1.70(m, 2H), 1.20(d, 6H), 0.80(d, 6H).







365




δ 7.4(m, 2H), 7.2(m, 2H), 4.8(m, 1H), 4.2(m, 2H),








3.0(s, 3H), 1.4(d, 3H), 1.3(t, 3H).







366




δ 8.61(m, 2H), 7.70(br d, 1H), 7.27(m, 3H), 7.07(t,








1H), 4.73(m, 1H), 4.62(s, 2H), 1.19(d, 6H).







367




δ 7.23(m, 2H), 7.11(m, 2H), 4.67(m, 1H), 4.2(m, 1H),








3.93(m, 1H), 3.6(m, 1H), 1.48(d, 3H), 1.18(d, 6H).







369




δ 7.37(q, 1H), 7.19(d, 2H), 4.64(m, 1H), 2.31(b, 1H),








1.4-0.77(m, 12H).







370




δ 7.39(m, 3H), 7.24(m, 2H), 4.64(m, 1H), 2.28(m, 1H),








1.3-1(m, 11H), 0.78(m, 1H).







372




δ 7.37(q, 1H), 6.92(m, 2H), 4.64(m, 1H), 2.31(m, 1H),








1.4-1.0(m, 11H), 0.78(m, 1H).







379




δ 7.38(m, 3H), 7.22(m, 2H), 4.83(s, 2H), 4.62(m, 1H),








4.46(q, 2H), 1.41(t, 3H), 1.21(d, 6H).







381




δ 7.22(m, 3H), 7.06(m, 3H), 4.85(s, 2H), 4.63(m, 1H),








4.48(m, 2H), 1.42(t, 3H), 1.19(d, 6H).







387




δ 7.3(m, 2H), 7.1(m, 2H), 4.93(m, 1H), 4.65(m, 1H), 1.8








(d, 3H), 1.2(d, 6H).







389




δ 7.23(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 3.46(t, 2H),








1.6(m, 2H), 1.26(m, 6H), 1.2(d, 6H), 0.86(t, 3H).







394




δ 7.28(m, 1H), 6.91(m, 2H), 4.65(m, 1H), 3.29(d, 2H),








2.11(m, 1H), 1.21(b, 6H), 0.87(D, h)







399




δ 7.24(m, 2H), 7.1(m, 2H), 4.64(m, 1H), 3.77(m, 2H),








2.45(m, 2H), 1.21(d, 6H).







400




δ 7.21(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 4.47(q, 1H),








2.19(s, 3H), 1.67(d, 3H), 1.2(d, 6H).







401




δ 7.05-7.24(m, 4H), 5.37-5.44(m, 1H), 4.58-4.67(m,








1H), 2.33(s, 3H), 1.78(d, 3H), 1.19(d, 6H).







408




δ 7.27(m, 1H), 6.89(m, 2H), 4.62(m, 1H), 4.2(m, 1H),








3.98(m, 1H), 3.6(m, 1H), 1.45(d, 3H), 1.21(d, 6H).







412




δ 7.20-7.10(m, 4H), 5.80(m, 1H), 5.40(m, 1H), 4.60








(m, 1H), 4.05(d, 1H), 4.00(d, 1H), 1.70(m, 2H), 1.20(d,








6H).







413




δ 7.20(m, 2H), 7.10(m, 2H), 6.00(m, 1H), 5.20(m, 2H),








4.60(m, 2H), 1.50(d, 3H), 1.20(d, 6H).







414




δ 7.36(m, 2H), 7.19(m, 2H), 6.02(m, 2H), 5.69(m, 1H),








4.64(septet, J=6.8Hz, 1H), 2.97(s, 2H), 1.20(d, J=6.8Hz,








8H), 0.17(s, 6H).







417




δ 7.38(m, 2H), 7.17(m, 2H), 4.65(m, 1H), 3.29(d, 2H),








2.01(m, 1H), 1.21(d, 6H), 0.88(d, 6H).







418




δ 7.38(m, 2H), 7.25(m, 2H), 4.75(s, 1H), 4.63(m, 1H),








4.6(m, 1H), 3.57(t, 2H), 2.31(t, 2H), 1.71(s, 3H), 1.2(d,








6H).







419




δ 7.38(m, 2H), 7.25(m, 2H), 4.62(m, 1H), 3.68(t, 2H),








2.73(t, 2H), 2.06(s, 3H), 1.2(d, 6H).







420




δ 7.38(m, 3H), 7.25(m, 2H), 4.53(d, 2H), 4.31(d, 2H),








3.67(s, 3H), 1.27(s, 3H), 1.2(d, 6H).







424




δ







425




δ 7.23(m, 2H), 7.08(m, 2H), 6.01(m, 2H), 5.70(dd, J=








16.5Hz, J=7.3Hz, 1H), 4.65(septet, J=6.8Hz, 1H), 2.97(s,








2H), 1.19(d, J=6.8Hz, 6H), 0.17(s, 6H).







426




δ 7.23(m, 2H), 7.05(m, 2H), 5.69(m, 1H), 5.29(s, 2H),








4.85(m, 2H), 4.65(septet, J=6.8Hz, 1H), 2.95(s, 2H),








1.58(d, J=8.1Hz, 2H), 1.19(d, J=6.8Hz, 6H).







427




δ 5.82(s, 1H), 4.25(m, 1H), 4.20(s, 1H), 4.00(t, 2H),








2.25(s, 1H), 1.20(m, 6H).







428




δ 5.78(s, 1H), 4.25(m, 1H), 4.00(m, 1H), 2.25(m, 1H),








2.20(m, 4H), 1.20(d, 6H).







429




δ 4.00(m, 1H), 3.50(m, 2H), 3.00(m, 1H), 2.20(m, 2H),








1.80(m, 4H), 1.20(t, 3H).







432




δ 7.35(m, 2H), 7.0(m, 1H), 4.9(m, 1H), 4.6(m, 1H), 1.8








(d, 3H), 1.2(br, 6H).







435




δ 7.4-7.2(m, 5H), 4.9(m, 1H), 4.62(m, 1H), 1.7(d, 3H),








1.2(d, 6H).







441




δ 7.3(m, 3H), 7.2(m, 3H), 5.0(m, 1H), 4.6(m, 1H), 3.2(s,








3H), 1.6(d, 3H), 1.1(d, 6H).







442




δ 7.37(m, 3H), 7.20(m, 2H), 5.40(q, 1H), 4.61(m, 1H),








2.62(s, 3H), 2.30(s, 3H), 1.76(d, 3H), 1.20(d, 6H).







443




δ 7.30(m, 1H), 6.90(t, 2H), 5.40(q, 1H), 4.60(m, 1H),








2.62(s, 3H), 2.32(s, 3H), 1.77(d, 3H), 1.20(m, 6H).







446




δ 7.2(m, 2H), 7.1(m, 2H), 5.1(m, 1H), 4.7(m, 1H), 3.9








(m, 1H), 3.7(m, 1H), 3.4(s, 3H), 3.3(s, 3H), 1.2(s, 6H).







447




δ 7.4(m, 3H), 7.3(m, 2H), 4.6(m, 1H), 4.1(m, 4H), 3.8








(d, 2H), 1.2(m, 12H).







448




δ 7.4(m, 3H), 7.3(m, 2H), 4.6(m, 1H), 4.3(m, 1H), 4.1








(m, 4H), 1.6(m, 6H), 1.2(m, 12H).







452




δ 7.2(m, 2H), 7.1(m, 2H), 6.1-5.2(m, 3H), 4.7(m, 1H),








3.6(m, 1H), 3.4(s, 3H), 3.4(s, 3H), 1.2(d, 6H).







453




δ 7.21(m, 2H), 7.08(m, 2H), 4.6(m, 1H), 3.99(t, 2H),








3.36(t, 2H), 2.97(s, 3H), 1.18(d, 6H).







454




δ 7.39(m, 3H), 7.26(m, 2H), 5.8(m, 1H), 5.38(m, 1H),








4.68(m, 1H), 3.99(d, 2H), 2.0(m, 2H), 1.2(d, 6H), 0.95








(t, 3H).







455




δ 7.39(m, 3H), 7.26(m, 2H), 6.0(m, 1H), 5.2(dd, 2H),








4.65(m, 1H), 4.2(m, 1H), 1.9(m, 2H), 1.21(d, 6H), 0.83








(t, 3H).







456




δ 7.39(m, 2H), 7.20(m, 2H), 4.65(m, 1H), 4.2(m, 1H),








3.91(m, 1H), 3.6(dd, 1H), 1.46(d, 3H), 1.21(d, 6H).







457




δ 7.4(m, 3H), 7.2(m, 2H), 5.0(s, 2H), 4.5-4.0(br, 1H),








1.6(m, 1H), 1.2(d, 6H).







458




δ 7.3(m, 2H), 7.1(m, 2H), 5.1(m, 1H), 4.7(m, 1H),








4.1(m, 1H), 3.8(m, 1H), 3.4(s, 3H), 1.2(d, 6H).







461




δ 7.27(m, 2H), 7.11(m, 2H), 4.68(m, 1H), 3.46(t, 2H),








1.64(m, 2H), 1.22(d, 6H), 0.44(m, 2H), 0.00(s, 9H).







463




δ 7.3-7.4(q, 1H), 6.8-7.0(m, 2H), 4.6-4.7(m,








2H), 3.73(s, 3H), 1.6(d, 3H), 1.2(d, 6H).







464




δ 7.4(m, 3H), 7.2(m, 2H), 4.6-4.7(m, 2H), 3.727(s,








3H), 1.6(d, 6H), 1.3(d, 3H).







465




δ 7.3-7.4(m, 1H), 6.8-7.0(m, 2H), 4.6-4.7(m,








1H), 4.1-4.3(m, 3H), 3.5-3.9(m, 1H), 3.0-3.3(m, 1H),








2.2-2.5(m, 1H), 1.2(m, 12H).







467




δ 7.39(m, 2H), 7.22(m, 2H), 4.93(s, 2H), 4.66(septet,








J=6.8Hz, 1H), 3.62(apparent t, J=8.3Hz, 2H), 1.22(d,








J=6.8Hz, 6H), 0.93(apparent t, J=8.3Hz, 2H), 0.00(s,








9H).







472




δ 7.35(m, 1H), 7.00(m, 2H), 4.70(m, 1H), 4.00(m, 1H),








3.38(s, 3H), 3.23(s, 3H), 1.35(d, 3H), 1.20(m, 6H).







478




δ 1.18(d, 6H), 1.68(d, 3H), 2.95(s, 3H) 2.98(s, 3H),








4.64(m, 1H), 4.83(q, 1H) 7.05(m, 2H), 7.22(m, 2H).







479




δ 1.20(d, 6H), 1.66(d, 3H), 2.94(s, 3H), 2.96(s, 3H),








4.65(m, 3H), 4.82(q, 1H), 7.21(m, 2H), 7.38(m, 2H).







481




δ 1.20(m, 6H), 1.68(d, 3H), 2.94(s, 3H), 2.99(s, 3H),








4.64(m, 1H), 4.82(q, 1H), 6.89(m, 2H), 7.33(m, 1H).







485




δ 7.39(m, 3H), 7.24(m, 2H), 4.64(m, 1H), 4.3(s, 2H),








2.64(m, 1H) 1.21(d, 6H), 1.16(d, 6H).







486




δ 7.34(q, 1H), 6.93(m, 2H), 4.64(m, 1H), 4.3(s, 2H),








2.64(m, 1H), 1.22(b, 6H), 1.16(d, 6H).







487




δ 7.37(d, 2H), 7.18(d, 2H), 4.64(m, 1H), 2.65(m, 1H),








1.19(m, 12H).







488




δ 7.20(m, 2H), 7.09(m, 2H), 4.64(m, 1H), 4.43(s, 2H),








1.92(m, 1H), 1.19(m, 8H), 1.04(m, 2H).







490




δ 7.34(m, 1H), 6.95(m, 2H), 4.64(m, 1H), 4.42(s, 2H),








1.92(m, 1H), 1.22(m, 8H), 1.03(m, 2H).







491




δ 9.53(s, 1H), 7.24(m, 2H), 7.1(m, 2H), 4.64(m, 1H),








4.35(s, 2H), 1.2(b, 6H).







492




δ 7.3-7.2(m, 2H), 7.1(m, 2H), 6.1(bs, 1H), 4.7(m, 1H),








4.14(s, 2H), 3.7-3.6(m, 4H), 1.20(d, 6H).







493




δ 7.3-7.2(m, 2H), 7.1(m, 2H), 5.9(bs, 1H), 4.7-4.6(m,








1H), 4.09(s, 2H), 3.6-3.5(t, 2H), 3.5(dt, 2H), 2.0(m,








2H), 1.20(d, 6H).







494




δ 7.4(m, 3H), 7.3-7.2(m, 2H), 4.7(m, 1H), 4.14(t, 2H),








4.02(s, 2H), 3.3(t, 2H), 1.9-1.8(m, 2H), 1.21(d, 6H).







495




δ 7.4(m, 3H), 7.3-7.2(m, 2H), 4.7-4.6(m, 1H), 4.3(t,








2H), 4.24(s, 2H), 3.9-3.8(t, 2H), 1.21(d, 6H).







496




δ 7.4-7.3(m, 3H), 7.2-7.1(m, 2H), 5.6(bs, 1H),








4.7-4.6(m, 1H), 3.9(s, 2H), 2.0(bs, 2H), 1.9(bs, 2H),








1.6-1.4(m, 4H), 1.2(d, 6H).







497




δ 7.3(m, 3H), 7.2(m, 2H), 5.8(s, 1H), 4.7-4.6(m, 1H),








3.94(s, 2H), 2.7(m, 2H), 2.4(m, 2H), 2.2(b, 2H), 1.2(d,








6H).







498




δ 8.7-8.6(bs, 1H), 8.5(bs, 1H), 7.7(m, 1H), 7.4-7.2(m,








6H), 5.5(s, 1H), 5.3(s, 1H), 4.7-4.6(m, 1H), 4.45(s, 2H),








1.2(d, 6H).







500




δ 7.3(m, 1H), 6.9(m, 2H), 4.64(m, 1H), 4.48(d of t, 2H),








3.65(t, 2H), 2.42(m, 2H), 1.2(m, 6H).







501




δ 7.3(m, 1H), 6.9(m, 2H), 4.87(m, 1H), 4.64(m, 1H),








3.86(m, 2H), 3.77(m, 2H), 3.64(t, 2H), 2.05(m, 2H), 1.2








(m, 6H).







502




δ 7.4(m, 1H), 6.9(m, 2H), 4.64(m, 1H), 4.57(m, 1H),








3.97(m, 2H), 3.63(m, 4H), 1.97(m, 3H), 1.2(m, 7H).







503




δ 7.3(m, 1H), 6.9(m, 2H), 4.88(s, 2H), 4.64(m, 1H),








3.93(s, 3H), 1.2(m, 6H).







504




δ 7.4(m, 1H), 6.9(m, 2H), 4.92(s, 2H), 4.65(m, 1H),








3.59(q, 2H), 1.2(m, 9H).







505




δ 7.4(m, 1H), 6.9(m, 2H), 4.97(s, 2H), 4.63(m, 1H),








3.72(m, 2H), 3.45(m, 2H), 3.30(s, 3H), 1.2(m, 6H).







506




δ 7.4(m, 1H), 6.9(m, 2H), 4.63(m, 1H), 4.05(m, 2H),








3.51(m, 2H), 2.04(s, 3H), 1.67(m, 4H), 1.2(m, 6H).







507




δ 7.35(m, 2H), 6.92(m, 2H), 4.64(m, 1H), 3.7(t, 2H),








2.65(m, 2H), 1.23(br s, 6H).







508




δ 7.3(m, 4H), 7.1(m, 2H), 6.9(m, 2H), 4.62(m, 1H),








3.69(m, 2H), 2.92(m, 2H), 1.2(m, 6H)







509




δ 7.3(m, 1H), 6.9(m, 2H), 4.65(m, 1H), 3.33(m, 2H),








1.2(m, 7H), 0.54(m, 2H), 0.33(m, 2H)







510




δ 7.3(m, 1H), 6.9(m, 2H), 4.63(m, 1H), 4.37(s, 2H),








2.43(s, 3H), 2.24(s, 3H), 1.2(m, 6H).







511




δ 7.75(d, 2H), 7.6(t, 1H), 7.45(t, 2H), 7.3(m, 1H),








6.89(m, 2H), 5.37(q, 1H), 4.65(m, 1H), 1.72(d, 3H), 1.2








(br s, 6H).







512




δ 7.3(m, 1H), 6.9(m, 2H), 4.65(m, 1H), 4.23(s, 2H),








3.36(q, 2H), 3.26(q, 2H), 1.21(m, 9H), 1.11(t, 3H).







513




δ 7.35(m, 1H), 6.92(m, 2H), 4.65(m, 1H), 3.66(s, 3H),








3.53(t, 2H), 2.31(t, 2H), 1.96(m, 2H), 1.22(br s, 6H).







514




δ .35(m, 1H), 6.92(m, 2H), 5.55(t, 1H), 4.65(m, 1H),








4.2(d, 2H), 2.12(s, 3H), 1.21(br s, 6H). (3:1 cis/trans








mix.)







515




δ 7.35(m, 1H), 6.92(m, 2H), 5.2(t, 1H), 4.65(m, 1H),








4.04(d, 2H), 1.72(m, 6H), 1.21(br s, 6H).







516




δ 7.35(m, 1H), 6.92(m, 2H), 5.73(m, 1H), 5.0(m, 2H),








4.65(m, 1H), 3.48(t, 2H), 2.04(q, 2H), 1.74 1.22(br s,








6H).







517




δ 7.32(m, 1H), 6.91(m, 2H), 4.65(m, 1H), 4.48(q, 1H),








2.19(s, 3H), 1.65(d, 3H), 1.22(br s, 6H).







518




δ 7.35(m, 1H), 6.89(m, 2H), 4.65(m, 1H), 2.93(s, 2H),








1.21(br s, 6H), 0.08(m, 9H).







519




δ 7.37(m, 1H), 6.92(m, 2H), 5.1(s, 1H), 4.87(s, 2H),








4.65(m, 1H), 4.13(q, 2H), 3.78(q, 2H), 1.23(







520




δ 7.3(m, 6H), 6.9(m, 2H), 4.98(s, 2H), 4.6(m, 3H),








1.21(br s, 6H).







521




δ 7.35(m, 1H), 6.9(m, 2H), 4.64(m, 1H), 3.5(d, 2H),








2.65(m, 1H), 2.0-1.7(m, 6H), 1.21(br s, 6H).







522




δ 7.35(m, 1H), 6.92(m, 2H), 4.65(m, 1H), 4.52(t, 1H),








4.36(t, 1H), 3.53(t, 2H), 1.85-1.6(m, 4H), 1.22(br s,








6H).







523




δ 7.35(m, 1H), 6.9(m, 2H), 5.8(m, 1H), 5.4(m, 1H),








4.65(m, 1H), 4.0(d, 2H), 2.03(m, 2H), 1.21(br s, 6H),








0.94(t, 3H)







524




δ 7.32(m, 1H), 6.92(m, 2H), 4.65(m, 1H), 4.24(s, 2H),








2.47(q, 2H), 1.21(br s, 6H), 1.1(t, 3H).







525




δ 7.33(m, 1H), 6.93(m, 2H), 4.65(m, 1H), 3.75(t, 2H),








2.48(m, 2H), 1.22(br s, 6H).







526




δ 7.33(m, 1H), 6.93(m, 2H), 4.65(m, 1H), 3.55(t, 2H),








2.1(m, 2H), 1.92(m, 2H), 1.23(br s, 6H)







527




δ 7.39(m, 2H), 7.22(m, 2H), 4.93(s, 2H), 4.66(septet,








J=6.8Hz, 1H), 3.62(apparent t, J=8.3Hz, 2H), 1.22(d,








J=6.8Hz, 6H), 0.93(apparent t, J=8.3Hz, 2H), 0.00(s,








9H).







528




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 3.5(t, 2H),








1.6(m, 2H), 1.3(m, 4H), 1.1(d, 6H), 0.875(t, 3H).







529




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 3.4(t, 2H),








1.6(m, 2H), 1.26(brd s, 6H), 1.1(d, 6H), 0.865(t, 3H).







530




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 4.5(t, 1H),








4.4(t, 1H), 3.6(t, 2H), 1.9-2.1(m, 2H), 1.2(d, 6H).







531




δ 7.3(d, 2H), 7.1(d, 2H), 4.875(m, 1H), 4.6-4.7(m, 1H),








3.7-3.9(m, 4H), 3.648(t, 2H), 2.046(m, 2H), 1.1(d, 6H).







532




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 4.561(m,








1H), 3.9-4.0(m, 2H), 3.6(m, 4H), 1.9-2.0(m, 3H),








1.3(brd s, 1H), 1.1(d, 6H).







533




δ 7.3(d, 2H), 7.1(d, 2H), 4.886(s, 2H), 4.6-4.7(m, 1H),








3.394(s, 3H), 1.2(d, 6H).







534




δ 7.4(d, 2H), 7.2(d, 2H), 4.922(s, 2H), 4.6-4.7(m, 1H),








3.6(q, 2H), 1.1-1.2(m, 9H).







535




δ 7.3(d, 2H), 7.1(d, 2H), 4.977(s, 2H), 4.6-4.7(m, 1H),








3.708(m, 2H), 3.470(m, 2H), 3.277(s, 3H), 1.2(d, 6H).







536




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 4.056(t, 2H),








3.508(t, 2H), 2.039(s, 3H), 1.6-1.8(m, 4H), 1.2(d, 6H).







537




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 3.7(t, 2H),








2.4-2.8(m, 2H), 1.2(d, 6H).







538




δ 7.3(d, 2H), 7.238(m, 2H), 7.166(m, 1H), 7.0-7.1(m,








4H), 4.6-4.7(m, 1H), 3.7(t, 2H), 2.9(t, 2H), 1.2(d, 6H).







539




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 3.3(d, 2H),








1.2(d, 6H), 1.1-1.2(m, 1H), 0.56(q, 2H), 0.3(q, 2H).







540




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 4.369(s,








2H), 2.436(s, 3H), 2.245(s, 3H), 1.1(d, 6H).







541




δ 7.77(d, 2H), 7.6(t, 1H), 7.4(t, 2H), 7.3(d, 2H), 7.1(d,








2H), 5.3-5.4(q, 1H), 4.6-4.7(m, 1H), 1.7(d, 3H), 1.1(d,








6H).







542




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 4.230(s, 2H),








3.4(q, 2H), 3.2-3.2(q, 2H), 1.239(t, 3H), 1.2(d, 6H),








1.1(t, 3H).







543




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 3.658(s,








3H), 3.5(t, 2H), 2.3-2.4(t, 2H), 1.9-2.0(m, 2H), 1.3(d,








6H).







544




δ 7.3(d, 2H), 7.1(d, 2H), 5.5(t, 1H), 4.6-4.7(m, 1H),








4.2(d, 2H), 2.1(s, 3H), 1.1(d, 6H) (3:1 cis/trans mixture).







545




δ 7.3(d, 2H), 7.1(d, 2H), 5.2(t, 1H), 4.6-4.7(m, 1H),








4.0(d, 2H), 1.735(s, 3H), 1.719(s, 3H), 1.1(d, 6H).







546




δ 7.3(d, 2H), 7.1(d, 2H), 5.6-5.8(m, 1H), 4.9(m, 2H),








4.6-4.7(m, 1H), 3.4(t, 2H), 2.0-2.1(q, 2H), 1.7-1.8(m,








2H), 1.2(d, 6H).







547




δ 7.4-7.37(m, 2H), 7.19-7.16(m, 2H), 4.65(m, 1H),








4.48(q, 1H), 2.19(s, 3H), 1.66(d, 3H), 1.2(d, 6H).







548




δ 7.38-7.35(m, 2H), 7.21-7.18(m, 2H), 4.65(m, 1H),








2.93(s, 2H), 1.2(d, 6H), 0.08(s, 9H).







549




δ 7.4(d, 2H), 7.2(d, 2H), 5.1(s, 1H), 4.9(s, 2H),








4.6-4.7(m, 1H), 4.1-4.2(q, 2H), 3.7-3.8(q, 2H),








1.3(t, 3H), 1.1-1.2(m, 9H).







550




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 3.4-3.5(d,








2H), 2.6-2.7(m, 1H), 2.0-2.1(m, 2H), 1.8-1.9(q, 2H),








1.1(d, 6H).







551




δ 7.3(d, 2H), 7.1(d, 2H), 4.6-4.7(m, 1H), 4.5(t, 1H),








4.3-4.4(t, 1H), 3.5(t, 2H), 1.6-1.8(m, 4H), 1.2(d, 6H).







552




δ 7.3(d, 2H), 7.1(d, 2H), 5.7-5.9(m, 1H), 5.3-5.5








(m, 1H), 4.6-4.7(m, 1H), 4.0(d, 2H), 2.0-2.1(m, 2H),








1.1(d, 6H), 0.9(t, 3H).







553




δ 7.4(d, 2H), 7.2(d, 2H), 4.6-4.7(m, 1H), 4.244(s, 2H),








2.4(q, 2H), 1.2(d, 6H), 1.087(t, 3H).







554




δ 7.4(d, 2H), 7.2(d, 2H), 4.6-4.7(m, 1H), 3.7(t, 2H),








2.4-2.6(m, 2H), 1.2(d, 6H).







555




δ 7.4(d, 2H), 7.2(d, 2H), 4.6-4.7(m, 1H), 3.5(t, 2H),








2.0-2.2(m, 2H), 1.8-2.0(m, 2H), 1.1(d, 6H).







556




δ 7.39(m, 3H), 7.3(m, 2H), 4.6-4.7(m, 1H), 3.45(t,








2H), 1.56(m, 2H), 1.3(m, 2H), 1.2(d, 6H), 0.9(t, 3H).







557




δ 7.38(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 3.44(t,








2H), 1.6(m, 2H), 1.3(m, 4H), 1.2(d, 6H), 0.86(t, 3H).







558




δ 7.387(m, 3H), 7.38(m, 2H), 4.6-4.7(m, 1H), 3.44(t,








2H), 1.6(m, 2H), 1.25(d, 6H), 1.2(s, 6H), 0.859(t, 3H).







559




δ 7.4(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 4.53(t, 1H),








4.37(t, 1H), 3.61-3.66(t, 2H), 1.9-2.1(m, 2H), 1.2(d,








6H).







560




δ 7.37(m, 3H), 7.26(m, 2H), 4.87(t, 1H), 4.6-4.7(m,








1H), 3.8-3.9(m, 2H), 3.7-3.8(m, 2H)m 3.63(t, 2H),








2.045(m, 2H), 1.2(d, 6H).







561




δ 7.3(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 4.56(t, 1H),








3.9-4.0(m, 2H), 3.6(m, 4H), 1.9(m, 3H), 1.259(t, 1H),








1.2(d, 6H).







562




δ 7.39(m, 3H), 7.26(m, 2H), 4.87(s, 2H), 4.6-








4.7(m, 1H), 3.377(s, 3H), 1.2(d, 6H).







563




δ 7.3(m, 3H), 7.27(m, 2H), 4.886(s, 2H), 4.6-4.7(m,








1H), 3.547-3.571(q, 2H), 1.2(d, 6H), 1.129-1.15(t, 3H).







564




δ 7.38(m, 3H), 7.26(m, 2H), 4.966(s, 2H), 4.6-4.7(m,








1H), 3.7(t, 2H), 3.4(t, 2H), 3.257(s, 3H), 1.2(d, 6H).







565




δ 7.39(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 4.046(t,








2H), 3.495(t, 2H), 2.033(s, 3H), 1.6-1.8(m, 4H), 1.2








(d, 2H).







566




δ 7.38(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 3.66-








3.707(t, 2H), 2.6-2.7(m, 2H), 1.2(d, 6H).







567




δ 7.38(m, 3H), 7.24(m, 5H), 7.12(d, 2H), 4.63(m, 1H),








3.67(t, 2H), 2.9(t, 2H), 1.2(d, 6H).







568




δ 7.39(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 3.3(d, 2H),








1.2(d, 6H), 1.1(m, 1H), 0.5(q, 2H), 0.3(q, 2H).







569




δ 7.38(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 4.353(s,








2H), 2.422(s, 3H), 2.225(s, 3H), 1.2(d, 6H).







570




δ 7.759(d, 2H), 7.438(t, 1H), 7.374(t, 3H), 7.37(m, 2H),








7.26(m, 2H), 5.3-5.4(q, 1H), 4.6-4.7(m, 1H), 1.7(d,








3H), 1.2(d, 6H).







571




δ 7.37(m, 3H), 7.25(m, 2H), 4.6-4.7(m, 1H), 4.2(s, 2H),








3.2-33(q, 2H), 3.3-3.4(q, 2H), 1.2(m, 9H), 1.1(t, 3H).







572




δ 7.39(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 3.6(s, 3H),








3.54(t, 2H), 2.3(t, 2H), 1.9(m, 2H), 1.2(d, 6H).







573




δ 7.39(m, 3H), 7.26(m, 2H), 5.5(t, 1H), 4.6-4.7(m, 1H),








4.2(d, 2H), 2.1(s, 3H), 1.2(d, 6H).







574




δ 7.39(m, 3H), 7.26(m, 2H), 5.1-5.2(t, 1H), 4.6-4.7(m,








1H), 4.01-4.039(d, 2H), 1.7(d, 6H), 1.2(d, 6H).







575




δ 7.39(m, 3H), 7.26(m, 2H), 5.6-5.8(m, 1H), 4.9-5.1(m,








2H), 4.6-4.7(m, 1H), 3.44-3.49(t, 2H), 2.0-2.1(q, 2H),








1.7-1.8(m, 2H), 1.2(d, 6H).







576




δ 7.39(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 4.4-4.5(q,








1H), 2.166(s, 3H), 1.6(d, 2H), 1.2(d, 6H).







577




δ 7.37(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 2.9(s, 2H),








1.2(d, 6H), 0.6-0.8(m, 9H).







578




δ 7.4(m, 3H), 7.26(m, 2H), 5.1(s, 1H), 4.862-4.866(s,








2H), 4.6-4.7(m, 1H), 4.1-4.2(q, 2H), 3.7-3.8(q, 2H),








1.17-1.28(m, 12H).







579




δ 7.4-7.2(m, 10H), 4.97(s, 2H), 4.63(m, 1H), 4.58(s,








2H), 1.2(d, 6H).







580




δ 7.38(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 3.47-3.49








(d, 2H), 2.6-2.7(m, 1H), 1.9-2.1(m, 2H), 1.8-1.9(q,








2H), 1.7-1.8(q, 2H), 1.2(d, 6H).







581




δ 7.39(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 4.5(t, 1H),








4.3-4.4(t, 1H), 3.5(t, 2H), 1.7-1.8(m, 3H), 1.6-1.7(m,








1H), 1.2(d, 6H).







582




δ 7.38(m, 3H), 7.26(m, 2H), 5.7-5.9(m, 1H), 5.3-5.4(m,








1H), 4.6-4.7(m, 1H), 4.0(d, 2H), 1.9-2.1(m, 2H), 1.2(d,








6H), 0.9-1.0(t, 3H).







583




δ 7.39(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 4.23(s,








2H), 2.45-2.48(q, 2H), 1.2(d, 6H), 1.1(t, 3H).







584




δ 7.39(m, 3H), 7.26(m, 2H), 4.6-4.7(m, 1H), 3.7(t, 2H),








2.4-2.6(m, 2H), 1.2(d, 6H).







585




δ 7.3(m, 2H), 7.1(m, 2H), 4.6-4.7(m, 1H), 3.5(t, 2H),








2.0-2.2(m, 2H), 1.8-2.0(m, 2H), 1.2(d, 6H).







587




δ 7.4(m, 3H), 7.3(m, 2H), 4.6(m, 1H), 4.1(m, 4H), 3.8








(d, 2H), 1.2(m, 12H).







592




δ 7.4(m, 2H), 7.2(m, 2H), 5.1(m, 1H), 4.7(m, 1H), 3.3(s,








3H), 1.7(d, 3H), 1.2(d, 6H).







593




δ 7.3(m, 1H), 6.9(m, 2H), 5.1(m, 1H), 4.7(m, 1H), 3.3(s,








3H), 1.7(d, 3H), 1.2(m, 6H).







594




δ 7.28(m, 1H), 6.92(m, 2H), 4.6(m, 1H), 4.2(m, 1H),








3.8(m, 1H), 3.4(m, 1H), 1.31(d, 3H), 1.26(d, 6H).







596




δ 7.22(m, 2H), 7.09(m, 2H), 4.65(m, 1h), 4.4(m, 2H),








4.2-3.6(m, 3H), 2.04(s, 3H), 1.21(d, 6H).







597




δ 7.39(m, 2H), 7.16(m, 2H), 4.6(m, 1H), 4.2-3.6(m,








2H), 1.22(d, 6H).







598




δ 7.28(m, 1H), 6.9(m, 2H), 4.63(m, 1H), 3.8(s, 2H),








1.26(b, 6H).







599




δ 7.4(d, 2H), 7.20(d, 2H), 4.65(m, 1H), 4.12(q, 4H),








4.80(d, 2H), 1.30(m, 12H).







600




δ 7.11(m, 3H), 5.80(m, 1H), 5.22(m, 3H), 4.03(d, 2H),








3.90(m, 2H), 3.26(s, 3H), 2.35(d, 6H), 1.41(d, 3H).







603




δ 7.38-7.41(m, 3H), 7.21-7.25(m, 2H), 4.82-4.89








(m, 1H), 4.59-4.68(m, 1H), 4.08-4.16(m, 1H),








3.68-3.74(m, 1H), 1.57(d, 3H), 1.21(d, 6H).







604




δ 7.29-7.37(m, 1H), 6.90-6.96(m, 2H), 4.83-4.90








(m, 1H), 4.58-4.67(m, 1H), 4.09-4.17(m, 1H),








3.68-3.74(m, 1H), 1.58(d, 3H), 1.22(br s, 6H).







605




δ 7.6(m, 1H), 7.48(m, 1H), 7.3(m, 3H), 7.2(m, 3H), 5.94








(s, 1H), 5.3(s, 1H), 4.6(m, 3H), 1.2(d, 6H).







606




δ 7.4-7.2(m, 7H), 6.9(m, 2H), 5.4(s, 1H), 5.1(s, 1H),








4.7-4.6(m, 1H), 4.4(s, 2H), 1.2(d, 6H).







607




δ 7.4(m, 3H), 7.3-7.2(m, 2H), 4.9(s, 1H), 4.8(s, 1H),








4.7-4.6(m, 1H), 3.9(s, 2H), 1.7(s, 3H), 1.2(d, 6H).







608




δ 7.4(m, 3H), 7.2(m, 2H), 5.4(s, 2H), 4.7-4.6(m, 1H),








4.2(s, 2H), 1.2(d, 6H).







609




δ 7.39(m, 3H), 7.26(m, 2H), 4.82(m, 1H), 4.64(m, 1H),








2.41(s, 1H), 1.60(d, 3H), 1.22(d, 6H).







614




δ 7.4(m, 3H), 7.2(m, 2H), 4.6-4.7(m, 1H), 4.0-4.2








(4H), 5.0(m, 1H), 3.9(m, 1H), 3.0-3.2(q of q, 2H), 1.2








(m, 16H).







615




δ 7.2(m, 2H), 7.0-7.1(t, 2H), 5.7(m, 1H), 4.6(m, 1H),








4.2(m, 2H), 3.9(m, 2H), 3.0-3.2(m, 2H), 1.1-1.3(m,








14H).







616




δ 7.2-7.3(m, 2H), 7.0-7.1(m, 2H), 4.6-4.7(m,








2H), 3.7(s, 3H), 1.66(d, 3H), 1.2(d, 6H).







617




δ 7.3(m, 2H), 7.1(m, 2H), 4.6(m, 1H), 4.3(m, 1H),








4.1(m, 4H), 1.6(m, 6H), 1.2(m, 12H).







623




δ 7.4(d, 2H), 7.2(d, 2H), 4.6-4.7(m, 2H), 3.742(s,








3H), 1.6(d, 3H), 1.2(d, 6H).







627




δ 7.20(m, 2H), 7.10(m, 2H), 4.70(m, 2H), 3.70(m, 2H),








3.60(t, 2H), 3.55(t, 2H), 3.30(s, 3H) 1.20(d, 6H).







629




δ 7.20(m, 2H), 7.10(m, 2H), 4.70(m, 2H), 3.70(m, 2H),








3.60(d, 2H), 3.45(m, 2H), 1.20(d, 6H), 1.10(t, 6H).







631




δ 7.35(m, 3H), 7.28(m, 2H), 4.70(m, 1H), 3.65(t, 2H),








3.54(t, 2H), 3.30(s, 3H), 1.22(d, 6H).







632




δ 7.35(m, 3H), 7.28(m, 2H), 4.70(m, 1H), 3.65(m, 2H),








3.55(d, 2H), 3.48(m, 2H), 1.20(d, 6H), 1.10(d, 6H).







634




δ 7.3(m, 1H), 6.92(m, 2H), 5.43(s, 2H), 4.65(m, 1H),








4.23(s, 2H), 1.21(bs, 6H).







635




δ 7.3(m, 1H), 6.9(m, 2H), 4.62(m, 1H), 3.46(t, 2H),








1.56(m, 2H), 1.2(m, 8H), 0.91(t, 3H).







636




δ 7.3(m, 1H), 6.9(m, 2H), 4.64(m, 1H), 3.45(t, 2H),








1.64(m, 2H), 1.2(m, 10H), 0.87(t, 3H).







637




δ 7.3(m, 1H), 6.9(m, 2H), 4.63(m, 1H), 3.45(t, 2H),








1.6(m, 2H), 1.2(m, 12H), 0.86(t, 3H).







639




δ 7.37(d, 2H), 7.17(d, 2H), 4.64(m, 1H), 4.43(s, 2H),








1.91(m, 1H), 1.2(m, 8H), 1.04(m, 2H).







640




δ 7.21(m, 2H), 7.09(m, 2H), 4.65(m, 1H), 4.19(s, 2H),








3.3(m, 1H), 2.4-1.8(m, 6H), 1.21(d, 6H).







642




δ 7.34(m, 1H), 6.94(m, 2H), 4.65(m, 1H), 4.19(s, 2H),








3.3(m, 1H), 2.4-1.8(m, 6H), 1.21(d, 6H).







643




δ 7.37(d, 2H), 7.17(d, 2H), 4.65(m, 1H), 4.19(s, 2H),








3.3(m, 1H), 2.4-1.8(m, 6H), 1.21(d, 6H).







648




δ 7.3(m, 2H), 7.2(m, 3H), 5.0(s, 1H), 4.8-4.6(m, 1H),








4.5(s, 1H), 4.0(s, 2H), 1.2(d, 6H).







649




δ 7.3(m, 3H), 7.2(m, 2H), 4.9(s, 1H), 4.8(s, 1H),








4.7-4.6(m, 1H), 4.0(s, 2H), 2.3-2.1(m, 1H), 1.2(d, 6H),








1.0(d, 6H).







650




δ 7.4-7.0(m, 10H), 5.0(ABm, 2H), 4.7-4.6(m, 1H),








3.9(s, 2H), 3.2(s, 2H), 1.2(d, 6H).







651




δ 7.3(m, 3H), 7.2(m, 2H), 6.5(s, 1H), 5.9(s, 1H), 5.0(m,








1H), 4.7-4.6(m, 1H), 3.66(s, 3H), 1.5(d, 3H), 1.2(d, 6H).







652




δ 7.3(m, 3H), 7.2(m, 2H), 5.6(m, 1H), 5.4(m, 1H),








4.7-4.6(m, 1H), 2.4(s, 1H), 1.73(s, 3H), 1.69(s, 3H),








1.2(d, 6H).







655




δ 7.4(m, 3H), 7.2(m, 2H), 6.4-6.3(m, 1H), 5.6-5.5(m,








1H), 4.7-4.6(m, 1H), 2.9(s, 1H), 1.6(s, 6H), 1.2(d, 6H).







656




δ 7.22(m, 2H), 7.09(m, 2H), 4.63(m, 2H), 3.95(m, 2H),








2.07(m, 2H), 1.94(m, 2H), 1.60(d, 3H), 1.18(d, 6H).







657




δ 7.40(m, 1H), 6.94(m, 2H), 4.82(m, 1H), 4.64(m, 1H),








2.40(m, 1H), 1.60(d, 3H), 1.20(d, 6H).







658




δ 7.39(m, 2H), 7.20(m, 2H), 4.80(m, 1H), 4.64(m, 1H),








2.42(m, 1H), 1.64(d, 3H), 1.21(d, 6H).







672




δ 7.26(m, 2H), 7.09(m, 2H), 4.67(m, 1H), 4.4(m, 1H),








3.9(m, 2H), 3.8(m, 2H), 1.22(d, 6H).







675




δ 7.35(m, 1H), 6.93(t, 2H), 4.6(m, 1H), 3.62(t, 2H),








2.39(t, 2H), 2.05(m, 2H), (br, 6H)







677




δ 7.39(m, 5H) 7.20(m, 2H), 7.10(m, 2H), 5.60(s, 1H),








4.60(m, 1.20(d, 6H), 3.78(s, 3H), 1.19(d, 6H).







681




δ 7.3(d, 2H), 7.2(d, 2H), 5.0(m, 1H), 4.6-4.7(m, 1H),








4.0-4.2(m, 4H), 3.0-3.3(m, 2H), 1.2-1.3(m, 12H).







682




δ 7.56(s, 1H), 7.36(m, 1H), 6.91(m, 2H), 4.60(m, 1H),








4.47(s, 2H), 4.15(q, 2H), 1.41(t, 3H), 1.21(br s, 6H).







683




δ 7.54(s, 1H), 7.38(m, 3H), 7.24(m, 2H), 4.63(m, 1H),








4.59(s, 2H), 4.14(q, 2H), 1.41(t, 3H), 1.21(d, 6H).







684




δ 7.56(s, 1H), 7.36(m, 2H), 7.19(m, 2H), 4.63(m, 1H),








4.48(s, 2H), 4.15(q, 2H), 1.41(t, 3H), 1.19(d, 6H).







685




δ 7.56(s, 1H), 7.22(m, 2H), 7.07(m, 2H), 4.63(m, 1H),








4.48(s, 2H), 4.15(q, 2H), 1.41(t, 3H), 1.19(d, 6H).







686




δ 7.68(s, 1H), 7.22(m, 2H), 7.07(m, 2H), 5.12(q, 1H),








4.63(m, 1H), 4.14(q, 2H), 1.73(d, 3H), 1.41(t, 3H), 1.18








(d, 6H).







687




δ 7.37(m, 1H), 6.92(m, 2H), 4.62(m, 1H), 3.81(t, 2H),








2.94(s, 3H), 2.92(s, 3H), 2.66(t, 2H), 1.22(m, 6H).







693




δ 9.52(s, 1H), 7.22(m, 3H), 7.1(m, 2H), 4.64(m, 1H),








4.44(q, 1H), 1.6(d, 3H), 1.2(d, 6H).







694




δ 7.37(m, 1H), 6.92(m, 2H), 5.99(m, 1H), 5.44(m, 1H),








4.64(m, 1H), 4.57(m, 1H), 2.2-1.6(m, 6H), 1.21(br, 6H).







696




δ 7.37(d, 2H), 7.17(d, 2H), 5.99(m, 1H), 5.44(m, 1H),








4.64(m, 1H), 4.57(m, 1H), 2.2-1.6(m, 6H), 1.21(d, 6H).







697




δ 7.4(m, 3H), 7.15(m, 2H), 4.65(m, 1H), 3.90(m, 8H),








2.20(m, 2H), 1.22(d, 6H).







698




δ 7.4(d, 2H), 7.20(d, 2H), 4.65(m, 1H), 3.90(m, 8H),








2.20(m, 2H), 1.22(d, 6H).







701




δ 7.35(d, 2H), 7.20(d, 2H), 4.65(m, 1H), 3.90(m, 1H),








2.85(m, 1H), 1.40-2.00(m, 6H), 1.20(d, 9H).







702




δ 7.40(m, 1H), 6.92(m, 2H), 4.65(m, 1H), 3.90(m, 1H),








2.85(m, 1H), 1.40-2.00(m, 6H), 1.25(m, 9H).







705




δ 7.22(m, 2H), 7.06(m, 2H), 4.78(q, 1H), 4.62(m, 1H),








3.64(m, 8H), 1.66(d, 3H), 1.19(d, 6H).







708




δ 7.29(m, 1H), 6.92(m, 2H), 4.65(m, 1H), 4.4-3.5(m,








5H), 2.04(s, 3H), 1.23(bs, 6H).







712




δ 7.28(m, 2H), 7.08(m, 2H), 4.62(m, 1H), 3.52(m, 4H),








1.8(m, 4H), 1.18(d, 6H).







713




δ 7.23(m, 2H), 7.08(m, 2H), 4.61(m, 1H), 3.66(t, 2H),








3.5(t, 2H), 2.11(m, 2H), 1.21(d, 6H).







714




δ 7.3(m, 1H), 6.92(m, 2H), 4.65(m, 1H), 4.25(m, 1H),








3.71(m, 2H), 1.49(d, 3H), 1.23(bs, 6H).







715




δ 7.40(m, 1H), 6.92(m, 2H), 4.65(m, 1H), 3.90(m, 1H),








3.56(q, 2H), 3.30(m, 2H), 1.82(m, 1H), 1.50(m, 5H),








1.20(m, 6H).







717




δ 7.40(m, 3H), 7.25(m, 2H), 4.65(m, 1H), 3.90(m, 1H),








2.85(m, 1H), 1.50-2.00(m, 6H), 1.25(d, 3H), 1.20(d,








6H)







718




δ 7.25(m, 2H), 7.10(m, 2H), 4.65(m, 1H), 3.90(m, 1H),








2.85(m, 1H), 1.50-2.00(m, 6H), 1.25(d, 3H), 1.20(d,








6H).







720




δ 7.3(m, 1H), 6.9(m, 2H), 4.6(m, 1H), 3.1(m, 1H), 1.5








(m, 3H), 1.4(m, 1H), 1.2(m, 6H), 0.6-0.3(m, 4H).







721




δ 7.22(m, 2H), 7.09(m, 2H), 4.92(m, 1H), 4.65(m, 1H),








4.39(m, 2H), 2.91(m, 2H), 1.68(d, 3H), 1.19(d, 6H).







723




δ 7.39(m, 7H) 7.20(m, 2H), 7.10(m, 2H), 5.60(s, 1H),








4.60(m, 1H), 3.78(s, 3H), 1.19(d, 6H).







724




δ 7.40(m, 7H), 7.15(d, 2H), 5.60(s, 1H), 4.60(m, 1H),








3.79(s, 3H), 1.20(d, 6H).







725




δ 7.4(m, 2H), 7.2(m, 2H), 5.1(m, 1H), 4.6(m, 1H), 4.1








(m, 1H), 3.8(m, 1H), 3.4(s, 3H), 1.2(d, 6H).







726




δ 7.4(m, 2H), 7.2(m, 2H), 5.1(m, 1H), 4.6(m, 1H), 4.1








(m, 1H), 3.9(m, 1H), 3.4(s, 3H), 3.3(s, 3H), 1.2(d, 6H).







727




δ 7.2(m, 2H), 7.1(m, 2H), 5.97(br, 1H), 4.65(m, 1H),








3.65(m, 2H), 3.45(m, 2H), 1.91(s, 3H), 1.19(d, 6H).







729




δ 7.39(m, 3H), 7.25(m, 2H), 4.91(q, 1H), 4.64(m, 1H),








4.37(m, 2H), 2.92(m, 2H), 1.67(d, 3H), 1.20(d, 6H).







730




δ 7.35(m, 1H), 6.93(m, 2H), 4.93(q, 1H), 4.65(m, 1H),








4.39(m, 2H), 2.94(m, 2H), 1.68(d, 3H), 1.20(d, 6H).







73 1




δ 8.4(s, 1H), 7.6(m, 1H), 7.5(m, 1H), 7.4(m, 3H), 7.2








(m, 2H), 5.84(s, 1H), 5.3(s, 1H), 4.7(m, 1H), 4.6(s, 2H),








1.2(d, 6H).







732




δ 7.3-7.2(m, 3H), 7.1-7.0(m, 2H), 6.4(s, 1H),








5.7(s, 1H), 4.7-4.6(m, 1H), 4.3(s, 2H), 3.75(s, 3H),








1.2(d, 6H).







734




δ 7.4(m, 3H), 7.2(m, 2H), 5.1(m, 1H), 4.6(m, 1H), 4.1








(m, 1H), 3.9(m, 1H), 3.4(s, 3H), 3.3(s, 3H), 1.2(d, 6H).







735




δ 7.4(m, 3H), 7.2(m, 2H), 5.1(m, 1H), 4.6(m, 1H), 4.1








(m, 1H), 3.8(m, 1H), 3.4(s, 3H), 1.2(d, 6H).







737




δ 7.3(m, 1H), 6.9(m, 2H), 5.1(m, 1H), 4.6(m, 1H), 4.1








(m, 1H), 3.8(m, 1H), 3.4(s, 3H), 1.2(d, 6H).







738




δ 7.3(m, 1H), 6.9(m, 2H), 5.1(m, 1H), 4.6(m, 1H), 4.1








(m, 1H), 3.9(m, 1H), 3.4(s, 3H), 3.3(s, 3H), 1.2(d, 6H).







742




δ 7.3(m, 1H), 6.9(m, 2H), 4.9(m, 1H), 4.7(m, 1H),








3.4-3.6(m, 2H), 2.1(m, 1H), 1.9(m, 1h), 1.2(m, 9H),








0.9(t, 3H).







744




δ 7.40(m, 1H), 6.92(m, 2H), 4.66(m, 1H), 3.67(m, 2H),








2.56(m, 2H), 1.95(m, 1H), 1.60(d, 6H).







746




δ 7.41(m, 3H), 7.39(m, 2H), 5.60(m, 1H), 4.62(m, 1H),








3.82(m, 2H) 1.20(d, 6H).







747




δ 7.38(m, 3H) 7.25(m, 2H), 4.66(m, 1H), 4.25(m, 1H),








3.65(m, 2H), 1.49(d, 3H), 1.20(d, 6H).







748




δ 7.39(m, 2H) 7.17(m, 2H), 4.62(m, 1H), 4.25(m, 1H),








3.65(m, 2H), 1.49(d, 3H), 1.20(d, 6H).







750




δ 7.39(m, 3H) 7.26(m, 2H), 4.63(m, 1H), 3.65(m, 2H),








3.48(m, 2H), 2.10(m, 2H), 1.20(d, 6H).







753




δ 7.22(m, 2H), 7.11(m, 2H), 4.64(m, 1H), 4.58(m, 1H),








2.42(m, 1H), 2.04(m, 1H), 1.94(m, 1H), 1.20(d, 6H),








0.99(t, 3H).







758




δ 1.20(m, 6H), 4.07(m, 2H), 4.17(s, 2H), 4.32(m, 2H),








4.62(m, 1H), 6.92(m, 2H), 7.36(m, 1H).







759




δ 7.38(d, 2H), 7.18(d, 2H), 4.92(q, 1H), 4.62(m, 1H),








4.39(m, 2H), 2.91(m, 2H), 1.68(d, 3H), 1.20(d, 6H).







163




δ 7.40(m, 1H), 6.92(m, 2H), 4.66(m, 1H), 3.67(m, 2H),








2.56(m, 2H), 1.95(m, 1H), 1.60(d, 6H).







764




δ 7.38(m, 1H), 6.93(m, 2H), 4.62(m, 1H), 4.25(s, 2H),








2.37(m, 1H), 1.25(d, 6H)







765




δ 1.20(m, 6H), 4.24(S, 2H), 4.25(M, 2H), 4.38(M, 2H),








4.63(M, 1H), 7.09(M, 2H), 7.24(M, 2H).







766




δ 7.25(m, 2H), 7.15(m, 1H), 4.95(br s, 1H), 4.65(m,








1H), 4.16(m, 2H), 3.39(s, 3H), 2.19(m, 1H), 1.92(m,








3H), 1.19(d, 6H).







767




δ 7.26(m, 2H), 7.11(m, 2H), 4.64(m, 1H), 3.67(t, 2H),








2.56(m, 2H), 1.96(m, 1H), 1.21(d, 6H).







768




δ 7.38(m, 3H), 7.26(m, 2H), 4.64(m, 1H), 3.66(t, 2H),








2.54(m, 2H), 1.92(m, 1H), 1.22(d, 6H).







769




δ 7.39(m, 3H), 7.24(m, 2H), 4.74(s, 2H), 4.62(m, 1H),








3.18(m, 1H), 1.35(d, 6H), 1.21(d 6H).







771




δ 8.3(d, 1H), 7.6(dd, 1H), 7.4(d, 1H), 4.7(septet,








1H), 4.2(septet, 1H), 1.40(d, 3H), 1.21(d, 3H).







772




δ 7.4(m, 2H), 7.2(m, 2H), 4.9(m, 1H), 4.7(m, 1H),








3.4-3.6(m, 2H), 2.1(m, 1H), 1.9(m, 1H), 1.2(m, 9H),








0.9(t, 3H).







773




δ 7.4(m, 2H), 7.2(m, 2H), 4.9(m, 1H), 4.7(m, 1H),








3.4-3.6(m, 2H), 2.1(m, 1H), 1.9(m, 1H), 1.2(m, 9H),








0.9(t, 3H).







774




δ 7.3(m, 1H), 6.9(m, 2H), 4.9(m, 1H), 4.7(m, 1H),








3.4-3.6(m, 2H), 2.1(m, 1H), 1.9(m, 1H), 1.2(m, 9H),








0.9(t, 3H).







776




δ 7.3(m, 1H), 6.90(m, 2H), 4.65(m, 1H), 4.20(m, 5H),








1.70(m, 3H), 1.25(m, 12H).







778




δ 7.4(m, 1H), 6.90(m, 2H), 4.65(m, 1H), 3.60(m, 7H),








2.85(m, 3H), 1.21(m, 6H).







779




δ 7.4(d, 2H), 7.2(d, 2H), 4.65(m, 1H), 3.60(m, 7H),








2.85(m, 3H), 1.21(m, 6H).







782




δ 7.22(m, 2H), 7.09(t, 2H), 5.93(t, 1H), 4.62(m, 1H),








4.21(d, 2H), 1.2(d, 6H).







783




δ 7.38(m, 1H), 6.96(m, 2H), 4.60(m, 2H), 2.40(m, 1H),








2.10-1.80(m, 2H), 1.22(m, 1H), 0.94(m, 3H).







784




δ 7.39(m, 2H), 7.20(m, 2H), 4.64(m, 1H), 4.25(m, 2H),








2.33(m, 1H), 1.21(d, 6H).







785




δ 7.35(m, 1H), 6.92(m, 2H), 5.32(q, 1H), 4.62(m, 1H),








2.31(s, 3H), 2.24(s, 3H), 1.83(d, 3H), 1.22(br, 6H).







792




δ 7.39(m, 3H) 7.25(m, 2H), 4.61(m, 1H), 3.52(m, 4H),








1.80(m, 4H), 1.20(d, 6H).







797




δ 7.4(m, 3H), 7.3-7.1(m, 2H), 5.5(bs, 1H), 4.7-4.6(m,








1H), 3.94(bs, 2H), 2.35(s, 2H), 2.3-2.2(m, 2H), 2.0(m,








2H), 1.2(d, 6H), 1.2(s, 6H).







800




δ 7.38(m, 3H), 7.25(m, 2H), 4.64(m, 1H), 2.35(m, 1H),








1.21(d, 6H), 1.15(s, 3H), 1.05(m, 1H), 0.94(m, 4H).







801




δ 7.37(d, 2H), 7.19(d, 2H), 4.64(m, 1H), 2.37(m, 1H),








1.19(m, 9H), 1.07(m, 1H), 0.96(m, 4H).







802




δ 737(m, 1H), 6.91(m, 2H), 4.64(m, 1H), 2.37(m, 1H),








1.19(m, 9H), 1.07(m, 1H), 0.96(m, 4H).







803




δ 7.39(m, 3H), 7.26(m, 2H), 4.64(m, 1H), 4.52(m, 1H),








2.40(m, 1H), 2.04(m, 1H), 1.92(m, 1H), 1.44 and 0.98(t,








3H), 1.22(d, 6H).







804




δ 7.38(m, 2H), 7.21(m, 2H), 4.64(m, 1H), 3.67(t, 2H),








2.56(m, 2H), 1.96(m, 1H), 1.22(d, 6H).







805




δ 7.25(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 4.40(m, 1H),








3.70(m, 4H), 1.20(d, 6H).







808




δ 7.39(m, 2H), 7.20(m, 2H), 7.64(m, 1H), 4.58(m, 1H),








2.43(m, 1H), 2.40(m, 1H), 1.92(m, 1H), 1.21(d, 6H),








0.97(t, 3H).







810




δ 7.22(m, 2H), 7.09(m, 2H), 4.46(m, 1H), 4.95(m, 1),








4.64(m, 1H), 3.02(m, 1H), 2.76(m, 1H), 1.68(d, 3H),








1.20(d, 6H).







811




δ 7.21(m, 2H), 7.11(m, 2H), 4.98(m, 1H), 4.64(m, 1H),








3.89(m, 1H), 2.98(dd, 1H), 2.69(dd, 1H), 1.5(d, 3H),








1.20(d, 6H).







812




δ 7.42(m, 3H), 7.40(m, 2H), 5.44(m, 1H), 4.93(m, 1H),








4.64(m, 1H), 2.80(m, 1H), 2.70(m, 1H), 1.28(d, 3H),








1.22(d, 6H).







814




δ 7.39(d, 2H), 7.17(d, 2H), 7.11(br s, 1H), 4.92(m, 1H),








4.64(m, 1H), 3.89(m, 1H), 3.02(m, 1H), 2.70(m, 1H),








1.52(d, 3H), 1.20(d, 6H).







815




δ 7.32(m, 1H), 7.11(br s, 1H), 6.94(m, 2H), 4.88(m,








1H), 4.64(m, 1H), 3.90(m, 1H), 3.01(m, 1H), 2.70(m,








1H), 1.51(d, 3H), 1.23(br, 6H).







816




δ 7.40(m, 3H), 7.23(m, 2H), 7.09(br s, 1H), 4.91(m,








1H), 4.66(m, 1H), 3.88(m, 1H), 3.00(m, 1H), 2.70(m,








1H), 1.50(d, 3H), 1.21(d, 6H).







817




δ 7.28(m, 1H), 6.91(m, 2H), 4.63(m, 1H), 4.11(m, 1H),








1.28(d, 3H), 1.22(d, 6H).







819




δ 7.22(m, 2H), 7.08(m, 2H), 4.62(m, 1H), 3.78(d, 1H),








3.50(d, 1H), 2.70(d, 1H), 2.60(d, 1H), 1.33(s, 3H),








1.18(d, 6H).







822




δ 7.40(m, 2H), 6.92(m, 2H), 4.60(m, 1H), 3.66(m, 2H),








3.50(m, 2H), 2.05(m, 2H), 1.26(d, 6H).







823




δ 7.40(m, 2H), 6.92(m, 2H), 4.61(m, 1H), 3.54(m, 4H),








1.80(m, 4H), 1.22(d, 6H).







824




δ 7.39(m, 3H), 7.24(m, 2H), 4.62(m, 1H), 4.30(m, 1H),








3.90(m, 1H), 3.70(m, 1H), 3.60(m, 1H), 3.30(s, 3H),








1.22(d, 6H).







825




δ 7.21(m, 2H), 7.08(m, 2H), 4.62(m, 1H), 4.30(m, 1H),








3.90(m, 1H), 3.71(m, 1H), 3.60(m, 1H), 3.30(s, 3H),








1.22(d, 6H).







829




δ 4.66(s, 1H), 4.5(m, 1H), 4.3(m, 1H), 1.48(d, 6H),








1.42(s, 9H), 1.28(d, 6H).







837




δ 7.20(m, 2H), 7.10(m, 2H), 5.65(m, 2H), 5.05(d, 1H),








4.65(m, 1H), 4.20(m, 4H), 1.45(d, 3H), 1.20(d, 6H).







839




δ 7.12-7.2(m, 3H), 4.62(m, 1H), 4.17(m, 1H), 1.39








(d, 6H), 1.25(d, 6H).







840




δ 7.23(m, 2H), 7.1(m, 2H), 4.2(m, 1H), 3.80(q, 2H),








1.40(d, 6H), 1.27(t, 3H).







841




δ 7.38(d, 2H), 7.18(d, 2H), 6.0(m, 1H), 5.25(m, 2H),








4.6(m, 2H), 1.5(d, 3H), 1.2(d, 6H).







842




δ 7.38(d, 2H), 6.93(m, 2H), 5.98(m, 1H), 5.24(m, 2H),








4.6(m, 2H), 1.49(d, 3H), 1.22(br, 6H).







843




δ 7.4(m, 3H), 7.25(m, 2H), 6.0(m, 1H), 5.22(m, 2H),








4.6(m, 2H), 1.48(d, 3H), 1.2(d, 6H).







845




δ 7.38(d, 2H), 6.93(m, 2H), 4.9(s, 2H), 4.64(m, 1H),








4.41(m, 1H), 3.45(m, 2H), 2.95(m, 2H), 1.21(d, 6H).







846




δ 7.4(m, 3H), 7.25(m, 2H), 4.89(s, 2H), 4.64(m, 1H),








4.41(m, 1H), 3.45(m, 2H), 2.95(m, 2H), 1.21(d, 6H).







849




δ 9.53(s, 1H), 7.39(d, 2H), 7.19(d, 2H), 4.64(m, 1H),








4.44(q, 1H), 1.6(d, 3H), 1.21(d, 6H).







850




δ 9.51(s, 1H), 7.4(d, 3H), 7.25(m, 2H), 4.64(m, 1H),








4.42(q, 1H), 1.58(d, 3H), 1.21(d, 6H).







852




δ 7.42(s, 1H), 7.37(m, 2H), 7.18(m, 2H), 4.63(m, 1H),








4.48(s, 2H), 3.81(s, 3H), 1.20(d, 6H).







853




δ 7.44(s, 1H), 7.38(m, 2H), 7.24(m, 3H), 4.63(m, 1H),








4.47(s, 2H), 3.80(s, 3H), 1.20(d, 6H).







854




δ 7.47(s, 1H), 7.37(m, 1H), 6.93(m, 2H), 4.62(m, 1H),








4.49(s, 2H), 3.81(s, 3H), 1.21(br s, 6H).







866




δ 7.34(m, 2H), 6.91(m, 2H), 5.33(m, 1H), 4.62(m, 1H),








3.92(s, 2H), 1.91(m, 3H), 1.21(br s, 6H).







871




δ 7.40(m, 2H), 7.19(m, 2H), 4.65(m, 1H), 4.30(m, 1H),








3.95(dd, 1H), 3.75(m, 1H), 3.60(m, 1H), 3.30(s, 3H),








1.22(d, 6H).







872




δ 7.30(m, 1H), 6.92(m, 2H), 4.62(m, 1H), 4.30(m, 1H),








3.90(m, 1H), 3.73(m, 2H), 3.60(m, 1H), 3.30(s, 3H),








1.26(d, 6H).







876




δ 7.36(m, 2H), 7.17(m, 2H), 4.60(m, 1H), 4.12(m, 1H),








1.20(d, 3H), 1.19(d, 6H).







882




δ 7.38(m, 3H), 7.25(m, 2H), 4.62(m, 2H), 2.40(m, 1H),








2.00-1.80(m, 2H), 1.50-1.30(m, 2H), 1.20(d, 6H),








0.92(t, 3H).







884




δ 7.23(m, 2H), 7.08(m, 2H), 5.75(m, 1H), 5.21(m, 2H),








4.65(m, 1H), 4.41(s, 1H), 4.32(s, 1H), 4.25(s, 1H), 3.98








(s, 1H), 3.91(d, 1H), 3.86(s, 1.5H), 3.78(d, 1H), 3.74(s,








1.5H), 1.20(d, 6H). syn/anti mixture







885




δ 7.37(m, 3H), 7.26(m, 2H), 5.75(m, 1H), 5.20(m, 2H),








4.63(m, 1H), 4.39(s, 1H), 4.31(s, 1H), 4.24(s, 1H),








3.94(s, 1H), 3.89(d, 1H), 3.84(s, 1.5H), 3.75(d, 1H),








3.73(s, 1.5H), 1.20(d, 6H). syn/anti mixture







886




δ 7.36(m, 1H), 6.91(m, 2H), 5.80(m, 1H), 5.21(m, 2H),








4.63(m, 1H), 4.40(s, 1H), 4.32(s, 1H), 4.25(s, 1H),








3.96(s, 1H), 3.92(d, 1H), 3.85(s, 1.5H), 3.80(d, 1H),








3.73(s, 1.5H), 1.20(br, 6H) syn/anti mixture







887




δ 7.36(d, 2H), 7.20(d, 2H), 5.76(m, 1H), 5.19(m, 2H),








4.64(m, 1H), 4.41(s, 1H), 4.32(s, 1H), 4.25(s, 1H),








3.95(s, 1H), 3.91(d, 1H), 3.86(s, 1.5H), 3.78(d, 1H),








3.74(s, 1.5H), 1.20(d, 6H). syn/anti mixture







888




δ 7.4(d, 2H), 7.29(d, 2H), 4.63(m, 1H), 4.15(m, 1H),








3.58(m, 2H), 1.49-1.27(m, 9H).







892




δ 7.20(m, 2H), 7.08(t, 2H), 4.65(m, 1H), 3.70(m, 1H),








3.42(m, 2H), 3.30(m, 2H), 3.12(s, 3H), 1.90(m, 3H),








1.50(m, 1H), 1.20(m, 6H).







898




δ 7.20(m, 2H), 7.08(t, 2H), 4.97(d, 1H), 4.65(m, 1H),








3.90(m, 2H), 3.80(m, 1H), 3.62(m, 1H), 3.47(m, 1H),








1.50(m, 4H), 1.40(d, 3H), 1.20(m, 6H).







900




δ 7.30(m, 9H), 4.63(m, 1H), 4.44(s, 1H), 4.39(s, 1H),








4.34(s, 1H), 4.29(s, 1H), 4.25(s, 1H), 3.96(s, 1H),








3.83(s, 1.5H), 3.71(s, 1.5H), 1.21(m, 6H).








syn/anti mixture







901




δ 7.30(m, 10H), 4.63(m, 1H), 4.44(s, 1H), 4.39(s, 1H),








4.34(s, 1H), 4.29(s, 1H), 4.25(s, 1H), 3.96(s, 1H), 3.83








(s, 1.5H), 3.71(s, 1.5H), 1.21(m, 6H). syn/anti mixture







902




δ 7.23(m, 2H), 7.08(m, 2H), 4.65(m, 1H), 4.39(s, 1H),








4.29(s, 1H), 4.20(s, 1H), 3.91(s, 1H), 3.86(s, 1.5H),








3.74(s, 1.5H), 3.28(s, 1.5H), 3.14(s, 1.5H), 120(d,








6H). syn/anti mixture







903




δ 7.37(m, 3H), 7.26(m, 2H), 4.64(m, 1H), 4.38(s, 1H),








4.28(s, 1H), 4.19(s, 1H), 3.89(s, 1H), 3.85(s, 1.5H),








3.74(s, 1.5H), 3.27(s, 1.5H), 3.10(s, 1.5H), 1.20(d,








6H). syn/anti mixture







904




δ 7.37(m, 3H), 7.26(m, 2H), 4.64(m, 1H), 4.38(s, 1H),








4.28(s, 1H), 4.19(s, 1H), 3.89(s, 1H), 3.85(s, 1.5H),








3.74(s, 1.5H), 3.27(s, 1.5H), 3.10(s, 1.5H), 1.20(d,








6H). 4:1 syn/anti mixture







905




δ 7.35(d, 2H), 7.27(d, 2H), 4.39(m, 2H), 4.15(m, 1H),








3.40(s, 3H), 3.38(s, 3H), 1.39(d, 6H), 1.26(d, 3H).







908




δ 7.36(m, 3H), 7.26(m, 2H), 4.35(m, 2H), 4.15(m, 1H),








1.70(d, 3H), 1.38(m, 6H).







909




δ 7.28(m, 2H), 7.09(m, 2H), 4.38(m, 2H), 4.18(m, 1H),








1.68(d, 3H), 1.38(m, 6H).







913




δ 7.4(m, 3H), 7.25(m, 2H), 4.64(m, 1H), 3.71(t, 2H),








2.84(t, 2H), 2.14(s, 3H), 1.21(d, 6H).







914




δ 9.73(s, 1H), 7.22(m, 2H), 7.09(m, 2H), 4.64(m, 1H),








3.81(t, 2H), 2.88(t, 2H), 1.2(d, 6H).







915




δ 7.35(m, 1H), 6.92(m, 2H), 4.63(m, 1H), 3.51(t, 2H),








2.45(t, 2H), 2.11(s, 3H), 1.89(m, 2H), 1.22(br, 6H).







916




δ 7.37(m, 2H), 7.18(m, 2H), 4.64(m, 1H), 3.51(t, 2H),








2.45(t, 2H), 2.11(s, 3H), 1.89(m, 2H), 1.22(br, 6H).







917




δ 7.37(t, 2H), 7.21(m, 2H), 4.62(m, 2H), 2.40(m,








1H), 2.00-1.80(m, 2H), 1.50-1.30(m, 2H), 1.20(d,








6H), 0.92(t, 3H).







919




δ 7.34(m, 5H), 4.42(m, 2H), 4.18(m, 1H), 3.74(s, 3H),








3.42(s, 3H), 1.37(d, 6H), 1.27(m, 3H).







920




δ 7.30(m, 2H), 7.09(m, 2H), 4.38(m, 2H), 4.18(m, 1H),








3.41(s, 3H), 3.38(s, 3H), 1.39(d, 6H), 1.27(m, 3H).







922




δ 7.36(d, 2H), 7.20(d, 2H), 4.64(m, 1H), 4.39(s, 1H),








4.29(s, 1H), 4.20(s, 1H), 3.91(s, 1H), 3.86(s, 1.5H),








3.74(s, 1.5H), 3.28(s, 1.5H), 3.14(s, 1.5H), 1.20(d,








6H). syn/anti mixture







923




δ 7.38(m, 1H), 6.91(m, 2H), 4.64(m, 1H), 4.39(s, 1H),








4.29(s, 1H), 4.19(s, 1H), 3.91(s, 1H), 3.86(s, 1.5H),








3.74(s, 1.5H), 3.29(s, 1.5H), 3.15(s, 1.5H), 1.20(br,








6H). syn/anti mixture







927




δ 7.37(m, 2H), 6.91(m, 2H), 6.15(m, 1H), 5.55(m, 1H),








5.00(m, 1H), 4.64(m, 1H), 2.7(m, 1H), 2.30(m, 2H),








1.98(m, 1H), 1.2(br, 6H).







929




δ 7.4(m, 3H), 7.25(m, 2H), 6.17(m, 1H), 5.55(m, 1H),








5.00(m, 1H), 4.64(m, 1H), 2.7(m, 1H), 2.3(m, 2H),








1.99(m, 1H), 1.2(d, 6H).







930




δ 7.24(m, 3H), 7.10(m, 2H), 4.65(m, 2H), 3.8(m, 2H),








3.39(m, 2H), 1.21(d, 6H).







935




δ 7.35(m, 1H), 6.91(m, 2H), 4.63(m, 1H), 3.74(t, 2H),








2.85(t, 2H), 2.15(s, 3H), 1.21(br, 6H).







947




δ 7.31(m, 1H), 6.89(m, 2H), 4.6(m, 1H), 3.75(m, 1H),








2.72(m, 4H), 2.4(m, 2H), 2.00(m, 2H), 1.23(m, 6H).







952




δ 7.51(m, 3H), 7.24(m, 2H), 6.86(q, 1H), 4.31(m,








1H), 1.97(d, 3H), 1.49(d, 6H).







953




δ 7.34(m, 5H), 4.22(m, 1H), 2.14(s, 3H), 1.92(s, 3H),








1.44(d, 6H).







955




δ 7.43(m, 5H), 4.64(m, 1H), 4.17(m, 1H), 3.79(d, 4H),








1.38(d, 6H).







956




δ 7.44(m, 2H), 7.12(m, 2H), 4.19(m, 1H), 4.13(m, 2H),








3.78(d, 4H), 1.40(d, 6H).







959




δ 7.38(m, 3H), 7.26(m, 2H), 4.64(m, 1H), 4.26(m, 1H),








2.41(m, 2H), 1.22(m, 6H), 1.10(d, 3H), 0.85(d, 3H).







962




δ 7.22(m, 2H), 7.10(m, 2H), 4.64(m, 1H), 3.51(t, 2H),








2.45(t, 2H), 2.11(s, 3H), 1.90(m, 2H), 1.2(d, 6H).







963




δ 7.39(m, 3H), 7.26(m, 2H), 4.64(m, 1H), 3.50(t, 2H),








2.43(t, 2H), 2.11(s, 3H), 1.89(m, 2H), 1.2(d, 6H).







964




δ 9.73(s, 1H), 7.37(m, 1H), 6.93(m, 2H), 4.63(m, 1H),








3.81(t, 2H), 2.89(t, 2H), 1.22(br, 6H).







965




δ 9.72(s, 1H), 7.39(m, 3H), 7.25(m, 2H), 4.64(m, 1H),








3.79(t, 2H), 2.87(t, 2H), 1.21(br, 6H).







967




δ 7.22(m, 2H), 7.08(m, 2H), 4.64(m, 1H), 3.94(m, 1H),








2.78(m, 1H), 2.58(m, 1H), 2.00-1.70(m, 3H), 1.26(m,








2H), 1.20(m, 6H), 0.90(m, 3H).















a1


H NMR data are in ppm downfield from tetramethylsilane. Couplings are designated by (s)-singlet, (d)-doublet, (t)-triplet, (q)-quartet, (m)-multiplet, (dd)-doublet of doublets, (dt)-doublet of triplets, (br s)-broad singlet.













Test A




Seeds of barnyardgrass (


Echinochloa crus


-


galli


), crabgrass (Digitaria spp.), morningglory (Ipomoea spp.), and velvetleaf (


Abutilon theophrasti


) were planted into a sandy loam soil and treated preemergence by soil drench with test chemicals formulated in a non-phytotoxic solvent mixture which includes a surfactant At the same time, these crop and weed species were also treated postemergence sprayed to runoff, with test chemicals formulated in the same manner.




Plants ranged in height from two to eighteen cm and were in the one to two leaf stage for the postemergence treatment. Treated plants and untreated controls were maintained in a greenhouse for approximately eleven days, after which all treated plants were compared to untreated controls and visually evaluated for injury. Plant response ratings, summarized in Table A, are based on a 0 to 10 scale where 0 is no effect and 10 is complete control.














TABLE A













COMPOUND























Rate 2000 g/ha




1




2




3




10




42




43




52




53




99




114











Pre-emergence







Barnyardgrass




9




9




9




10




0




0




9




8




9




10







Crabgrass




9




2




3




9




0




1




10




9




10




10







Morningglory




0




0




0




1




0




0




0




0




2




6







Velvetleaf




0




0




0




2




0




0




0




0




3




6

















COMPOUND



















Rate 2000 g/ha




127




128




136




137




177




183











Pre-emergence







Barnyardgrass




9




0




9




10




9




9







Crabgrass




8




0




10




10




9




5







Morningglory




0




0




0




3




0




0







Velvetleaf




0




0




0




5




1




0

















COMPOUND

















Rate 2000 g/ha




184




225




377




386











Pre-emergence







Barnyardgrass




9




10




0




0







Crabgrass




9




10




0




0







Morningglory




0




8




0




0







Velvetleaf




0




7




0




0

















COMPOUND























Rate 1000 g/ha




1




2




3




10




42




43




52




53




99




114











Barnyardgrass




8




8




6




9




0




0




5




3




7




8







Crabgrass




5




0




0




8




0




0




8




6




7




7







Morningglory




0




0




0




0




0




0




1




0




2




10







Velvetleaf




0




0




0




4




0




0




1




1




2




5

















COMPOUND



















Rate 1000 g/ha




127




128




136




137




177




183











Barnyardgrass




6




0




4




8




0




0







Crabgrass




7




0




6




8




3




1







Morningglory




0




0




9




10




0




0







Velvetleaf




0




0




2




2




2




0

















COMPOUND

















Rate 1000 g/ha




184




225




377




386











Postemergence







Barnyardgrass




2




9




0




0







Crabgrass




1




9




0




0







Morningglory




10




10




0




0







Velvetleaf




2




3




0




0















Test B




Seeds of bedstraw (


Galium aparine


), blackgrass (


Alopecurus myosuroides


), surinam grass (


Brachiaria decumbens


), cocklebur (


Xanthium strumarium


), corn (


Zea mays


), crabgrass (


Digitaria sanguinalis


), giant foxtail (


Setaria faberii


), morningglory (


Ipomoea hederacea


), pigweed (


Amaranthus retroflexus


), rape (


Brassica napus


), soybean (


Glycine max


), sugar beet (


Beta vulgaris


), velvetleaf (


Abutilon theophrasti


), wheat (


Triticum aestivum


), wild oat (


Avena fatua


) and purple nutsedge (


Cyperus rotundus


) tubers were planted and treated preemnergence with test chemicals formulated in a non-phytotoxic solvent mixture which included a surfactant.




At the same time, these crop and weed species were also treated with postemergence applications of test chemicals formulated in the same manner. Plants ranged in height from 2 to 18 cm (1- to 4-leaf stage) for postemergence treatments. Plant species in the flood test consisted of rice (


Oryza sativa


), smallflower flatsedge (


Cyperus difformis


), duck salad (


Heteranthera limosa


) and bamyardgrass (


Echinochloa crus


-


galli


) grown to the 2-leaf stage for testing. Treated plants and controls were maintained in a greenhouse for twelve to sixteen days, after which all species were compared to controls and visually evaluated. Plant response ratings, summarized in Table B, are based on a scale of 0 to 10 where 0 is no effect and 10 is complete control. A dash (−) response means no test result.















TABLE B













COMPOUND













































Rate 2000 g/ha




7




18




30




36




46




47




78




86




87




93




94




103




105




107




108




109




111




113




116




117




118




119




121




122




123




124




125




139




154




177




183




274









Pre-emergence






Barnyardgrass




0




9




0




0




9




8




3




0




0




0




7




0




0




0




0




9




9




9




9




3




6




0




9




0




0




0




0




6




0




0




0




0






Ducksalad




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




6




0




8




8




1




0




0




0




0




0




0




0




2




0




0




0




0






Rice




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




7




0




7




4




0




0




0




5




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




8




0




7




0




0




0




8




0




0




5




0




8




0




9




9




4




0




0




9




0




0




0




0




0




0




0




0




0

















COMPOUND
















Rate 2000 g/ha




157




177




183









Postemergence






B. signalgrass









0




0






Barnyardgrass




0
















Bedstraw





















Blackgrass









6




0






Cocklebur









0




2






Corn









0




0






Crabgrass









0




0






Ducksalad




0
















Giant foxtail









2




0






Morningglory









1




5






Nutsedge









0




0






Rape









3




0






Redroot pigweed









3




0






Rice




0
















S. Flatsedge




0
















Soybean









4




3






Sugarbeets









0




0






Velvetleaf









4




1






Wheat









3




0






Wild oats









2




0

















COMPOUND















Rate 2000 g/ha




177




183









Preemergence






B. signalgrass




9




2






Bedstraw




10




10






Blackgrass




9




2






Cocklebur




2




0






Corn




0




0






Crabgrass




9




2






Giant foxtail




10




9






Morningglory




0




0






Nutsedge




0




0






Rape




0




0






Redroot pigweed




0




0






Soybean




0




0






Sugarbeets




0




0






Velvetleaf




3




0






Wheat




2




0






Wild oats




10




3
















COMPOUND












































Rate 1000 g/ha




7




18




30




35




36




46




47




78




86




87




93




94




103




105




107




108




109




111




113




116




117




118




119




121




122




123




124




125




139




154




177




183




184









Pre-emergence






Barnyardgrass




0




9




0




0




0




0




6




0




0




0




0




0




0




0




0




0




8




0




0




0




0




3




0




9




0




0




0




0




0




0




0




0




3






Ducksalad




0




0




0




0




0




2




3




0




0




0




0




0




0




0




0




0




1




0




1




1




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0
















COMPOUND









































Rate 1000 g/ha




244




247




248




274




279




280




302




306




307




308




309




310




317




322




331




332




333




365




447




448




587




599




600




616




617




623




662




677




678









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




6




0




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0

















COMPOUND
















Rate 1000 g/ha




679




680




681









Pre-emergence






Barnyardgrass




0




0




0






Ducksalad




0




0




0






Rice




0




0




0






S. Flatsedge




0




0




0
















COMPOUND












































Rate 1000 g/ha




1




2




3




4




5




6




7




8




9




12




13




99




127




157




176




177




183




184




247




279




280




302




365




447




448




587




599




600




616




617




623




662




677









Postemergence






B. signalgrass




6




2




0




4




4




7




6




3




0




0




6




4




0









2




0




0




3




0




0




0




0




0




2




0




5




0




0




5




3




0




2




1






Barnyardgrass




0




0




0




4




4




8




0




0




0




0




0




8









0




0
































































































Bedstraw




0




0




0




8




4




3




4




3









0




0









0









9



















0




0




0




0



















7









0
























0






Blackgrass




8




9




3




6




8




7




6




5




3




0




8




5




0









7




3




0




7




0




6




0




6




0




7




2









6




0









6




7




6




4






Cocklebur




0




0




2




8




8




0




2




2




4




0




0




4




0









6




0




0




2




0




0




0




0




0




0




0




0




0




0




3




3




0




5




1






Corn




0




8




0




0




0




4




0




3




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0






Crabgrass




9




4




7




8




6




7




5




6




0




0




9




8




0









9




0




0




2




0









0




1




0




0




0




3




0




3




8




7




3




8




6






Ducksalad




0




0




0




3




0




0




0




0




0




0




0




3









0




0
































































































Giant foxtail




8




8




8




6




7




7




6




4




0




0




7




2




0









7




0




0




3




0




4




0




7




0




0




0




4




4




3




7




6




2




8




5






Morningglory




0




5




0




3




9




7




3




6




2




0




0




9




0









7




1




4




9




4




3




0




2




0




10




8




9




6




0




10




6




10




7











Nutsedge




0




0




0




0




0
























0




0




0




0














0




0




0




0




0




0




0




0




0




0




0




0




0









0














0






Rape




4




0




0




3




5




2




0




0




0




0




1




7




0









0




0




0




3




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0






Redroot pigweed




9




0




0




8




8




4




0




5




3




0




0




7




0









1




2




0




6




0




4




3




3




0




0




0




0




0




0




3




0




5




0




4






Rice




0




0




0




0




0




3




0




0




0




0




0




0









0




0
































































































S. Flatsedge




0




0




0




4




2




3




0




0




0




0




0




3









0




0
































































































Soybean




2




4




2




5




6




6




5




5




1




1




3




3




0









4




3




2




4




1




4




5




5




3




6




6




6




4




4




4




7




3









7






Sugarbeets




5




0




0




4




7




3




2




2




0




0




0




5




0









4




0




0




0




0




4




0




2




0




0




0




0




0




0




2




0




0




0




1






Velvetleaf




0




0




0




7




7




1




0




1




0




0




0




7




0









3




0




1




2




0




0




0




0




0




0




2




2




3




0




1




2




2




0




3






Wheat




0




0




0




0




2




0




2




3




0




0




0




2




0









4




3




0




3




0




1




0




1




0




0




0




3




0




0




0




0




1




0




0






Wild oats




0




0




0




0




1




4




3




3




0




0




2




3




0









4




2




0




5




0




0




0




0




0




0




4




0




0




0









0




2




1




0

















COMPOUND





















Rate 1000 g/ha




678




679




680




681




736




775




777




778









Postemergence






B. signalgrass




4




0




3




0




7




9




8




6






Barnyardgrass














































Bedstraw




0
























7




6




7






Blackgrass




6




1




3




4




7




4




4




4






Cocklebur




3




1




0




0




10




0




0




0






Corn




0




0




1




0




4




0




0




0






Crabgrass









2




9




2




6




9









9






Ducksalad














































Giant foxtail




7




5




8




3




6




9




9




9






Morningglory









2




7









7




8




8




8






Nutsedge









0














5




0




3




3






Rape




2




0




0




0




0




0




0




3






Redroot pigweed




5




2




5




7




3




6




8




6






Rice














































S. Flatsedge














































Soybean




2














3




6




6




6




7






Sugarbeets




0




0




2




7




0




0




7




9






Velvetleaf




6




3




4




2




4




3




5




3






Wheat




2




0




0




0




2




9




3




2






Wild oats




3




0




1




1




3




0




3




2
















COMPOUND












































Rate 1000 g/ha




1




2




3




4




5




6




7




8




9




12




13




99




127




176




177




183




184




247




279




280




302




365




447




448




587




599




600




616




617




623




662




677




678









Preemergence






B. signalgrass




8




6




0




10




8




5




3




6




0




6




8




6




0




3




5




0




5




0




0




0




7




0




6




4




10




3




0




6




8




4




9




9




0






Bedstraw




0




0




0




6




0




0




0




0




0




0




3




0




0




6




10




7




2




0




0




0




0




0









0




3




8




0




4




0


























Blackgrass




4




7




0




10




8




7




2




4




0




4




9




7




0




7




7




1




7




0




0




0




6




0




3




4




10




8




0




8




10




2




9




4




1






Cocklebur














0




0




0




2




0




0




0




0









7









0









0




3




0




0




0




0




0




0









0




3




0




0




0




0




9




0




0






Corn




7




8




0




0




0




5




0




3




3




0




0




2




0




2




0




0




2




0




0




0




0




0




0




2




4




0




0




2




0




0




5




0




0






Crabgrass




9




6




2




10




7




10




8




9




3




6




8




10




7




10




8




0




9




3




4




0




7




8




9




9




10




8




0




6




8




0




9




9




3






Giant foxtail




9




10




10




10




10




9




9




10




7




8




8




10




9




10




10




6




10




7




7




0




10




9




10




9




10




10




0




9




10




9




10




10




6






Morningglory




0




0




0




0




0




0




0




0




0




0




2




3




0




0




0




0




2




0




0




0




0




0




2




0




3




0




0




0




0




0




3




0




1






Nutsedge



















0




0




0




0




0




0




0




0




10









10




0




0














0




0




0




0




0




0




0




0




0




0




8




0




10




0




0






Rape




0




0




0




3




0




0




0




0




0




0




0




6




0




3




0




0




0




0




0




0




8




0




0




0




2




3




0




6




0




2




4




3




0






Redroot pigweed




2




0




0




8




10




7




2




7




0




0




3




10




10




0




0




0




2




0




0




0




3




0




0




0




3




4




0




10




0




5




7




8




4






Soybean




0




3




0




1




0




0




0




0




0




0




0




2




0




2




0




0




0




0




0




0




0




0









0




2




0




3




5




1




0




3




0




0






Sugarbeets




0




0




0




4




0




0




0




0




0




0




0




6




0




6




0




0




2




0




0




0




4




0




0




0




3




2




0




7




0




7




0




7




0






Velvetleaf




3




2




0




0




0




4




0




4




0




0




2




0




0




5




0




0




3




0




0




0




4




0




0




0




4




0




0




5




0




0




2




0




5






Wheat




0




0




0




0




0




3




0




0




0




0




0




2




2




4




0




0




0




0




0




0




0




0




0




0




7




0




0




0




2




3




5




0




0






Wild oats




2




4




0




8




6




6




0




3




0




0




7




7




8




5




10




0




4




0




0




0




6




0




10




5




10




0




0




10




9




2




9




2




0

















COMPOUND
























Rate 1000 g/ha




679




680




681




697




698




723




724




736




775




777




778









Preemergence






B. signalgrass




0




0




4




9




4




6




0




9





















Bedstraw



















0




0




0




0









2




3




10






Blackgrass




5




4




6




10




9




6




2




10




10




10




10






Cocklebur




0




0









0




0




0




0




2




0









0






Corn




2




0




0




0




0




0




0




9




4




0




2






Crabgrass




3




3




8




9




9




9




9




9




10




10




10






Giant foxtail




8




7




9




10




10




10




10




8




10




10




10






Morningglory




0




0




0




5




0




0




0




6




5




7




0






Nutsedge









0




0




0









0




0




8




9




1




10






Rape




0




0




0




0




8




2




0




2




7




7




6






Redroot pigweed




6




7




5




0




0




5




3




2




10




9




10






Soybean




0




0




0




0




3




0




0




3




2




0




7






Sugarbeets




0




0




0




0




0




0




0




5




3




3




7






Velvetleaf




0




4




0




2




0




0




0




3




4




3




3






Wheat




0




0




0




7




6




0




0




9




9




9




8






Wild oats




0




2




3




9




10




8




0




10




9




9




9

















COMPOUND















































Rate 500 g/ha




7




18




30




35




36




46




47




69




70




71




72




78




86




87




93




94




103




105




107




108




109




111




113




116




117




118




119




121




122




123




124




125




129




131









Pre-emergence






Barnyardgrass




0




8




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




8




0




0




0




0




9




9






Ducksalad




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




9






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




8






S. Flatsedge




0




6




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




9




8
















COMPOUND








































Rate 500 g/ha




139




146




154




165




166




177




180




181




182




183




184




185




186




187




189




190




191




192




193




194




195




196




197




198




201




202




203




204




205









Pre-emergence






Barnyardgrass




0




5




0




1




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0






Ducksalad




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0
















COMPOUND








































Rate 500 g/ha




206




207




208




210




211




212




214




215




216




218




219




220




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237




238









Pre-emergence






Barnyardgrass




0




7




0




0




0




0




0




0




0




0




9




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




2




0




0




0




2




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




239




240




241




242




243




244




245




246




247




248




249




250




251




252




253




254




255




256




257




258




259




264




265




266




267




268




269




270




271









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




272




273




274




276




277




278




279




280




281




282




283




284




286




290




291




293




294




297




298




299




300




301




302




303




304




305




306




307




308









Pre-emergence






Barnyardgrass




0




3




0




8




9




0




0




0




2




9




6




9




4




5




6




5




9




0




0




9




0




0




0




0




4




0




0




0




0






Ducksalad




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




2




0




0




0




0




0




1




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




5




0




0




0




0




4




5




0




0




0




0




0




4




3




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




309




310




311




312




313




314




315




316




317




319




320




321




323




325




326




327




328




329




330




331




332




333




334




335




336




337




338




339




340









Pre-emergence






Barnyardgrass




0




7




0




0




0




0




0




9




0




2




0




0




0




0




9




0




0




0




0




0




0




0




0




4




0




5




9




9




9






Ducksalad




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




5






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




1




0






S. Flatsedge




0




3




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




9
















COMPOUND








































Rate 500 g/ha




341




346




350




351




353




354




358




365




366




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388









Pre-emergence






Barnyardgrass




9




0




0




0




9




0




9




0




0




0




7




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




3




0




0




0




0




0




2




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




2




0




0




0




4




0




8




0




0




0




5




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




9




0




0




0




7




0




8




0




0




0




4




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




389




390




391




393




394




395




401




402




403




405




406




407




408




409




410




411




414




437




438




439




441




443




444




445




446




447




448




449




451









Pre-emergence






Barnyardgrass




0




9




0




0




8




0




0




9




7




0




0




0




0




3




9




9




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




3




3




0




0




3




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice









4




0




0




1




0




0




2




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




7




0




0




8




0




0




2




6




0




0




0




0




2




9




9




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




452




453




454




455




456




457




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




482




485









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




486




487




488




489




490




492




493




494




495




496




498




499




509




521




528




529




531




532




538




539




546




550




552




556




558




560




561




567




568









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




9




0




0




0




0




0




1




6




0




0




0




6






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




2






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0














0




8









0









0









0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




4
















COMPOUND








































Rate 500 g/ha




570




577




580




586




587




588




589




590




591




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609




610




611




612









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




5




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




1




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




2




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0
















COMPOUND








































Rate 500 g/ha




613




615




616




617




618




619




620




621




622




623




624




625




627




628




629




630




631




632




633




634




636




637




638




639




640




641




642




643




645









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




4




0




0




0




2




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




646




647




649




650




651




655




657




658




659




660




661




662




663




664




665




666




667




668




671




674




675




676




677




678




679




680




681




692




694









Pre-emergence






Barnyardgrass




0




0




2




0




0




0




0




0




7




0




0




0




0




0




6




5




0




0




0




0




0




0




0




0




0




0




0




9




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




100




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0






S. Flatsedge




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




100




0

















COMPOUND






























Rate 500 g/ha




695




696




697




699




701




702




705




706




715




720




721




724




740




741




758




765




793









Pre-emergence






Barnyardgrass




0




0




0




8




0




0




2




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




9




3




0




0




0




0




0




0




0




0




0




0




0




8






Rice




0




0




0




4









0




2




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




8




0




0




0




0




0




0




0




0




0




8




0




0




8
















COMPOUND























































Rate 500 g/ha




1




2




3




4




5




6




7




8




9




10




11




12




13




14




15




16




17




18




19




20




21




24




25




26




27




28




29




30




31




32




33




34




35




36




37




38




39




40




41




42




43




44




45




46









Postemergence






B. signalgrass




7




0




0




2




0




5




3




0




0




4




0




0




5




0




0




0




0




2




0




0




0




3




2












































0




0




4




0




0




0




0




0




0




0




0




2




0






Barnyardgrass




0




0




0




4




2




0




0




0




0




0




0




0




0









0




0




9




10




0




0




0




8




8




0




9




10




0




0




0




9




6




0




0




5









0














0




0




0




0




0




0






Bedstraw




0




0




0




7




4




0




0




3




0




0




0




0




0




1




4




0




7




9




8




5




6




8




7












































7




6









0




5




0




2














2




0
















Blackgrass




2




8




0




6




4




7




3




2




2




7




0




0




4




3




3




2




5




3




2




2




0




6




7












































9




7




6




0




8




0




7




4




0




4




0




4




6






Cocklebur




0




0




0




6




5




0




0




1




0




3




0




0




0




0




8




0




3




2




0




0




7




2




5












































4




5




4




1




1




0




0




3




0




1




0




5




2






Corn




0




6




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




3




0




0












































0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




8




0




6




8




6




5




3




0




0




9




0




0




9




8




8




0




9




9









7




2




10




9












































9




7




8




3




9




4




7




7




0




2




0




3




3






Ducksalad




0




0




0




2




0




0




0




0




0




0




0




0




0









0




0




0




7




0




0




0




0




0




0




0




4




0




0




0




2




0




0




0




0









0














0




0




0




0




0




0






Giant foxtail




8




7




7




4




4




5




5




2




0




8




0




0




7




3




0




3




5




3




1




1




2




8




8












































8




7




3




0




8




0




3




1




0




0




0




9




6






Morningglory




0




0




0




3









5




0




2




0




3




0




0




0




6




7




3




7




3




2




8




8









2












































8




8




9




1




10




0




7




6




1




4




1




3




2






Nutsedge




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0

















































0




0




0









0




0




0




0




0




0




0




0




0






Rape




2




0




0




2




4




0




0




0




0




0




0




0




1




0




0




0




0




1




0




0




0




2




0












































0




2




0




0




0




0




0




0




0









0




0




0






Redroot pigweed




8




0




0




7




7




0




0




0




3




0




0




0




0




6




6




0




6




6




5




4




0




6




4












































7




9




7




0




0




0









5




2




6




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




3




5




0




2




0




0




3




0




2




3




0




0




0




0




4




0




0




2









0














0




0




0




0




0




0






S. Flatsedge




0




0




0




2




0




0




0




0




0




0




0




0




0









0




0




0




9




0




6




0




0




2




0




9




10




0




0




0




0




5




0




0




0









0









0




0




0




0




0




0











Soybean




1




1




1




4




5




5




2




5




0




4




0




0




2




2




2




3




5




6




4




4




7




3




3












































0




1




7




1




1




5




4




4




2




3




2




1




2






Sugarbeets




0




0




0




4




4




0




2




0




0




0




0




0




0




2




6




0




3




5




5




3




0




4




0












































0




4




3




2




2




0




2




0




0




3




0




7




4






Velvetleaf




0




0




0




4




5




0




0




0




0




4




0




0




0




5




5




3




2




2




0




0




7




0




0












































2




4









0




0




0




1









0




0




0




1




2






Wheat




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0












































0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




1




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2












































0




0




0




0




0




0




0




2




0




0




0




0




0
















COMPOUND























































Rate 500 g/ha




47




48




49




50




51




52




53




54




55




56




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




84




85




86




87




88




89




90









Postemergence






B. signalgrass




0




0




0









0




1




0




0




0




0




0




0




0




0




1




4




0




0




0




0




0




0









0




0




0




3




2




8




9




2




6




0




0




8




0




0









0




0




2




2




0




0






Barnyardgrass









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




3




0




0
























0




0




0




0




0




7




9




9




0




0




0




0




0




0














0




0






Bedstraw







































7




0




0




0




0




0




7



















0




0




2




8









6




0




0




0




7




8




0




4




0




8




8




6




5




1




0









0




8




8




9




3











Blackgrass




0




0




0









0




0




0




2




0




0




0




0




0




0




7




2




0




0




0




3




0




2




0




0




0




0




2




3




9




8




4




7




3




5




6




3




0









0




3




4




6




0




0






Cocklebur




2




2




0









0




0




4




2




0




0




0




0




0




0




1




6




0




0




0




0




1




2




0




0




0




0




2




4




1




4




4




3




2




1




0




0




1









0




2




2




5




2




5






Corn




0




0




0









0




4




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0









0




0




2




0




1




0






Crabgrass




2




8




9









4




6




10




5




0




0




0




0




4




2




0




7




2




0




0




0




0




0




1




0




0




0




6




7




9




9




0




9




8




9




9




0




0









0




9




9




9




2




4






Ducksalad









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0
























0




0




0




0




0




0




3




2




0




0




0




0




0




0














0




0






Giant foxtail




2




3




9









3




4




3




5




0




0




0




0




4




0




0




2




2




0




0




0




0




0




1




0




0




0




4




2




8




9




2




4




4




7




7




0




0









0




5




6




3




2




1






Morningglory




6




1




3









1




1




6




2




3




1




1




0




1




2




8




6




4




0




2




2




6




3




0




0




0




0




4




4




3




7




0




10




8




10




6




10




0









0




8




9




10




2




4






Nutsedge




0




0




0









0




0




0




0




0




0




0




0




0




0




0




3




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0






Rape




0




0




0









0




0




3




0




0




0




0




0




0




4




3




0




0




0




0




0




2




0




0




0




0




0









2




0




2




3




4




3




3




0




0




0









0




4




3




3




0




0






Redroot pigweed




2




0




0









0




0




10




4




0




0




0




0




0




6




4




0




2




0




0




4




4




0




0




0




0




0




0




0




0




4




0




6




4




4




2




0




0









0




7




2




5




5




7






Rice









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0
























0




0




2




3




0




2




3




2




0




0




0




0




0




0














0




0






S. Flatsedge









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0
























0




0




0




0




3




4




10




3




0




0




0




0




0




0














0




0






Soybean




2




1




1









1




2




3




0




2




2




1




2




7




3




5




3




3




1




1




3




1




3




3




0




0




0




3




1




2




2




1




4




2




2




3




1




0









0




3




5




1




1




4






Sugarbeets




0




0




0









0




0




2




0




0




0




0




0




0




0




6




5




3




0




0




0




2




3




0




0




0




0




0




0




0




3




0




7




6




7




3




2




0









0




6




8




7




6




3






Velvetleaf




0




0




0









0




0




1




0




0




0




0




0




0




0




0




7




5




0




4




2




0




3




2




0




0




0




5




4




0




4




0




4




3




0




2




0




4









0




2




1




0




3











Wheat




3




0




0









0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2




3




4




3




4




0




0




0




0




0




0









0




0




2




0




0




0






Wild oats




3




0




0









0




1




2




0




0




0




0




0




0




0




0




3




2




0




0




0




0




0




0




0




0




0




6




2




2




5




3




2




0




0




0




0




0









0




0




3




0




0




0
















COMPOUND











































Rate 500 g/ha




91




92




93




94




95




96




97




99




101




102




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120




121




122




123




124









Postemergence






B. signalgrass




8




7




9




2




5




0




0




2




0




0




2




0




3




0




8




6




8




3




0




4




8




7




8




9




9




9




5




8




3




0




5




0






Barnyardgrass














0




9




4




0




0




5




0




0














0




0









0




0




0




0




0




0




0




0




4




3














0




6




0




0




0






Bedstraw














7









2




0




3




8




0




3









6




3




7




9




6





























7
























8




2




6




3









0






Blackgrass




8




8




8




6




5




0




5




6




0




0




4




6




8




3




8




8




8




8




7




7




8




8




7




9




9




9




8




8




6




6




7




0






Cocklebur




4




3




4




3




2




2




1




3




0




0




0




3




4




4




3




2




5




3




3




2




4




0




2




5




1




0




0




4




5




3




1




0






Corn




5




4




5




0




0




0




0




0




0




2




2




0




2




0




6




0




5




4




0




0




6




0




0




7




7




3




0




4




0




0




0




0






Crabgrass




9




9




9




9




8




8









8




0




5




9




8




9




6




9




9




9




8




9




9




9




9




6




9




9




9




8




9




9




5




9




0






Ducksalad














0




2




0




0




2




2




0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




0




0




0




0






Giant foxtail




9




9




9




8




6




3




4




7




0




2




7




8




8




3




8




8




9




8




9




8




9




9




9




9




9




9




8




8




8




9




9




0






Morningglory




9




10




10




10




8




2




3




5




1




3




10




10




4




10




3




3




5




5




8




10




10




8




6




7




10




7




8




8




9




4




10




2






Nutsedge




0




2




3




0




0




0




0




0




0




0




0




0




2




0




6




4




4




0




0




0




2




0




0




9




7




0




0









0




0




0




0






Rape




10




6




5




3




0




0




3




6




0




0




3




2




2




0




8




2




6




6




4




4




7




7




0




9




6




0




4




0




3




4




2




0






Redroot pigweed




8




5




7




4




5




0




5




7




0




0




4




7




3




6




8




3




8




6




6




5




7




3




4




8




6




0




6




3




5




5




2




0






Rice














4




0




4




2




3




0




0




0














0




0









0




0




0




0




0




0




0




0




0




0









0




3




0




0




0




0






S. Flatsedge














6




9




5




3




2




2




0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




6




0




0




0






Soybean




5




5




7




5




1




1




2




4




3




0




6




5




6




1




5




5




7




7




5




7




7




7




4




8




7




2




6




6




6




5




4




5






Sugarbeets




6




6




5




3




4




0




0




5




0




0




3




3




0




0




7




2




7




3




4




3




6




5




3




8




7




2




4




0




4




2




2




0






Velvetleaf














6




6




0




0




3




5




0




3




4




3




4




2




7




5




6




2




2




1




8




3




0




8




8




0




3




6




4




3









0






Wheat




6




6




5




0




0




0




0




0




0




0




0




0




2




0




8




2




6




1




0




0




6




0




0




8




8




2




3




4




0




0




4




0






Wild oats




5




5




5




1




3




0




0




0




0




0




0




2




4




0




9




3




7




2




2




1




6




2




0




8




8




2




6




2




0




0




2




0
















COMPOUND








































Rate 500 g/ha




125




126




127




128




129




130




131




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149




150




151




152




153









Postemergence






B. signalgrass




0




0




0




0




6




8




9




7




2




2




0




3




8




8




7




1




0




0




5




3




2




9




8




7




0




0




7




0




0






Barnyardgrass




0




0




0




0


































0




0



















8




3




9




10




8




9




9




9




4




0




0




8




0




0






Bedstraw




0




0




0




0




3




8




9




7




7
























9




5




6




4




4




8




5




5




8




8




6




0




0




7




0




0






Blackgrass




0




0




0




0




3




8




9




9




4




7




0




5




8




9




8




6




0




3




8




8




6




8




8




7




0




0




9




2




0






Cocklebur




0




0




0




0




0




3




5




0




3




1




0




4




4




3




2




4




0




0




4




0




0




4




0




3




0




0




2




0




0






Corn




0




0




0




0




4




3




7




6




0




0




0




0




5




7




2




0




0




0




0




0




0




0




8




0




0




0




6




0




0






Crabgrass




0




0




0




0




9




9




9




9




4




9









9




9




9




9




9




9




5




9




9




8




9




9




9




0




5




9




3




0






Ducksalad




0




0




0




0


































0




0



















0




0




0




5




0




2




6




3




0




0




0




2




0




0






Giant foxtail




0




0




0




0




9




9




9




9




4




3




0




7




9




9




9




6




2




3




7




6




4




9




9




9




0




4




8




3




0






Morningglory




2




0




0




0




8




3




10




7




8




8




1




10




8




10




9




8




3




7




8




3




10




9




3




5




0




0




6




0




0






Nutsedge




0




0




0




0




0




0




2




4




0




0




0




0




4









4




0




0




0




0




0




0




6




2




0




0




0




5




0




0






Rape




0




0




0




0




0




2




9




0




0




0




0




4




7




7




4




2




0




0




3




4




3




5




5




4




0




0




2




0




0






Redroot pigweed




0




0




0




0




3




6




10




2




2




0




0




6




6




8




4




3




9




0




6




2




2




8




5




5




0




0




7




0




0






Rice




0




0




0




0


































0




0



















4




0




4




4




4




0




7




5




0




0




0




0




0




0






S. Flatsedge




0




0




0




0


































0




0



















0




0




4




8




7




8




9




9




2




0




0




8




0




0






Soybean




4




0




0




0




4




5




8




6




3




1




3




5




8




4




5




5




3




3




5




3




5




8




8




5




0




3




4




1




0






Sugarbeets




0




0




0




0




0




4




8




2




2




2




0




8




6




8




2




0




0




0




6




4




0




6




2




4




0




0




3




0




0






Velvetleaf




0




0




0




0




0




5




8




3




5




4




0




2




5




7




6




2




4




2




2




0




2




6




3




1




0




0




5




0




0






Wheat




0




0




0




0




2




8




6




6




2




0




0




0




6




8




4




0




0




0




0




0




0




6




7




5




0




0




8




0




0






Wild oats




0




0




0




0




2




8




10




3




0




0




0




3




5




8




4




1




0




0




0




1




2




7




7




5




0




0




8




0




0
















COMPOUND








































Rate 500 g/ha




154




157




158




159




160




161




162




163




164




165




166




167




168




169




170




171




172




173




174




175




176




177




178




179




180




181




182




183




184









Postemergence






B. signalgrass




2




0




0




0




0




7




4




6




0




8




0




0




0




7




10




0




0




0




0




0




0




0




2




0




0




0




0




0




0






Barnyardgrass




0




0




0




0




0



















0
























0




0




0
























0




0


































0






Bedstraw



















0




0




4




6




9









8




5



















2
























0




8




6




0




10




0




0




0




3




6






Blackgrass




0




2




5




0




0




4




6




8




0




8




8




5




7




9




9




0




5




2




3




0




3




2









6




0




0




0




0




4






Cocklebur




2




0




0




0




0




3




2




3




0




0




0




2




2




3




0




3




2




2




3




3




3




3




0




1




0




0




0




0




1






Corn




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




5




7




4




0




0




9




8




9




9




9




4




9




9




9




9




7




9




8




8




0




6




3




2




9




0




0




0




0




2






Ducksalad




0




0




0




0




0



















0
























0




0




0
























0




2









































Giant foxtail




3




4




5




0




0




7




3




8




7




8




4




0




3




9




8




0




0




0




1




0




6




0




2




4




0




0




0




0




2






Morningglory




2




1




2




4




0




10




10




8




2




4




2




8




10




7




2




2




8




10




5




4




3




4




3




5




0




0




0




2




7






Nutsedge




0




0




0




0




0




0




2




3




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




4




0




4




0




2









0




0




3




3




0




0




0




2




0




0




0




0




2




0




0




0




0




6






Redroot pigweed




6




0




4




0




0




5




0




3




0




4




3




7




0




3




6




5




7




0




6




0




0




3




7




8




0




0




0




0




7






Rice




0




0




0




0




0



















0
























0




0




0
























0




0









































S. Flatsedge




0




0




0




0




0



















0
























0




0




0
























0




0









































Soybean




3




2




5




3




0




4




4




3




2




6




3




5




2




6




7




3




5




4




4




1




4




4




2




1




0




0




0




2




3






Sugarbeets




0




0




0




0




0




7




0




5




0




6




0




0




0




0




4




2




0




5




6




0




0




0




0




6




0




0




0




0




6






Velvetleaf




0




0




0




0




0




6




4




6




0




1




0




2




1




0




5




3




2




0




0




3




2




3




0




3




0




0




0




0




5






Wheat




0




0




0




0




0




0




0




5




0




3




3




0




0




2




7




0




0




0




0




3




2




4




2




0




0




0




0




0




3






Wild oats




1




0




0




0




0




0




4




3




0




3




2




0




0




2




6




0




0




0




0




0




0




0




0




2




0




0




0




0




2
















COMPOUND








































Rate 500 g/ha




185




187




188




189




190




191




192




193




194




195




196




197




198




199




201




202




203




204




205




206




207




208




210




211




212




214




215




216




218









Postemergence






B. signalgrass




0




0




0




0




0




1




2




0




3




1




0




0




0









0




0




0




0




0




0




0




3




0




0




7




0




3




8




7






Barnyardgrass





































































8

















































































Bedstraw




3




0




5




0




0




0




0




0




0




7




0














2




0




4




0




7




0




0




5




5









8




7




8




8









8






Blackgrass




0




0




3




0




0




3









0




3




6




0




0




0




9




4




6




0




7




0




0




4




7




2




4




7




5




5




8




8






Cocklebur




2




0




0




0




0




3




5




0




2




2




0




0




0




3




0




2




0




1




2




0




3




0




2




0




5




0




0




3




4






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0






Crabgrass




1




0




3




0




0




6




2




0




2




5




0




2




0




8




0




4




0




5




1




0




3




3




0




3




9




5




2




7




9






Ducksalad





































































2

















































































Giant foxtail




1




0




4




0




0




2




1




0




2




3




0




3




0




7




0




2




0




3




0




0




2




1




0




3




9




4




5




6




8






Morningglory




2




0




0




0




0




8




6




2




2




3




0




0




3




8




3




9




0




8




2




5




3




3




7




6




8




7




3




10




9






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




2




0




2




0




0




0




0




0




0




4




0




0




0




0




2




0




0




3




3




3




0




3




7






Redroot pigweed




4




0




3




0




0




0




7




0




0




4




0




0




0




6




3




7




0




7




0




0




0




0




6




5




7




3




6




3




7






Rice





































































0

















































































S. Flatsedge





































































7

















































































Soybean




3




0




3




0




0




4




3




2




1




5




0




0




1




7




3




3




0




7




2




2




5




2




3




4




4




3




1




2




7






Sugarbeets




0




0




7




0




0




0




5




0




0




2




0




0




0




2




4




4




0




0




0




0




2




0




4




2




5




0




0




2




4






Velvetleaf




3




0




0




0




0




2




4




0




0




2




0




0




0




5




3




0




0




2




0




0




2




1




2




3




7




0




0




0




3






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




7




6




8




2




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




2




3




0




2
















COMPOUND








































Rate 500 g/ha




219




220




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237




238




239




240




241




242




243




245




246




247




248




249









Postemergence






B. signalgrass




8




8




1




0




0




9




9




0




0




0




0




0




8




1




0




0




0




0




0




0




0




6




9




9




8




1




0




0




0






Barnyardgrass























































































































































Bedstraw




8




9




5




5




4




0




7




8




2




0




0




0




2




5




0




0




4




3




8




3




5




7




8




5




9




9




0




0




0






Blackgrass




8




8




4




1




4




8




9




7




0




0




0




0




7




5




0




0




0




0




5




3




5




9




9




9




8




8




0




0




0






Cocklebur




4




5




0




2




1




0




2




3




0




0




0




0




4




2




3




0




0




0




0




1




1




1




7




0




1




2




0




0




0






Corn




5




6




0




0




0




6




6




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




6




7




7




0




0




0




0






Crabgrass




8




9




2




3




0




8




8




3




0




0




2




2




2




6




0




0




0




0




5




6




4




9




9




9




8




3




0




0




0






Ducksalad























































































































































Giant foxtail




9




8




1




1




0




9




7




0




0




0




1




0




3




6




0




0




0




0




2




6




2




8




9




8




8




8




0




0




0






Morningglory




7




8




3




6




6




6




7




10




9




0




7




4




8




8




2




7




6




6




5




9




10




8




8




8




9




9




2




0




3






Nutsedge




0




0









0




0




2




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




5




7




0




3




0




0




0






Rape




7




4




0




0




0




2




6




0




0




0




0




0




2




3




0




0




0




0




6




0




0




4




8




3




5




0




0




0




0






Redroot pigweed




8




4




0




5




7




2




0




7




2




0




0




0




4




4




0




0




0




3




5




7




7




7




8




7




9




3




0




0




3






Rice























































































































































S. Flatsedge























































































































































Soybean




7




7




2




4




2




4




6




5




1




2




5




1




4




5




1




0




3




1




2




3




3




4




6




8




5




4




0




1




4






Sugarbeets




7




2




0




3




4




2




2




5




4




0




0




0




3




4




0




0




0




0




0




0




3




5




8




5




7




0




0




0




2






Velvetleaf




4




2




3




3




4




3




0




3




0




2




0




0




3




3




0




0




3




2




2




3




3




1




7




7




7




3




0




0




0






Wheat




7




6




0




0




0




8




9




5




0




0




0




0




0




0




0




0




0




0




0




0




2




8




8




8




8




4




0




0




0






Wild oats




6




2




0




2




0




2




3




2




0




0




0




0




0




2




0




0




0




0




0




0




2




2




8




4




8




0




0




0




0
















COMPOUND








































Rate 500 g/ha




251




253




254




255




257




258




259




260




261




262




263




265




266




267




268




269




270




271




272




273




274




276




277




278




279




280




281




282




283









Postemergence






B. signalgrass




2




0




0




8




0




8




0




0




0




0




0




0




2




3









0




0




5




0




0




0




0




3




0




0




0




0




2




2






Barnyardgrass























































































































































Bedstraw




9




0




4




8




0




8





























8




6




7









7




0




8




4




0




0




3




8




8




0




0









8




6






Blackgrass




8




0




0




9




2




7




0




0




5




0




5




7




8




8









5




0




8




6




4




0




8




8




0




4




0




2




8




7






Cocklebur




3




0




0




2




0




1




3




0




1




0




0




0




2




3




0




2




0




4




1




0




0




0




2




3




0




0




0




2




2






Corn




0




0




0




6




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




9




0




0




3




4




5




0




0




0




0




2




3




5




7




0




1




0




5




0




3




0




7




6




0




0




0




0




0




1






Ducksalad























































































































































Giant foxtail




8




0




0




8




2




7




0




0




0




0




3




2




7




7




0




2




0




7




0




2




0




6




6




0




1




0




0




2




7






Morningglory




9




0




9




8




8




10




8




4




6




7




7




8




8




8




7




7




0




8




7




3




0




8




9




4




2




0




5




9




10






Nutsedge




0




0




0




6




0




0




0




0




0




0




0




0




3




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




2




3




5




3









0




0




0




0




3




7




2









0




0




6




0




0




0




0




3




0




0




0




0




8




7






Redroot pigweed




4




0




6




8




6




3




7




6




2




4




0




4




7




6









6




0




8




4




4




1




2




5




4




2




1




6




8




7






Rice























































































































































S. Flatsedge























































































































































Soybean




6




0




2




6




4




6




6




1




4




4




1




4




8




6









3




2




6




1




4




5




7




8




1




4




5




3




4




7






Sugarbeets




2




0




7




3




5




2




3




3




0




0




0




3




7




4









0




0




6




0




0




1




2




5




0




0




0




4




7




2






Velvetleaf




0




0




2




1




1




0




1




1




1




2




2




3




5




3




0




3




0




3




0




2




0




0




1




2




0




0




1




3




3






Wheat




2




0




0




8




0




6




3




0




2




0




2




0




6




4









4




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




4




0




3




0




0




0




0




0




0




2




4









3




0




3




0




0




0




0




2




0




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




284




286




292




293




294




297




298




299




300




301




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




319




320




321









Postemergence






B. signalgrass




1




2




0




7




0




0




0




8




0




0




0




0




0




0




0




0




0




0




7




0




0




0




3




4




2




8




0




0




0






Barnyardgrass























































































































































Bedstraw




9




6




0




9




9



















0









0




0














0




0




0




0




5




2



















































Blackgrass




8




8




0




9




8




0




0




9




0




0




2




0




4




0




0




0




0




2




9




0




0




0




5




8




7




9




3




0




4






Cocklebur




2




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




7




0




0




0




1




0




0




1




0




0




0






Corn




0




0




0




3




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




3




0




0




0






Crabgrass




1




6




0




9




2




0




0




5




0




0




0




0




3




0




0




0




0




0




9




0




0




0




4




5




0




8




3




4




8






Ducksalad























































































































































Giant foxtail




8




3




0




9




4




0




0




8




0




0




4




0




2




0




0




0




0




0




8




0




0




0




7




7




3




8




0




3




8






Morningglory




8




8




2




7




9




0




3




9




0




0




2




0




6




2




5




3




2




2




8




10




0




7




6




3




8




6




4




3




9






Nutsedge




0




0




0




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




3




0




0









0




0




0






Rape




8




6




0




0




4




0




0




8




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




2




2




0




3




0






Redroot pigweed




8




7




0




6




4




0




0




8




0




0




2




3




6




6




0




0




0




0




7




0




0




2




2




0




5




6




0




7











Rice























































































































































S. Flatsedge























































































































































Soybean




5




2




1




5




6




3




4




7




2




0




5




3




5




5




2




3




2




3




6




3




3




4




4




4




4




7




4




4




3






Sugarbeets




6




2




0




3




0




0




0




7




0




0




2




0




2




0




0




0




0




0




3




0




0




0




0




0




0




4




0




6




6






Velvetleaf




2




1




0




6




0




0




0




7




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




0




3




4




3




0




0






Wheat




0




5




0




7




2




0




0




7




0




0




0




0




0




0




0




0




0




0




8




0




0




0




3




4




4




6




0




0




0






Wild oats




0




3




0




8




3




0




0




4




0




0




0




0




0




0




0




0




0




0




7




0




0




0




3




0




4




0




0




0




0
















COMPOUND








































Rate 500 g/ha




322




323




325




326




327




328




329




330




331




332




333




334




335




336




337




338




339




340




341




342




343




344




345




348




349




350




351




352




353









Postemergence






B. signalgrass




3




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




1




7




0




0




7




0




4




4




7




0






Barnyardgrass



































































































9




2




0




0




7




9




5




5




3











Bedstraw




4







































0









0




0




4




0




4




5




8




8




8




5




3




0




0




7




3














4











Blackgrass




8




0




7




1




7




5




0




0




0




0




0




0




0




0




0




0




2




8




2




4




6




0




0




7




6




7




4




8




9






Cocklebur




4




0




3




2




0




0




4




0




0




0




0




0




0




0









0




0




0









0




4




0




0




2




1




3




2




0




1






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




3




0




0




0




6




0






Crabgrass




5




0




0




3




1




2




0




0




0




3




0




0




0




0




0




0




2




2




2




3




6




0




0




6




3




7




9




4




3






Ducksalad



































































































4




0




0




0




4




4




3




4




2











Giant foxtail




4




0




0




2




0




1




0




0




0




0




0




0




0




0




0




0




0




6




2




7




9




0




0




9




9




9




9




9




8






Morningglory




8




3




8




10




10




10




0




4




0




0




0




0




0




0




0




2




10




10




10




9




9




0




0




10




10




9




6




8




10






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




6




0




0




0




2




0






Rape




0




0




2




3




2




0




0




0




0




0




0




0




0




0




0




0




5




6




2




4




3




0




0




5




0




2




5




0




4






Redroot pigweed




6




0




7




7




7




5




0




0




0




4




0




0




0




0




0




0




6









6




8




5




2




0




5




4




3




7




4




6






Rice



































































































0




0




0




0




0




0




0




0




3











S. Flatsedge








































































































0




0




0




7









8




8




7











Soybean




5




2




3




6




7




6




2




1




0




3




4




2




2




2




2




2




4




3




3




7




3




2




0




4




2




3




2




4




6






Sugarbeets




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




3




0




0




3




0




0




2




0




6






Velvetleaf




2




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




3




2




0




5




0




0




6




0




6




6




3




2






Wheat




3




0




5




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




4




3




2




2




7




0






Wild oats




2




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




4




0




0




7




3




5




5




7




2
















COMPOUND








































Rate 500 g/ha




354




355




356




357




358




359




360




361




363




364




365




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385









Postemergence






B. signalgrass




2




2




1




7




2




0




7




4




5




1




0




4




7




3




6




6




7




0




0




8




0




2




0




0




0




0




0




7




8






Barnyardgrass




9




8




7




6









0




7














0



















2




2









6


































































Bedstraw









0




3




5




6




0




4




8




9




0
































































0









0




4




0




0




3






Blackgrass




9




6




7




7




8




2




7




8




8




2




0




8




8




5




5




8




10




0









8




0









0




0




0




2




8









8






Cocklebur




1




4




0




2




0




1




0




2




2




2




0




2




5




0




3




0




3




2




0




0




0




1




0




6




0




0




0




0




0






Corn




0




0




3




3




0




0




7




0




6




3




0




0




7




0




5




1




3




0




0




2




0




0




0




0




0




0




0




0




0






Crabgrass




3




2




3




5




7




0




5




5




9




2




0




8




8




9




9




9




9




2




3




9




0




2




0




7




0




1




4




8




9






Ducksalad




5




0




2




2









0




0














0



















2




3









6


































































Giant foxtail




9




8




8




9




8




0




8




5




9




8




0




8




9




9




9




9




9




6




8




9




0




8




7




9




0




4




6




9




9






Morningglory




8




8




10




8




7




0




5









3




4




0




7




7




10




10




10




10




8




10




6




0




10




10




10




7




0




0




0




5






Nutsedge




0




0




0




2




0




0




4




0




0




0




0




3




0




3




5




0




0




0




0




6




0




0




0




0




0




0




0




0




0






Rape




4




0




0




4




4




0




0




4




2




0




0




4




5




3




3




0




5




5




7




2




0




3




0




0




6




0




0









0






Redroot pigweed




7




3




0




8




6




0




6




7




5




0




0




7




7




4




3




5




9




6




6




3




0




2




1




5




2




0




0




0




0






Rice




2




0




0




2




0




0




3














0



















0




2









2


































































S. Flatsedge




9




8




7




8









0




8














3



















4




7









8


































































Soybean




7




3




5




3




7




3




3




5




7




3




2




2




5




1




4




4




3




4




4




2




0




2




2




1




2




5




5




3




2






Sugarbeets




3




0




0




0




4




0




7




6




3




1




0




7




3




2




0




0




8




4




4




3




0




0




0




0




0




0




0




0




0






Velvetleaf




2




2




0




4




3




2




4




3




6




0




0




3




7




3




4




3




2




2




1




4




0




3




0




3




0




0




0




0




0






Wheat




0




3




4




7




5




2




6




2




6




0




0




6




6




4




3









2




0




0




6




0




0




0




0




0




0




0




3




5






Wild oats




3




5




3




6




7




0




5




6




7




0




0




8




5




4




5




4




8




0









8




0




0




0




0




0




0




0




4




3
















COMPOUND








































Rate 500 g/ha




387




388




389




390




391




393




394




395




396




397




398




400




401




402




403




404




405




406




407




408




409




410




411




414




415




416




417




418




419









Postemergence






B. signalgrass




8




8




0




8




0




0




9




0




0




8




8




4




0




5




6




6




0




0




0




5




9




7




9




6




6




9




0




2




2






Barnyardgrass












































0




0




0




0
































































0




0




8




0




0






Bedstraw









6




7




7




0














4














9














8




8
























9




5




7




8














7




6









0






Blackgrass




9




10




6




9




0




8









5




6




9




9




8




0




9




10




10




5




0




7




10




10




9




9




7




9




9




0




6




4






Cocklebur




0




0




0




7




0




0




4




0




0




0




0




0




1




5




0




3




0




0




0




3




1




1




3




0




4




5




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




7




3




4




0




2




7




0




0




0






Crabgrass




7




9




7




9




0




8




9




5




2




9




9




9




3




9




9




8




0




0




3




9




9




10




8




9




9




9




2




6




1






Ducksalad












































0




0




0




0
































































0




0




3




2




0






Giant foxtail




9




9




8




10




0




9




9




6




2




9




9




9




6




9




9




9




6




0




8




9




9




9




9




9




9




9




8




9




6






Morningglory




6




5




10




9




0




0




7









8




6




8




6




7




10




10




10




5




2




10




7




10




8




6




8




7




9




9




10




5






Nutsedge




5




6




0









0




0









0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0






Rape




0




0




4




10




0



















6




2




2




0




7




9




7




8




2




0









2









7




8




0




1




3




2




0




0






Redroot pigweed




0




3




7




9




0




0




7




0




0




6




5




0




2




7




2




7




0




0




0




7




5




2




9




0




3




7




3




0




0






Rice












































0




0




0




0
































































0




0




0




0




2






S. Flatsedge












































0




0




0




0
































































3




0




9




4




3






Soybean




1




1




3




5




0




2




5




1




6




6




6




4




1




8




8




7




3




2




2




4




5




6




7




3




7




7




6




6




3






Sugarbeets




2




4




0




7




0




7




5




0




3




0




0




0




0




2




3




4




0




0




0




6




0




8




7




0




0




2




6




0




0






Velvetleaf




3




6




0




8




0




0




3




2




0




0




5




0




3




4




6




6




0




0




2




4




0




0




6




0




2




6




0




0




2






Wheat




0




8




0




7




0




0




4




3




0




4




3




0




0




0




4




3




0




0




0




2




7




4




8




0




3




7




0




0




0






Wild oats




0




6




0




9




0




0




6




3




0




5




0




0




0




3




5




8




0




0




0




3




4




5




9




2




3




7




0




3




0
















COMPOUND








































Rate 500 g/ha




420




421




422




423




424




425




426




427




428




429




430




431




432




433




434




435




436




437




438




439




440




441




443




444




445




446




447




448




449









Postemergence






B. signalgrass




7




10




0




0




0




8




8




0




0




0




8




2




0




6




0




3




8




0




0




0




8




0




0




4




0




8




0




0




4






Barnyardgrass




0




3




0




0




0




7




0




0




5




7




0




0




0




0




0




0




0



















0














































Bedstraw




5




7














0









9



















3














7









0







































































Blackgrass




6




10




0




2




0




9




8




4




4




3




8




5




4




10




0




8




9




0




2




0




8




0




0




7




0




9




2




0











Cocklebur




0




6




0




0




0




0




0




2




1




0




1




0




0




0




0




0




0




1




3




0




0




0




0




0




2




0




0




0




3






Corn




0




7




0




0




0




2




4




0




0




0




4




0




0




3




0




0




5




0




3




0




0




0




0




0




0




5




0




0




0






Crabgrass




8




8




0




1




0




9




9




2




3




3




9




2




6




9




4




8




9




3




9




0




9




0




0




9




7




9




0




0




2






Ducksalad




0




2




0




0




0




0




0




0




5




6




0




0




0




0




0




0




0



















0














































Giant foxtail




9




9




0




2




0




9




9




4




0




4




9




6




8




8




4




9




9




7




9




0




9




0




0




9




2




9




0




0




3






Morningglory




10




10




0




8




1




10




9




1




3




3




3




2




2




7




1




9




10




9




10




0









0




4




3




8




3




7




5




5






Nutsedge




0




2




0




0




0




0




3




0




0




0




6




0




0




0




0




3




3




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




8




0




0




0




3




4




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




2




0




0




0




3






Redroot pigweed




0




8




0




0




0




2




6




0




3




0




3




0




0




3




0




2




7




0




0




0




4




0




0




2




4




0




0




0




4






Rice




0




2




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0



















0














































S. Flatsedge




0




0




0




0




0




6




0




0




9




9




0




0




0




0




0




0




0



















0














































Soybean




4




8




4




2




2




3




7




2




3




3




3




2




2




2




1




3




4




2




6




0




7




0




2




2




2




4




4




5




2






Sugarbeets




0




6




0




0




0




4




3




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




3




0




0




0




0




3






Velvetleaf




0




7




0




0




0




2




2




2




7




2




3




2




2




4




0




0




3




0




0




0




2




0




0




3




5




3




0




0




0






Wheat




5




7




0




0




0




6




2




0




0




0




0




0




0




3




0




0




7




0




0




0




4




0




0




0




0




3




0




0




3






Wild oats




2




8




0




0




0




3




2




0




0




0




0




0




3




2




0




3




3




3




0




0




5




0




0




2




0




3




0




0




4
















COMPOUND








































Rate 500 g/ha




451




452




453




454




455




456




457




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




482









Postemergence






B. signalgrass




2




0




5




2




5




2




0




3




0




2




0




0




0




0




7




0




0




6




0




6




5




0




4




0




5




8




7




6




0






Barnyardgrass























































































































































Bedstraw












































8




8







































6
























8
























0











Blackgrass




6




5




6




2




9




8




0




8




8




8




3




0




2




8




9




7




8




9




0




7




8




0




8




2




6




8




7




8




0






Cocklebur




0




0




0




0




0




2




0




2




0




0




3




0




2




0




1




5




4




3




0




0




1




0




4




0




0




0




0




1




0






Corn




0




0




0




0




0




0




0




2




0




0




0




0




0




2




2




0




0




4




0




0




3




0




0




0




0




2




4




2




0






Crabgrass




6




6




10




9




9




7




0




9




8




9




2




0




2




8




9




6




9




9




0




9




8




8




9




0




7




9




9




8




3






Ducksalad























































































































































Giant foxtail




7




7




9




9




9




8




0




9




5




1




0




0




6




9




9




4




9




9




0




8




8




7




8




0




7




9




8




8




2






Morningglory




3




3




2




10




9




5




0




6




10




8




8




0




2




3




2









5




10




1




5




7




2




2




2




10




8




10




8




8






Nutsedge




0




0




0




0




0




0




0




4




0




0




0









0




0




0




0




2




2




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




2




0




0




2




4




0




0




0




0




0




0




6




0




2




0




3




0




0




2




0




1




0




0




0




0






Redroot pigweed




3




0




3




6




8




5




0




0




3




2




0




0




0




3




7




6




7




6




0




5




4




0




6




4




2




6




3




2




3






Rice























































































































































S. Flatsedge























































































































































Soybean




1




2




2




3




4




2




2




4




7




4




4




2




1




1




5




2




3




5




1




3




2




1




4




2




2




3




3




4




1






Sugarbeets




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




7




0




4




0




0




3




0




0




0




0




0




0




0




0






Velvetleaf




0




2




2




3




3




3




0




0




0




0




0




0




0




4




1




5




5




2




0




4




2




0




2




2




0




0




1




0




0






Wheat




0




0




0




0




0




0




0




2




0




0




0




0




0




4




6




0




0




6




0




3




3




0




0




0




0




7




0









0






Wild oats




4




0




0




4




7




0




0




2




0




0




0




0




0




5




0




2




0




5




0




0




3




0









0




0




0




0




3




0
















COMPOUND








































Rate 500 g/ha




485




486




487




488




489




490




492




493




494




495




496




497




498




499




500




501




504




505




506




508




509




510




511




512




513




514




515




516




517









Postemergence






B. signalgrass




5




5




0




7




8




7




0




0




0




0




4




0




0




0




8




7




9




8




0




3




7




6




3




5




8




5




3




5




8






Barnyardgrass























































































































































Bedstraw




6




8




6




9



























































9




9









9
























































Blackgrass




8




8




1




8




8




5




0




0




0




0




5




0




5




4




6




7




8




7




6




6




9




6




2




6




8




5




1




7




6






Cocklebur




0




0




0




0




0




0




0




0




0




0




1




0




0




4




5




5




6




4




6




4




4




4




0




7




7




5




5




5




4






Corn




0




3




0




0




4




0




0




0




0




0




0




0




0




0




6




6




6




6




0




3




1




0




0




0




3




5




0




0




4






Crabgrass




8




9




5




9




9




7




0




4









0




2




0




2




0




9




8




10




9




8




9




9




9




9




9




9




10




9




9




9






Ducksalad























































































































































Giant foxtail




8




9




8




9




9




8




0




0




0




0




0




0




3




2




9




8




9




9




8




8




8




9




9




8




8




9




9




9




9






Morningglory




10




2




10




8




10




3




8




0




0




7




8




0




4




6




3




4




6




7




5




7




5




6




5




7




9




7




6




7




2






Nutsedge




0




0




0




2




0




0




0




0




0




0




0




0




0




0




2




2




3




2




0




0









0




0









5




0




0
















Rape




0




1




3




0




0




0




0




0




0




0




0




0




0




0




8




7




8




2




7




8




4




9




4




0




7




8




6




9




4






Redroot pigweed




2




2




3




2




2




2




7




0




0




0




3




0




0




0




10




5




9




9




0




9




5









7




9




7




8




5




8




7






Rice























































































































































S. Flatsedge























































































































































Soybean




5




4




5




5




7




6




0




2




1




0




3




2




1




3




4




5




7




5




4




5




5




8




4




7




8




7




7




7




8






Sugarbeets




0




2




0




1




0




0




0




0




0




0




0




0




0




0




9




8




9




9




7




9




7




8




2




7




7




5




3




8




3






Velvetleaf




4




6




2




1




5




1




0




0




0




0




0




0




2




0




5




3




7




4




4




2




7




7




2




1




7




5




8




4




6






Wheat




5




5




0




3




2




0




0




0




0




0




3




0




0




0




5




3




6




4




4




0




2




3




0




2




6




0




0




7




4






Wild oats




4




3




0




5




3




7




0




0




0




0




2




0




0




0




7




3




7




3




2




4




8




5




0




1




6




3




0




5




3
















COMPOUND








































Rate 500 g/ha




519




520




521




522




523




524




525




526




527




528




531




532




533




534




535




536




540




541




543




544




545




546




549




550




551




552




553




554




555









Postemergence






B. signalgrass




0




2




3




7




7




9




8




6




9




0




4




0




4




6




3




0




3




2




3




3




2




0




3




2




4




0




5




3




4






Barnyardgrass























































































































































Bedstraw




0














10



















9









8




3




0
























9




5




2




3




7




9




8




0




9




10




7




9











Blackgrass




0




6




9




8




4




8




8




7




7




5




6




0




7




7




8




0




7




0




2




3




0




6




3




2




7




7




7









5






Cocklebur




0




0




0




3




2




3




2




2




2




3




5




4




4




0




0




0




0




5




1




3









0




4




2




0




4




2




3




3






Corn




0




0




0




5




2




5




2




2




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Crabgrass




6




9




10




9




10




9




9




10




10




10




10




9




9




8




6




3




8




3




7




9




9




10




9









9




9




9




9




10






Ducksalad























































































































































Giant foxtail




6




9




9




9




6




9




9




8




9




9




9




8




9




8




5




0




3




2




3









5




7




7




9




5




7




7




8




8






Morningglory




0




10




5




5




4




2




3




7




6




5









5




7




3




3




2




6




3




7




10









10




4




8




3




7




0




7




6






Nutsedge




0




0




0




0




0




0




5




2









6




3









0




2




0




0




0




0




0




0














0




2




0




0









0




0






Rape




0




9




3




9




2




3




8




4




2




3




2




2




4




7




0




0









3




0




3




3




7




7




3




5




7









3




5






Redroot pigweed




0




0




4




9




3




0




8




4




0




0




0




2




9




7




0




8




2




3




0




2




0




3




8




0




7




3




0









2






Rice























































































































































S. Flatsedge























































































































































Soybean




4




4




5




6




5




4









3




5




5




6




5




4




7




8




6




1




2




2




2




2




4




3




3




3




3









3




2






Sugarbeets




0




2




4




6




0




0




8




0




2




2




6




0




4




2




0




0




6




4




3




3




3




5




4




5




8




7




2









0






Velvetleaf




4




6




3




7




4




6




3




8




3




5




3




2




8




2




2




0




1




0




3




0









2




4




2




3




3









0




4






Wheat




0




0




2




5




2




5




5




0




0




0




0




0




2




5




2




0




0




0




0




0




0




0




2




0




3




3




3









2






Wild oats




0




0




2




7




2




5




6




0




0




0




0




0




0




3




2




0




2




2




3




2




0




2




2




3




5




3




2









2
















COMPOUND








































Rate 500 g/ha




556




557




558




559




560




561




562




563




564




565




566




567




568




569




570




571




572




573




574




575




576




577




578




579




580




581




582




584




585









Postemergence






B. signalgrass




7




2




3




9




7




8




7




7




8




0




9




0




7




4




0




5




0




0




0




3




2




3




0




2




8




8




3




9




7






Barnyardgrass























































































































































Bedstraw




0














4









7









0




0




0









0












































9



















9




9





















Blackgrass




6




0




2




7




7




6




3




4




4




0




6




0




9




3




0




0




0




0









3




7




0




2




5




7




4




7




7




7






Cocklebur




0




0




0




2




0




0




2




2




2




2




3




2




6




2




0




0




0




3




2




2




0




2




0




0




6




3




4




4




7






Corn




0




2




0




7




4




3




7




8




6




0




2




0




5




2




0




0




0




0




0




0




4




2




0




0




0




6




0




4




5






Crabgrass




2




4




8




9




8




9




10




9




9




3




9




8




9




6




0




3




8




9




2




9




9




3




9




8









9




3




9




9






Ducksalad























































































































































Giant foxtail




9




6




8




9




8




8




8




9




9




3




9




0




9




4




0




3




0




9




8









8




8




8




7




8




9




7




9




9






Morningglory




10




8




10




10




10




9




10




10




10




9




10




10




10




10




10




10




10




10




10




10




4




10




10




10




10




10




10




3




10






Nutsedge




0




0




0




2




5




4




5









0




0




0




0




0




0




0




0














0














0




0



















0




3




0






Rape




2




0




2




2




7




4




7




5




2




0




9




0




3




0




0




0




4




2




3




3




0




0




4




3




8




7




3




9




5






Redroot pigweed




4




0




0




8




9




7




9




5




3




6




5




0




2




4




0




0




0




7




5




7




4




0




3




3




9




9




7




7




7






Rice























































































































































S. Flatsedge























































































































































Soybean




8




2




4




6




3




5




5




5




5




3




6




6




6




4




3




4




7




6




7




6




4




5




4




4




4




5




3




4




3






Sugarbeets




0




0




2




8




6




4




5




0




2




0




5




0




2




0




0




0




0









0




2




0









4




0




6




8




7




8




7






Velvetleaf




2




2




2




3




0




0




6




4




3




4




5




2




8




3




0




0




7




2




2




3




0




0




3




0




3




6




0




5




5






Wheat




3




0




0




3




6




7




5




0




2




0




4




0




5




0




0




0




0




0




2




2




0




0




0




0




3




4




0




6




4






Wild oats




2




0




0




5




2




2




4




0




2




0




4




0




6




0




0




0




0




0




0




0




0




0




0




0




7




5




3




7




2
















COMPOUND








































Rate 500 g/ha




586




587




588




589




590




591




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609




610




611




612




613




615




616









Postemergence






B. signalgrass




7




0




8




3




0




0




0




0




3




6




0




0




0




0




7




7




0




0




0




0




7




10




8




9




8




9




8




0




4






Barnyardgrass























































































































































Bedstraw









3



























































0




8
























0



















9




9




9




9
















Blackgrass




8




6




8




3




0




0




0




0




5




9




0




0




0




0




8




9




0




0




0




1




7




9




8




10




9




10




9




0




5






Cocklebur




0




0




0




0




0




0




0




0




4




2




0




0




0




0




1




0




0




0




0




0




0




0




3




2




3




2




2




0




0






Corn




3




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




2




0




7




5




6




0




0




0




0






Crabgrass




9




2









3




2




0




2









9




9




2




0




0




3




9




9




0




3




3









9




7









9




9




10




9









7






Ducksalad























































































































































Giant foxtail




9




2




8




3




0




0




0




0




9




9




3




0




0




3




9




9




0




4




2




3




9




9




9




9




9




9




9




6




6






Morningglory









7




10




6




4




3




2




2




7




6




2




0




6




0




1




3




3




2




10









10




10




10




9




8




10




8




1




10






Nutsedge




0




0




0









0




0




0




0




3




5




0




0




0




0




0




0




0




0




0




0




7









6




6




3




2




4









0






Rape




0




0




0




2




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




4




0




7




3




5




3




7




7




0




0






Redroot pigweed




2




0




0




2




0




0




0




0




4




7




0




0




0




0




4




6




0




0




0




2




5




8




9




7




8




7




8




0




1






Rice























































































































































S. Flatsedge























































































































































Soybean




3




6




7




3




3




2




1




1




4




4




3




0




2




4




6




7




2




1




5



















7




9




8




8




8




3




4






Sugarbeets




0




0




0




0




0




0




0




0




5




3




0




0




0




0




0




0




0




0




0




0




0




5




1




0




2




1




0




0




2






Velvetleaf




1




0




7




5




2




0




0




0




5




7




0




0




0




0




4




0




2




0




0




3




5




6




8




7




5




6




8




0




1






Wheat




0




0




3




0




0




0




0




0




0




3




0




0




0




0




3




0




0




0




2




0




4




0




6




5




8




5




6




0




0






Wild oats




0




0




0









0




0




0




0




0




4




0




0




0




0




0




3




0




0




2




0




4




6




4




9




7




9




9




0




0
















COMPOUND








































Rate 500 g/ha




617




618




619




620




621




622




623




624




625




627




628




629




630




631




632




633




634




635




636




638




639




640




641




642




643




645




646




647




648









Postemergence






B. signalgrass




0




0




2




0




0




0




0




8




5




8




8




7




3




8




6




5




5




8




3




6




2




4




4




0




2




0




0




8




0






Barnyardgrass























































































































































Bedstraw























































































































































Blackgrass




0




0




0




0




0




0




6




9




7




9




9




8




9




9




8




8




8









5




7




6




5




6




6




4




0




0




8




0






Cocklebur




2




0




0




0




0




2




0




6




0




3




7




2




0




2




0




0




2




3




3




4




2




5




0




0




0




7




0




4




2






Corn




0




0




0




0




0




0




0




5




3




8




7




6




5




8




5




0




0




2




2




3




0




0




0




0




0




0




0




6




0






Crabgrass




0




0




2




3









5




0









8




9




9




9









9









9




9




9




9




9




8




6




6




5




6




3




1




9




7






Ducksalad























































































































































Giant foxtail




0




0




3









7




7




0




9




9




9




9




9




9




9




9




8




9




9




9




8




7




4




6




7




0




2




0




9




3






Morningglory




3




0




1









8




2




10




2




2




6




2




3




4




10




10




5




2




7




6




7




7




6




9




3




6




3




4




6




10






Nutsedge




0









0




0




0




0









3



















0




0














0




0









0




7



















0




0









0




6




0






Rape




0




0




3




0




0




0




0




3




0




5




6




3




4




2




0




0




0




9




7




0




3




0




0




0




0




0




0




7




2






Redroot pigweed




0




0




2




0




0




0




2




2




0




8




7




8




5




6




1




2




3




7




8




6




6




4




4




2




3




4




7




8




10






Rice























































































































































S. Flatsedge























































































































































Soybean




7














2




7









3




7




5




7




8




9




1
























4




4




5




3




4




1





























3






Sugarbeets




0




0




0




0




0




2




0




2




0




4




3




0




0




1




0




2




0




7




5




0




0




1




0




0




0




0




3




7




3






Velvetleaf




2




0




2




0




0




0




0




2




0




8




8




7




6




7




0




0




4




6




3




4




3




3




3




3




3




0




0




6




0






Wheat




0




0




0




0




0




0




1




4




0




8




7




0




3




7




5




0




0




2




2




3




4




0




0




0




0




0




0




6




0






Wild oats




0




0




0




0




0




0




1









1




7




5




2




3




4




3




0




2




5




0




3




1




0




1




1




1




0




0




3




0
















COMPOUND








































Rate 500 g/ha




649




650




652




653




654




655




657




658




659




660




661




662




663




664




665




666




667




668




670




671




672




674




675




676




677




678




679




680




681









Postemergence






B. signalgrass




0




2




2




2




0




2




6




0




8




5




7




2




0




7




5




7




7




5




8




8




4




8




8




8




0




2




0




0




0






Barnyardgrass























































































































































Bedstraw
























0
























0












































8




0




6
























0




0




0











Blackgrass




0




3




0




0




0




3




8




7




7




6









3




2




9




8




8




8




9




5




8




6




9




9




8




1




3




0




1




0






Cocklebur




2




0




0




0




0




0




5




5




2




2




0




0




2




6




2




7




5




2




3




1




7




4




3




2




1




2




0




0




0






Corn




0




4




0




0




0




0




1




0




6




2




0




0




0




0




3




0




5




3




6




5




0




7




6




0




0




0




0




0




0






Crabgrass









9




6




2




7




9




9









8




7




8




2




4




9




9




9




10




10




8




9




9




9




9




9




4




6









3




0






Ducksalad























































































































































Giant foxtail




7




8




8




7




7




9




8




6




8




8




8




5




4




9




9




9




9




9




9




9




9




9




9




9




4




6




4




5




0






Morningglory




8




10




7




1




10









9




10




10




7




0




7




4




10




8




7




6




4




4




6














4




2




7




8




2




1




7






Nutsedge




0




4




0




0



















2




0




0









5




0




0




0




0




0




0




5




0




5









8




0




0




0




0




0











Rape




0




3




0




0




0




3




3




3




1




0




0




0




0




3




4




4




6




4




4




2




3




5




3




0




0




0




0




0




0






Redroot pigweed




0




6




6




0




0




7




7




7




7




6




4




0




0




6




7




6




7




7




9




5




8




7




8




5




3




2




0




0




6






Rice























































































































































S. Flatsedge























































































































































Soybean




3




5




3




0




0




4









4




7




6




3




2





























6




5




4




5




7




5




3




2




2




1




3




1






Sugarbeets




0




0




2




0




0




2




3




2




4




0




0




0




4




0




4




4




3




6




2




3




3




5




4




2




1




0




0




0




0






Velvetleaf




0




2




0




0




0




0




4




6




6




3




0




0




2




6




7




6




8




7




4




3




7




8




8




3




3




3




0




0




0






Wheat




0




0




2




0




0




0




5




0




5




0




3




0




0




2




4




3




5




0




4




6




0




7




7




5




0




0




0




0




0






Wild oats




0




0




0




0




0




1




2




2




3




0




5




1




0




7




5




3




6




0




3




0




0




3




7




3




0




0




0




0




0
















COMPOUND








































Rate 500 g/ha




708




709




710




711




712




713




714




736




739




740




741




743




744




745




746




747




748




749




750




751




752




753




754




756




757




758




759




760




761









Postemergence






B. signalgrass




2




0




7




8




8




7




6




0




7




2









7




6




6




8




6




7




3




6




7




6




7




8




2




1




7




7




5




3






Barnyardgrass























































































































































Bedstraw














8









8



















6




0




9




8









9




9









9









10




7




2




6



















8














3






Blackgrass




2




0




6




7




6




7




7




3




6




7




0




5




5




9




8




8




8




6




8




7




6




4




5




3




4




6




8




3




0






Cocklebur




0




3




0




7




3




6




3




3




3




3




0




3




0




4




4




4









4




3




2




3




4




0




0




2




4




2




1




0






Corn




0




0




2




4




0




5




0




4




0




0




0




0




5




0




5




5




0




1




5




2




0




1




5




0




0




3




0




1




0






Crabgrass




4




8




9




10




9




9




9




4




9




9









9




9




9




10




9




9




9









9




10




9




9




3




6




9




8









0






Ducksalad























































































































































Giant foxtail




5




9




9




9




9




9




8




7




9




9




4




8




8




9




9




9




9




9




8




9




9




9




8




0




7




9




8




7




3






Morningglory




5




6




8




4




10




10




2




5




8




7




3




10




4




8




10




10




7




5




10




9




9




10




10




10




9




8




4




3











Nutsedge




0




6




3




5




0




3




5




2




3




0




0




9




6




0




4




0




0




0









10




0




3




0




0




0




0




0




0




0






Rape




0




0




5




4




4




6




9




0




2




0




0




3




8




7




7




9




7




6




7




5




4




0




0




3




0




2




0




5




0






Redroot pigweed




5




8




9




10




8




9




9




0




5




8




7




8




8




6




9




8




8




7




7




9




9




7









3




7




8




4




3




6






Rice























































































































































S. Flatsedge























































































































































Soybean




4




4




5




6




5




5




3




3




5




6




3




4




5




5




6




8




5




5




7




7




6




4




2




2




4




5




3




5




3






Sugarbeets




0




0




6




3




6




5




7




0




4




2




4




4




5




4




4




3




7




4




6




3




3




5




3




0




3




8




0




0




6






Velvetleaf




5




6




6




6




6




7




3




3




3




2




1




4




2




7




7




7




4




3




6




3




2




2




0




0




4




7




6




3




0






Wheat




0




0




6




5




5




2




6




2




6




4




3




6




7




3




6




4









0




2




3




5




5




5




0




0




6




0




0




0






Wild oats




0




0




6




4




3




5




9




3




0




0









3




2




4




7




2




0




2




0




5




0




2




0




0




0




2




3




4




0

















COMPOUND





























Rate 500 g/ha




762




763




764




765




766




767




772




773




774




775




777




778




780




790




791




792









Postemergence






B. signalgrass




3




5




3




8









7




0




0




0




3




3




6




5




7




0




2






Barnyardgrass






















































































Bedstraw




0




4




5









3




9




0




0




0




7




3




4









5




3











Blackgrass




0




5




8




7









9




0




0




0




7




4




4




4




5




6




7






Cocklebur




0




3




5




3




6




2




0




0




0




0




0




0




0




0




5




3






Corn




2




2




4




3




4




2




0




0




0




0




0




0




6




4




1




3






Crabgrass




8




9




9




9




9




9




0




0




0




9




9




9




7




9




9




9






Ducksalad






















































































Giant foxtail









9




8




9




9




9




0




0




0




9




9




9




9




8




9




9






Morningglory




2




7




5




8




2




7




2




0




0




6




8




6




8




10




9




10






Nutsedge




3




6




3




3




5




7




0




0




0









3









4




7




0




0






Rape




0




3




7




1




0









0




0




0




0




0




3




0




3




6




7






Redroot pigweed




6




8




7




8




8




9




0




0




0




3




4




4




0




5




8











Rice






















































































S. Flatsedge






















































































Soybean




4




5




4




5




4




7




0




0




0




6




6




4




4




4




5




7






Sugarbeets




6




4




7




4




2




7




0




0




0




0




5




2




0




7




5




2






Velvetleaf




3




2




4




7




5




3




0




0




0




2




5




3




4




7




6




7






Wheat




0




3









5




3




2




0




0




0




0




3




2




2




5




0




3






Wild oats




2




1




3




2




2




3




0




0




0




0




3




2




2




3




0




6
















COMPOUND




















































Rate 500 g/ha




1




2




3




4




5




6




7




8




9




10




11




12




13




14




15




16




17




18




19




20




21




24




25




34




35




36




37




38




39




40




41




42




43




44




45




46




47




48




49




51




 52 53 54 55 56









Preemergence






B. signalgrass




6




0




0




9




3




0




0




5




0




8




0




0




4




2




0




0




7




8




2




0




0




6




7




3




7




8




0




8




0




7




7




0




0




0




9




3




0




0




0




0




  6 3 2 0 0






Bedstraw




0




0




0




4




0




0




0




0




0




0




0




0




0




4




7




0




2




3




0




6









0




3




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




 — — 0 0 0






Blackgrass




2




0




0




8




5




2




0




0




0




9




0




2




6




2




0




0




9




5




3




5




0




4




8




6




3




7




0




10




0




6




4




0




1




1




0




7




0




2




0




0




  4 4 2 0 0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0














0




0




0




0




0




0




0




0




0




0




0




0




0




 — 0 0 0 0






Corn




5




7




0




0




0




2




0




0




0




4




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




  0 0 0 0 0






Crabgrass




8




0




0




10




6




9




8




6




3




7




8




0




5




9




10




2




10




10




10




7




7




10




10




10




10




10




5




10




6




10




10




0




0




2




9




10




5




7




9




2




 10 10 8 0 0






Giant foxtail




9




7




8




10




9




9




8




10




3




9




3




2




8




9




10




8




10




9




5




9




9




9




10




10




10




10




3




10




10




10




10




0




0




1




10




10




3




10




10




8




 10 10 7 0 0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




  0 0 0 0 0






Nutsedge



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




  0 0 0 0 0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




3




0




0




1




0




3




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




  0 0 0 0 0






Redroot pigweed




2




0




0









7




7




0




5




0




0




0




0




0




6




8




0




10




9









9




8




9




8




6




0




7




0




10




6




6




7




0




4




0




8




9




0




0




0




0




  6 3 0 0 0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




2




0




0




0




0




0




0




3




0




0




0




0




0




  0 0 0 0 0






Sugarbeets




0




0




0




3




0




0




0




0




0




0




0




0




0




0




6




0




6




4




2




7




8




9




2




4




0




5




0




6




0




6




0




0




0




0




8




6




0




0




0




0




  0 3 0 0 0






Velvetleaf




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




3




2




0




0




0




0




  0 0 0 0 0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




  0 0 0 0 0






Wild oats




0




0




0




7




6




3




0




2




0




0




0




0




2




0




0




0




3




5




0




0




0




2




7




7




6




7




0




8




0




5




4




0




0




0




0




0




0




2




0




0




  1 0 0 0 0
















COMPOUND






















































Rate 500 g/ha




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




85




86




87




88




89




90




91




92




93




94




95




96




97




99




101




201









Preemergence






B. signalgrass




0




0




0




0




5




0




0




0




0




0




2




8




0




0




0




0




0




0




8




8




0




9




5




4




8




0




0




0




7




5




5




0




3




10









8




5




7




2




4




3




0




0






Bedstraw




0




0




0




5




2




4




3









3




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




2




0




0




8




1




3




0




0




2









0




0




0






Blackgrass




0




0




0




0




6




4




0




0




0




0




2




4




0




0




0




0




0




0




9




8




0




6




6




6




6




0




0




0




8




7




6




0




6




10




10




10




9




6




8




3




4




0




4






Cocklebur




0




0




0









0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3



















0




0




0




0









0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




4




0




0




0




0




2




0




0




0




9




9




9




6




0




0




0




0




0




0






Crabgrass




0




0




5




1




8




9




2




3




9




8




7




10




4




0




0




4




9




8




10




8




3




10




10




10




8




0




0




0




10




10




10




2




8




10




10




10




10




8




9




4




10




0




4






Giant foxtail




0




0




3




5




10




10




3




4




9




9




8




10




4




0




0




2




10




10




10




9




5




9




9




9




8




0




0




0




10




10




10




2




10




10




10




10




10




8




8




8




10




0




10






Morningglory




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




3




6




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




6









3




6




0




10




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0









0









0




0




0




0




6




0




0






Rape




0




0




0




0




0




0









0




3




0




0




6




0




0




0




0




0




5




10




0




0




5




0




5




0




0




0




0




4




5




0




0




0




10




10




10




5




3




3




6




3




0




0






Redroot pigweed




0




0




0




0




3




0




0




0




3




0




10




10




0




0




0




0




0




3




10




8




0




6




10




7




0




0




0




0




8




10




10




0




6




10




10




10




4




9




8




10




10




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




2




0




0




7




9




9




0




0




0




2




0




0




0






Sugarbeets




0




0




0




5




6




0




0




0




0




0




3




0




0




0




0




0




0




4




4




0




0




5




2




5




0




0




0




0




3




9




8




0




0




10




9




9




2




3




2




9




4




0




0






Velvetleaf




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




3




7




3




3




3




0




0




0




5




0




2




0




0




8




8




10




3




0




0




0




3




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




2




0




3




2




0




2




0




0




0




0




0




0




0




0




6




7




8




0




0




0




2




2




0




0






Wild oats




0




0




0




0




3




0




0




0




0




2




2




2




0




0




0




0




0




0




8




4




0




6




4




5




8




0




0




0




5




3




5




0




3




10




10




10




6




5




7




5




5




0




0
















COMPOUND








































Rate 500 g/ha




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120




121




122




123




124




125




126




127




128




129




130




131









Preemergence






B. signalgrass




7




6




10




2




10




9




10




7




4




5




10




10




10




10




10




10




9




8




9




5




2




0




0




0




0




0




7




9




9






Bedstraw




0




0




5




4




10




8




10




7




3




0




8




0




0




9




0




0




8




0




5




0




0




0




0




0




0




0




0




10




10






Blackgrass




5




7




10




2




10




10




10




7




5




5




10




10




6




10




10




7




9




8




9




3




7




0




0




0




0




2




4




10




10






Cocklebur




0




0




0




0




0




0




5




0




0




0




3









0




5




0




0









0




0









0




0




0




0




0




0









0




2






Corn




0




2




3




0




9




9




9




4




4




2




10




9




0




9




9




0




2




0




0




0




0




0




0




0




0




0




4




6




10






Crabgrass









9




9




8




10




10




10




10




9




10




10




9




9




10




10




10




10




9




9




8




7




0




0




0




0




0




9




10




10






Giant foxtail




9




10




10




10




10




10




10




10




10




10




10




10




10




10




10




10




10




10




10




9




10




0




0




0




4




8




9




10




10






Morningglory




0




0




0




0




7




0




10




0




0




2




8




1




0




8




6




0




5




0




0




0




0




0




0




0




0




0




0




4




7






Nutsedge




0




0




0




0




6




0




0




0




0




0




0




0




0




0




7




0




6




0




0




0




0




0




0




0




0




0




0




3




0






Rape




0




0




6




2




10




9




10




8




4




5




10




10




5




10




10




0




9




3




0




3




0




0




0




0




0




0




0




10




10






Redroot pigweed




7




4




10




4




10




10




10




8




8




9




10




10




8




10




10




10




10




8




8




8




9




0




0




0




7




0




7




10




10






Soybean




0




0




0




0




8




2




9




6




5




4




9




3




0




9




9




0




0




0




0




0




0




0




0




0




0




0




2




4




8






Sugarbeets




4




6




9




2




10




8




10




5




4




0




10




7




5




10




10




0




8




7




7




4




7




0




0




0




0




0




5




10




10






Velvetleaf




3




0




6




0




10




5




10




7




7




5




8




6




2




10




10




4




6




3




0




3




6




0




0




0




0




0




6




10




10






Wheat




2




4




2




0




8




3




10




3




3




0




8




8




0




8




8




0




5




6




3




0




7




0




0




0




0




0




3




4




10






Wild oats




6




7




9




0




10




9




10




5




4




6




10




10




4




10




10




6




9




8




6




5




6




0




0




0




0




0




6




10




10
















COMPOUND








































Rate 500 g/ha




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149




150




151




152




153




154




157




158




159




160




161




162









Preemergence






B. signalgrass




9




7




8




4




5




9




9




9




2




0




0




5




7




5




10




10




7




0




0




7




6




0




4




0




0




0




0




5




7






Bedstraw




10




0




3




4




0




10




10




9




0




0




0




0




4




4




7




8




2




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




10




5




2




4




6




10




9




10




4




0




0




6




7




7




10




10




9




0




0




10




3




0




5




5




3




0




0




9




3






Cocklebur




0




2




0




0









0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




8




0




0




0




0




4




9




7




0




0




0




0




4




0




9




9




0




0




0




9




0




0




0




0




2




0




0




0




0






Crabgrass




9




5




9




4




8




10




10




10




10




7




4




10




9




8




10




10




9




0




6




10




3




0




0




6




7




0




0




9




10






Giant foxtail




10




10




10









10




10




10




10




10




6




6




10




8




8




10




10




10




0




5




10




5




0




8




10




8




0




0




10




9






Morningglory




2




0




1




0




0




1




4




0




0




0




0




0




0




1




4




7




1




0




0




0




0




0




0




3




2




0




0




0




0






Nutsedge




9




0




0




0














7




0




0




0




0




0




0




0




3




4




0




0









2




0




0




0




0




0




0




0




0




0






Rape




8




2




6




0




0




10




10




9




0




0




0




6




2




0




10




10




9




0




0




10




0




0




0




0




0




0




0




3




9






Redroot pigweed




7




3




2




4




10




10




10




10




0




0




0




10




5




4




10




10




10




0




9




10




0




0




9




0




2




0




0




10




7






Soybean




4




0




0




0




0




5




8




2




1




0




0




1




0




0




4




9




0




0




0




7




0




0




0




0




0




0




0




0




0






Sugarbeets




8




5




7




0




9




10




10




6




1




0




0




9




6




3




10




7




10




0




0




10




0




0




6




0




0




0




0




0




0






Velvetleaf




10




2




7




0




4




10




10




7




0




0




0




0




0




5




8




7




8




0




3




10




0




0




0




0




0




0




0




0




0






Wheat




4




0




0




0




0




5




9




4




0




0




0




0




0




0




8




8




6




0




0




5




0




0




0




0




0




0




0




2




0






Wild oats




9




4




2




0




3




10




10




9




1




0




0




5




2




3




10




10




8




0




2




10




0




0




5




0




2




0




0




6




5
















COMPOUND








































Rate 500 g/ha




163




164




165




166




167




168




169




170




171




172




173




174




175




176




177




178




179




180




181




182




183




184




185




187




188




189




190




191




192









Preemergence






B. signalgrass




2




0




6




4




8




5




7




10




5




8




4




4




0




0




0




9




9




0




0




0




4




8




0




0




7




6




0




3




6






Bedstraw




4




0




4




0




5




0




10




9




0




5




0




3




9




0




10




0




0




0









0




7




2




0




0




0




0




4




0




0






Blackgrass




10




0




8




5




3




2




10




10




2




3




6




2




0




3




6




3




2




0




0




0




0




7




0




0




0




7




3




6




7






Cocklebur




0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




0




0




0




2









0




0




0




0




0




0






Corn




2




0




0




0




0




0




6




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4






Crabgrass




9




4




8




7




10




7




10




10




10




10




9




10




8




10




9




9




9




0




0




0




3




9




9




0




0




3




0




8




9






Giant foxtail




10




2




9




7




10




10




10




10




10




10




10




10




8




10




10




9




10




0




0




0




3




10




9




0




7




6




0




10




10






Morningglory




0




0




3




0




0




0




0




10




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3






Nutsedge




0




0




0




0




0




0




3




9




0




0




0









3




0




0




0




10




0




0




0




0




0




0




0




0




0




0




0











Rape




8




0




10




0




5




0




10




10




4




5




0




4




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




9






Redroot pigweed




9




0




1




0




8




0




8




10




6




8




5




9




0




0




0




10




10




0




0




0




0




1




0




0




0




0




0




6




9






Soybean




0




0




0




2




0




0




5




9




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Sugarbeets




6




0




4




0




5




7




8




10




0




5




6




6




0




2




0




0




0




0




0




0




0




0




0




0




6




0




0




0




8






Velvetleaf




5




0




4




6




3




6




8




10




0




3




0




0




0




2




0




0




5




0




0




0




0




7




0




0




2




0




0




0




6






Wheat




4




0




2




0




0




0




4




8




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




2




0




2




0






Wild oats




10




0




6




2




6




3




10




10




5




6




3




0




0




5




2




3




3




0




0




0




0




3




0




0




0




3




0




7




7
















COMPOUND








































Rate 500 g/ha




193




194




195




196




197




198




199




201




202




203




204




205




206




207




208




210




211




212




214




215




216




218




219




220




222




223




224




225




226









Preemergence






B. signalgrass




0




3




6




0




0




0




9




4




0




0




2




0




0




0




0




0




5




5




0




2




4




7




9




8




0




4




4




7




10






Bedstraw




0




10




2




0




0




0




0




0




2




0




0




0




0




0




0




0




10




10




0




0




0




3




9




10




0




3




0




2




0






Blackgrass




0




8




6




0




0




0




10




4




2




0




5




0




0




7




3




4




9




9




3




6




4




10




10




10




0




5




5




10




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5









0




0




2




0






Corn




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




2




0




6




7




7




0




0




0




6




9






Crabgrass




7









9




0




3




0




10




9




9




0




8




8




8




4




6




8




3




5




4




4




8




7




10




10




9




9




10




10




10






Giant foxtail




6




9




10




0




3




3




10




10




10




0




10




3




9




10




10




5




8




10




6




5




9




10




10




10




9




9




10




10




10






Morningglory




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




1




6




0




1




0




8




8






Nutsedge




0




0









0




0




0




10














0




0









0




0




0




0









0









0




0




0





























10











Rape




0




7




0




0




0




0




0




0




0




0




3




0




0




2




0




3




4




8




0




2




0




2




10




8




0




0




0




6




10






Redroot pigweed




0




10




0




0




0




0




10




0




3




0




0




0




3




8




2




8




7




10




9




6




8




10




10




10




4




7




4




10




9






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




6




0




3




0




0




0




6




0






Sugarbeets




0




3




2




0




0




0




6




0




1




0




0




0




0




0




0




3




8




8




0




7




0




7




8




8




0




0




0




6




6






Velvetleaf




0




3




0




0




0




0




0




0




1




0




0




0




0




5




3




0




0




5




0




0




0




2




10




8




3




0




0




7




7






Wheat




0




2




0




0




0




0




0




2




2




0




2




0




0




0




0




0




5




7




0




0




0




3




9




8




0




0




0




8




8






Wild oats




0




8




4




0




0




0




7




5




5




0




6




0




0




0




3




2




5




7




0




2




0




9




9




8




1




4




2




10




10
















COMPOUND








































Rate 500 g/ha




227




228




229




230




231




232




233




234




235




236




237




238




239




240




241




242




243




245




246




247




248




249




251




253




254




255




257




258




259









Preemergence






B. signalgrass




2




0




0




0




0




5




4




0




0




3




0




0




5




3




4




10




10




10




5




0




0




0




9




0




0




9




3




8




9






Bedstraw




3




0




0




0




0




0




0




0




0




0




0




3




0




0




10




10




9




10




2




0




0




0




10




0




0




0




0




10




10






Blackgrass




10




0




0




2




0




8




9




0




0




5




0




0




4




2




10




10




10




10




10




0




0




0




10




0




4




10




0




8




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0









0




0




0




3




5




6




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




9




9




8




3




0




0




0




5




0




0




8




0




5




3






Crabgrass




10




2




0




9




7




10




10




0




0




5




3




10




10




9




10




10




10




10




10




2




0




2




10




0




3




9




5




10




7






Giant foxtail




10




9




0




9




8




9




10




0




0




10




4




10




10




10




10




10




10




10




10




3




0




5




10




0




10




10




9




10




10






Morningglory




0




0




0




2




6




0




2




0




0




0




2




3




0




0




5




10




10




6




0




0




0




0




4




0




0




0




4




0




0






Nutsedge









0




0




0




0














0
























0









10




10














0









0




0









0




0









0









0






Rape




10




0




0




0




0




0




3




0




0




0




0




10




0




0




9




10




10




10




10




0




0




0




10




0




6




5




0




7




9






Redroot pigweed




10




0




0




0




0




7




8




0




0




0




0




9




0




0




10




10




10




10




3




0




0




0




10




0




0




10




4




10




8






Soybean




2




0




0




0




0




0




0




0




0




0




0




0




0




0




4




7




9




8




2




0




0




0




0




0




0




0




0




3




0






Sugarbeets




8




0




0




0




0




4




8




0




0




0




0




6




0




0




6




8




10




10




8




0




0




0




10




0




6




7




0




7




0






Velvetleaf




2




0




0




0




0




0




7




0




0




0




0




3




5




2




7




10




10




10




5




0




0




0




7




0




0




7




0




7




5






Wheat




0




0




0




0




0




0




0




0




0




0




0




2




2




0




5




10




9




9




5




0




0




0




8




0




0




8




4




7




0






Wild oats




3




0




0




0




0




8




6




0




0




2




0




3




3




0




8




10




9




10




8




0




0




0




9




0




2




10




4




6




4
















COMPOUND








































Rate 500 g/ha




260




261




262




263




265




266




267




268




269




270




271




272




273




274




276




277




278




279




280




281




282




283




284




286




292




293




294




297




298









Preemergence






B. signalgrass




3




3




0




0




4




7




9




0




7




0




10




0




3




0




10




10




0




0




0




0




7




10




8




8




0




9




9




0




0






Bedstraw




5









0




0




0




9




2




0




0




0




10




3









0




0




2




0




0




0




10




2




9




8




0




0




0




0




0











Blackgrass




3




4




4




0









9




8




0




7




0




10




0




0




0




10




10




0




0




0




4




8




10




10




7




0




9




10




0




0






Cocklebur




0




0




0














0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0






Corn




0




0




0




0




0




0




3




0




0




0




3




0




0




0




0




3




0




0




0




0




0




0




0




0




0









2




0




0






Crabgrass




9




5




3




2




6




6




8




0




6




0




8




2




9




5




7




10




4




1




0




10




8




7




9




10




0




8




10




7




0






Giant foxtail




10




9




7




9




10




8




9




0









0




10




6




9




9




10




10




8




7




0




10




10




10




10




10




0




10




10




7











Morningglory




0




0




0




0




0




1




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




2




0




0




4




0




0




0






Nutsedge









0




0




0




0




0




0














0




0




0




0




0









0














0




0









0




0









0









0




0




0






Rape




0




0




0




0




0




5




0




0




0




0




10




0




0




0




10




2




0




0




0




0




2




8




7




7




0




10




3




0




0






Redroot pigweed




4




0




0




0




0




9




7




0




4




0




10




3




0




0




4




5




0




0




0




0




9




10




8




10




0




10




2




0




0






Soybean




0




0




0




0




0




0




0




0




4




0




1




0




0




0




0




4




0




0




0




0




0




0




3




0




0




2




0




0




0






Sugarbeets




0




0




0




0




0




7




5




0




4




0




8




0




7




0




7




7




0




0




0




0




3




5




6




4




0




8




2




0




0






Velvetleaf




0




0




0




3




0




4




3




0




0




0




8




0




1




0




3




7




0




0




0




0




0




7




7




5




0




8




4




0




0






Wheat




0




0




0




0




1




6




0




0




0




0




3




0




0




0




3




4




0




0




0




0




0




6




0




2




0




9




0




0




0






Wild oats




0




0




0




0




5




7




2




0




4




0




8




2




3




0




6




8




0




0




0




3




7




7




5




6




0




9




8




0




0
















COMPOUND








































Rate 500 g/ha




299




300




301




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




319




320




321




322




323




325




326




327




328




329









Preemergence






B. signalgrass




10




2




0




3




0




0




5




0




4




0




2




8




0




0




0




6




6




9




8




3




3




5




3




0




0




7




7




5




0






Bedstraw




10




8




0




0









0




0




0




0




0




0




10




0




0




0




3









6









7




0




3




2









0


























Blackgrass




10




0




0




5




0




0




4




0




4




0




6




10




0




0




0




10




10




10




10




4




6




7




7




0




7




8




7




7




0






Cocklebur




0














0




0




0




0




0









0




0




4




0




0




0




0




0




2




0




0




0




0




4




0




0




0




0




0




0






Corn




8




0




0




0




0




0




0




0




2




0




4




5




0




0




0




0




3




5




5




0




0




0




0




0




0




2




0




0




0






Crabgrass




9




7




0




7









8




7




0




2




0




6




7




0




0




0




8




7




10




8




3




7




4




7




2




2




5




5




5




3






Giant foxtail




10




10




0




9




0




6




10




9




9




0




9




10




0




0




0




10




10




10




10




9




7




10




10




2




10




9




9




9




3






Morningglory




7




0




0




0




3




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0






Nutsedge









0




0




0




0




0









0




0




0




0




10




0




0




0




0




0









0




0




0




0




0




0









0




0




0











Rape




10




0




0









0




0




0




0




0




0




0




10




0




0




0




7




0




4




10




0




0




0




2




0




0




1




2




0











Redroot pigweed




10




0




0




0




0




0




7




0




4




0




2




10




0




0




0




9




3




10




10




0




0




0




8




0




0




7




3




4




0






Soybean




7




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0






Sugarbeets




10




0




0




2




0




6




3




0




2




0




0




10




0




0




0




6




2




4




8




0




0




0




4




0




0




2




3




0




0






Velvetleaf




8




0




0




0




0




0




0




0




2




0




2




8




0




0




0




5




0




6




8




0




0




0




0




0




0




0




0




0




0






Wheat




8




2




0




0




0




0




0




0




0




0




0




7




0




0




0




3




7




2




8




0




0




0




0




0




0




2




4




0




0






Wild oats




8




3




0




5




0




0




1




0




8




0




2




9




0




0




0




3




3




6




10




0




0




5




3




0




2




3




4




1




0
















COMPOUND








































Rate 500 g/ha




330




331




332




333




334




335




336




337




338




339




340




341




342




343




344




345




348




349




350




351




352




353




354




355




356




357




358




359




360









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




2




0




6




8




0




0




7




4




4




4




7




5




5




6




5




7




7




0




7






Bedstraw




0




0









0




0









0




0




0




0




5




2



















0




9









10




10









3




0




9




9




10




10




0











Blackgrass









0




0




0




0




0




0




3




0




3




8




7




7




10




0




0




9




4




8




8




10




8




9




10




9




10




10




0




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0



















0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




9




2




7




6




9




7




6




4




6




9




6




0




9






Crabgrass




0




0




5




3




0




2




0




3




0




5




9




8




9




10




1




0




10




9




10




10




10




10




10




10




10




10




10




0




10






Giant foxtail




0




0




7




2




0




10




0




9




9




10




10




10




10




10




8




0




10




10




10




10




10




10




10




10




10




10




10




0




10






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




2




0




2




1




0




2




0




7




5




0




10






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




9




0




0




0




0




0




6




0




0




7






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




6









0




7




4




10




9




7




5




5




5




5




8




4




0




0






Redroot pigweed




0




0




3




0




0




0




0




0




0




0




4




8




0




10




0




0




10




7




10




10




10




10




10




10




10




10




10




0




10






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




2




2




2




0




1




0




0




0




1




0




5






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




6




4




9




8




7




4




6




3




5




6




3




0




7






Velvetleaf




0




0




0




0




0




0




0




0




0




0




2




2




0




7




0




0




7




3




6




5




7




6




7




5




5




7




8




0




7






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




3




5




0




0




0




0




3




2




6




2




2




2




6




9




3




0




8






Wild oats




0




0




0




0




0




0




0




0




0




0




3




2




4




9




0




0




10




9




7




4




10




6




8




9









10




10




0




10
















COMPOUND








































Rate 500 g/ha




361




363




364




365




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388




389




390




391




393




394









Preemergence






B. signalgrass




6




6




3




0




5




8




2




5




4




8




2




5




8




0




0




0




0




0




6




6




7




9




2




6




4




10




0




2




10






Bedstraw




2




10




3




0




10




10



















10




0









10









0














0





























7




10


























Blackgrass




10




10




4




0




10




10




5




10




10




10




7




6




10




0




0




0




2




2




7




7




7




10




2




6




9




10




0




3




10






Cocklebur




0




0




0




0









0




0




10




0




2




0




0




0




0




0




0









0









0




0




0




0




0




0









0




0




0






Corn




6




7




0




0




5




10




0




9




7




9




3




0




7




0




0




0




0




2




2




0




5




0




0




9




4




7




0




0




5






Crabgrass




9




9




5




4




10




10




10




10




10




10




10




9




10




0




10




8




9




9




10




10




9




10




9




10




10




10




0




8




10






Giant foxtail




10




10




10




3




10




10




10




10




10




10




10




10




10




0




10




9




10




9




10




10




10




10




9




10




10




10




0




10




10






Morningglory




0




6




0




0




2




5




0




3




3




3




1




0




0




0




0




0




0




0




0




0




2




2




0




0




1




7




0




2




2






Nutsedge




0




2









0




0




10




5




10




9




10




0




0




0




0




0




0




0




0




0




0




0




0




0









0




2




0




0




6






Rape




6




5




2




0




10




10




5




10




10




10









7




8




0




0




0




0




0




0




0




0




4




0




8




8




8




0




0




9






Redroot pigweed




10




10




0




0




10




10




10




10




10




10




10









10




0




0




0




6




0




0




3




0




10




9




10




10




10




0




10




10






Soybean




1




0




0




0




0




8




4




7




2




2




2




0




0




0




0




0




0




0




0




0




3




0




0




4




3




3




0




0




2






Sugarbeets




6




8




0




0




9




10




4









10




10




7




4




7




0




0




0




0




0




0




0




2




7




2




6




4




8




0




3




7






Velvetleaf




5




7




0




0




6




10




6




6




6




7




0




0




7




0




0




0




0




0




0




0




3




3




3




6




2




7




0




0




7






Wheat




6




7




0




0




0




10




0




7




4




6




0




0




3




0




0




0




0




0




0




0




3




8




0




8




0




9




0




0




9






Wild oats




10




10




3




0




7




10




7




10




6




10




0




0




9




0




0




0




4




0




4




0




6




10




7




10




4




10




0




3




10
















COMPOUND








































Rate 500 g/ha




395




396




397




398




400




401




402




403




404




405




406




407




408




409




410




411




414




415




416




417




418




419




420




421




422




423




424




425




426









Preemergence






B. signalgrass




0




5




10




10




4




0




9




7




10




0




0




0




7




9




10




10




5




6




9




7




6




8




8




9




0




0




0




9




8






Bedstraw




0





























10









10














0
























0


































































Blackgrass




0




5




10




10




0




2




10




9




10




0




0




0




10




10




10




10




10




9




10




9




0




3




10




10




0




0




0




10




9






Cocklebur




0




0




0




0




0




0




0









0




0




0




0




0




2




0




0




0




0




4




0




0




0




0




0




0




0




0




2




0






Corn




0




0




8




8




2




0




9




6




6









0




0




8




10




9




9




0




4




6




0









0




2




8




0




0




0




9




6






Crabgrass




2




10




10




10




10




10




10




10




10




10




6




9




10




10




10




10




10




10




10




10




10




9




10




10




0




2




0




10




10






Giant foxtail




2




10




10




10




10




8




10




10




10




10




9




10




10




10




10




10




10




10




10




10




10




5




10




10




0




4




0




10




10






Morningglory




0




0




4




0




0




0




2




0




5




0




0




0




7




5




0




4




0




0




8




0




0




2




8




8




0




0




0




4




6






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




8









2









0




4




0




0




0




10




0




0




0




0




5




0






Rape




0




0




10




10




0




0




8




7




8




0




0




0




8




6




8




10




0




10




10




6




9




2




8




10




0




0




0




10




10






Redroot pigweed




0




8




10




10




6




0




10




9




10




0




0




0




10




10




8




10




0




10




10




10




8




10




5




10




0




0




0




3




10






Soybean




0




0




0




0




0




3




1




2




3




3




0




0




0




8




3




1




0




0




9




0




0




0




0




10




0




0




0




0




0






Sugarbeets




0




2




9




9




4




0




8




5




8




0




0




0




8




9




0




8




0




8




9




6




2




5




3




10




0




0




0




2




6






Velvetleaf




0




0




6




7




2




0




8




5




7




0




0




0




7




8




8




8




0




7




8




6




6




4




7




10




0




0




0




6




5






Wheat




0




0




3




2




0




0




6




0




5




0




0




0




7




10




8




10




0




3




10




2




2




0




7




9




0




0




0




4




6






Wild oats




0




4




10




8




0




0




10




8




10




0




0




0




8




8




10




10




7




6




10




4




0




2




5




10




3




0




0




10




10
















COMPOUND








































Rate 500 g/ha




427




428




429




430




431




432




433




434




435




436




437




438




439




440




441




443




444




445




446




447




448




449




451




452




453




454




455




456




457









Preemergence






B. signalgrass




4




3




4




3




0




0




6




0




1




10




0




2




0




8




0




10




8




3




8




0




2




0




0




0




6




4




9




2




0






Bedstraw








































































































0




4


































0






Blackgrass




6




2




3




9




3




2




9




0




2




9




0




3




0




10




0




0




8




1




10




0




2




3




0




2




5




6




7




6




0






Cocklebur




0




0




0




0









0




3




0




0




0




0




0




0




0




0




0




0









0




0









0




0




0




0




0




0




0




0






Corn




0




0




0




2




0




0




0




0




0




9




0




0




0




0




0




0




0




0




6




0




0




0




0




0




3




3




7




0




0






Crabgrass




10




10




10




10




3




9




10




1




9




10




2




10




0




10




0




9




10




9




9




9




9




9




7




5




7




9




10




9




0






Giant foxtail




10




10




10




10




3




9




10




2




9




10




3




10




0




10




0




10




10




9




10




8




9




10




7




7




10




10




10




10




8






Morningglory




0




0




0




0




0




0




3




0




0




1




0




2




0




0




0




0




0




0




9




0




0




0




0




0




3




0




4




3




0






Nutsedge




0




0




0




0




0




0




0




0




0




5




0









0









0




0




0




0




0




0




0




0




0




0









0




3




0




0






Rape




0




0




0




4




3




0




7




0




0




10




0




2




0




3




0




0




2




2




10




0




0




0




0




0




3




0




9




0




0






Redroot pigweed




0




0




0




7




0




0




10




4




8




10




0




10




0




10




0




6




10




10




10




0




0




3




0




0




10




10




10




5




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




3




0




2




0




0




2




0




0




0




0




2




0




0






Sugarbeets




0




0




0




0




0




0




8




0




1




5




0




0




0




7




0




0




0




0




8




0




0




0




0




0




5




0




6




3




0






Velvetleaf




0




0




0




7




0




0




6




0




2




7




0




6




0




7




0




0




4




3




10




0




0




0




0




0




6




6




6




2




0






Wheat




0




0




0




5




0




0




2




0




0




5




0




0




0




7




0




0




0




0




7




0




0




0




0




0




6




0




2




0




0






Wild oats




3




2




0




3




2




0




8




0




3




10




0




3




0




9




0




0




4




0




10




7




0




0




0




0




8




2




10




3




0
















COMPOUND








































Rate 500 g/ha




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




482




485




486




487




488




489




490




492









Preemergence






B. signalgrass




4




1




0




0




0




2




5




9




2




4




10




6




10




10




0




7




0




6




10




9




9




0




8




8




5




10




9




8




0






Bedstraw
























0














2




0


































0









3









0












































0






Blackgrass




9




6




3




0




0




4




10




8




2




9




10









10




10




3




9




0




8




10




9




9




4




9




10




9




10




10




9




0






Cocklebur




0




0




0




0




0




0




0




0




6




0




0




0




0




2




0




0




0




0




0









0




0




0




0




0




0




0









0






Corn




3




0




2




0




0




0




2




4




0




2




9




0




3




7




0




4




0




0




0




3




3




0




7




8




0




6




5




5




0






Crabgrass




10




10




9




3




0




2




10




10




8




9




10




9




10




10




7




10




0




10




10




10




10




8




10




10




10




10




10




10




3






Giant foxtail




10




10




9




3




0




10




10




10




9




10




10




3




10




10




7




10




0




10




10




10




10




9




10




10




10




10




10




10




9






Morningglory




0




0




0




0




0




0




0




0




0




2




1




0




0




5




0




0




0




0




2




4




0




0




4




0




0




0




1




0




0






Nutsedge




0




0




0




0




0




0




0









0




0









0




0




10









0




0




0




3









0




0




0




0




0




0




0




0




0






Rape




4




0




0




0




0




0




5




3




7




6




10




0




10




4




0




4




0




2




6




4




0




0




2




6




0




10




9




8




0






Redroot pigweed




8




7




0




0




0




10




10




10




9




10




10




0




10




10




10




7




4




8




10




6




9




0




9




9




10




10




10




8




0






Soybean




2




0




0




0




0




0









4




0




0




2




0




0




3




0




0




0




4




0




0




1




0




0




2




0




1




3




4




0






Sugarbeets




8




0




0




0




0




0




5




4




2




6




10




0




4




6




0




3




0




0




7




4




0




0




2




6




0




7




5




5




0






Velvetleaf




6




0




0




0




0




2




8




4




1




4




7




0




6




7




0




0




0




0




7




5




0




2




3




0




0




6




7




4




4






Wheat




2




0




0




0




0




0




0




1




0




6




6




0




0




0




0




0




0




0




8




7




2




0




5




0




0




5




6




4




0






Wild oats




10




0




0




0




0




0




3




7




0




7




10




3




7




10




0




8




0




7




10




7




7




3




8




8




6




10




9




8




0
















COMPOUND








































Rate 500 g/ha




493




494




495




496




497




498




499




500




501




502




503




504




505




506




508




509




510




511




512




513




514




515




516




517




519




520




521




522




523









Preemergence






B. signalgrass




0




0




0




8




0




0




2




10




10




10




9




10




6




0




8




9




9




0




10




9




10




9




10




0




0




0




9




9




5






Bedstraw




0




0














0














10




9




10




10




8




9




4




0




9




4




0




3




4




0




3




7




0




0




0




0




10




0






Blackgrass




0




0




0




2




0




0




1




10




9




10




10




10




6




9




8




10




8




0




10




10




7




8




10




4




4




0




3




9




7






Cocklebur




0




0




0




0




0




0




4




2




3




9




3




0




2




0




0




5




0




0




0




0




0




0




0




0




0




0




0









0






Corn




0




0




0




0




0




0




0




8









9




9




6




6




0




4




6




5




0




3




4




5




5




0




3




0




0




3




9




9






Crabgrass




2




0




0




9




0




5




8




10




9




10




9




10




8




6




10




10




9




10




9




5




10




9




10




7




10




10




10




10




10






Giant foxtail




10




0




0




9




0




8




10




10




10




10




10




10




10




8




10




10




10




10




10




10




10




10




10




10




10




10




10




10




10






Morningglory




0




0




0




0




0




0




0




9




5




4




7




4




3




0




0




3




5




0




0




3




0




0




0




0




0




0




0




4




0






Nutsedge




0




0




0




0




0




0




0




10




9









2




8




8




10









0




0




0









0




0




0




0




0




0




0




0




10




0






Rape




0




0




0




0




0




0




0




10




10




9




9




10




9




8




3




10




9




0




5




7




8




10




9




4




0




0




2




6




7






Redroot pigweed




0




0




0




8




0




0




0




10




10




10




10




10




10




10




10




10




10




8




10




10




10




10




10




10




0




0




0




10




9






Soybean




0




1




0




0




0




0




0




8




8




5




7




5




5




0




0









0




0




0




5




0




0




0




0




0




0




0




10




0






Sugarbeets




0




0




0




0




0




0




0




10




8




7




9




9




8




0




6




7




7




0




5




0




6




7




7




5




0




0




3




7




9






Velvetleaf




0




0




0




0




0




0




0




10




5




8




8




10




10




0




0




8




6




0




0




0




5




6




7




3




0




0




3




9




5






Wheat




0




0




0




0




0




0




0




8




8




7




8




8




8




2




2




7




0




0




6




7




4




7




5




6




0




0




0




8




4






Wild oats




0




0




0




0




0




0




0




10




10




10




9




10




9




7




7




9




7




2




10




10




6




9




9




5




0




0




2




9




0
















COMPOUND








































Rate 500 g/ha




524




525




526




527




528




531




532




533




534




535




536




540




541




543




544




545




546




549




550




551




552




553




554




555




556




557




558




559




560









Preemergence






B. signalgrass









9
























0




9









0




0




8




5




6




8




5




2




0




10




9




9




8




10




8




9




7




6




9




9






Bedstraw









0
























0




0









0




0




0




3




0




9




10









5




3




10




8




10




0




0




0




0




0




0




8






Blackgrass









8
























0




9









0




0




9




2




2




6




9




3









9




9




8









7




8




10




8




9




10




9






Cocklebur




2









0




3




0




0




0




0




0




0




0




10









10




0




0




0




0




0




0




0




10




0




9




0




0




0




2




0






Corn




9




8




2




0




0




0




0




6




3




2




0




2




0




0




0




0




0




0




0




5




0




3




2




2




0




0




0




6




5






Crabgrass




10




10




10




10




10




10




10




10




10




10




2




10




10









10




10




10




10




10




10




10




10




10




10




10




10




9




10




10






Giant foxtail




10




10




10




10




10




10




10




10




10




10




10




10




10




9




10




10




10




10




10




10




10




10




10




10




10




10




10




10




10






Morningglory




2




6




2




2




3




0




0




0




0




2









0




0




0




0




8




0




0




0




0




0




2




0




0




0




0




0




8




3






Nutsedge




4




0




0




0




0




0




0




0









0




0




0




0




8




0




0




0




0




6




0




0




0




0




0




0




0




0









10






Rape









4
























0




7









3




0




7




0




0




6




2




0




0




9




9




0









3




0




8




2




2




10




8






Redroot pigweed









3









4














0




8









4




0




10




0









10




10














10




10




4









10




7




5




6




2




10




9






Soybean




0




0




0




0




0




0




0




0









0




0




0




0




2




0




0




0




0




0




0




0




3




3




2




0




0




0




3




3






Sugarbeets









9




8




6














3




7














3




4




2









4




6




2




3




8




9




5









6




5




0




4




2




9




7






Velvetleaf




4




4




3




2




0




5




4




5




3









0




0




0




0




0




0




2




0




4




4




0




2




0




6




3




0




0




9




5






Wheat









3
























0




0









0




0




0




3




0




0




2




0




0




2




6




4









6




3




4




3




2




9




8






Wild oats









8
























0




9









0




0




8




5




0




4




6




3




3




8




9




6









9




7




6




7




2




9




7
















COMPOUND








































Rate 500 g/ha




561




562




563




564




565




566




567




568




569




570




571




572




573




574




575




576




577




578




579




580




581




582




584




585




586




587




588




589




590









Preemergence






B. signalgrass




9




10




10




7




0




9




9




9




9




0




9




0




10




9









9




7




9




3




9




9




4




9




9




10




7




8




0




0






Bedstraw




8




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




6




9




6




9




8









2





















Blackgrass




9




10




9




9




0




10




7




9




9




0




9




0




6




2




2




9




6




4




0




7




7




0









8




10




8




8




0




0






Cocklebur




0




2




2




0




0




0




0




2




0




0




0




0




0




0




0




0




0




3




0




3




0




0




0




3




0




0




0




0




0






Corn




5




9




9




9




0




9




5




9




9




0




0




0




3




0




3




2




3




4




3




5




9




0




3




5




0




0




5




0




0






Crabgrass




9




10




9




9




2




10




9




10




9




10




3




0




10




9




9




9




10




10




10




9




9




7




9




10




10




9




9




9




3






Giant foxtail




7




8




10




9




2




10




9




10




10




9




9




7




10




10




10




9




10




10




10




10




10




8




10




10




10




9




10




10




7






Morningglory




4




8




3




4




0




0




0




6




0




0




4




0




4




0




2




0




9




0




0




0




6




2




3




5




4




0




0




0




0






Nutsedge
























0




0




0




3




0




0




0




0




0




0









8




0




0




3




5




8




0




0




10




2




0




0




9




0






Rape




9




10




9




3




0




10




0




7




9




0




2




0




3




0




2




7




0




4




0




8




7




3




4




10




4




1




0




0




0






Redroot pigweed




9




10




9




3




9




10




9




8




10




8




9




5




9




9




10




10




0




10




3




10




10




9




9




10




10




2




9




0




0






Soybean




2




9




6




8




0




0




0




9




0




0




3




0




0




0




0




0




0




0




0




0




7




0




0




3




0




2




5




0




0






Sugarbeets




8




9




4




3




0




6




2




8




3




2




0




0




2




3




2




6




0




3




0




5




9




0




5




6




8




0




6




0




0






Velvetleaf




2




7




7




8




0




2




0




7




7




0




0




2




3




2




2




3




4




2




0




5




10




4




5




6




7




2




5




0




0






Wheat




9




9




10




7




0




7




0




5




4




0




9




0




0




0




0




8




0




2




0




5




5




0




3




3




8




3




8




0




0






Wild oats




9




10




10




7




0




10




0




8




9




0




7




0




0




3




2




8




0




2




0




5




8




0




9




9




10




9




7




0




0
















COMPOUND








































Rate 500 g/ha




591




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609




610




611




612




613




615




616




617




618




619




620




621









Preemergence






B. signalgrass




0




0




0




7




9




0




0




3




0




8




7




0




0




0




0




8




10




10




10




10




10




9




0




1




5




0




3




0




0






Bedstraw



















9




10




0




0




0




0









0









0




0
























10




10




10









0




0




0




0




0




0




0






Blackgrass




0




0




0




9




10




0




0




6




0




9




9




0




0




0




3




9




9




10




10




10




10




10




4




6




6




0




0




0




0






Cocklebur




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




3




3




1




0




8




0




0




0




0




0




0




0






Corn




0




0




0




4




6




0




0




0




0




3




2




0




0




0




0




6




1




9




8




9




9




9




0




0




0




0




2




0




0






Crabgrass




0




2




0




9




10




6




0




8




0




10




10




0




1




10




8




9




10




9




10




10




10




10




0




1




8




2




8




6




8






Giant foxtail




0




0




0




10




9




4




0




10




0




10




10




0




7




10




9




10




10




10




10




10




10




10




7




5




9




0




8




9




10






Morningglory




0




0




0




6




6




0




0




0




0




0




0




0




0









0




0




4




5




8




6




10




10




0




0




0




0




0




0




0






Nutsedge




0




0




2




6




4




0




0




0




0









0




0




0




0




0




0




0




4




3




2




3




2




0




0




5




0









0




0






Rape




0




0




0




9




10




0




0




0




0




5




3




0




0




0




0




7




7




10




10




10




10




10




0




3




0




0




0




0




0






Redroot pigweed




0




0




0




10




10




0




0




0




0




10




8




0




0




0




0




10




7




10




10




10




10




10




4




10




0




0




0




0




0






Soybean




0




0




0




4




4




0




0




0




0




1




0




0




0




0




0




4




4




7




8




7




3




2




0




0




0




0




0




0




3






Sugarbeets




0




0




0




8




9




0




0




20




0




5




5




0




0




0




0




5




4




8




8




6




7




10




6




1




0




0




0




0




0






Velvetleaf




0




0




0




7




9




0




0




0




0




7




6




0




0




0




0




8




7




9




10




8




8




8




0




4




0




0




4




0




0






Wheat




0




0




0




2




6




0




0




0




0




6




0




0




0




0




0




3




0




6




6




7




8




6




0




0




0




0




0




0




0






Wild oats




0




0




0




5




9




0




0




0




0




8




8




0




0




0




3




6




6




10




10




8




10




10




0




2




3




0




0




0




0
















COMPOUND








































Rate 500 g/ha




622




623




624




625




627




628




629




630




631




632




633




634




635




636




637




638




639




640




641




642




643




645




646




647




648




649




650




652




653









Preemergence






B. signalgrass




4




2




8




10




9




10




8




8




10




10




6




10




9




9




8




8




7




9




8




8




6




0




0




10




5




0




4




2




0






Bedstraw




2









3









8




10




8




7
























9




9




4

















































0




0




5




0




0






Blackgrass




6









9




9




10




10




10




10




10




10




7




9




8




7




9




9




2




8




8




7




8




0




0




10




5




0




3




2




0






Cocklebur









0




0




0




7




7




7




0




2




0




0




0




0




0




0




9




2




0




0




0




0




0




0




7




0




0




0




3




0






Corn




0




0




6




3




9




9




8




5




9




5




2




0




8




3




0




8




0




0




2




0




0




0




0




10




0




0




0




0




0






Crabgrass




8









9




10




9




10




10




9




9




9




9




10




9




10




10




10




9




10




9




10




10




5




0




9




9




9




9




9




8






Giant foxtail




9




9




10




10




10




10




10




10




10




10




10




10




10




10




10




10




9




9




9




10




10




7




0




10




9




9




10




9




8






Morningglory




0




0




0




3




8




7




4




2




7




5




0




0




6




2




0




7




0




0




0




0




0




0




0




7




0




0




1




0




0






Nutsedge




3




0




0




0




10




9




5




3




8




0




0




0




4




10




0




8




0




0




3




0




0




0




0









0




0




5




3




0






Rape




0




2




7




4




10




9




9




0




8




4




4




7




9




10




3




10




10




6




0




9




6




0




0




10




0




0




2




0




0






Redroot pigweed




10




0




10




8




10




10




10




10




10




10




4




10




10




10




10




10




10




7




7




8




5




4




0




10




2




0




9




0




3






Soybean




0




0




7




0




5




7




0




3




9




0




0




0




2




4




0




3




3




0




0




0




0




0




0




1




0




0




0




0




0






Sugarbeets




3




2




8




0




9




7




7




7




8




0




0




6




9




7




5




10




6




6




0




4




0




0




0




8




0




0




4




0




0






Velvetleaf




4




0




8




6




10




10




8




7




9




7




0




6




7




4




2




10




3




0




0




3




0




0




0




9




0




0




0




1




0






Wheat




0




0




7




3




5




10




3




8




9




0




0




0




4




2




0




7




0




2




0




0




0




0




0




8




0




0




0




0




0






Wild oats




3




2




6




5




5




10




9




8




9




3




5




7




9




5




3




10




3




6




5




4




1




0




0




10




0




0




0




0




2
















COMPOUND








































Rate 500 g/ha




654




655




657




658




659




660




661




662




663




664




665




666




667




668




669




670




671




672




673




674




675




676




677




678




679




680




681




682




683









Preemergence






B. signalgrass




7




0




10




8




8




4




4




7




0




8




8




8




8




9




10




10




9




8




8




8




10




8




5




0




0




0




0




8




9






Bedstraw




0




0
































































9




9









0




6




0




10


































0




0






Blackgrass




7




3




9




7




9




7




7




9




0




8




9




10




10




10




10




10




10




8




9




9




10




8




0




0




0




4




3




9




9






Cocklebur




0




0




2




0




0




0




0




2




0




3




0




0




0




0




0




2




1









2




0




0




0




0




0




0




0




0




0




0






Corn




0




0




8




2




9




0




0




3




0




0




3




10




10




9




9




9




9




0




6




8




9




6




0




0




0




0




0




0




3






Crabgrass




9




9




9




9




10




9




9




6




0




10




10




10




10




8




10




10




9




10




10




9




10




7




7




1




1




3




7




9




10






Giant foxtail




9




9




9




10




10




10




10




10




9




10




10




10




10




10




10




10




10




10




10




10




10




10




10




4




8




4




9




10




10






Morningglory




0




0




6




0




6




0




0




1




7




4




4




3




6




5




0




8




8




2




2




7




6




0




0




0




0




0




0




3




2






Nutsedge




0




0




6




2




0




0




0




7




0




0














7




0




6




10




6




0




6




6




7




0




0




0




0




0




0




0




0






Rape




0




0




10




8




10




4




0




0




4




6




9




10




10




9




9




10




8




8




2




8




10




6




0




0




0




0




0




7




0






Redroot pigweed




5




4




10




10




10




10




8




7




7




10




10




10




10




10




10




10




10




8




10




10




10




10









0




1




3




3




7




6






Soybean




0




0




3




3




2




0




1




0




2




0




2




4




7




6




6




9




3




0




0




7




4




3




0




0




0




0




0




0




0






Sugarbeets




0




0




9




7




5




0




0




0




0




5




7




8




10




9




9




9




9




8




3




9




10




8




0




0




0




0




0




7




0






Velvetleaf




0




0




10




5




7




0




0




2




3




5




7




8




10




8




0




8




9




4




8




10




10




7




0




2




0




0




0




0




0






Wheat




0




0




7




3




7




0




0




0




3




5




4




7




6




7




8




9




8




0









8




9




5




0




0




0




0




0




0




0






Wild oats




2




0




8




4




9




3




0




9




0




7




8




9




10




9




10




9




5




7




8




10




10




4




0




0




0




0




0




8




8
















COMPOUND








































Rate 500 g/ha




684




685




686




687




689




691




692




693




694




695




696




697




698




699




700




701




702




703




704




706




707




708




709




710




711




712




713




714




715









Preemergence






B. signalgrass




5




9




9




10




10




10




9




0




8




6




9




5




5




10




10




0




8




8




9




10




10




0




0




9




8




8




9




10




10






Bedstraw




0




0




0




0




5









1




0









0




0




0




0




0




8




0




0




0














10




0




0




7




7




5




6
















Blackgrass




7




10




9




10




10




10




10




2




10




9




9




6




8




10




10




6




10




8




10




10




10




5




0




10




9




9




9




9




10






Cocklebur




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




4




2




9




7




3




0




1




3




5




0




0




9




6




0




4




0




2




7




2




0




0




5




5




0




6




6




8






Crabgrass




9




9




10




9




10




10




10




0




10




9




10




9




9




10




10




10




10




10




8




9




10




10




7




10




10




10




10




10




10






Giant foxtail




10




10




10




10




10




10




10




2




10




10




10




10




10




10




10




10




10




10




8




10




10




9




7




10




10




10




10




10




10






Morningglory




4




1




0




7




4




0




2




0




2




0




0




4




0




6




6




0




0




3




1




2




6




0




0




4




5




0




0




3




6






Nutsedge














0




4









0




0




0




0




0









0




0




0




0




0




0




0









4




0
























0




0









0






Rape




0




6




6




8




9




8




6




0




4




0




3




0




8




9




5




2




2




2




5




7




10




0




0




9




8




8




8




10




10






Redroot pigweed




7




8




7




9




8




9




9




0




9




5




8




0




0




6




3




0




5




5




9




10




10




6




7




10




10




9




10




10




10






Soybean




0




0




0




4




2




2




0




0




0




0




0




0




2




2




0




0




0




0




0




4




0




0




0




6




1




0




3




0




6






Sugarbeets




0




6




5




9




7




8




3




0




1




0




6




0




0




7




6




0




3




2




5




7




8




0




3




8




8




8




8




6




8






Velvetleaf




5




0




0




9




4




0




1




0




2




0




4




0




0




7




6




4




2




0




0




7




8




6




0




8




7




6




6




0




7






Wheat




0




0




0




7




7




3




0




0




0




6




2




2




3




7




0




0




0




3




6




7




6




0




0




8




8




0




5




6




6






Wild oats




4




4




7




10




9




9




9




0




7




6




8




2




9




10




10




2




9




2




9




8




10




0




0




10




10




8




9




6




10
















COMPOUND








































Rate 500 g/ha




717




718




719




720




721




723




724




725




726




728




729




730




732




733




734




735




736




737




738




739




740




741




742




743




744




745




746




747




748









Preemergence






B. signalgrass




7




9




9




10




10




2




0




4




9




9




10




9




0




10




9




10




8




9




10














2




0




8




9




10









9




10






Bedstraw




0




0




0




10




10




0




0




0




0




2




8




4




0




0




0




0




8




0




0




10




0




5




0




8




8




5









0




0






Blackgrass




10




10




10




10




10




2




0




7




9




10




10




10




0




10




10




10




9




10




10




10




9




0




0




9




9




9









8




9






Cocklebur




0




0




0









2




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0









0




10




0




0




4




0




0






Corn




9




3




5









8




0




0




0




2




0




9




9




0




0




9




9




2




6




9




2




0




0




0




0




7




2




4




9




4






Crabgrass




10




10




9




10




9




9




7




8




10




7




10




10




0




9




10




10




9




10




10




10




9




10




0




9




10




10




10




10




10






Giant foxtail




10




10




10




10




10




10




9




10




10




8




10




10




0




9




10




10




9




10




10




10




10




10




0




9




10




10




10




10




10






Morningglory




0




0




3




2




5




0




0




3




1




2




8




2




0




2




6




2




6




3




4




0




0




0




0




0




0




3




8




7




0






Nutsedge




0




0




0




0




3









0




0




0









2




3




0



















10




0




8




0




0




0




0




9




7




5




5




2




2






Rape




4




3




6




9




10




0




0




0




7




8




10




7




0




5




7




8




2




6




8




2









0




0




9




9




7














7






Redroot pigweed




8




8




10




10




10




0




0




3




8




9




10




10




0




7




8




9




2




8




8




10




10




7




0




10




9




10














10






Soybean




0




0




0




0




7




0




0




0




0




0




2




3




0




0




7




0




2




0




0




0




0




0




0




0




0




0




5




9




0






Sugarbeets




3




2




8




8




8




0




0




2




5




4




7




7




0




0




8




7




3




6




8




4




5




4




0




6




7




4














7






Velvetleaf




0




0




0




3




10




0




0




0




0




0




8




6




0




1




7




3




4




5




8




3




3




3




0




3




2




6




8




7




0






Wheat




0




2




5




5




8




0




0




0




0




7




6




0




0




0




9




2




8




2




8




3




3




4




0




5




5




0














5






Wild oats




10




8




9




9




10




0




0




6




9




10




10




9




0




8




10




10




9




9




10




4




6




7




0




9




9




8














8
















COMPOUND








































Rate 500 g/ha




749




750




751




752




753




754




755




756




757




758




759




760




761




762




763




764




765




766




767




772




773




774




775




777




778




780




790




791




792









Preemergence






B. signalgrass




10



















9




9




0




3




7




8




8




10




3




9




8




10




7




10









0




0




0



















4




9
















Bedstraw




4









10




10




3




0




0




0




0




4




0




6




0




0




8




8




8




9




8




0




0




0




2




0




10




2




9
















Blackgrass




9









10




10




9




9




0




7




7




9




8




9




0




9




10




9




9




9




10




0




0




0




10




10




10




9




10
















Cocklebur




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0




2




10




0




0






Corn




0




6




9




0




0




0




0




0




0




3




0




4




0




0




0




9




2




3




5




0




0




0




3




0




0




9




9




0




4






Crabgrass




10




10




10




10




9




9




0




9




9




10




9




10




3




0




9




10




10




10




10




0




0




0




10




10




10




10




10




10




10






Giant foxtail




10




10




10




10




9




9




2




9




9




10




10




10




9




9




9




10




10




10




10




0




0




0




10




10




10




10




10




10




10






Morningglory




0




6




5




0




0




1




0




0




0




0




0




0




0




0




5




2




0




3




0




0




0




0




2




5




0




2




7




0




0






Nutsedge









9




0




0




0




10




0




7




0









0




0




0




6




5




4




0




4




0




0




0




0




0









9









0




0




0






Rape




5









9




5




7




8




0




0




0




8




4




5




0




0




9




10




8




9




10




0




0




0




0




2




5




6




8
















Redroot pigweed




9









10




10




10




9




0




0




3




10




4




9




0




3




10




10




10




10




10




0




0




0




9




2




9




6




10
















Soybean




3




5




9




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




2




0




0




0




1




0




1




3




2




5




0






Sugarbeets




7









7




3




8




7




0




0




0




8




5




6




0




4




6




8




9




9




9




0




0




0




3




3




6




6




7
















Velvetleaf




2




7




8




2




2




5




0




0




0




7




0




0




0




5




3




8




7




10




2




0




0




0




0




0




0




5




7




0




5






Wheat




1









10




0




3




9




0




0




3




7




8




3




0




0




7




7




8




10




5




0




0




0




8




9




8




9




9
















Wild oats




8









10




8




9




9




0




0




5




9




8




6




0




0




9




7




9




10




9




0




0




0




8




9




8




9




10



























COMPOUND















































Rate 250 g/ha




7




18




30




35




36




46




47




69




70




71




72




78




86




87




93




94




103




105




107




108




109




111




113




116




117




118




119




121




122




123




124




125




129




131









Pre-emergence






Barnyardgrass




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




9






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




7






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




5






S. Flatsedge




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




8
















COMPOUND








































Rate 250 g/ha




139




146




154




165




166




177




180




181




182




183




184




185




186




187




189




190




191




192




193




194




195




196




197




198




200




201




202




203




204









Pre-emergence






Barnyardgrass




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




205




206




207




208




210




211




212




213




214




215




216




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232




233




234









Pre-emergence






Barnyardgrass




0




0




2




0




0




0




0




0




0




0




0




0




0




8




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




235




236




237




238




239




240




241




242




243




244




245




246




247




248




249




250




251




252




253




254




255




256




257




258




259




264




265




266




267









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




268




269




270




271




272




273




274




276




277




278




279




280




281




282




283




284




285




286




288




289




290




291




293




294




295




296




297




298




299









Pre-emergence






Barnyardgrass




0




0




0




9




0




4




0




8




1




0




0




0




4




9




6




4




7




0




9




3




4




4




0




9




0




0




0




0




6






Ducksalad




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




3




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0
















COMPOUND








































Rate 250 g/ha




300




301




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




318




319




320




321




322




323




324




325




326




327




328









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




8




9




0




0




0




0




0




7




0




0




0




8




3




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




329




330




331




332




333




334




335




336




337




338




339




340




341




346




350




351




353




354




358




365




366




367




368




369




370




371




372




373




374









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




9




10




9




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




2




9




0




0




0




2




0




8




0




0




0




2




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




375




376




378




379




380




381




382




383




384




385




387




388




389




390




391




392




393




394




395




401




402




403




404




405




406




407




408




409




411









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




6




0




0




8




2




9




0




0




0




0




3




9






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




5




0




0




0




0




0




2






Rice




0




0




0




0




0




0




0




0




0




0




0




0









1




0




0




0




1




0




0




2




0




7




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




8




0




0




0




0




2




9
















COMPOUND








































Rate 250 g/ha




414




437




438




439




441




442




443




444




445




446




447




448




449




450




451




452




453




454




455




456




457




458




459




460




461




462




463




465




466









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




467




468




469




470




471




472




473




474




476




477




478




479




480




482




483




465




486




487




488




489




490




492




493




494




495




496




498




499




509









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




521




528




529




531




532




538




539




546




550




552




556




558




560




561




567




568




570




577




580




586




587




588




569




590




591




592




593




594




595









Pre-emergence






Barnyardgrass




0




0




0




0




9




0




0




0




0




0




0




2




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0














0




9









0









0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




596




598




599




600




601




602




603




604




605




606




607




608




609




610




611




612




613




614




615




616




617




618




619




620




621




622




623




624




625









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




627




628




629




630




631




632




633




634




636




637




638




639




640




641




642




643




644




645




646




647




649




650




651




655




656




657




658




659




660









Pre-emergence






Barnyardgrass




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND









































Rate 250 g/ha




661




662




663




664




665




666




667




668




671




674




675




676




677




678




679




680




681




692




694




695




696




697




699




701




702




705




706




715




720









Pre-emergence






Barnyardgrass




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




8




0




0




2




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




9




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




5









0




2




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




9




0




0




0




0




0




0

















COMPOUND



















Rate 250 g/ha




721




724




740




741




758




765









Pre-emergence






Barnyardgrass




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0






Rice




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0
















COMPOUND























































Rate 250 g/ha




1




2




3




4




5




6




7




8




9




10




11




12




13




14




15




16




17




18




19




20




21




22




23




24




25




26




27




28




29




30




31




32




33




34




35




36




37




38




39




40




41




42




43




44









Postemergence






B. signalgrass




7




0




0




0




0




2




0




0




0




4




0




0




2




0




0




0




0




0




0




0




0




2




0




3




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




2




9




0




0




0




0




0




0




0




0




8




9




0




0




0




8




3




0




0




2









0














0




0




0




0






Bedstraw




0




0




0




7




4




0




0




2




0




0




0




0




0




0




0




0




3




7




7




4




0




4




0




8




7




0




0




8




0




0




0




0




2




6




3









0




0



















0




0




0






Blackgrass




0




4




0




5




5




7




2




2




0




4




0




0




3




0




0




0




4




3




0




0




0




3




0




3




6




0




0




6




0




2




9




7




5




6




1




4




0




7




0




4




3




0




0




0






Cocklebur




0




0




0




6




5




0




0




0




0




1




0




0




0




0




5




0




2




1




0




0




5




0




0




1




2




0




0




3




0




0




1




0




6




0




4




0




0




1




0




0




1




0




0




0






Corn




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




5




0




0




8




6




2




1




0




0




9




0




0




5




0




3




0




6




7




0




3




0




9




6




9




9




1




0




9




0




9




9




3




2




3




1




3




0




8




3




6




5




0




2




0






Ducksalad




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0














0




0




0




0






Giant foxtail




2




7




3




3




7




4




3




0




0




8




0




0




2




0




0




0




2




1




0




1




0




4




2




3




8




0




0




4




0




3




4




0




3




2




1




3




0




4




0




1




1




0




0




0






Morningglory




0




0




0




3




3




2









0




0




2




0




0




0




4




6




1




7




2




0




7




2




2




10




10




2




3




0




2




0




6




3




8




9




5




8




9




0




1




0




6




2




0




3




0






Nutsedge




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




4




0




0




5




7




0




0




0




0




0




0




0




0




3




2




0




2




1




2




3




0




2




0




6




0




0




0




2




0




0




0




0




3




6




9




7




0




0




0




2




3




0









0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




0




0




0









0














0




0




0




0






S. Flatsedge




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




4




0




0




0




0




0




0




0




0




0




2




2




0




0




0









0














0




0




0




0






Soybean




0




1




1




4




5




3




1




4




0




3




0




0




2




2




2




1




2




3




3




3




2




4




4




3




3




2




2




3




2




2




1




2




3




0




1




5




0




0




4




4




4




0




3




1






Sugarbeets




0




0




0




3




4




0




0




0




0




0




0




0




0




0




0




0




3




0




0









0




0




0




0




0




0




0




1




0




0




0




0




6




0









0




0




0




0




2




0




0




1




0






Velvetleaf




0




0




0




3




5




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




1




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND























































Rate 250 g/ha




45




46




47




48




49




50




51




52




53




54




55




56




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




84




85




86




87




88









Postemergence






B. signalgrass




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




6




5




0




4




0




0




4




0




0









0




0




0




0






Barnyardgrass




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




3




3




8




0




0




0




0




0




0




0











Bedstraw














6




0




5









0




8









4




0




0




0




0




0




7




6




2




3




0




0




0




7




7




5




0




0




0




7




5




0




2




0




4




7




0




2




0




0









0




6




6




9






Blackgrass




4




6




0




0




0









0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




2




0




2




0




0




0




0




0




0




7




6




0




3




3




3




4




0




0









0




1




1




6






Cocklebur




2




1




2




0




0









0




0




4




0




0




0




0




0




0




0




0




6




0




0




0




0




1




2




0




0




0




0




0




0




1




3




0




2




2




0




0




0




1









0




2




2




1






Corn




0




0




0




0




0









0




3




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




00




0




0






Crabgrass




2




3




0




3




8









3




5




6




2




0




0




0




0




2




1




0




0




0




0




0




0




0




0




1




0




0




0




2




4




9




8




0




5




4




9




8




0




0









0




5




5




9






Ducksalad




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0











Giant foxtail




9




1




0




2




9









0




3




3




3




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




2









8




7




0




3




3




3




6




0




0









0




3




3




3






Morningglory




0




1




4




0




0









0




1




5




2




2




1




1




0




1




2




4




2




4




0




1




1




2




2




0




0




0




0




4




3




1




4




0




10




7




10




2




10




0









0




7




7




10






Nutsedge




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Rape




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




3




0




0




0









0




2




2




0






Redroot pigweed




0




0




0




0




0









0




0




6




2




0




0




0




0




0




4




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




3




4




0




0




0









0




5




5




3






Rice




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




2




3




0




0




0




0




0




0




0




0




0




0




0











S. Flatsedge




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0
























0




0




0




0




0




0




4




3




0




0




0




0




0




0




0











Soybean




1




1




2




1




1









0




2




3




0




1




2




1




1




2




3




4




2




2




0




1




2




1




3




2




0




0




0




3




1




2




2




1




2




1




1




1




0




0









0




2




2




1






Sugarbeets




1




0




0




0




0









0




0




1




0




0




0




0




0




0




0




2




0




2




0




0




0




0




0




0




0




0




0




0




0




0




2




0




4




4




4




0




0




0









0




3




3




7






Velvetleaf




0




0




0




0




0









0




0




1




0




0




0




0




0




0




0




0




2




5




0




3




0




0




2




0




0




0




0




4




4




0




3




0




3




0




0




0




0




2









0




0




0




0






Wheat




0




0




2




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0









0




0




0




0






Wild oats




0




0




0




0




0









0




1




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




0




0




0




0









0




0




0




0
















COMPOUND












































Rate 250 g/ha




89




90




91




92




93




94




95




96




97




98




99




100




101




102




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120




121









Postemergence






B. signalgrass




0




0




8




7




8




0




3




0




0




0




0




0




0




0




0




0




3




0




8




3




8




0




0




0




8




5




0




9




9




2




3




7




3






Barnyardgrass




0




0














0




0




0




0




0




9




0









0




0














0




0









0




0




0




0




0




0




0




0




0




2














0




0






Bedstraw




0





























0




0




1









8




0









0




0









2




3




4




2




9




8




7




7




7




6




4




9




2




0




4
















Blackgrass




0




0




8




7




8




3




4




0




3




0




6




0




0




0




4




5




7




1




8




7




8




4




5




5




8




7




6




9




9




7




7




6




2






Cocklebur




2




3




4




2




2




1




1




0




1




0




2




0




0




0




0




2




1




2




1




0




4




2




2




2




1




0




1




3




0




0




0




3




2






Corn




0




0




3




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




3




0




0




0




5




0




0




2




6




0




0




2




0






Crabgrass




0




2




9




9




9




8




6




3




4




2




4




0




0




0




6




5




7




3




9




8




9




3




3




4




9




9




2




9




9




7




8




9




9






Ducksalad




0




0














0




0




0




0




2




3




2









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




0






Giant foxtail




0




1




8




9




9




5




1




0




3




2




2




0




0




0




3




4




7




3




8




8




9




5




5




7




9




9




5




9




9




9




8




8




7






Morningglory




0




4




8




10




10




10




2




1




3




2




3




0




1




1




10




10




3




8




3




3




5




5




5




10




8




4




6




4




7




5




7




8




6






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




4




0




0




0




0




0




0




0




8




7




0




0




0




0






Rape




0




0




4




4




4




2




0




0




0




0




4




0




0




0




1




0




0




0




3




0




4




4




3




3




7




3




0




8




2




0




2




0




2






Redroot pigweed




0




6




6




4




7




2




3




0









0




5




0




0




0




2




3




0




0




5




0




8




5




4




5




6




3




0




8




0




0




2




0




3






Rice




0




0














0




0




2




0




0




6




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0









0




2




0






S. Flatsedge




0




0














0




0




0




0




0




8




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




5






Soybean




0




4




4




3




5




5




1




1




1




1




3




0




3




0




4




5




3




1




4




5




7




5




4




4




7




5




4




6




5




2




4




4




6






Sugarbeets




0




3




6




6




3




2




4




0




0




0




4




0




0




0




2




1




0




0




5




2




6




3




3




3




5




4




3




8




3




0




0




0




4






Velvetleaf




0




0




3




0




0




4




0




0




2




0




3




0




0




0




1




3




3




2




5




4




6




1




0




1




7




3




0




7




6




0




3




2




4






Wheat




0




0




4




5




4




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




5




0




0




0




4




0




0




7




6




0




3




0




0






Wild oats




0




0




3




1




2




0




0




0




0




0




0




0




0




0




0




0




2




0




5




3




4




0




1




0




6




2




0




7




4




0




3




0




0
















COMPOUND








































Rate 250 g/ha




122




123




124




125




126




127




128




129




130




131




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149




150









Postemergence






B. signalgrass




0




3




0




0




0




0




0




4




7




8




4




2




0




0




1




5




8




6




0




0




0




0




1




0




8




8




5




0




0






Barnyardgrass




0




0




0




0




0




0




0


































0




0




0




8




0




2




0




2




8




0




7




1




6




0




0




0






Bedstraw
























0




0




0




3




6




9




2




7




4




2




8




8




8




5




5




2




3




6




3




3




7




7




6




0




0






Blackgrass




4




6




0




0




0




0




0




3




7




8




8




2




0




0




3




8




9




7




4




0




0




5




5




5




8




8




7




0




0






Cocklebur




3




0




0




0




0




0




0




0




0




5




0




2




0




0




2




3




2




2




3




0




0




3




0




0




3




0




0




0




0






Corn




0




0




0




0




0




0




0




2




2




6




4




0




0




0




0




3




7




2




0




0




0




0




0




0




0




6




0




0




0






Crabgrass




4




8




0




0




0




0




0




8




9




8




8




4




4




0




8




9




9




9




9




4




4




8




9




8




9




9




8




0




2






Ducksalad




0




0




0




0




0




0




0


































0




0




0




2




0




0




0




0




0




0




0




5




0




0




0




0






Giant foxtail




6




8




0




0




0




0




0




9




9




9




9




3




0




0




7




9




9




9




4




0




2




5




5




2




9




8




8




0




2






Morningglory




4




10




0




2




0




0




0




8




2




8




6




4




8




1




10




7




6




6




8




3




4




8




2




10




8




3




3




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




3




6




0




0




0




0




0




0




0




0




0




0




0




0






Rape




3




0




0




0




0




0




0




0









7




0




0




0




0




2




6




2




2




1




0




0




0




0




3




3




4




3




0




0






Redroot pigweed




2




2




0




0




0




0




0




2




3




8




0




0




0




0




6




5




7




4




2




2




0




5




0




0




6




5









0




0






Rice




0




0




0




0




0




0




0


































0




0




0




8




0




2




0




2




2




0




0




2




2




0




0




0






S. Flatsedge




0




0




0




0




0




0




0


































0




0




0




7




0




0




0




0




2




0




5




3




3




0




0




0






Soybean




3




4




4




4




0




0




0




4




3




8




4




3




1




3




4




7




4




4




3




3




3




4




3




4




6




6




4




0




1






Sugarbeets




0




1




0




0




0




0




0




0




2




6




0




0




0




0




7




5




6




2




0




0




0




6




0




0




4




2




4




0




0






Velvetleaf




3




0




0




0




0




0




0




0




5




8




3




2




0




0




0




4




4




5




0




0




2




2




0




0




6




0




0




0




0






Wheat




0




1




0




0




0




0




0




2




3




5




2




0




0




0




0




5




8




4




0




0




0




0




0




0




5




5




3




0




0






Wild oats




0




0




0




0




0




0




0




2




5




9




2




0




0




0




0




4




3




4




0




0




0




0




0




0




6




5




5




0




0

















COMPOUND









































Rate 250 g/ha




151




152




153




154




155




156




157




158




159




160




161




162




163




164




165




166




167




168




169




170




171




172




173




174




175




176




177




178









Postemergence






B. signalgrass




6




0




0




0




0




0




0




0




0




0




2




0




5




0




5




0




0




0




0




9




0




0




0




0




0




0




0




0






Barnyardgrass




0




0




0




0




0




0




0




0




0




0



















0
























0




0




0
























0




0











Bedstraw




4




0




0




0




0




0




0




0




0




0




4




3




7









4




1




8




8




7




0




8




8




4




6




0




2




5




0






Blackgrass




8




0




0




0




2




0




0




2




0




0




3




0




6




0




7




7




5




2




5




9




0




5




2




0




0




0




0




0






Cocklebur




2




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




2




0




0




3




0




1




2




2




2




0




0






Corn




2




0




0




0




2




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




9




2




0




1




8




0




2




3




0




0




7




6




8




2




9




3




9




2




9




9




2




9




5




7




0




3




2




0






Ducksalad




0




0




0




0




0




0




0




0




0




0



















0
























0




0




0
























0




2











Giant foxtail




8




0




0




1




6




0




4




4




0




0




3




2




8




0




5




1




0




1




6




8




0




0




0




0




0




0




0




0






Morningglory




6




0




0




1




2




2




1




2




3




0




7




10




5




0




3




2




5




10




5




1




2




5




10




5




3




2




2




2






Nutsedge




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




5




0




0




2




0




0




0




2




0




0




4




0




3




0




4




2




3




0




0




6




0




3




0




6




0




0




0











Rice




0




0




0




0




0




0




0




0




0




0



















0
























0




0




0
























0




0











S. Flatsedge




0




0




0




0




0




0




0




0




0




0



















0
























0




0




0
























0




0











Soybean




4




1




0




2




1




1




1




4




3




0




4




4




3




2




6




2




3




2




3




4




1




3




2




2




1




2




2




2






Sugarbeets




3




0




0




0




0




0




0




0




0




0




4




0




4




0




3




0




0




0




0




2




2




0




0




6




0




0




0




0






Velvetleaf




3




0




0




0




0




0




0




0




0




0




2




4




6




0




1




0




0




1




0




5




0




0




0




0




3




2




0




0






Wheat




4




0




0




0




0




0




0




0




0




0




0




0




2




0




2




0




0




0




0




6




0




0




0




0




0




0




0




0






Wild oats




6




0




0




0




0




0




0




0




0




0




0




0




3




0




3




0




0




0




0




3




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




179




180




181




182




183




184




185




186




187




188




189




190




191




192




193




194




195




196




197




198




199




200




201




202




203




204




205




206




207









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass








































































































0














































Bedstraw




5




0




0




0




7




3




3




8




0




3




0




0




0




0




0




0









0




0




0




0




0




0




4




0




6




0




0




5






Blackgrass




4




0




0




0




0




3




0




4




0




0




0




0




0




0




0




2




5




0




0




0




9




0




0




5




0




3




0




0




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




2




2




0




0




0




0




0




0




2




0




1




1




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




2




0




0




0




0




0









2




0




3




0




0




3




1




0




0




2




0




0




0




8




2




0




1




0




2




1




0




2






Ducksalad








































































































0














































Giant foxtail




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




2




1




0




0




0




2




0




0




0




0




0




0




0




1






Morningglory




5




0




0




0




1




6




1




2




0




0




0




0




2




6




1




1




1




0




5




2




4




2




1




8




0




3




1




2




2






Nutsedge




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0






Rape




0




0




0




0




0




3




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0






Redroot pigweed




4




0




0




0




0




7




3




0




0




0




0




0




0




3




0




0




2




0




0




0




2




0




0




6




0




4




0




3




0






Rice








































































































0














































S. Flatsedge








































































































2














































Soybean




1




0




0




0




2




3




3




2




0




2




0




0




3




3




1




0




4




0




0




0




7




2




2




3




0




1




2




2




2






Sugarbeets




2




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




4




0




0




0




0




0






Velvetleaf




0




0




0




0




0




1




0




0




0




0




0




0




2




3




0




0




2




0




0




0




0




1




1




0




0




1




0




0




1






Wheat




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




208




210




211




212




213




214




215




216




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237









Postemergence






B. signalgrass




0




0




0




7




2




0




3




5




7




3




5




8




8




0




0




0




5




6




0




0




0




0




0




1




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




4









2




3




2




6




2




0









8




8




9




4




4




4




0




5




8




0




0




0




0




2




3




0




0




0




2






Blackgrass




0




0




4




6




2




4




4




8




6




7




8




8




9




3




3




3




9




8




7




0




0




0




0




6




2




0




0




0




0






Cocklebur




0




0




0




2




0




0




0




0




0




3




4




3




0




0




0




0




0




0




2




0




0




0




0




2




2




0




0




0




0






Corn




0




0




0




0




0




0




0




2




0




0




4




6




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




1




8




2




3




2




4




3




5




6




7




8




0




1




3




g




3




0




0




0




0




0




1




1




0




0




0




0






Ducksalad























































































































































Giant foxtail




0




0




2




6




2




0




3




4




7




7




8




8




7




0




0




4




8




7




0




0




0




0




0




2




3




0




0




0




0






Morningglory




1




3




6




4




7




6




3




7




0




8




7




8




0




3




4




5




6




7




8




3




0




2




3




8




3




1




6




5




3






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




2




0




3




3




0




0




0




6




7




3




4




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0






Redroot pigweed




0




2




4









7




1




6




2




0




3




8




3




8




0




3




4




0




0




5




0




0




0




0




6




2




0




0




0




2






Rice























































































































































S. Flatsedge























































































































































Soybean




2




1




4




3




2




3




1




1




1




6




7




7




3




3




3




4




5




3




4




1




1




4




1




4




3




0




0




2




1






Sugarbeets




0




0




2




0




4




0




0




0




0




2




4




2




4




0




2




4




3




0




3




3




0




0




0




2




0




0




0




0




0






Velvetleaf




1




2




1




5




0




0




0




0




0




2




2




2




0




2




2




0




0




0




0




0




0




0




0




2




3




0




0




1




0






Wheat




0




0




0




0




2




3




6




0




3




0




7




6




4




0




0




0




7




7




3




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




2




0




2




0




0




1




4




2




2




0




0




0




3




0




0




0




0




0




0




0




2




0




0




0




0
















COMPOUND








































Rate 250 g/ha




238




239




240




241




242




243




244




245




246




247




248




249




250




251




252




253




254




255




256




257




258




259




260




261




262




263




264




265




266









Postemergence






B. signalgrass




0




0




0




4




8




9




0




6




0




0




0




0




0




0




0




0




0




2




0




0




4




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




8




3




3




7




7




5




0




9




9




0




0




0




9




7




0




0




4




2




0




0




7





























6




3




5






Blackgrass




0




2




0




8




9




9




0




7




6




0




0




0




2




8




5




0




0




7




0




1




7




0




0




0




0




3




3




5




6






Cocklebur




0




1




1




1




7




4




0




0




1




0




0




0




1




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




2






Corn




0




0




0




0




0




5




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




2




2




2




8




9




9




0




8




0




0




0




0




0




6




6




0




0




2




1




2




2




0




0




0




0




0




0




2




3






Ducksalad























































































































































Giant foxtail




0




1




0




6




8




8




0




8




5




0




0




0




0




7




4




0




0




6




0




0




4




0




0




0




0




0




0




2




5






Morningglory




3




3




10




5




7




7




0




9




9




2




0




0




6




7




3




0




9




8









8




7




7




3




6




5




4




10




6




5






Nutsedge




0




0




0




0














0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




4




0




0




2




4




2




0




2




0




0




0




0




3




0




0




0




2




3




2




2




0




0




0




0




0




0




0




1




6






Redroot pigweed




0




3




2




0




4




7




0




9




2




0




0




0




0




2




0




0




3




2




4




4




2




6




3




1




3




0




0




3




5






Rice























































































































































S. Flatsedge























































































































































Soybean




1




1




2




3




6




5




0




4




3




0




0




4




2




4




1




0




2




6




4




3




5




4




1




4




3




1




3




3




7






Sugarbeets




0




0




0




0




5




2




0




3




0




0




0




0




3




0




0




0




0




0




3




2




0




2




2




0




0




0




1




3




3






Velvetleaf




2




3




1




0




7




4




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




1




1




1




1




0




0




2




5






Wheat




0




0




0




4




8




7




0




6




2




0




0




0




0




0




0




0




0




4




0




0




4




3




0




0




0




0




0




0




5






Wild oats




0




0




0




0




4




3




0




5




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




267




268




269




270




271




272




273




274




276




277




278




279




280




281




282




283




284




285




286




288




289




292




293




294




295




296




297




298




299









Postemergence






B. signalgrass




0




0




0




0




2




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




3




0




7




0




5




0




0




0




7






Barnyardgrass























































































































































Bedstraw




4




0




4




0




8




0




0




0




3




8




6




0




0









7




5




6




7




5




0




8




0




3




8




4




0





















Blackgrass




5




0




2




0




8




2




2




0




4




8




0




2




0




0




5




7




7




7




5




2




9




0




9




7




9




0




0




0




8






Cocklebur




1




0




1




0




1




1




0




0




0




1




0




0




0




0




2




2




2




0




0




1




2




0




0




0




0




0




0




0




4






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3






Crabgrass




3




0




0




0




1




0




1




0




6




5




0




0




0




0




0




1




1




7




2




3




9




0




9




2




8




0




0




0




4






Ducksalad























































































































































Giant foxtail




2




0




0




0




4




0




0




0




4




4




0




0




0




0




0




4




3




0




2




0




7




0




8




2




9




0




0




0




8






Morningglory




3




2




5




0




8




1




2




0




6




8




4




2




0




3




7




9




7




5




8




8




8




2




5




9




7




1




0




3




6






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0






Rape




0




0




0




0




4




0




0




0




0




3




0




0




0




0




6




4




4




0




5




3




2




0




0




2




3




0




0




0




7






Redroot pigweed




0




0




5




0




7




2




2




1




1




4




0




2




0




5




7




5




6




0




6




0




7




0




2




0




7




0




0




0




6






Rice























































































































































S. Flatsedge























































































































































Soybean




3




0




3




2




5




1




3




5




6




6




1




2




3




3




4




5




4




3




2




2




4




1




2




4




4




1




3




3




6






Sugarbeets




2




0




0




0




4




0




0




0




2




4




0




0




0




0




7




2




5




3




2




0




0




0




3




0




0




0




0




0




4






Velvetleaf




1




0




3




0




0




0




0




0




0




1




0




0




0




1




3




1




2




1




0




1




3




0




2




0




5




0




0




0




6






Wheat




3




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




7




0




7




0




3




0




0




0




6






Wild oats




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




3




0




3




0




2




0




0




0




3
















COMPOUND








































Rate 250 g/ha




300




301




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




318




319




320




321




322




323




324




325




326




327




328









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0









0



















0




0




0




0




7




0




0




7









6









8




0














8




4









0









7




7




4






Blackgrass




0




0




0




0




0




0




0




0




0




0




9




0




0




0




5




5




4




8




0




0




0




0




1




0




0




3




0




3




5






Cocklebur




0




0




0




0




0




0




0




0




0




0




2




0




0




0




1




0




0




0




5




0




0




0




0




0




2




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




2




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




0




0




0




0




9




0




0




0




4




5




0




8




0




0




0




2




2




0




0




0




1




0




0






Ducksalad























































































































































Giant foxtail




0




0




2




0




0




0




0




0




0




0




8




0




0




0




3




4




2




8




0




0




0




1




1




0




0




0




0




0




0






Morningglory




0




0




2




0




3




0









2




2




2




7




8




0




3




3




0




5




3




3




4




3




8




7




2




0




8









8




10






Nutsedge




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




1




0




0




3




0




0




0




0




0




1




2




0






Redroot pigweed




0




0




2




2




5




4




0




0




0




0




3




0




0




2




0




0




3




3




0




0




6




4




3




0




0




4




4




6




3






Rice























































































































































S. Flatsedge























































































































































Soybean




2




0




3




3




5




4




2




2




1




2




4




3




3




3




4




3




4




6




1




1




3




3




4




2




1




1




5




6




5






Sugarbeets




0




0




1




0




0




0




0




0




0




0




2




0




0




0




0




0




0




1




0




0




2




5




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




6




0




0




0




3




0




2




5




0




0




0




0




0




0




0




2




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




3




0




0




0




2




0




2




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




329




330




331




332




333




334




335




336




337




338




339




340




341




342




343




344




345




348




349




350




351




352




353




354




355




356




357




358




359









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




4




0




0




0




7




0




0




0




1




4




1




0






Barnyardgrass





































































9




0




0




0




3




9




3




3




3









7




8




7




4




9




0






Bedstraw



















0




0









0




0




2




2




7




7




4




5




0




0




0




4



















2














0




3




0




3




0






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




3




2




2




5




0




0




6




4




7




4




8




4




7




6




6




6




8




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




2




0




0




0






Crabgrass




0




0




0




1




0




0




0




0




0




0




0




0




0




0




3




0




0




6




1




7




4




3




2




2




2




0




2




4




0






Ducksalad





































































2




0




0




0




3




0




3




4




2









3




0




2




0




5




0






Giant foxtail




0




0




0




0




0




0




0




0




0




0




0




0




0




2




6




0




0




9




5




8




8




9




7




8




4




7




9




8




0






Morningglory




0




0




0




0




0




0




0




0




0




0




8




10




8









4




0




0




10




10




6




6




7




4




7




7




6




6




7




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




2




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




3




6




2




4




0




0




0




0




0




0




2




0




2




3




0




0




0




2




0






Redroot pigweed




0




0




0




3




0




0




0




0




0




0




4




6




3




5




3




0




0




2




3




2




3




3




4




4




0




0




5




4




0






Rice





































































0




0




0




0




0




0




0




0




3









0




0




0




2




0




0






S. Flatsedge





































































7




0




0




0




6




7




7




6




7









8




8




7




0




9




0






Soybean




1




1




0




2




2




0




2




1




1




2




2




2




2




6




3




2




0




3




2




1




2




4




6




7




2




3




2




5




2






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




3




1




0




0




0




2




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




1




0




2




0




0




5




0




0




2




2




2




0




0




0




3




2




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




3




3




0




2




4




0




0




2




3




6




3




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




3




2




3




2




2




0




0




5




3




5




5




0
















COMPOUND








































Rate 250 g/ha




360




361




362




363




364




365




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388




389




390




391









Postemergence






B. signalgrass




5




3




7




1




0




0




0




6




0




4




3




4




0




0




2




0




0




0




0




0




0




0




6




6




3




8




0




5




0






Barnyardgrass




6



















0



















0




0









4



























































































Bedstraw




2




8




9




7




0














4












































0




0









0




4




0




0




0




0









5
















Blackgrass




6




8




8




7




0




0




0




8




5




4




6




7




0




0




5




0




0




0




0




0




2




2




9




2




7









6




9




0






Cocklebur




0




0









2




0




0




0




3




0




2




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0






Corn




6




0




0




2




2




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




5




2




6




5




0




0




8




8




2




7




8




8




1




0




7




0




0




0




2




0




0




4




8




9




2




8




4




7




0






Ducksalad




0



















0



















2




3









6



























































































Giant foxtail




8




5




9




9




6




0




8




9




2




8




8




9




3




2




8




0




3




2




9




0




3




6




9




9




3




8




7




9




0






Morningglory




4




7




1




1




0




0




6




5




10




10




7




7




8




10




5




0




10




8




5




2




0




0




0




2




1




4




8




7




0






Nutsedge




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




3




0






Rape




0




3




0




0




0




0




0




2




0




2




0




3




2




2




0




0




0




0




0




0




0




0




0




0




0









2




10




0






Redroot pigweed




3




6




6




2




0




0




0




4




0




0




2




6




4




2




0




0




0




1




0




0




0




0




0




0




0




0




0




9




0






Rice




3



















0



















0




2









2



























































































S. Flatsedge




4



















0



















2




4









8



























































































Soybean




2




5




6




6




3




2




1




5




1




3




1




2




4




2




1




0




0




1




1




2




4




3




3




2




0




1




2




3




0






Sugarbeets




2




5




2




3




0




0




0




2




0




0




0




2




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0






Velvetleaf




0




0




7




3




0




0




2




3




0




0




2




2




1




0




2




0




0




0




0




0




0




0




0




0




0




2




0




7




0






Wheat




4




0




6




5




0




0




0




4




0




0




0




0




0




0




2




0




0




0




0




0




0




0




2




0




0




3




0




3




0






Wild oats




3




6




6




1




0




0




0




3




0




3




3




5




0




0




6




0




0




0




0




0




0




0




0




2




0




0




0




7




0
















COMPOUND








































Rate 250 g/ha




392




393




394




395




396




397




398




400




401




402




403




404




405




406




407




408




409




410




411




414




415




416




417




418




419




420




421




422




423









Postemergence






B. signalgrass




7




0




2




0




0




2




2




3




0




2




3









0




0




0




0




8




5




5




1




2




8




0




0




0




5




7




0




0






Barnyardgrass
























0




0




0




0
































































0




0




0




0




0




0




2




0




0






Bedstraw














5




0





























7









8



















8




2









7



















0









0




3




7
















Blackgrass




10




3




9




0




3




9




9




8




0









10




10




0




0




0




9




9




9




9




5




8




9




0




4




0




6




8




0




0






Cocklebur




2




0




0




0




0




0




0




0




0




4




0




2




0




0




0




0









0




3




0




1




0




0




0




0




0




1




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




1




5




0




0




0




0




3




0




0






Crabgrass




7




5




8




2




2




9




9




6




2




5




8




5




0




0




1




8




9




8




8




6




8




9




2




3




0




8




8




0




0






Ducksalad
























0




0




0




0
































































0




0




2




2




0




0




2




0




0






Giant foxtail




9




9




8




5




2




9




9




9




2




9




9




9




0




0




3




9




9




9




9




6




9




9




1




8




1




8




9




0




0






Morningglory




7




0




6




0




8




5




3




3




6




8




8




7




5




2




10




7




9




8




6




7




6




9




9




8




5




4




9




0











Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




3




0




0




0




0




2




0









8




4




4




0




0




0









3




7




7




0




0




3




0




0




0




0




3




0




0






Redroot pigweed




6




0




2




0




0




4




3




0




1




5




1




5




0




0




0




0




4




0




7




0




0




2




0




0




0




0




5




0




0






Rice
























0




0




0




0
































































0




0




0




0




0




0




2




0




0






S. Flatsedge
























0




0




0




0
































































3




0




9




4




0




0




0




0




0






Soybean




2




2




5




1




3




5




4




4




1




6




6




6




2




2




2




3




5




5




5




2




4




6




4




4




3




3




7




3




2






Sugarbeets




0




0




1




0




0




0




0




0




0




2




0




1




0




0




0




0




0




7




4




0




0




0




0




0




0




0




3




0




0






Velvetleaf




2




0




0




2




0




0




0




0




0




4




0




0




0




0




0




0




0




0




4




0




2




0




0




0




0




0




4




0




0






Wheat




0




0




3




0




0




2




0




0




0




0




1




0




0




0




0




1




4




0




4




0




2




5




0




0




0




0




5




0




0






Wild oats




7




0




6




0




0




2




0




0




0




0




2




5




0




0




0




2




0




5




3




0




2




4




0




0




0




0




4




0




0
















COMPOUND








































Rate 250 g/ha




424




425




426




427




428




429




430




431




432




433




434




435




436




437




438




439




440




441




442




443




444




445




446




447




448




449




450




451




452









Postemergence






B. signalgrass




0




7




7




0




0




0




6




0




0




3




0




1




0




0




0




0




2




0




0




0




4




0




6




0




0




0




0




0




0






Barnyardgrass




0




1




0




0




2




1




0




0




0




0




0




0




0



















0


































































Bedstraw




0









9



















0














5









0




0




0




0









2







































0


























Blackgrass




0




8




8




0




3




3




7




2




4




7




0




6




0




0




2




0




4




0




0




0




5




0




8




0




0




0




2




2




3






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




2




0




0




0




2




0




0




0






Corn




0




0




2




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




8




9




1




0




2




8




0




6




4




1




7




1




1




8




0




9




0




0




0




9




3




9




0




0




2




4




4




6






Ducksalad




0




0




0




0




3




6




0




0




0




0




0




0




0



















0


































































Giant foxtail




0




8




9




3




0




2




9




0




6




6




1




8




1




0




9




0




9




0




0




0




8




1




9




0




0




0




7




3




7






Morningglory




0




6




9




0




2




2




3




1




1




4




1




6




2




4




9




0




8




0




7




4




1




4




3




4




2




5




1




1




2






Nutsedge




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0






Redroot pigweed




0




2




5




0




0




0




3




0




0




2




0




2




0




0




0




0




3




0




0




0














0




0




0




2




0




0




0






Rice




0




0




0




0




2




0




0




0




0




0




0




0




0



















0


































































S. Flatsedge




0




2




0




0




0




3




0




0




0




0




0




0




0



















0


































































Soybean




1




2




6




1




2




2




3




1




2




2




1




1




0




0




2




0




6




0




0




1




2




1




4




2




2




2




1




1




1






Sugarbeets




0




3




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




1




2




2




2




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




3




2




0




0




0




2




0




0






Wheat




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0






Wild oats




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




453




454




455




456




457




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




481




482




483









Postemergence






B. signalgrass




2




0




1




0




0




0




0




0




0




0




0




0




3




0




0




2




0




4




2




0




1




0




5




5




3




5




6




0




0






Barnyardgrass























































































































































Bedstraw


































6





























4














6
























8



















0




0









0











Blackgrass




6




2




9




4




0




8




8









0




0




0




6




8




0




7




9




0




3




2




0




8




0




6




8




4




3




2




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




3




0




0






Crabgrass




4




3




4




4




0




8




5




9




0




0




2




5




9




0




9




9




0




8




8




3




6




0




5




8




6




7




2




1




0






Ducksalad























































































































































Giant foxtail




7




8




7




3




0




9




2




0




0




0




6




5




9




2




9




9




0




7




8




6




7




0




6




8




6




8




8




0




0






Morningglory




2




10




8




5




0




3









7




7




0




2




2




2




7




4




10




0




4




4




2




1




0




10




7




10




7




2




8




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0






Redroot pigweed




0




2




5




3




0




0




0




1




0




0




0




0




3




3




4




2




0




2




3




0




2




0




2




3




2




1




0




2




0






Rice























































































































































S. Flatsedge























































































































































Soybean




1




2




4




2




1




2




6




4




3









1




1




4




0




1




4




1




3




2




1




4




2




2




2




3




3




4




1




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




3




0




0




0




0




0




0




0




0




3




0




0




2




0




0




2




2




0




0




2




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




2




0




0




0




0




0






Wild oats




0




0




0




0




0




2




0




0




0




0




0




0




0




2




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 250 g/ha




485




486




487




488




489




490




492




493




494




495




496




497




498




499




500




501




504




505




506




508




509




510




511




512




513




514




515




516




517









Postemergence






B. signalgrass




4




1




0




6




6




4




0




0




0




0




0




0




0




0




7




7




8




8




0




3




2




4




0




4




6




3




0




3




6






Barnyardgrass























































































































































Bedstraw




2




4




6




4




5





























0



















9












































7































Blackgrass




7




8




0




8




8









0




0




0




0




3




0









2




6




6




7




7




5




6




6




5




0




6




8




5




0




7




6






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




2




3




2




6




0




2




4




0




4




0




3




6




3




3




3




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




4




2




6




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




7




5




5




8




8




6




0




0









0




0




0




0




0




8




9




9




9




7




9




9




8




7




5




6




9




9









8






Ducksalad























































































































































Giant foxtail




8




8




4




9




9




8




0




0




0




0




0




0




2




0




8




9




9




9




4




8




8




8




5




7




8




9




9




8




9






Morningglory




10




2




10




8




10




3




8




0




0




2




8




0




3




4




3




3




4




5




3




4




2




5




4




6




6




7




6




6




2






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




2




0




0









0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




7




7




2




2




8




3




6




1




0




4




6




5




8




0






Redroot pigweed




0




0




2




1




0




0




4




0




0




0




3




0




0




0




8




5




9




0




0




7




0




8




7




8




6




6




5




8




4






Rice























































































































































S. Flatsedge























































































































































Soybean




4




4




5




5




5




5




0




2




1




0




3




2




1




2




4




3




6




6




4




5




5




7




4




5




8




7




7




7




6






Sugarbeets




0




0




0




1




0




0




0




0




0




0




0




0




0




0




9




7




7




5




6




8




4




6









2




6




4




3




7




2






Velvetleaf




0




2




0




0




0




1




0




0




0




0




0




0




0




0




5




3




6




4




2




1




5




6




2




1




5




5




5




4




0






Wheat




1




1




0




3




0




0




0




0




0




0




0




0




0




0




3




2




5




4




2




0




0




0




0




0




6




0




0




5




3






Wild oats




0




0




0




0




1




5




0




0




0




0




0




0




0




0




2




3




7




3




0




2




4




2




0




1









0




0




5




0
















COMPOUND








































Rate 250 g/ha




518




519




520




521




522




523




524




525




526




527




528




531




532




533




534




535




536




540




541




543




544




545




546




548




549




550




551




552




553









Postemergence






B. signalgrass




7




0




0




0




7




2




2




2




4




0




0




0




0









0




0




0




0




0




3




0




2




0




0




0




2




2




0




3






Barnyardgrass























































































































































Bedstraw









0














9









9



















0




0




0



















0




10




5









2




2




9




9




0




0




4




10




2






Blackgrass




7




0




0




7




8




3




9




8




9




4




0




0




0









7




7




0




2




0




0




0




0




3




3




2




2




7




0




3






Cocklebur




0




0




0




0




3




2




0




2




0




2




2




2




2




2




0




0




0




0




5




0




3




8




0




0




0




1




0




2




0






Corn




0




0




0




0




3




2




3




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




10




6




4




10




8




6




8




9




9




9




9




9




7




9




4




5




5




5




0




3




8




3




7









6




10




8









8






Ducksalad























































































































































Giant foxtail




2




4




4




9









4




8




9




7




8




3




9




4




9




4




5




0




0




0




0




6




3




4




0




2




9




5




3




6






Morningglory




8




0




4




3




4




4




2




2




6




5




5




4




5




7




2




2




2




5




1




4




10




10




5




8




4




9




4




2




0






Nutsedge














0




0




0




0









5




0




0




0




0









0




2




0




0




0




0




0




0














0









0









0




0






Rape




7




0




0




2




0




2




0




3









0




3




0




2









0




0




0




7




3




0




2




0




7




7




5









7




4




7






Redroot pigweed




0




0









0




4




3




0




9




2




0




0




0




0









3




0




0




2




0




0




0




0




0




2




0




0




3




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




5




4




4




5









5




3




5




3




4




5




6




5




4




6




6




4




1




1




2




0




2




2




2




2




3




3




3




3






Sugarbeets




3




0




0




0




6




0




0




6




0




0




0




0




0









3




0




0




6




0




2




1




0




4




3




0




2




5




3




0






Velvetleaf




4




4




4




2




7




3




5




3




7




3




4




0




2




4




2




0




0




0




0




0




0




6









0




4




0




3




2




5






Wheat




0




0




0




0




5




0




0




5




0




0




0




0




0









3




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Wild oats




2




0




0




0




7




0




0




4




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




4




0




0




2
















COMPOUND








































Rate 250 g/ha




554




555




556




557




558




559




560




561




562




563




564




565




566




567




568




569




570




571




572




573




574




575




576




577




578




579




580




581




582









Postemergence






B. signalgrass




0




0




4




2




0




9




6




6




5




5




3




0




8




0




7




0




0




0




0




0




0




0




0




0




0




2




5




7




0






Barnyardgrass























































































































































Bedstraw




7




9




0




0




0




0




0









4
























0
























0



















5














10




0









9






Blackgrass




7




2




3




0




2




7




7




6




3




4




4




0




3




0




8




2




0




0




0




0




6




0




2




0




0




2




7




4




3






Cocklebur




0




0




0




0




0




0




0




0




2




0




0




2




2




0




1




2




0




0




0




2




2




0




0




0




0




0




3




3




2






Corn




0




0




0




0




0




6




2




0




7




4




0




0




2




0




4




0




0




0




0




0




0




0




2




0




0




0




0




5




0






Crabgrass




9




9




2




4




8




9




3




4




7




8




8




0




10




7




9




6




0









6




9









9




9




3




4




6




9




7




3






Ducksalad























































































































































Giant foxtail




8




8




9




6




5




9




7




7




8




8




7




0




8




0




9




4




0




2




0




9




6




8




7




2




7




5




8




8




9






Morningglory




5




5




4









10




9




9




5




10




10




10




7




6




4




10




10




10




10




5




10




10




9




4




10




10




10




8




7




10






Nutsedge




0




0




0




0




0




2




3









5




0




0




0














0




0




0




0




0




0




0




0




0














0





















Rape




0









0




0




0




2




4




4




0




5




2




0




9




0




2




0




0




0




3




3




0




3




0




0




4




0




7




7




0






Redroot pigweed




7




2




3




0




0




3




8




0




9




5




3




6









0




0




4




0




0




0




4




0




4




0




0




3




0




5




8




7






Rice























































































































































S. Flatsedge























































































































































Soybean




3




2




3




0




4




5




2




3




4




3




5




3




6




4




6




4




3




2




5




4




6




5




3




3




3




3




4




4




3






Sugarbeets




7




0




0




0




2




2




0









3




0




2




0









0




1




0




0




0




0




0




0









0




0




0




0




5




7




3






Velvetleaf




0




2




0




0




0




2




0




0




6




2




2




4




5




0




5




2




0




0




0




0




2




2




0




0




4




0




2




6




0






Wheat




2




0




2




0




0




2




3




3




7




0









0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




4




0






Wild oats




2




0




2




0




0




4




2




2




0




0









0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




3




5




0
















COMPOUND








































Rate 250 g/ha




584




585




586




587




588




589




590




591




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609




610




611




612




613









Postemergence






B. signalgrass




7




0




3




0




4




0




0




0




0




0




2




6




0




0




0




0




4




5




0




0




0




0




4









5




7




7




7




6






Barnyardgrass























































































































































Bedstraw




9









0





































































3




3



















0



















4




6




6




8






Blackgrass




7




6




3




3




6




2




0




0




0




0




5




9




0




0




0




0




7




8




0




0




0




0




6




8




8




9




9




9




9






Cocklebur




4




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




2




0




2






Corn




3




0




2




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




2




2




4




0




0






Crabgrass




6




9




8









6




1




0




0




0




0




9




9




0




0




0









5




4




0




3




1




3




8




7




9




9




9




9




9






Ducksalad























































































































































Giant foxtail




9




8




8




0




8




0




0




0




0




0




7




9




0




0




0




0




7




9




0




3




0




0




7




7




9




9




9




9




9






Morningglory




5




10




10




6




10




5




3




2




2




0




2




3




0




0




1




0




1




2




2




2




9




10




8




8




10




8




8




8




8






Nutsedge




0




0




0




0














0




0




0




0




3




0









0









0




0




0




0




0




0









0




0




0




5




3




0




2






Rape




9




5




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




3




0




5




1




3




2




0




3






Redroot pigweed




2




3




0




0




0




2




0




0




0




0




3




3




0




0




0




0




2




3




0




0




0




1




0




7




2




6




3




4




7






Rice























































































































































S. Flatsedge























































































































































Soybean




3




4




3




6




4




3




3




2




1




0









4




2




0




2




3




5




5




2




1




3




2




6




4









8




8




7




6






Sugarbeets




5




4




0




0




0




0




0




0




0




0




5




3




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0






Velvetleaf




3




4




0




0




0




5




2




0




0




0




3




7




0




0




0




0




0




0




0




0




0




0




3




4




7




7




5




3




5






Wheat




3




2




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




1




0




2




0




2




4




2




2




2






Wild oats




2




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




1




0




0




5




0




5




4




6




9
















COMPOUND








































Rate 250 g/ha




8 614




615




616




617




618




619




620




621




622




623




624




625




627




628




629




630




631




632




633




634




635




636




638




639




640




641




642




643




644









Postemergence






B. signalgrass




0




0




1




0




0




0




0




0




0




0




7




2




7




8




3




1




6




2




0




0




2




0




6




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




3









0














0












































8














0




0




0




9




9









































Blackgrass




0




0




0




0




0




0




0




0




0




4




8




7




9




9




8




3




6




6




4




8




7




3




6




2









2




6




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




2




0




0




6




0




0




0




0




0




2




3




3




2




2




2




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




2




0




7




7




4




2




6




3




0




0




0




2




2




0




0




0




0




0




0






Crabgrass




5




4




4




2




0




0



















0




7




4




9




9




8




8




9




8




3




7




8




9




8




2




3




3




0




0




0






Ducksalad























































































































































Giant foxtail




2




6




3




4




0




0




0




1




6




0




8




5




9




9




9




8




9




8




3




9




8




9




8




6




0




3




4




0




0






Morningglory




2




1




4




0




0




1




2




2




2




8




1




1




6




2




3




2




4




2




5




2




4




6




3




7




6




7




0




4




0






Nutsedge




0




0




0









0




0




0




0




0




0




0




0




6









0









0




0




0














0














0




4




0




0











Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




2




0




0




0




7




7




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




1




0




0




0




0




2




0




6




7




2




1









0




1




2




3




6




0




4




4




3




0




0




3






Rice























































































































































S. Flatsedge























































































































































Soybean




4




3




4




3




6




1




1




5




6




0




7




3




4









7




5




8




4




2




3




4




4




3




3




0




1




2




1











Sugarbeets




0




0




0




0




0




0




0




0




2




0




0




0




0




3




0




0




0




0




0




0




7




5




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




2




0




0




0




0




0




0




8




8




5




4




7




0




0




3




2




3




4




0




3




0




3




0




0






Wheat




0




0




0




0




0




0




0




0




0




1




0




0




6




7




0




0




6




0




0




0




2




0




3




0




0




0




0




0




0






Wild oats









0




0




0




0




0




0




0




0




0




0




0




6




5









0




1




0




0




0




5




0




1




1




0




1




1




1




0
















COMPOUND








































Rate 250 g/ha




645




646




647




648




649




650




652




653




654




655




656




657




658




659




660




661




662




663




664




665




666




667




668




670




671




672




674




675




676









Postemergence






B. signalgrass




0




0




7




0




0




0




0




0




0




2




5




4




0




5




0




2




0




0




4




1




5




6




4




7




6




3




8




8




7






Barnyardgrass























































































































































Bedstraw




0




0


































0



















0


































0
























0




4




0




6











Blackgrass




0




0




7




0




0




0




0




0




0




0




9




8




6




7




3




4




0




0




9




8




8




8




8




5




8




6




8




7




6






Cocklebur




3




0




4




0




0




0




0




0




0




0




0




4




2




0




2




0




0




0




2




0




4




4




2




2




0




2




2




3




0






Corn




0




0




5




0




0




2




0




0




0




0




0




1




0




4




0




0




0




0




0




0




0




4




3




5




0




0




6




0




0






Crabgrass




0




0




9




0









7




0




0




2




8




8




9




2




6




5




7




0




0




9




9




9




9




9




8




8




7




9




9











Ducksalad























































































































































Giant foxtail




0




0




9




0




2




8




4




2




5









9




7




7




8




5




4




2




0




9




8




8




9




9




9




9




8




9




9




8






Morningglory




1




0




2




10




7




10




5




1




10




9




2




5




7




10




6




0




9




4




9




6




7




4




4




6




1




8




10




2




2






Nutsedge




0




0









0




0




2









0




0




0




0




7














0




0




0




0




0




0




0




0




0




5









0




7




0




0






Rape




0




0




2




0




0




0




0









0




2




0




3




0




0




0




0




0




0




3




3




0














4




0




2




1




1




0






Redroot pigweed




2




0




6




10




0




0









0




0




3




0




5




7




2




5




2




0




0




4




6




2




5




6




8




3




8




3




8




3






Rice























































































































































S. Flatsedge























































































































































Soybean




1




1




3




3




3




4




1




0




0




2




2




4




4




5




4









2




3




5




4




7




5




3




4




3




5




5




5




3






Sugarbeets




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




2




2




0




2




0




2




0






Velvetleaf




0




0




6




0




0




0




0




0




0




0




0




4




2




6




3




0




0




0




5




6




6




7




4




5




0




7




7




4




3






Wheat




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




3




4




2






Wild oats




0




0




2




0




0




0




0




0




0




0




0




2




1




0




0




1




1




0




5




2




3




4




0




3




0




0




0




5




0
















COMPOUND








































Rate 250 g/ha




677




678




679




680




681




708




709




710




711




712




713




714




722




736




739




740




741




743




744




745




746




747




748




749




750




751




752




753




754









Postemergence






B. signalgrass




0




0




0




0




0




0




0




6




6




4




5




6




2




0




2




0




4




3




5




6




6




4




4




3




6




6




2




2




6






Barnyardgrass























































































































































Bedstraw









0




0




0




0














6




8





























4









4




4









7




8









9




3




7









2









0






Blackgrass




0




0




0




0




0




2




0




6




7




5




7




6




0




2




3




4




0




5




5




8




8




8




7




6




7




6




6




4




5






Cocklebur




0




0




0




0




0




0




0




0




2




3




3




2




0




0




2




3




0




0




0




0




2




2




0




4




1




2









0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




3




0




4




4




0




0




0




0




0




0




2






Crabgrass




0




0




0




1




0




0




6




9




9




9




9




9




2




3









9




9




7




8




9




9




9




8




9




9




9




8




6




9






Ducksalad























































































































































Giant foxtail




2




1




0




0




0




4




8




9




9




8




9




7




4




2




9




8




3




8




8




9




9




9




8




9




8




9




9




8




8






Morningglory




4




6




0




1




0




2




2




4




4




10




7




2




10




6




6




3




5




2




2




3




10




10




6




5




8




8




8




9




10






Nutsedge




0




0




0




0




0




0




0




0




3




0




0




5




0




0




0




0




0




3




3




0




2




0




0




0




7




0




0




2











Rape




0




0




0




0




0




0




0




3




2




4




6




8




0




0




0




0




0




0




3




5




7




4




6




6




6




5




4




0




0






Redroot pigweed




3




0




0




0




2




0




8




9




9




6




9




9




8









3




4




7




5




0




5




8




7




6




4




7




9




5




6




0






Rice























































































































































S. Flatsedge























































































































































Soybean




1




2




1




0




0




4




3




4




5




5




5




4




0




4




4




4




3




4




4




5




4




7




4




5




7




7




6




4




2






Sugarbeets




0




0




0




0




0




0




0




3




2









0




7




0




0




3




2




4




4




0




4




4




0




6




4




3




3




3




5




0






Velvetleaf




0




0




0




0




0




3




4




6




6




6




6




2




0




2




0




2




0




0




0




3




6




4




0




3




5




2




2




2




0






Wheat




0




0




0




0




0




0




0




4




3




0




2




3




2




2




2




0




0




3




5




0









4




0




0




2




5




5




0




5






Wild oats




0




0




0




0




0




0




0




5




2




0




1




4




2




3




0




0




3




0




0




4




6




2




0




0




0




3




0




0




0

















COMPOUND




































Rate 250 g/ha




756




757




758




759




760




761




762




763




764




765




766




767




772




773




774




775




776




777




778




780




790




791




792









Postemergence






B. signalgrass




0




0




6




6




0




3




2




5




2




7




8




6




0




0




0




3




0




2




6




5




7




0




0






Barnyardgrass

























































































































Bedstraw




3




0




7














0




0



















0




7




0




0




0




2




3




2




3









0




3











Blackgrass




0




3




6




7




0




0




0




5




6




7




6




9




0




0




0




4




2




2




4




4




5




5











Cocklebur




0




2




4




1




0




0




0




1




2




0




2




2




0




0




0




0




0




0




0




0




0




0




3






Corn




0




0




0




0




1




0




2




0




0




0




4




0




0




0




0




0




0




0




0




3




4




1




2






Crabgrass




0




6




8




8




9




0




3




8




9




7




6




9




0




0




0




7




2




7




8




7




9




9











Ducksalad

























































































































Giant foxtail




0




5




9




8




7









8




9




8




9




9




9




0




0




0




7




2




8




9




9




8




8




9






Morningglory




10




7




4




3




3




7




2




7




2




6




2




5




0




0




0




6









8




4




7




7




9




10






Nutsedge




0




0




0




0




0




0




0




3




0




0









0




0




0




0




0




0




0









4




5




0




0






Rape




0




0




0




0




2




0




0




0




3




0




0









0




0




0




0




2




0




2




0




3




5




7






Redroot pigweed




0




5




8




0




2




6




6




3




7









6




9




0




0




0




3




2




4




4




0




5




6




6






Rice

























































































































S. Flatsedge

























































































































Soybean




2




4




5




3




4




3




4




3




3




5




4




4




0




0




0




6




2




3




4




0




4




5




5






Sugarbeets




0




3




3




0




0




3




6




2




3




0




2




5




0




0




0




0




3




3




0




0




0




2




2






Velvetleaf




0




3




6




6




0




0




3




0




4




7




3




2




0




0




0




2




3




3




3




4




5




6




6






Wheat




0




0




5




0




0




0




0




4




7




3




3




2




0




0




0




0




0




2




2




0




4




0




1






Wild oats




0




0




1




2




0




0




0









2




0




2




0




0




0




0




0




0




2




2




2




0




0




2
















COMPOUND























































Rate 250 g/ha




1




2




3




4




5




6




7




8




9




10




11




12




13




14




15




16




17




18




19




20




21




22




23




24




25




26




27




28




29




30




31




32




33




34




35




36




37




38




39




40




41




42




43




44









Preemergence






B. signalgrass




0




0




0




8




3




0




0




4




0




8




0




0




2




0




0




0




6




7




2




0




0




4




0




4




7




2




0




0




0




4




6




2




7




2




3




8




0




8




0




5




4




0




0




0






Bedstraw




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




4




0




0




0




0




0




1




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0






Blackgrass




0




0




0




8




3




0




0




0




0




8




0




0




0




0




0




0




3




5




2




1




0




6




2




4




8




0




0




3




2




7




2




4




0




6




2




6




0




10




0




1




2




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0









0




0




0




0









0




0




0




0




0




0




0









0




0




0




0




0




0









0




0




0




0




0




0




0









0




0




0




0




0




0






Corn




0




6




0




0




0




1




0




0




0




0




0




0




0




0









0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




8




0




0




10




3



















0









0




0




5




9









2




9




8




7




6




7




8




3




9




10




3




0




9




7




10




9




9




7




10




6




9




3




10




5




7




8




0




0




0






Giant foxtail




8




7




1




10




8




4




5




9




0




9




0




0




8




9









3




7




8




4




7




8




7




3




9




10




4




0




7




3




10




8




9




9




10




10




10




2




10









10




10




0




0




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




2




1




0




0




0




0




0




0




0




0




0




0




0






Nutsedge



















0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0









0




0




0




0




0




0






Redroot pigweed




0




0




0




8




7




5




0




5




0




0




0




0




0




0




0




0




10




8




2




4




6




5




0




6




8




0




0




1




5




7




3




0




0




6




0




6




0




10




6




4




1




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




8




0




0




0




0




0




0




0




0




0




0




3




0




3




2




1




2




3




7




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




2




0









0




0




0




0




0




0









0




0




0




0




0




0




1




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




4




6




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




6




0




0




3




0




8




4




2




2




2




2




6




0




6




0




0




0




0




0




0
















COMPOUND























































Rate 250 g/ha




45




46




47




48




49




51




52




53




54




55




56




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




85




86




87




88




89




90









Preemergence






B. signalgrass




4




2




0




0




0




0




0




2




0




0




0




0




0




0




0




5




0




0




0




0




0




0




4




0




0




0




0




0




0




2




2




0




5




3




0




3




0




0




0




4




4




2




0











Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




2




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




2




0




2




0




0




3




1




0




0




0




0




0




0




0




5




2




0




0




0




0




2




2




0




0




0




0




0




0




7




4




0




4




6




4




6




0




0




0




5




5




4




0




3






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




1




10




2




7




9




2




6




7




3




0




0




0




0




0




1




7




6




1




2




4




4




4




10




2




0




0




0




8




5




10




8




2




9




9




10




8




0




0




0




10




10




10




0




8






Giant foxtail




10




10




3




10




10




4




7




8




3




0




0




0




0




3




4




9




9




2




3




4




6




8




10




4




0




0




2




9




8




9




9




3




9




9




8




8




0




0




0




10




10




10




0




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2









0




10




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




5




0




4




0




0




0




0




0




0




0




0




0






Redroot pigweed




8




6




0




0




0




0




1




0




0




0




0




0




0




0




0




1




0




0




0




0




0




9




7




0




0




0




0




0




0




7




3




0




6




7




7




0




0




0




0




8




8




10




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




7




3




0




0




0




0




0




0




0




0




0




0




0




0




3




5




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




5




1




4




0




0




0




0




3




3




6




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




2




0




0




0




0




3




3




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




8




4




0




6




3




3




3




0




0




0




4




4




2




0




2
















COMPOUND











































Rate 250 g/ha




91




92




93




94




95




96




97




98




99




100




101




102




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120




121




122









Preemergence






B. signalgrass




10




10









1




3




1




3




0




2




0




0




0




7




5




5




0




10




7




10









1




3




10




7




4




10




9




3




7




6




8




0






Bedstraw




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




10




8




10




5




0




0




7




0




0




9




0




0




2




0




2




0






Blackgrass




10




10




10




8




4




3




1




8




4




0




0




2




3




6




8




0




10




9




10




7




2




2




10




10




0




10




10




3




9




7




7




0






Cocklebur









0









0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0









0






Corn




8




5




8




3




0




0




0




0




0




0




0




0




0




0




2




0




9




6




7




4




4




0




8




7




0




6




7




0




0




0




0




0






Crabgrass




10




8




9




6




8




7




1




8




10




0




0




0




9




1




8




8




10




9




10




9




9




10




10




9




7




10




10




10




8




9




8




8






Giant foxtail




10




10




10




9




7




3




4




10




10




0




0




9




9




10




10




10




10




10




10




10




10




10




10




10




9




10




10




10




10




9




8




9






Morningglory




4




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




6




0




0




2




7




0




0




4




2




0




2




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0






Rape




10




10




8




2




3




0




5




0




0




0




0




0




0




0




4




0




9




7




9




4




4




0




10




6




0




10




10




0




7




0




0




0






Redroot pigweed




10




9




10




0




9




7




4




5




4




0




0




0




6




0




9




0




10




10




10




7




8




7




10




10




6




10




10




2




10




8




8




8






Soybean




4




4




7




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




8




5




4




0




9




0




0




9




8




0




0




0




0




0






Sugarbeets




9




8




8




0




2




0




5




3




2




0




0




0




0




1




4




0




10




4




10




2




3




0




9




7




0




10




9




0




8




4




7




0






Velvetleaf




7




6




6




0




0




0




0




2




0




0




0




0




3




0




5




0




10




4




10




5




3




4




8




5




2




10




10




0




5




0




0




0






Wheat




4




7




6




0




0




0




0




1




2




0




0




0




0




0




0




0




7




2




9




0




0




0




7




2




0




8




7




0




3




2




0




0






Wild oats




10




9




10




4




2




2




2




2




3




0




0




0




3




4




3




0




10




9




10




5




2




2




10




9




0




10




10




6




6




6




5




3
















COMPOUND








































Rate 250 g/ha




123




124




125




126




127




128




129




130




131




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149




150




151









Preemergence






B. signalgrass




0




0




0




0




0




0









9




8




7




5




6




3




5




7




6




8




0




0




0




2




5




3




10




8




7




0




0




5






Bedstraw




0




0




0




0




0




0




0




2




10




9




0




0




0




0




7




10




2




0




0




0




0




0




0




10




2




0




0




0




0






Blackgrass




4




0









0




0




0




2




9




10




9




3




2




0




4




9




9




9




4




0




0




5




4




4




10




10




7




0




0




10






Cocklebur




0




0




0




0




0




0




0




0




2









0




0




0




0




0




0




0




0




0




0









0




0




0




1




0




0




0




0






Corn




0




0




0




0




0




0




2




6




9




7




0




0




0




0




0




8




4




0




0




0




0




2




0




8




8




0




0




0




5






Crabgrass




5




0




0




0




0




0




7




9




9




9




5




9




0




7




10




10




10




5




3




2




8




7




4




9




8




9




0




5




10






Giant foxtail




9




0









0




2




0




8




10




10




9




9




10




0




10




10




10




10









3




5




9




8




5




10




9




9




0




3




10






Morningglory




0




0




0




0




0




0




0




3




5




0




0




0




0




0




0




3




0




0




0




0




0




0




0




3




2




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




10




10




0




0




0




0




0




10




10




4




0




0




0




4




0




0




10




8




6




0




0




10






Redroot pigweed




5




0




0




0




3




0




2




10




10




7




0




0




4




10




10




10




10




0




0




0




4




0




2




10




9




9




0




8




10






Soybean




0




0




0




0




0




0




0




3




8




2




0




0




0




0




3




5




0




0




0




0




0




0




0




2




9




0




0




0




3






Sugarbeets




5




0




0




0




0




0




3




10




10




6




3




4




0




8




10




10




4




0




0




0




3




2




0




10




6




8




0




0




10






Velvetleaf




3




0




0




0




0




0




4




8




9




6




2




2




0




0




7




10




5




0




0




0




0




0




0




8




6




8




0




0




10






Wheat




5




0




0




0




0




0




3









8




2




0




0




0




0




5




6




2




0




0




0




0




0




0




8




7




3




0




0




4






Wild oats




6




0




0




0




0




0




6




10




10




8




2




2




0




0




9









8




1




0




0




5




2




0




10




9




6




0




0




10
















COMPOUND








































Rate 250 g/ha




152




153




154




155




156




157




158




159




160




161




162




163




164




165




166




167




168




169




170




171




172




173




174




175




176




177




178




179




180









Preemergence






B. signalgrass




4




0




0




0




2




0




0




0




0




5




3




2




0




6




0




5




2




7




10




3




5




3




0




0




0




0




8









0






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




4




0




3




0




3




0




7




6




0




3




0









9




0




9




0




0




0






Blackgrass




0




0




3




2




3




5









0




0




7




2




10




0




6




4




3




2




8




10




0




3




0




2




0




2




6




0




2




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




3




6




0




0




0




0




0




0




0




0




0




0






Crabgrass




1




0




0




6




6




4




4




0




0




9




9




8




0




8




7




10




7




10




10




10




10




8




8




6




9




9




8




9




0






Giant foxtail




3




0









2




7




8




7




0




0




9




9




8




0




8




5




10




10




10




10




10




10




9




10




8




10




10




8




10




0






Morningglory




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0









3




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




4




7




0




4




0




0




0




6




10









0




0




0




0




0




0




0




2




0






Redroot pigweed




0




0




8




3




9




0




0




0




0




4




0




6




0




0




0




8




0




8




10




5




8




0




8




0




0




0




6




7




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




4




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




4




0




0




0




0




0




0




0




0




4




0




4




0




5




4




7




8




0




5




3




6




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




5




0




4




5




0




0




6




10




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




3




8




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




4




0




0




0




0




0




0




3




2




7




0




4




0




3




1




8




10




4




3




2




0




0




3




0




0




0




0
















COMPOUND








































Rate 250 g/ha




181




182




183




184




185




186




187




188




189




190




191




192




193




194




195




196




197




198




199




200




201




202




203




204




205




206




207




208




210









Preemergence






B. signalgrass




0




0




4




8




0




0




0




6




3




0




0




6




0




0




1




0




0




0




6




0




0




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0






Blackgrass




0




0




0




5




0




3




0




0




4




0




4




6




0




3




3




0




0




0




10




7




4




5




0




2




0




0




4




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




7




7




6




0




0




0




0




8




7




6




9




5




0




0




0




10




6




9




6




0




8




1




3




3




6




3






Giant foxtail




0




0




0




10




9




9




0




4




3




0




9




10




5




8




8




0




0




0




10




6




8




7




0




10




0




8




9




9




3






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0









0




0




0




0




0









0




0









0




0




0




0



















0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




4




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




2




0




0




0




0




1




5




0




8




0




0




0




0




10




0




0




8




0




0




0




0




2




0




2






Soybean




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




5




0




0




3




0




0




0




0




0




0




0






Velvetleaf




0




0




0




2




0




2




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




3




0




3




5




0




3




0




0




0




0




4




0




3




0




0




3




0




0




0




0




2
















COMPOUND








































Rate 250 g/ha




211




212




213




214




215




216




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237




238




239









Preemergence






B. signalgrass




0




5




0




0




2




4




0




6




9




8




6




0




3




4




7




9




0




0




0




0




0




1




4




0




0




0




0




0




4






Bedstraw




0




0




0




0




0




0




0




0




8




10




4




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




9




7




0




3









4




8




9




10




10




7




0




4




3




10




10




10




0




0




0




0




8




8




0




0




5




0




0




4






Cocklebur




0




0









0




0




0




0




0




0









0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




5




5




0




0




0




0




4




6




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




5




3




1




4




8




8




6




9




8




8




8




7




9




10




10




10




1




0




7




0




9




9




0




0




5




2




10




10






Giant foxtail




7




9




4




6




3




7




10




10




10




10




10




7









9




10




10




10




9




0




8




3




8




9




0




0




9




4




10




10






Morningglory




0




0




3




0




0




0




0




0




0




1




0




0




1




0




4




7




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge









0














0




0




0



















0




0














8









0




0




0




0




0









0
























0











Rape




0




6




0




0




0




0




4




0




6




8




8




0




0




0




0




7




8




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




3




10




5




6




5




2




10




8




9




8




10




0




7




0




10




7




10




0




0




0




0




5




7




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




2




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




5




0




0




2




0




0




6




4




8




10




0




0




0




5




5




6




0




0




0




0




4




4




0




0




0




0




3




0






Velvetleaf




0




5




0




0




0




0




5




0




7




4




0




0




0




0




6




6




0




0




0




0




0




0




2




0




0




0




0




0




2






Wheat




0




5




0




0




0




0




8




0




8




8




2




0




0




0




8




8




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




5




3




0




0




2




0




2




7




8




7




4




0




2




0




10




9




3




0




0




0




0




3




2




0




0




0




0




0




3
















COMPOUND








































Rate 250 g/ha




240




241




242




243




244




245




246




247




248




249




250




251




252




253




254




255




256




257




258




259




260




261




262




263




264




265




266




267




268









Preemergence






B. signalgrass




0




4




9




7




0




8




3




0




0




0




0




7




0




0




0




3




0




0




7




8




0




0




0




0




5




0




0




0




0






Bedstraw




0




7




9




5




0




9




0




0




0




0




0




10




0




0




0




0




0




0




3




10














0




0




0




0




8




0




0






Blackgrass




0




7




10




10




0




10




6




0




0




0




0




9




4




0




0




10




0




0




8




10




2




1




2




0




4




0




9




2




0






Cocklebur




0




0




2




0




0




2




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




6




6




0




7




0




0




0




0




0




0




0




0




0




0




0




0




3




3




0




0




0




0




0




0




0




2




0






Crabgrass




9




10




10




9




0




9




10




2




0




0




8




9




4




0




0




7




2




2




9









6




5




2




0




3




2




5




1




0






Giant foxtail




10




10




10




10




0




10




10




2




0




3




10




10




10




0




6




10




9




6




10




9




8




9









9




7




8




6




9




0






Morningglory




0




3




5




8




0




6




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




10




10




0




0









0




0




0




0
























0









0




0









0




0




0




0




0




0




0




0




0




0






Rape




0




5




10




9




0




10




10




0




0




0




0




9




3




0




2




0




0




0




5









0




0




0




0




0




0




5




0




0






Redroot pigweed




0




9




10




10




0




10




0




0




0




0




3




10




0




0




0




5




0




0




7




2




4




0




0




0




0




0




6




6




0






Soybean




0




0




6




8




0




2




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




3




0




0




0




0






Sugarbeets




0




6









7




0




10




2




0




0




0




5




10




3




0




2




6




0




0




5




0




0




0




0




0




1




0




7




0




0






Velvetleaf




0




5




8




10




0




10




4




0




0




0




0




5




2




0




0




5




0




0




5




4




0




0




0




0




0




0




0




0




0






Wheat




0




3




9




8




0




7




0




0




0




0




0




0




2




0




0




4




0




0




4




0




0




0




0




0




2




0




4




0




0






Wild oats




0




8




9




9




0




10




6




0




0




0




0




8




3




0




0




5




0




0




5




4




0




0




0




0




5




2




5




0




0
















COMPOUND








































Rate 250 g/ha




269




270




271




272




273




274




276




277




278




279




280




281




282




283




284




285




286




288




289




292




293




294




295




296




297




298




299




300




301









Preemergence






B. signalgrass




6




0




8




0




2




0




10




10




0




0




0




0




2




10




5




10




8




6




8




0




7




7




8




0




0




0




9




0




0






Bedstraw




0




0




10




0




0




0




0




0




0




0




0




6




2




1




8




8




0




10




7




0




0




0




0




0




0









10




0




0






Blackgrass




3




0




10




0









0




10




10




0




0




0




2




4




9




8




5




7




6




9




0




9




6




10




0




0




0




10




0




0






Cocklebur




0




0




0




0




0




0




0




0




0









0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




9




0




0




0




0




0




8




0




0






Crabgrass




3




0




7




0




6




1




6




9




2




0




0




10




6









8




8




10




10




4




0




8




9




7




0




7




0




9




4




0






Giant foxtail




10




0




10




6




8




6




10




10




2




6




0




10




10




10




9




10




10




10




10




0




9




10




10




0




7









10




9




0






Morningglory




0




0




2




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




6




0




0






Nutsedge









0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0









0




0









0




0






Rape




0




0




10




0




0




0




1




1




0




0




0




0




7




2




7




3




3




0




10




0




8




0




10




0




0




0




10




0




0






Redroot pigweed




4




0




10




0




0




0




2




0




0




0




0




0




7




10




7




5




2




0




8




0




10




0




6




0




0




0




10




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




6




0




0






Sugarbeets




0




0




8




0




6




0




1




2




0




0




0




0




0




2




6




0




0




0




8




0




4




0




3




0




0




0




9




0




0






Velvetleaf




0




0




7




0




0




0




0




6




0




0




0




0




0




5




0




3




3




3




7




0




7




3




3




0




0




0




8




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




2




2




0




8




0




6




0




0




0




8




0




0






Wild oats




2




0




6




0




0




0




4




7




0




0




0




2




5




4




3




3




4




5




8




0




8




3




9




0




0




0




8




0




0
















COMPOUND








































Rate 250 g/ha




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




318




319




320




321




322




323




324




325




326




327




328




329




330









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




7




0




0




0




6




3




9




7




0




2




2




3




1




0




0




0




3




1




0




0




0






Bedstraw




0




0




0




0




0




0




0




0




5




0




0




0




0









3









0




0



















0




0




0
























0






Blackgrass




2




0




0




0




0




2




0




2




10




0




0




0




10




7




10




8




0




2




5




6




5




0




0




2




7




4




4




0




0






Cocklebur




0




0




0




0




0




0




0




0




2




0




0




0




0









0









0




0









0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




2




0




6




6




0




0




0




2




7




0




0




0




7




7




8




8




0




2




3




3




5




0




0




1




3




3




3




0




0






Giant foxtail




7




0




6




9




8




9




0




9




10




0




0




0




7




9




10




10




0




9




6




9




9




0




0




8




8




9




8




0




0






Morningglory




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




10




0




0




0



















0









0




0









0









0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




10




0




0




0




3




0




4




8




0




0




0




0




0




0




0




0




0




0




0









0






Redroot pigweed




0




0




0




3




0




0




0




0




10




0




0




0




2




0




10




7




0




0




0




0




8




0




0




0




6




1




0




0




0






Soybean




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




2




0




6




0




0




0




0




0




10




0




0




0




2




1




0




7




0




0




0




0




2




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




7




0




0




0




3




0




3




6




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




5




0




0




0




0




2




2




7




0




0




0




0




0




0




0




0




0









0




0




0






Wild oats




2




0




0




0




0




0




0




0




9




0




0




0




2




0




6




8




0




0




0




2




2




0




0




0




3




0




0




0




0
















COMPOUND








































Rate 250 g/ha




331




332




333




334




335




336




337




338




339




340




341




342




343




344




345




348




349




350




351




352




353




354




355




356




357




358




359




360




361









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




1




0




2




6




0




0




5









2




2




7




5




5




3




5




6




5




0




7




4






Bedstraw









0




0




0




0




0




0




0




0














0














0














10




9














0




0









10




10




0









0






Blackgrass




0




0




0




0




0




0




2




0




2




3




6




3




9




0




0




9




4




8




3




10




7




8




5




9




9




10




0




9




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0









0




0




0









0




0




0




0




0














0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




3




6




3




3




3




2




6




2




0




4




1






Crabgrass




0




3




0




0




2




0




0




0




2




8




2




9









0




0




10




8




10




10




10




10




9




10




9




9




10




0




10




7






Giant foxtail




0




4




0




0




10




0




2




0




9




10




10




10




10




3




0




10




10




10




10




10




10




10




10




10




10




10




0




10




10






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




1




0




0




0




2




3




0




7




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




2




0




7




6




0




1




5




0




4




8




4




0




0




5






Redroot pigweed




0




0




0




0




0




0




0




0




0




3




0




0




10




0




0




10




2




10




10




10




10




10




10




8




10




10




0




10




8






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




3




4




4




6




3




2




2




2




2




5




3




0




6




6






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




7




3




4




4




6




4




6




3




3




5




5




0




7




4






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




2




2




0




0




0




9




1




0




7




2






Wild oats




0




0




0




0




0




0




0




0




0




2




0




0




9




0




0




8




3




5




2




9




4




6




0




10




10




9




0




10




8
















COMPOUND








































Rate 250 g/ha




362




363




364




365




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388




389




390




391




392




393









Preemergence






B. signalgrass




7




5




0




0




4




8




2




2




2




6




0




2




4




0




0




0




0




0




2




0




3




7




1




3




0




9




0




9




0






Bedstraw




10




10




0




0




10




10









3









10









0




10









0




0









0

















































10











Blackgrass




10




10




1




0




8




10




2




9




10




10




5




5




9




0




0




0




0




0




3




2




3




6




0




5




6




9




0




10




0






Cocklebur




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0






Corn




9




3




0




0




2




7




0




4




2




9




3




0




2




0




0




0




0




0




0




0









0




0









0









0




9




0






Crabgrass




8




7




2




0




10




10




9




9




10




10




10




9




10




0




9




7




7




3




9




9




9




9




8




10




9




10




0




10




3






Giant foxtail




10




10




9




0




10




10




10




10




10




10




10




10




10




0




10




6




9




5




9




10




10




10




9




10




10




10




0




10




10






Morningglory




6




5




0




0




0




3




0




2




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0






Nutsedge




3




0




0




0




0




10




0




5




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




6




3




0




0




5




6




2




6




9




10




0




2




6




0




0




0




0




0




0




0




0




0




0




2




0




8




0




5




0






Redroot pigweed




10




7




0




0




10




10




10




10




10




10




7




0




10




0




0




0




3




0




0




0




0




7




6




6




4




10




0




10




2






Soybean




6




0




0




0




0




7




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0






Sugarbeets




8




7




0




0




7




10




2




5




6




10




4




0




4




0




0




0




0




0




0




0




0




2




1




3




0




8




0




7




2






Velvetleaf




6




6




0




0




5




10




0




5




5




6




0




0




4




0




0




0




0




0




0




0




1




3




0




2




0




6




0




5




0






Wheat




8




6




0




0




0




8




0




2




2




0




0




0




2




0




0




0




0




0




0




0




2




3




0




4




0




8




0




8




0






Wild oats




10




10




0




0




3




10




0




2




3




9




0




0




9




0




0




0




0




0




0




0




6




7




3




10




1




10




0




10




0
















COMPOUND








































Rate 250 g/ha




394




395




396




397




398




400




401




402




403




404




405




406




407




408




409




410




411




414




415




416




417




418




419




420




421




422




423




424




425









Preemergence






B. signalgrass




8




0




3




9




6




2




0




4




5




8




0




0




0




4




7




7




7




1




6




7




7




6




2




6




9




0




0




0




8






Bedstraw









0







































10









0




0
























0





























































Blackgrass




10




0




3




10




8




0




0




9




7




9




0




0




0




9




10




8




9




3




9




10




7




7




0




8




10




0




0




0




9






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0









0




0




0




0






Corn




3




0




0




3




0




2




0




3




2




2




0




0




0




4




8




4




8




0




3




3




0




2




0




0




8




0




0




0




0






Crabgrass




10




0




10




10




10




10




8




10




10




10




8




2




5




10




10




10




10




9




9




10




9




10




4




9




9




0









0




10






Giant foxtail




10




0




10




10




10




10




7




10




10




10




9




2




9




10




10




10




10




10




10




10




10




10




2




10




10




0




3




0




10






Morningglory




0




0




0




0




0




0




0




2




0




4




0




0




0




0




5




0




2




0




0




6




0




0




1




2




7




0




0




0




2






Nutsedge




2




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




3




0




0




0




0




0




0




0




0




3






Rape




7




0




0




10




8




0




0




5




5




7




0




0




0




6




4




2




9




0




10




9




5




0




2




0




10




0




0




0




2






Redroot pigwee 6




d




0




4




10




10




6




0




4




9




10




0




0




0




10




8




2




10




0




6




10




4




8




6




2




10




0




0




0




3






Soybean




1




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




7




0




0




0




0




5




0




0




0




0






Sugarbeets




4




0




0




7




4




2




0




3




3




6




0




0




0




8




8




0




8




0




6




7




2




2




3




2




10




0




0




0




2






Velvetleaf




7




0




0




6




6




0




0




3




3




5




0




0




0




7




6




6




6




0




6




6




2




5




1




6




10




0




0




0




2






Wheat




6




0




0




2




0




0




0




3




0




4




0




0




0




4




9




7




7




0




2




7




0




0




0




2




7




0




0




0




3






Wild oats




10




0




2




7




3




0




0




8




5




10




0




0




0




5




7




7




8




2




6




8




2




0




0




2




10




0




0




0




4
















COMPOUND








































Rate 250 g/ha




426




427




428




429




430




431




432




433




434




435




436




437




438




439




440




441




442




443




444




445




446




447




448




449




450




451




452




453




454









Preemergence






B. signalgrass




6




3




0




0




3




0




0




2




0




0




0




0




0




0




8




0




0




0




1




2




7




0




0




0




3




0




0




6




4






Bedstraw
































































0

















































0




0































Blackgrass




9




4




0




0




7




0




0




3




0




0




0




0




2




0




10




0




0




0




8




0




8




0




0




0




4




0




2




3




2






Cocklebur




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Crabgrass




10




9




9




10




10









8




10




0




6




0




0




9




0




10




0




8




9




9




3




9




8




4




9




8




1




5




6




8






Giant foxtail




10




10




8




10




10




2




6




10




0




3




0




0




10




0




10




0




3




10




10




5




10




7




3




8




9




4




4




10




10






Morningglory




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0






Rape




8




0




0




0




0




0




0




3




0




0




0




0




0




0




3




0




0




0




0




0




8




0




0




0




0




0




0




0




0






Redroot pigweed




8




0




0




0




2




0




0




7




0




4




0




0




5




0




7




0




0




0




10




4




10




0




0




0




7




0




0




6




9






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2









2




0




0




0




3




0




0




0




0






Sugarbeets




4




0




0




0




0




0




0




4




0




0




0




0




0




0




4




0




0




0




0




0




6




0




0




0




0




0




0




2




0






Velvetleaf




2




0




0




0




4




0




0




4




0




1




0




0




5




0




0




0




0




0




0




2




7




0




0




0




0




0




0




2




5






Wheat




2




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




3




0




0




0




0




0




0




3




0






Wild oats




8




2




0




0




3




2




0




6




0




2




0




0




1




0




9




0




0




0




0




0




8




2




0




0




0




0




0




2




0
















COMPOUND








































Rate 250 g/ha




455




456




457




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




481




482




483




485




486









Preemergence






B. signalgrass




9




0




0




4




1




0




0




0




0




3




6




0




3




7




4




10




9




0




7




0




4




9




6




7




9




0




0




8




6






Bedstraw














0



















0




0



















0

















































8




0



















0
















Blackgrass




6




3




0




8




5




0




0




0




2




6




7




2




5




9




7




10




10




0




4




0




7




10




8




8




10




0




0




8




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0











Corn




4




0




0




0




0




0




0




0




0




0




0




0




0




8




0




2




2




0




0




0




0




0




0




0




0




0




0




0




5






Crabgrass




10




8




0




9




9




6




0




0




2




4




10




6




9




10




8




10




10




4




9




0




10




10




9




8




8




8




0




10




10






Giant foxtail




10




10




0




10




10




8




0




0




3




10




10




9




9




10




0




10




10




4




10




0




9




10




10




10




9




8




0




10




10






Morningglory




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




4




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0






Rape




8




0




0




3




0




0




0




0




0




2




0




7




3




10




0




7




0




0




2




0




0




4




1




0




0




0




0




0




6






Redroot pigweed




10




3




0




6




4




0




0




0




10




9




9




7




8




10




0




10




10




10




5




2




6




9




6




8




3




0




0









9






Soybean




0




0




0




0




0




0




0




0




0




7




2




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0






Sugarbeets




3




2




0




2




0




0




0




0




0




3




2




1




2




8




0




2




3




0




0




0




0




3




2




0




2




0




0




0




4






Velvetleaf




5




1




0




2




0




0




0




0




0




7




4




0




1




6




0




3




3




0




0




0




0




3




1




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




1




3




0




2




0




0




3




0






Wild oats




9




2




0




3




0




0




0




0




0




2




3




0




3




10




0




7




8




0




4




0




5




9




5




4




8




0




0




6




5
















COMPOUND








































Rate 250 g/ha




487




488




489




490




492




493




494




495




496




497




498




499




500




501




502




503




504




505




506




508




509




510




511




512




513




514




515




516




517









Preemergence






B. signalgrass




3




7




8




6




0




0




0




0




1




0




0




0




9




9




10




8




10




2




0




8




8




8




0




10




5




8




8




9




0






Bedstraw
























0




0




0














0









0




9




10




10




6




8




8




0




0




10




0




0




0




0




0




0




1




0






Blackgrass




7




8




9




9




0




0




0




0




2




0




0




0




10




9




10




9




10




7




4




5




8




7




0




9




4




5




5




8




4






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0






Corn




0




0




0




3




0




0




0




0




0




0




0




0









7




9




8




5




5




0




0




0




3




0




0




3




3




3




0




0






Crabgrass




10




10




10




9




3




2




0




0




9




0




3




8




9




9




10




8




9




7




0




10




9




9




6




7




4




9




7




9




7






Giant foxtail




10




10




10




9




2




9




0




0




9




0









9




10




10




10




9




10




9




5




10




9




9




6




10




7




10




10




10




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




7




5




4




6




1




0




0




0




3




1




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0









0




0




0




0




0




7




9




6




2




7




9




3




0




0




0




0




0




0




0




0




0




0






Rape




0




8




4




6




0




0




0




0




0




0




0




0




10




3




6




9




10




8




3




0




3




8




0




3




7




7




6




7




0






Redroot pigweed




8




10




4




8




0




0




0




0




2




0




0




0




10




10




10




10




10




10




10




9




8




10




6




10




8




9




9




8




9






Soybean









1




2




0




0




0




1




0




0




0




0




0




6




3




4




6




1




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




7




4




3




0




0




0




0




0




0




0




0




10




6




5




7




8




6




0




6




7




6




0




2




0




5




6




4




2






Velvetleaf




0




6




6




2




0




0




0




0




0




0




0




0




10




4




5




7




6




4




0




0




7




4




0




0




0




2




2




3




2






Wheat




0




0




0




4




0




0




0




0




0




0




0




0




8




7




7




6




6




7




2




0




3




0




0




4




5




3




5




4




6






Wild oats




3




8




9




7




0




0




0




0




0




0




0




0




9




9




10




10




10




9




3




7




7









0




9




7




6




7




8




5
















COMPOUND








































Rate 250 g/ha




518




519




520




521




522




523




524




525




526




527




528




531




532




533




534




535




536




540




541




543




544




545




546




548




549




550




551




552




553









Preemergence






B. signalgrass




10




0




0




0




9




9




2









9




4




0




2




0




9




9




0




0




0




0




4




6




0




0




3




0




9




9









9






Bedstraw




0




0




0




0




10




0









0




7









0




0









0




0









0




0




0




0




7




0




8




10




5




0









0




2






Blackgrass




7




4




0




0




9




7




4









10




2




0




9




0




9




9




0




0




0




0




0




2




2




0




3




6




7




9




0




7






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9









0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




7




0




7




4




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




10




10




10




10




10




9




10




10




10




10




10




10




10




10




10




0




10




10




6




10




10




10




10




10




10




10




8




10






Giant foxtail




0




10




10




10




10




10




9




10




10




10




10




10




10




10




10




10




10




10




10




9




10




10




10




10




10




10




10




10




10






Morningglory




0




0




0




0




2




0




2




0




0




0




0




0




0




0




2




0









0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0









0




0




10




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




2




4




4




7









9




2




0




0




0




7




6




2




0




2




0




0




3




0




0




2




0




6




3




0




3






Redroot pigweed




4




0




0




0




10




9




8









4




4




0




0




0




8




0




4




0




3




0




9




3




9




10




2









9




10




4




9






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Sugarbeets




2




0




0




3




5




7




6









8




6




0




3




2




7




6




5




2




0




0




6




0




2




2




2




0




5




7




0




3






Velvetleaf




0




0




0




2




8




2




4




3




2




2




0




2




0




5




2




2




0




0




0




0




0




0




0




0




0




2




2




0




0






Wheat




3




0




0




0




2




0




7









8




0




0




0




0




0




3




0




0




0




3




0




0




0




0




0









2




3




0




0






Wild oats




8




0




0




0




4




0




8









9




3




0




0




0




9




9




0




0




2




5




0




2




2




0




2




0




2




3




0




3
















COMPOUND








































Rate 250 g/ha




554




555




556




557




558




559




560




561




562




563




564




565




566




567




568




569




570




571




572




573




574




575




576




577




578




579




580




581




582









Preemergence






B. signalgrass




6









7




7




3




9




7




8




10




9




6




0




10




2




8




9




0




3




0




9




10




10




6




4




9




2




6




2




2






Bedstraw




0




0




0




0




0




0




5




2




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




6




7




6






Blackgrass




4




0




10




8




6




10




9




9




10




9




5




0




10




0




8




9




0




3




0




2




2




7




6




3




0




0




7




0




0






Cocklebur




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




6




5




2




9




4




4




0




2




0




5




0




0




0




0




0




0




0




0




2




2




0




2




7




0






Crabgrass









10




9




10




9




10




9




9




10




10




9




0




9




9




9




9




9




3




0




9




9




9




9




9




9




10




9




8




0






Giant foxtail




9




10




10




10




9




10




10




6




8




10




9




0




10




10




10




9




9




9




4




9




10




10




9




9




10




10




10




9




8






Morningglory




0




0




0




0




0




4




3




2




0




0




2




0




0




0




2




0




0




2




0




0




0




0




0




8




0




0




0




4




0






Nutsedge




0




0




0




0




0









7









0




0









0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




4




0






Rape




0




0




3




0




2




10




7




5




10




9




0




0




7




0




5




4




0




0




0




3




0




2




2




0




2




0




7




2




0






Redroot pigweed









3




5




3




2




10




9




9




10




9




3




0




9




8




4




9




0




9




0




9









10




10




0




9




2




10




9




4






Soybean




3




0




0




0




0




3




1




0




9




3




4




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




5




0






Sugarbeets




0









0




3




0




9




3




2




9




3




3




0




6




0




6




0




0




0




0




2




0




0




4




0




3




0




4




0




0






Velvetleaf




0




0




3




0




0




6




2




0




0




6




6




0




0




0




6




0




0




0




0




0




2




0




0




3




2




0




2




5




4






Wheat









2




3




0




0




9




6




6




9




9




7




0




6




0




0




0




0




3




0




0




0




0




8




0




0




0




2




2




0






Wild oats




2




0




4




0




0




9




5




5




10




9




4




0




8




0




6




6




0




3




0




0




0




2




3




0




2




0




2




0




0
















COMPOUND








































Rate 250 g/ha




584




585




586




587




588




589




590




591




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609




610




611




612




613









Preemergence






B. signalgrass









9




8




5




5




0




0




0




0




0




5




7




0




0




2




0




8




7




0




0




0




0




8









9




9




10




10




9






Bedstraw




9




9














0
























0




2









0




0




0




0




0




0









0




0



















8


























Blackgrass




8




8




9




6




5




0




0




0




0




0




9




10




0




0




3




0




8




6




0




0




0




0




8




7




9




10




10




10




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Corn




2




3




0




0




0




0




0




0




0




0




2




4




0




0




0




0




0




0




0




0




0




0




0




0




6




7




9




8




9






Crabgrass




9




9




10




8




8




7




2




0




2




0




9




9




1




0




5




0




10




9




0




0




5




7




9




10




8




10




10




10




10






Giant foxtail




9




9




10




9




8




10




7




0




0




0




10




10




0




0




9




0




10




10




0




3




10




9




10




10




10




10




10




10




10






Morningglory




4




2




1




0




0




0




0




0




0




0




3




2




0




0




0




0




0




0




0




0




0




0




0




0




4




6




3




2




7






Nutsedge




0




0




0




0




0









0




0




0




0




3




4




0




0




0




0









0




0




0




0




0




0




0




4




2




0




0




0






Rape




4




9




0




0




0




0




0




0




0




0




6




7




0




0




0




0




0




3




0




0




0




0




7




5




6




10




8




8




10






Redroot pigweed




9




10




10




1




9




0




0




0




0




0




10




10




0




0




0




0




10




8




0




0




0




0




9




7




8




10




10




10




10






Soybean




0




0




0




0




5




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




1




6




8




4




2




0






Sugarbeets




3




7




1




0




0




0




0




0




0




0




5




9




0




0




0




0




5




4




0




0




0




0




0




3




7




8




5




6




8






Velvetleaf




2




7




2




0




2




0




0




0




0




0




6




9




0




0




0




0




5




6




0




0




0




0




7




6




8




8




8




7




7






Wheat




0




5




3




1




3




0




0




0




0




0




0




3




0




0




0




0




2




0




0




0




0




0




3




0




3




5




6




5




5






Wild oats




4




9




10




7




2




0




0




0




0




0




2




9




0




0




0




0




8




5




0




0




0




0




2




3




8




9




8




9




9
















COMPOUND








































Rate 250 g/ha




614




615




616




617




618




619




620




621




622




623




624




625




627




628




629




630




631




632




633




634




635




636




637




638




639




640




641




642




643









Preemergence






B. signalgrass




0




0




0




4




0




0




0




0




0




0




6




8




8




8




5




7




10




6




6




7




9




8




8




8




5




4




6




5




2






Bedstraw




0




0




0




0




0




0




0




0














0









8




10




3




0




0



















7




9




2




































Blackgrass




3




0




4




6




0




0




0




0




3




0




8




7




9




10




8




8




9




7




5




8




9




4




9




9




2




0




2




4




0






Cocklebur




0




0




0




0









0




0




0




0




0




0




0




6




4




3









0




0




0




0




0




0




0




4




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




2




0




6




7




6




3




8




4




0




0




2




0




0









0




0




0




0




0






Crabgrass




8




0




0




5




0




6




0




7




7




0




9




8




9




9




9




9




9




8




9




10




9




10




10




9




9




9




7




10




9






Giant foxtail




9




0




7




9




2




7




2




7




9




8




10




10




10




10




10




10




10




10




10




10




10




10




10




10




9




10




9




10




10






Morningglory




0




0




0




0




0




0




0




0




0




0




0




2




6




5




0




0




4




4




0




0




0




0




0




2




0




0




0




0




0






Nutsedge




0




0




0




0









0




0




0




0




0




0




0




7




6




5




0




4




0




0




0




3




0




0




5




0









0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




1









9




4




4




0




6




0




1




6




7




7




2




8




3




3









4




0






Redroot pigweed




0




0




8




0




0




0




0




0




10




0




3




4




10




9




10




10




10




6




2




10




10




10




7




10




2




2




0




2




0






Soybean




0




0




0




0




0




0




0




0




0




0




3




0




0




4




0




0




9




0




0




0




0




0




0




3




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




7




0




8




7




3




4




4




0




0




5




8




6




3




6




0




6




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




1




1




10




9




6




6




7




6




0




4




3




2




0




5




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




6




0




7




7




3




3




8




0




0




0




3




0




0




3




0




0




0




0




0






Wild oats




0




0




0




2




0




0




0




0




0




0




6




3




5




8




9




8




8




3




3




5




9




0




0




10




0




3




0




2




0
















COMPOUND








































Rate 250 g/ha




644




645




646




647




648




649




650




652




653




654




655




656




657




658




659




660




661




662




663




664




665




666




667




668




669




670




671




672




673









Preemergence






B. signalgrass




2




0




0




9




0




0




0




2




0




0




0




6




9




8




4




4




3




3




0




5




8




7




8




8




10




10




7




6




7






Bedstraw
























0




0




0




0




0




0




0





































































9




9









0




4






Blackgrass




0




0




0




10




2




0




0




0




0




2




2




5




7




7




7




6




4




4




0




6




8




9




8




10




10




10




8




8




9






Cocklebur




0




0




0




1









0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0






Corn




0




0




0




5




0




0




0




0




0




0




0




0









2




7




0




0




0




0




0




0




8




7




4




9




8




3




0




4






Crabgrass




3




4




0




9




9




5




9




8




6




7




8




8




9




8









8




3




4




0




9




9




9




10




8




9




10




8




10




10






Giant foxtail




6




5




0




10




9




9




10




9




2




9




9




10




9




9




9




10




8




9




5




10




10




10




10




9




10




10




10




10




10






Morningglory




3




0




0




7




0




0




1




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




3




0




0




8




5




0




0






Nutsedge









0




0









0




0




7




0









0




0




0




5




0




0




0




0




4




0




0




0




0




3




0









8




6




0




2






Rape




2




0




0




10




0




0




0




0




0




0




0




0




10




5




2




3




0




0




0




1




8




10




10




8




8




10




0




7




2






Redroot pigweed




0




0




0




10




0




0




7




0




0




3




2




6




10




9




9




7




3




3




7




7




9




10




10




10




10




10




10




7




10






Soybean




0




0




0




1




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




3




6




1




3




8




0




0




0






Sugarbeets




0




0




0




8




0




0




0




0




0




0




0




3




10




6




0




0




0




0




0




0




6




7




8




6




8




9




9




7




3






Velvetleaf




0




0




0




8




0




0




0




0




0




0




0




6




8




3




6




0




0




0




0




5




4




7




8




7




0




8




7




3




3






Wheat




0




0




0




8




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




4




4




5




5




8




9




3




0




0






Wild oats




0




0




0




9




0




0




0




0




0




0




0




6




8




3




3




2




0




0




0




3




7




9




8




8




10




9




7




5




9
















COMPOUND








































Rate 250 g/ha




674




675




676




677




678




679




680




681




682




683




684




685




686




687




689




691




692




693




694




695




696




697




698




699




700




701




702




703




704









Preemergence






B. signalgrass




8




8




4




3




0




0




0




0




7




4




4




9




7




10




9




9




10




0




6




5









0




3




9




8




0




2




3




8






Bedstraw









10


































0




0




0




0




0









7




9




1




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




9




9




4




0




0




0




0




1




8




7




4




10




8




9




10




10




10




0




9




6




7




2




2




10




8




2




9




6




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




5




6




3




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




1




0




0




0




0




8




3




0




0




0




0






Crabgrass




9




9




6




6




0




0




3




2




9




9




9




9




10




4




10




10




10




0




9




9




9




4




8




10




10




10




10




9




8






Giant foxtail




10




10




10




8




0




3




4




6




10




9




10




10




10




6




10




10




10




2




10




10




10




5




9




10




10




10




10




9




8






Morningglory




7




3




0




0




0




0




0




0




2




0




1




1




0




3




3




0




1




0




2




0




0




4




0




5




0




0




0




1




1






Nutsedge




5




3




0




0









0




0




0




0




0




0









0




0




0









0




0









0




0




0




0




0




0









0




0




0






Rape




5




7




5




0




0




0




0




0




3




0




0




2




2




8




7




6




3




6




0




0




2




0




0




9




2




0




0




0




1






Redroot pigweed




10




10









7




0




0




0




0




5




5




1




5




7




9




7




8




8




0




8




5




6




0




0




6




2




0




5




4











Soybean




5




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




0




0




0




2




0




0




0




0




0






Sugarbeets




7




8




5




0




0




0




0




0




3




0




0




1




2




9




6




5




2




0




0




0




3




0




0




7




3




0




3




0




4






Velvetleaf




8




10




4




0




0




0




0




0




0




0




0




0




0




6




6




0




1




0




1




0




2




0




0




5




0




0




0




0




0






Wheat




8




5




2




0




0




0




0




0




0




0




0




0




0




7




2




0




0




0




0




0




0




0




2




6




0




0




0




0




6






Wild oats




8




7




3




0




0




0




0




0




2




0




2









5




10




9




9




10




0




3




0




6




0




0




10




9




2




7




2




2
















COMPOUND








































Rate 250 g/ha




706




707




708




709




710




711




712




713




714




715




716




717




718




719




720




721




722




723




724




725




726




727




728




729




730




732




733




734




735









Preemergence






B. signalgrass




8




9




0




0




8




7




8




8




10




9




0




7




7




7




10




8




0




2




0




4




7




7




8




10




7




0




8




9




9






Bedstraw




0




10




0




0




5




6




2




2




9




0




0




0




0




0




10




10




0




0




0




0




0




0




0




8




0




0




0




0




0






Blackgrass




10




10




3




0




9




8




8




9




9




9




0




10




9




9




10




10




0




0




0




7




8




8




9




10




10




0




8




9




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




2




0




0




0




0




0




0




5




2




0




3




0




0




4




5




0




0




0




0




0




0




0




6




4




0




0




9




8






Crabgrass




8




9




10




7




10




10




10




10




10




10




0




10




10




8




10




9




0




2




7




8




9




9









9




9




0




9




9




10






Giant foxtail




7




10




8




7




10




10




10




10




10




10




0




10




10




8




10




10




4




9




7




10




10




10




8




9




10




0




9




10




10






Morningglory




1




4




0




0




0




3




0




0




0




2




0




0




0




3









2




2




0




0




1




1




0




2




2




0




0




2




3




2






Nutsedge




0




0




0









0




0




0




0




0




0









0




0




0









0




0




0




0









0




0














3




0




0




0




0






Rape




3




10




0




0




8




7




7




8




6




8




0




0




2




2




9




9




0




0




0




0




0




1




6




3




2




0




3




5




8






Redroot pigweed




10




10









5




10




9




8




8




10




10




0




8




6




10




10




10




0




0




0




0




7




5




8




10




10




0




5




8




8






Soybean




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0






Sugarbeets




4




8




0




0




8




8




7




7




4




7




0




2




2




6




8




7




0




0




0




0




5




0




4




0




4




0




0




5




6






Velvetleaf




5




5




2




0




7




6




3




5




2




6




0




0




0




0




3




8




0




0




0




0




0




0




0




4




6




0




0




5




3






Wheat




5




2




0




0




7




8




0




1




6




3




0




0




0




3




5




3




0




0




0




0




0




0




5




4




0




0




0




8











Wild oats




8




9




0




0




9




9




3




8




6




9




0




9









9




9




8




0




0




0




4




8




3




10




10




7




0




2




10




8
















COMPOUND








































Rate 250 g/ha




736




737




738




739




740




741




742




743




744




745




746




747




748




749




750




751




752




753




754




755




756




757




758




759




760




761




762




763




764









Preemergence






B. signalgrass




3




8




10














2




0




4




9




10




9









3




8




8














9




8




0




0




2




7




8




10




0




6




9




9






Bedstraw




0




0




0




10




0




0




0




0




0




5














0




0




0




9




10




3




0




0




0




0




3




0




0




0




0




7




5






Blackgrass




4




9




10




3




8




0




0




9




9




9




10














6




8




10




9




9




9




0




4




3




8




5




6




0




7




9




8






Cocklebur




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




2




3




7




2




0




0




0




0




5




2




3




6




0




0









8




0




0




0




0




0




0









0




0




0




0




0




6






Crabgrass




4




10




9




9




9




5




0




9




9




10




10




10




10




10




9




10




10




9




9




0




9




9




10




8




10




5




4




10




10






Giant foxtail




9




10




10




9




9




9




0




9




9




10




10




10




10




10




10




10




10




9




9




0




9




9




10




10




10




8




9




9




10






Morningglory




2




2




2




0




0




0




0




0




0




0




6




0




0




0




6




5




0




0




1




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




4




0




0




0




0




2




5




0









4




0




0




7




0









0




3




0




0




0




0




0




0




0




0









0






Rape




0




5




6




0




5




0




0




9




6




7




9




10




0




0




8




7




5




7




6




0




0




0




4




0




2




0




0




6




9






Redroot pigweed




2




6




8




9




9




0




0




9




9




10




10




8




10




7




10




10




10




9




9




0




0




2




8




3




9




0




3




10




10






Soybean




2




0




0




0




0




0




0




0




0




0




5




0




0




2




5




7




0




0




0




0




0




0




0




0




0




0




0




0




3






Sugarbeets




0




6




6




2




3




0




0




4




7




4




7




7




2




6




5




5




3




1




3




0




0




0




7




4




3




0




4




3




5






Velvetleaf




0




4




6




2




0




3




0




3




0




4




7




7




0




0




7




8




0









3




0




0




0




4




0




0




0




0




1




5






Wheat




3




2




5




0




0




0




0




0




3




0




8




0




0




1




5




5




0




3




7




0




0




0




5




3




0




0




0




5











Wild oats




9




8




10




0




2




0




0




5




9




8




10




3




2




5




7




10




7




8




8




0




0




2




8




5




2




0




0




9




6

















COMPOUND



























Rate 250 g/ha




765




766




767




772




773




774




775




776




777




778




780




790




791




792









Preemergence






B. signalgrass




7




10









0




0




0
























8




9




0




9






Bedstraw




2




10









0




0




0




0




0









0




0




7









4






Blackgrass




8




8




10




0




0




0




9




2




10




10




9




9




7




8






Cocklebur




0









0




0




0




0




0









0




0




2




10




0




0






Corn




0




0




0




0




0




0




0




1




0




0




6




8




0




4






Crabgrass




10




10




10




0




0




0




9




9




10




10




10




10




10




10






Giant foxtail




10




9




10




0




0




0




10




9




10




10




10




lo




10




10






Morningglory




0




3




0




0




0




0




0




2




1




0




0




2




0




0






Nutsedge




0




4




0




0




0




0




0




0




2




9




0




0




0




0






Rape




5




9




9




0




0




0




0




0




0




3




2




6




3




4






Redroot pigweed




10




10




10




0




0




0




8




0









3




6




9




5




9






Soybean




0




0




2




0




0




0




0




0




0




1




2




0




5




0






Sugarbeets




8




8




8




0




0




0




3




0




2




2




4




6




0




6






Velvetleaf




6




8




2




0




0




0




0




0




0




0




3




7




0




3






Wheat




7




4




5




0




0




0




7




2




3




4




5




7




0




0






Wild oats




8




7




9




0




0




0




2




2




8




8




4




5




5




8

















COMPOUND












































Rate 125 g/ha




18




35




47




69




70




71




72




129




131




146




165




166




180




181




182




183




184




185




186




187




189




190




191




192




193




194




195




196




197




198




200









Pre-emergence






Barnyardgrass




2




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




5




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




201




202




203




204




205




206




207




208




210




211




212




214




215




216




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




232




233




234




235




236




237




238




239




240




241




242




243




244




245




246




247




248




249




250




251




252




253




254




255




256




257




258




259




264









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




265




266




267




268




269




270




271




272




273




274




276




277




278




279




280




281




282




283




284




285




286




287




288




289




290




291




293




294




295









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




3




0




4




0




6




2




0




0




0




0




7




3




1




0




0




0




4




0




4




4




0




3




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0
















COMPOUND








































Rate 125 g/ha




296




297




298




299




300




301




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




318




319




320




321




322




323




324









Pre-emergence






Barnyardgrass




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




3




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




325




326




327




328




329




330




331




332




333




334




335




336




337




338




339




340




341




346




350




351




353




354




358




365




366




367




368




369




370









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




6




8




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




2




0




6




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388




389




390




391




392




393




395




401




402




403




404




405




406




407









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




5




4




9




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









1




0




0




0




0




0




1




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0













COMPOUND








































Rate 125 g/ha




408




409




410




411




414




437




438




439




441




442




443




444




445




446




447




448




449




450




451




452




453




454




455




456




457




458




459




460




461









Pre-emergence






Barnyardgrass




0




2




4




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




482




483




485




486




487




488




489




490




492




493




494




495









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




496




498




499




509




521




528




529




531




532




538




539




546




550




552




556




558




560




561




567




568




570




577




580




586




587




588




589




590




591









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0














0




1









0









0









0









0




0




0




1




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609




610




611




612




613




614




615




616




617




618




619




620




621









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




622




623




624




625




627




628




629




630




631




632




633




634




636




637




638




639




640




641




642




643




644




645




646




647




649




650




651




655




656









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




657




658




659




660




661




662




663




664




665




666




667




668




671




674




675




676




677




678




679




680




681




692




694




695




696




697




699




701




702









Pre-emergence






Barnyardgrass




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




4




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




8




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0









0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




7




0




0

















COMPOUND
























Rate 125 g/ha




705




706




715




720




721




724




740




741




758




765




793









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




7






Rice




1




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




7
















COMPOUND






















































Rate 125 g/ha




1




2




3




4




5




6




7




8




9




10




11




12




13




14




15




16




17




18




19




20




21




22




23




24




25




26




27




28




29




30




31




32




33




34




35




36




37




38




39




40




41




42




43









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0









0














0




0




0






Bedstraw




0




0




0




5




3




0




0




2




0




0




0




0




0




0




0




0




0




7




6




3




0




2




0




3




4




0




0









0




0




0




0




1




4




2









0




0



















0




0






Blackgrass




0




0




0




4




4




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




1




5




0




0




2




0




0




4




0




5




2




0




3




0




3




0




0




0




0




0






Cocklebur




0




0




0




2




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




5




3




0




0




0




0




6




0




0




1




0




1




0




3




3




0




0




0




4




1




8




7




0




0




6




0




8




2




2




2




0




0




3




0




7




0




1




1




0




2






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0














0




0




0




0






Giant foxtail




0




0




0




5




1




2




0




0




0




5




0




0




0




0




0




0




2




1




0




0




0




2




2




2




5




0




0




2




0




2




0




0




1




0




0




3




0




2




0




0




0




0




0






Morningglory




0




0




0




2




2




0




0




0




0




2




0




0




0




2




2




1




7




1




0




7




2




2




8




9




1




1




0




2




0




1




1




7




8




2




7




9




0




0




0




6




2




0




3






Nutsedge




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




2




0




0




4




7




0




0




0




0




0




0




0




0




2




0




0




0




1




0




3




0




1




0




2




0




0




0




1




0




0




0




0




2




0




7




5




0




0




0




1




0




0




2






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0














0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0














0




0




0






Soybean




0




0




0




4




5




3




0




3




0




3




0




0




1




2




2




1




2




3




3




3




2




3




3




3




3




1




1




3




2




1




1




2




3




0




1




5




0




0




4




3




3




0




3






Sugarbeets




0




0




0




2




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




2




0




3




0




0




0




0




0




0




0




1






Velvetleaf




0




0




0




3




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND























































Rate 125 g/ha




44




45




46




47




48




49




50




51




52




53




54




55




56




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




84




85




86




87









Postemergence






B. signalgrass




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




1




0




0









0




0




0






Barnyardgrass




0




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




0




0




3




0




0




0




0




0




0




0






Bedstraw




0




5




0




3




0




0









0




5




3




0




0




0




0




0




0




7




3




0




0




0




0




0




5




7




4




0




0




0




0




0




0




0




0




0




3




0




0




0




0









0




4




4






Blackgrass




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




5




2




0




3




0




2




3




0




0









0




0




0






Cocklebur




0




1




1




0




0




0









0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0









0




1




1






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0






Crabgrass




0




0




0




0




1




1









0




1




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




4




0




2




4




9




5




0




0









0




3




3






Ducksalad




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Giant foxtail




0




0




1




0




0




4









0




3




3




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




4




0




3




2




2




2




0




0









0




2




2






Morningglory




0




0




0




2




0




0









0




1




1




0




1




1




1




0




1




2




2




2




2




0




1




1




2




2




0




0




0




0




3




2




1




2




0




8




5




8




2




7




0









0




7




7






Nutsedge




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0






Rape




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0









0




0




0






Redroot pigweed




0




0




0




0




0




0









0




0




3




0




0




0




0




0




0




4




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




3




0




0




0









0




0




0






Rice




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Soybean




0




1




1




2




1




1









0




2




3




0




1




2




1




1




1




3




3




1




2




0




1




1




1




2




2




0




0




0




0









1




1




0




1




1




1




0




0




0









0




2




2






Sugarbeets




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4









3




0




0




0









0




3




3






Velvetleaf




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




3




0




3




0




0




0




0




0




0




0




3




4




0




0




0




2




0




0




0




0




2









0




0




0






Wheat




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0






Wild oats




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0
















COMPOUND












































Rate 125 g/ha




88




89




90




91




92




93




94




95




96




97




98




99




100




101




102




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120









Postemergence






B. signalgrass




2




0




0




4




5




5




0




0




0




0




0




0




0




0




0




0




0




2




0




7




3




7




0




0




0




7




0




0




9




8




0




0




4






Barnyardgrass









0




0














0




0




0




0




0




9




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0






Bedstraw




8




0





























0




0




0









5




0









0














0




0




3




0




8









5




0




4




6




0




6




0




0




2











Blackgrass




5




0




0




8




7




8




0




0




0




0




0




3




0




0




0




1




0




6




0




7




7




8




4




3




4




8




2




4




9




9




4




3




4






Cocklebur




0




1




3




3




1




1




1




0




0




0




0




2




0




0




0




0




0




0




2




0




0




3




2




0




1




1




0




0




0




0




0




0




1






Corn




0




0




0




2




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




1




0




0




0




5




0




0




0






Crabgrass




0




0




2




9




8




8




3




0




3




2




0




2




0




0




0




4




4




7




0




8




8




9




3




2




4




9




8




0




9




9




7




3




7






Ducksalad









0




0














0




0




0




0




0




2




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0






Giant foxtail




3




0




0




8




8




7




0




0




0




0




0




0




0




0




0




1




3




3




2




8




7




9




2




2




7




9




9




4




9




9




8




8




6






Morningglory




10




0




3




7




8




10




10




1




1




1




0




3




0




0




0




10




10




2




7




3




3




3




5




5




10




5




4




3




4




7




4




7




7






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




3




0




0




0




0




0




0




0




7




7




0




0




0






Rape




0




0




0




3




3




3




2




0




0




0




0




2




0




0




0




0




0




0




0




2




0




3




4




3




2




3




3




0




0




0




0




0




0






Redroot pigweed




3




0




5




4




3




4




0




3




0




0




0




4




0




0




0




0




3




0




0




0




0




5




4




3




3




4




2




0




0




0




0




0




0






Rice









0




0














0




0




0




0




0




4




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0






S. Flatsedge









0




0














0




0




0




0




0




8




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0






Soybean




1




0




4




3




3




5




5




1




1




0




1




2




0




2




0




4




5




1




0




4




3




6




3




3




4




6




3




1




6




5




1




2




3






Sugarbeets




5




0




0




6




4




3




2




2




0




0




0




4




0




0




0




2




1




0




0




2




0




4




3




3




2




4




3




3




3




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




5




4




2




0




0




0




1




1




0




4




3




0




2




0






Wheat




0




0




0




1




2




3




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




3




0




0




6




6




0




0




0






Wild oats




0




0




0




2




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




2




0




0




7




3




0




0




0
















COMPOUND








































Rate 125 g/ha




121




122




123




124




125




126




127




128




129




130




131




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




2




5




3




0




0




0




0




4




7




2




0




0




0




0




0




0




8




7




3




0






Barnyardgrass




0




0




0




0




0




0




0




0


































0




0




0




0




0




0




0




0




8




0




6




0




0




0




0






Bedstraw





























0




0




0




0









8




0




4




4




0




5




8




7




2




5




2




2




6




2




2




6




4




5




0






Blackgrass




0




0




6




0




0




0




0




0




0




5




8




2




2




0




0




0




6




9




2




3




0




0




3




4




1




8




7




7




0






Cocklebur




2




2




0




0




0




0




0




0




0




0




3




0




2




0




0




2




0




0




0




0




0




0




3




0




0




2




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




4




2




0




0




0




0




0




0




0




5




0




0






Crabgrass




6




3




4




0




0




0




0




0




4




9




7




7




2




0




0




2




8




9




8




1




0




3




8




5




3




9




9




8




0






Ducksalad




0




0




0




0




0




0




0




0


































0




0




0




0




0




0




0




0




0




0




0




3




0




0




0






Giant foxtail




1




2




5




0




0




0




0




0




6




9




8




9




2




0




0




4




8




9




8




1




0




2




2




2




0




9




8




8




0






Morningglory




6




3




9




0




0




0




0




0




4




2




7




6




3




6




1




10




7




5




5




8




2




3




6




2




8




5




3




3




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




2




4




0




0




0




0




0









0




2




0




0




0




0




0




2




2




1




2




0






Redroot pigweed




2




1









0




0




0




0




0




0




3




6




0




0




0




0




4




4




5




3




1




0




0




5




0




0




6




3




2




0






Rice




0




0




0




0




0




0




0




0


































0




0




0




7




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




5




0




0




0




0




0




0




0


































0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Soybean




5




3




4




3




4




0




0




0




2




2




7




3




3




1




2




4




6




3




2




3




3




3




3




3




3




6




5




4




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




4




3




0




0




0




0




0




6




0




0




3




0




3




0






Velvetleaf




0




0




0




0




0




0




0




0




0




3




7




2




0




0




0




0




0




4




4




0




0




1




2




0




0




2




0




0




0






Wheat




0




0




1




0




0




0




0




0




0




1




3




2




0




0




0




0




0




8




2




0




0




0




0




0




0




2




4




1




0






Wild oats




0




0




0




0




0




0




0




0




0




2




3




2




0




0




0




0




2




2




2




0




0




0




0




0




0




3




3




1




0
















COMPOUND








































Rate 125 g/ha




150




151




152




153




154




155




156




157




158




159




160




161




162




163




164




165




166




167




168




169




170




171




172




173




174




175




176




177




178









Postemergence






B. signalgrass




0




4




0




0




0




0




0




0




0




0




0




0




0




2




0




1




0




0




0




0




6




0




0




0




0




0




0




0




0






Barnyardgrass




0




0




0




0




0




0




0









0




0




0



















0
























0




0




0
























0




0











Bedstraw




0




3




0




0




0




0




0




0




0




0




0




3




2




4




0




0




0




0




3




2




0




7




0




0




4




0




0




0




0






Blackgrass




0




8




0




0




0




0




0




0




1




0




0




0




0




4




0




3




4




0




0




4




9




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




2




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




9




0




0




0




2




0




0




0




0




0




2




2




7




0




4




1




3




1




8




9




0




3




4




4




0




0




0




0






Ducksalad




0




0




0




0




0




0




0









0




0




0



















0
























0




0




0
























0




0











Giant foxtail




1




8




0




0




0




3




0




1




0




0




0




0




2




7




0




1




0




0




0




2




7




0




0




0




0




0




0




0




0






Morningglory




0









0




0




0




0




1




1




2




2




0




5




6




2




0




3




1




5




8




1




1




1




5




10




5




1




2




0




2






Nutsedge




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




3




0




0




0




0




0




0




2




0




0




0




0




2




0




2




0




0




0




0




0




0




0




0




4




0




0




0




7






Rice




0




0




0




0




0




0




0









0




0




0



















0
























0




0




0
























0




0











S. Flatsedge




0




0




0




0




0




0




0









0




0




0



















0
























0




0




0
























0




0











Soybean




1




4




0




0




2




1




1




1




3




3




0




2




4




2




1




4




0




3




1




1




3




1




3




2




2




1




2




1




1






Sugarbeets




0




3




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0









0




0




0




0




0




0




0




0




0




0




3




4




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Wheat




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




6




0




0




0




0




0




0




0




0






Wild oats




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




179




180




181




182




183




184




185




186




187




188




189




190




191




192




193




194




195




196




197




198




199




200




201




202




203




204




205




206




207









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass








































































































0














































Bedstraw




5




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




2




0




0




0




0




0






Blackgrass




2




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




3




0




0




0




4




0




0




3




0




2




0




0




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




2




1




0




1




2




0




0




0




0




0




0




0




0




0




1




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




1




0




0




0




0




0




2




1




0




0




0




0




0




0




2




1




0




0




0




0




0




0




0






Ducksalad








































































































0














































Giant foxtail




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




2




0




0




0




0




0




0




0




0






Morningglory




5




0




0




0




0




6




1




2




0




0




0




0




2




3




0




0




0




0




5




0




4




0




1




5




0




3




0




1




2






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




4




1




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0






Rice








































































































0














































S. Flatsedge








































































































0














































Soybean




1




0




0




0




1




1




2




1




0




2




0




0




3




3




1




0




3




0




0




0




2




2




1




2




0




1




1




1




2






Sugarbeets




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0






Velvetleaf




0




0




0




0




0




1




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




1




0




0




1






Wheat




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND









































Rate 125 g/ha




208




210




211




212




213




214




215




216




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237









Postemergence






B. signalgrass




0




0




0




4




0




0




0




2




7




0




2




7




3




0




0




0




5




2




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




2




7




0




3




0




0




0




0




8




6




8




7




3




3




3




0




3




8




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




0




3




6




0




4




0




4




6




5




7




7




9




0




0




0




9




5




2




0




0




0




0




2




0




0




0




0




0






Cocklebur




0




0




0




2




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




6




0




3




0




2




2




4




4




5




6




0




0




0




8




0




0




0




0




0




0




1




0




0




0




0




0






Ducksalad























































































































































Giant foxtail




0




0




0




6




0




0




0




2




2




5




7




6




7




0




0




0




8




7




0




0




0




0




0




0




0




0




0




0




0






Morningglory




1




2




6




3




6




3




2




4




0




4




6




5




0




1




3




2




3




7




4




3




0




2




2




8




3




0




2




4




2






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




2




0




2




0




0




0




0




1




3




0




4




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0






Redroot pigweed




0




0




4




5




7




0




0




0




0




1




7




1




8




0




2




2




0




0




2




0




0




0




0




3




0




0




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




1




1




4




2




1




1




1




1




1




4




5




5




2




3




3




3




3




2




3




0




0




0




1




3




3




0




0




1




1






Sugarbeets




0




0




2




0




3




0




0




0




0




2




4




0




4




0




1




2




0




0




0




0




0




0




0




2




0




0




0




0




0






Velvetleaf




1




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0






Wheat




0




0




0




0




0




0




3




0




2




0




6




4




2




0




0




0




6




4




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




238




239




240




241




242




243




244




245




246




247




248




249




250




251




252




253




254




255




256




257




258




259




260




261




262




263




264




265




266









Postemergence






B. signalgrass




0




0




0




2




8




4




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




2




3




3




3




5




4




0




9




7




0




0




0




0




6




0




0




4




0




0




0




4




0




7









0




0




6




2




0






Blackgrass




0




0




0




7




9




8




0




7




2




0




0




0




0




4




2




0




0




2




0




0




5




0




0




0




0




0




2




4




5






Cocklebur




0




1




1




0




5




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0






Corn




0




0




0




0









2




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




7




9




8




0




7




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




1




0






Ducksalad























































































































































Giant foxtail




0




0




0




3




8




7




0




8




0




0




0




0




0




2




4




0




0




3




0




0









0




0




0




0




0




0




0




0






Morningglory




2




2




5




4




7




7




0




9




8




1




0




0




6




7




2




0




9




7




8




8




6




7




2




4




4




2




10




6




4






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




0




2




0




0




0




0




0




0




0




0




3






Redroot pigweed




0




0




2




0




4




2




0




6




2




0




0




0




0




0




0




0




2




0




1




3




2




3




2




0




3




0




0




2




3






Rice























































































































































S. Flatsedge























































































































































Soybean




1




1




1




2




5




4




0




3




1




0




0




3




2




2




1




0




1




6




3




3




4




3




1




3




3




0




3




3




7






Sugarbeets




0




0




0




0




2




0




0




2




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0






Velvetleaf




1




1




1




0




4




2




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




1




0




0




0




0






Wheat




0




0




0




2




7




4




0




5




0




0




0




0




0




0




0




0




0




4




0




0




0




3




0




0




0




0




0




0




5






Wild oats




0




0




0




0




2




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




267




268




269




270




271




272




273




274




276




277




278




279




280




281




282




283




284




285




286




287




288




289




290




291




292




293




294




295




296









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




3




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




0




4




0




6




0




0




0




0




6




0




0




0









5




1




5




5




2




8




0




3




0




3




0




2




6




4




0






Blackgrass




0




0




0




0




4




0




1




0




1




8




0




0




0




0




2




6




5




2




2




9




0




9




0




2




0




9




0




7




0






Cocklebur




0




0









0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




1




0




1




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




1




0




0




0




0




2




0




0




0




0




0




0




1




3




0




5




0




5




0




0




0




8




0




3




0






Ducksalad























































































































































Giant foxtail




0




0




0




0




3




0




0




0




1




3




0




0




0




0




0




3




2




0




0




8




0




5




0




0




0




8




0




6




0






Morningglory




1




2




3




0




2




1




0




0




6




8




3




1




0




2




6




9




7




5




3




2




8




6




6




4




1




5




6




5




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




3




0




0




0






Rape




0




0




0




0




3




0




0




0




0




2




0




0




0




0




3




3




3




0




2




0




2




2




0




1




0




0




0




0




0






Redroot pigweed




0




0




4




0




5




0




0




0




0




2




0




0




0




2




6




4




4




0




3




6




0




5




0




0




0




2




0




5




0






Rice























































































































































S. Flatsedge























































































































































Soybean




2




0




1




0




5




1




3




3




5




4




1




0




1









3




4




4




2




1




3




2




3




2




3




0




2




3




2




0






Sugarbeets




0




0




0




0




2




0




0




0




0




2




0




0




0




0




6




2




3




2




2




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




1




0




0




0




1




0




0




0




0




0




4




0




0




0




0




0




2




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




5




0




5




0




0




0




6




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




3




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




297




298




299




300




301




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




318




319




320




321




322




323




324




325









Postemergence






B. signalgrass




0




0




3




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




0




7




0




0




0




0




0




0




0




0




0




0




4




0




0




7




4




4




2




6




0




0




0




4




0




0




0




8






Blackgrass




0




0




8




0




0




0




0




0




0




0




0




0




0




7




0




0




0




4




3




1




8




0




0




0




0




0




0




0




0






Cocklebur




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




3




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




2




0




5




0




0




0




0




0




0




0




0






Ducksalad























































































































































Giant foxtail




0




0




7




0




0




1




0




0




0




0




0




0




0




7




0




0




0




0




3




0




5




0




0




0




0




0




0




0




0






Morningglory




0




3




5




0




0




1




0




3




0




2




2




0




1




5




4




0




3




2




0




4




3




0




2




1




7




4




0




0




6






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0






Redroot pigweed




0




0




3




0




0




1




0




3




3




0




0




0




0




0




0




0




0




0




0




2




0




0




0




6




3




3




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




3




3




6




2




0




2




2




4




4




2




2




1




2




4




2




2




2




3




3




3




4




0




1




3









3




1




1




2






Sugarbeets




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




3




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




326




327




328




329




330




331




332




333




334




335




336




337




338




339




340




341




342




343




344




345




348




349




350




351




352




353




354




355




356









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




1




0




0




0




2




0




0




0




0






Barnyardgrass




















































































2




0




0




0




2




2




0




3




3









4




8




0






Bedstraw




5




7




1




0




0




0




0




0




0




0




0




1




2




2




7




0




5




0




0




0




2




3














0














0




0






Blackgrass




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




3




4




4




2




8




4




5




3




6






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




1




0




0




2




0




1




1




3




0




2




0




0






Ducksalad




















































































0




0




0




0




3




0




2




0




0









3




0




0






Giant foxtail




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




8




0




8




7




2




3




4




2




4






Morningglory




7




8




8




0




0




0




0




0




0




0




0




0




0




2




7




7




7




2




0




0




9




5




6




4




6




3




5




5




6






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




1




2




0




0




0




0




0




0




0




0




0




0




2




0




0




0






Redroot pigweed




4




5




3




0




0




0




1




0




0




0




0




0




0




2




4




0




2




0




0




0




0




2




0




0




3




3




3




0




0






Rice




















































































0




0




0




0




0




0




0




0




3









0




0




0






S. Flatsedge




















































































4




0




0




0




6




5




2




6




7









8




2




4






Soybean




5




6




2




1




1




0




2




2




1




2




1




1




1




1




2




2




5




1




2




0




2




2




1




1




2




4




5




2




3






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




1




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




3




0




0




0




3




0




0




2




3






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




3




0




0




0




0




0




0




3




3
















COMPOUND









































Rate 125 g/ha




357




358




359




360




361




362




363




364




365




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388









Postemergence






B. signalgrass




0




0




0




0




0




5




0




0




0




0




5




0




2




0




2




0




0




0




0




0




0




0




0




0




0




3




3




1




6






Barnyardgrass




2




2




0




2



















0



















0




0









0












































































Bedstraw




0




2




0




0




7




9




4




0
































































0









0









0




0









0











Blackgrass




6




6




0




5




7




8




7




0




0




0




7




0




4




2




4




0




0




5




0




0




0




0




0




0




0




4




0




3




8






Cocklebur




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




2




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




2




0




0




2




2




6




2




0




0




2




8




0




7




4




2




0




0




4




0




0




0




1




0




0




1




7




7




2




4






Ducksalad




0




2




0




0



















0



















0




2









6












































































Giant foxtail




8




8




0




8




4




8




4




3




0




3




8




0




8




7




9




3




0




6




0




0




0




2




0




3




0




8




9




3




8






Morningglory




2




5




0




4




2




1




1




0




0




5




4




10




10




7




7




8




5




1




0




7




7




5




2




0




0




0




1




1




3






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0











Rape




0




1




0




0




3




0




0




0




0




0




0




0




0




0









1




2




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




3




0




0




5




4




0




0




0




0




3




0




0




0




3




3




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0



















0



















0




0









0












































































S. Flatsedge




0




0




0




4



















0



















2




3









2












































































Soybean




2




4




2




2




4




5




5




2




0




1




5




0




2




1




1




3




2




1




0




0




1




1




2




3




3




2




2




0




1






Sugarbeets




0




0




0




0




5




0




1




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




2




2




0




0




0




4




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Wheat




5




3




0




4




0




4




4




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




4




3




0




3




2




6




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




389




390




391




392




393




394




395




396




397




398




400




401




402




403




404




405




406




407




408




409




410




411




414




415




416




417




418




419




420









Postemergence






B. signalgrass




0




5




0




5




0




1




0




0




0




0




2




0




2




2




2




0




0




0




0




5




0




3




0




0




6




0




0




0




2






Barnyardgrass







































0




0




0




0
































































0




0




0




0




0




0






Bedstraw


































0





























3




2
























6




2
























3




0









0




0






Blackgrass




0














10




2









0




2




8




6




4




0









9









0




0




0




2




8




8









2




3




9




0




4




0




2






Cocklebur




0




0




0




2




0




0




0




0




0




0




0




0




1




0




2




0




0




0




0




0




0




1




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0






Crabgrass




3




7




0




2




1




2




2




0




6




3









0




3




3




3




0




0




0




4




9




4




4




3




1




6




0




0




0




2






Ducksalad







































0




0




0




0
































































0




0




0




0




0




0






Giant foxtail




2




9




0




9




8




7




3




0




8




8




8




0




8




3




9




0




0




0




9




8




9




9









8




8




0




0




0




8






Morningglory




3




3




0




7




0




2




0




5




5




2




1




3




5




6




6




2




1




10




6




8




6









7




4




8




3




3




2




4






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape









8




0




0









0




0




0




0




0




0









8




3




3




0




0




0




0














6




0




0




0




0




0




0




0






Redroot pigweed




0




5




0




0




0




0




0




0




0




0




0




0




4




0




2




0




0




0




0




2




0




3




0




0




2




0




0




0




0






Rice







































0




0




0




0
































































0




0




0




0




0




0






S. Flatsedge







































0




0




0




0
































































2




0




6




3




0




0






Soybean




2




2




0




1




1




4




0




2




5




3




2




1




5




4




4




2




1




1




2




4




4




4




2




3




6




4




4




2




2






Sugarbeets




0




2




0




0




0




0




0




0




0




0




0




0




2




0




1




0




0




0




0




0




6




0




0




0




0




0




0




0




0






Velvetleaf




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0






Wild oats




0




1




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




2




0




0




0




0
















COMPOUND








































Rate 125 g/ha




421




422




423




424




425




426




427




428




429




430




431




432




433




434




435




436




437




438




439




440




441




442




443




444




445




446




447




448




449









Postemergence






B. signalgrass




3




0




0




0




2




5




0




0




0




1




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0



















0



















































Bedstraw




4














0





























0














2




0




0




0




0




0









0







































0











Blackgrass




8




0




0




0




3




6




0




0




2




3




0




2




5




0




0




0




0




0




0




0




0




0




0




2




0




8




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




7




0




0




0




7




6




0




0




1




2




0




0




2




0




2




0




1




4




0




2




0




0




0




2




1




9




0




0











Ducksalad




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0



















0



















































Giant foxtail




9




0




0




0




7




7




2




0




1




8




0




3




4




0




3




0




0




5




0




4




0




0




0




7




0




9




0




0




0






Morningglory




8




0




2




0




5




7




0




1




1




2




1




1




2




0




2




0




1




8




0




8




0




4




3




0




4




2




2




0




5






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




2




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




1




0




0




0




2




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0



















0



















































S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0



















0



















































Soybean




6




3




2




0




1




4




1




1




2




1




1




1




2




0




1




0




0




1




0




6




0




0




1




1




1




2




1




1




1






Sugarbeets




0




0




0




0




2




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Wheat




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




450




451




452




453




454




455




456




457




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




0




1




0




0




0




2




3






Barnyardgrass























































































































































Bedstraw









0





























0
























0


































0



















6









0




0




0




0






Blackgrass




0




0




0




0




0




8




4




0




3




1









0




0




0




2









0




5




7




0




2




0




0









0




0




2




0




3






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




2




0





























0




8




1




6




0




0




0




1




9




0









6




0




3




7




2




5




0




2




3




3




6






Ducksalad























































































































































Giant foxtail




5




0




4




5




2




7




2




0




9




0




0




0




0




0




5









0




3




9




0




1




7




2




6




0




2




6




3




5






Morningglory




0




1




2




0




9




8




3




0




0




8




7




7




0




0




1




2




7




3




9




0




3




3




1




1




0




7




3




10




4






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2




0




2




0




0




0




2




0




1




0




0




2




2




0






Rice























































































































































S. Flatsedge























































































































































Soybean




1




1




1




1




2




2




3




0




1




3




3




3




1




1




1




4




0




1




1




0




2




2




1




4




1




1




2




1




3






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf 0





0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




1




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




481




482




483




485




486




487




488




489




490




492




493




494




495




496




497




498




499




500




501




504




505




506




508




509




510




511




512




513




514









Postemergence






B. signalgrass




0




0




0




0




0




0




4




2




4




0




0




0




0




0




0




0




0




5




6




3




3




0




0




0




4




0




1




3




0






Barnyardgrass























































































































































Bedstraw









0









0




1




2




2




3




3





























0














9









8





























8





















Blackgrass




0




0




0




7




6




0




8




6




4




0




0




0




0




3




0




0




0




4




6




7




4




0




3




5




5




0




3




4




3






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




3




0




0




1




0




3




0




2




3




1






Corn




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




2




3




0




0




0




0




0




0




0




0






Crabgrass




2




0




0




6




3




3




7




5




6









0




0




0




0




0









0




9




8




8




7




3




9




9




8




3




2




4




9






Ducksalad























































































































































Giant foxtail




2




0




0




7




7




2




8




8




8




0




0




0




0




0




0




2




0




8




8




9




8









8




7




6




3




3




5




9






Morningglory




0




7




0




10




1




10




2




7




3




5




0




0




1




8




0




3




3




3




3




4




5




0




3









5




4




5




3




7






Nutsedge









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




2




0









0




0




0









0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




2




4




0




0




5




0




4




1




0




4




6






Redroot pigweed




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




9




4




8




0




0




7




0




7




6




7




6




2






Rice























































































































































S. Flatsedge























































































































































Soybean




4




1




0




4




4




4




4




5




5




0




0




0




0




3




1




1




1




4




3




6




2




2




4




3




7




4




4




7




7






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




5




7




5




6




1




0




4




0




0




4




3






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




4




0




0




1




4




4




1




0




3




2






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0














3




2




0




0




0




0




0




0




5




0






Wild oats




0




0




0




0




0




0




0




1




5




0




0




0




0




0




0




0




0




0




0




6




2




0




0




0




0




0




0




4




0
















COMPOUND








































Rate 125 g/ha




515




516




517




518




519




520




521




522




523




524




525




526




527




528




531




532




533




534




535




536




540




541




543




544




545




546




548




549




550









Postemergence






B. signalgrass




0




0




4




7




0




0




0




5




0




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




6









7
























0




0
























0




0




0



















0




3









0




2




0




9




4




0




0






Blackgrass




0




4




3




7




0




0




2




8




0




2




6




6




3




0




0




0




2




2




4




0




0




0




0




0




0




0




0




0




0






Cocklebur




3




3




0




0




0




0




0




3




2




0




2




0




0




0




0




0




2




0




0




0




0




0




0




3




3




0




0




0




0






Corn




0




0




0




0




0




0




0




3




0




2




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




8




9




7




2




2




3




4




8




8




8









9




4




9




8




4




8




5









5




5




0









8




2




7




5




3




7






Ducksalad























































































































































Giant foxtail




9




5




8




0




4




4




8




8




2




8




8




3




8




3




8




4




8




3









0




0




0




0




0




0









0




2




6






Morningglory




2




3




2




5




0




4




4




4




3




2




2




6




3




3




4




3




4




2




2




2




4




1




2




4




4




4









4




1






Nutsedge




0




0




0




0




0




0




0




0




0









0




0









0




0




0




0




2




0




0




0




0




0




0














0




0




0






Rape




4




4




0




7




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




0




3






Redroot pigweed




4









4




0




0




3




0




4




2




0




2




0




0




0




0




0




9




3




0




0




0




0




0




0




0









0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




4




4




6




5




3




4




4




6




5









5




3




4




3




3




2




4




4




6




4




1




0




2




2




1




1




2




2




2






Sugarbeets




3




0




0




3




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Velvetleaf




4




4




0




2




2




4




0




5




3




0




3




4




2




4




0




0




4




2




0




0




0




0




0




0




3




0




0




0




0






Wheat




0




1




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




2




0




2




0




0




0




4




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2
















COMPOUND








































Rate 125 g/ha




551




552




553




554




555




556




557




558




559




560




561




562




563




564




565




566




567




568




569




570




571




572




573




574




575




576




577




578




579









Postemergence






B. signalgrass




0




0




0




0




0




2




2









9




3




0









4









0




8




0




4




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




5




2




5




9




0









0




0



















0









0









0




2












































4




8




0






Blackgrass




7




0




0




3




2




3




0




0




7




5




5




3




0




4




0




2




0




8




0




0




0




0




0




6




0




0




0




0




0






Cocklebur




0




0









0




0




0




0




0




0




0




0




2




0




0




0




2




0




1




2




0




0




0




0




2




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




6




9




3









0




2




5




0




4




4




3




5




9




3




0




8




7




8




0




0




0




0




9




2




2




3




0




2




6






Ducksalad























































































































































Giant foxtail









3




7




6




0




7




6




2




9




7




4




7




8




3




0




8




0




9




3




0




0




0




3




7




2




3




2




4




2






Morningglory




2




1




0




2




2




2




8




10




10




7




4




4




6




7




5




5




4




10




10




10




10




3




10




10




6




2




9




10




10






Nutsedge









0




0




0




0




0




0




0




0




3




2









0









0




0









0




0




0




0




0




0









0




0














0






Rape




7




6




6




0




5




0




0




0




0









4




0




0




0




0




0




0




0




0




0




0




3




2




0




0




0




0




2




0






Redroot pigweed




0




0




0




5




0




3




0




0




0




5




0




9




0




3




0




5




0




0




0




0




0




0




0




0




0




0




0




3




0






Rice























































































































































S. Flatsedge























































































































































Soybean




2




3




2




2




4




0




0




3




4




2




5




3




5




5




3




4




4




5




5




0




2




3




2




4




5




2




2




3




2






Sugarbeets




3




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




5




0




0




3




3




0




0




0




0




0




0




0




2




0




0




0




2




0






Wheat




0




0









0




0




0




0




0




2




0




2




4




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




2




0




0




2




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




580




581




582




584




585




586




587




588




589




590




591




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609




610









Postemergence






B. signalgrass




2




5




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




10




1




6






Barnyardgrass























































































































































Bedstraw









8




7




5




8




0






















































0



















3
























0









0











Blackgrass




6




4









7




6




1




3




0




0




0




0




0




0




5




7




0




0




0




0









6




0




0




0




0




4




6




8




9






Cocklebur




3









0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




1






Corn




0




4




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




7




0




7




5




3




0




2




0




0




0




0




0




7




8




0




0




0




1




4




4




0









0




3









3




9




9






Ducksalad























































































































































Giant foxtail




6




8




4




8




6




2




0




4




0




0




0




0




0




7




9




0




0




0




0




7




8




0




2




0




0




6




7




9




7






Morningglory




7




8




10




4




8




10




4




7




3




3




0




1




0




2




2




0




0




1




0




1




1




0




1




6




10




8




7




10




8






Nutsedge




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0






Rape




6




7




0




4




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




5




0




2






Redroot pigweed




5




8




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




0




5




0




2






Rice























































































































































S. Flatsedge























































































































































Soybean




4




4




3




3




0




3




4




4




3




1




1




1




0




0









2




0




2




2




4




3




0




1




2




2




4




4




6




7






Sugarbeets




4




5




0




2




2




0




0




0




0




0




0




0




0




5




3




0




0




0




0




0




0




0




0




0




0




0




5




0




0






Velvetleaf




2




4




0




3




3




0




0




0




2




0




0




0




0




3




4




0




0




0




0




0




0




0




0




0




0




0




0




3




3






Wheat




0




4




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0









0




1






Wild oats




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




4




0




3
















COMPOUND








































Rate 125 g/ha




611




612




613




614




615




616




617




618




619




620




621




41 622




623




624




625




627




628




629




630




631




632




633




634




635




636




638




639




640




641









Postemergence






B. signalgrass




3




3




3




0




0




0




0




0




0




0




0




0




0




7




0




7




8




1




0




3




0




0




0




0




0




4




0




0




0






Barnyardgrass























































































































































Bedstraw



















0




0




0
























0



















0














5














0




0




0




7




7


























Blackgrass




9




9




9




0




0




0




0




0




0




0




0




0




3




5




2




8




8




8




0




8




4




0




6




3




0




4




0




4




0






Cocklebur




2




0




2




0




0




0




0









0




0




0




0




0




0




0




0




1




0




0




0




0




0




1




2




3




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




6




3




0




5




3




0




0




0




2




2




0




0




0






Crabgrass




8




8




9




1




0




2




0




0




0




2




3




2




0




7




0




8









3




5




9




6




0




3




9




9




5









2




0






Ducksalad























































































































































Giant foxtail




8




9




9




0




0




3




0




0




0




0




0




3




0




8




3









9




8




7




9




7




0




8




8




7




6




0




0




0






Morningglory




8




8




7




2




1




0




0




0




1









2




1




6




1




1




6




2




2




2




4




1




2




1




4




2




2




3




3




1






Nutsedge




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0




5




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




6




0




0




0




0






Redroot pigweed




2




2




2




0




0




0




0




0




0




0




0




0




0




0




0




3




3









0




0




0




0




2




0




0




0




4




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




7




5




5




3




1









1




0




1




1




5




4




0




3




2




4









6









5




2




2




2




4




2




1




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




2




0




0




0




0






Velvetleaf




3




3




4




0




0




0




0




0




0




0




0




0




0




0




0




4




6




5




4




4




0




0




0




0




3




2




0




3




0






Wheat




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




3




4




0




0




2




0




0




0




0




0




0




0




0




0






Wild oats




2




6




7




0




0




0




0




0




0




0




0




0




0




0




0




2




3




0




0




0




0




0




0




0




0




1




1




0




1
















COMPOUND








































Rate 125 g/ha




642




643




644




645




646




647




648




649




650




652




653




654




655




656




657




658




659




660




661




662




663




664




665




666




667




668




670




671




672









Postemergence






B. signalgrass




0




0




0




0




0




6




0




0




0




0




0




0




0




2




2




0




5




0




0




0




0




0




0




4




4




2




7




1




3






Barnyardgrass























































































































































Bedstraw


































0

















































0




0




0
























0









0









0











Blackgrass




0




0




0




0




0









0




0




0




0




0




0




0




7




8




3




6




0




0




0




0




7




7




8




8




8




4




6




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




1




3




0




2




0




1






Corn




0




0




0




0




0




2




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




4




0




4




0




0






Crabgrass




0




0




0




0




0




9




0




2




1




0




0




0




8




0




8




2




6




1




2




0




0




1




7




9




8




9




8




1




6






Ducksalad























































































































































Giant foxtail




0




0




0




0




0




9




0




2




2




3




0




2




7




9




8




3




7




4




3




0




0




6




4




8




9




9




9




5




5






Morningglory




0




4




0




0




0




0




10




7




10




3




1




4









2




5




7




10




4




0




7




0




2




6




1




2




3




3




1




8






Nutsedge




0




0




0




0




0




0




0




0




2




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




4




0




0






Rape




0




0




0




0




0




0




0




0




0









0




0




2




0




2




0




0




0




0




0




0




0




0




0




4




3




2




0




3






Redroot pigweed




0




0




3




2




0




4




3




0




6




0




0




0




2




0




2




6




0




2




0




0




0




2




3




1




5




5




7




1











Rice























































































































































S. Flatsedge























































































































































Soybean




2




1




0




1




1




3




2




2




4




0




0




0




2




2




1




4




3




3




1




1




0




4




2




4




3




2




2




2




2






Sugarbeets




0




0




0




0




0




2




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0






Velvetleaf




0




0




0




0




0




5




0




0




0




0




0




0




0




0




3




0




3




2




0




0




0




0




2




2




6




0




5




0




6






Wheat




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




1




1




0




0




0




0




0




0




0




0




0




0




0




0




2




1




0




0




0




1




0




0




0




0




4




0




0




0




0
















COMPOUND








































Rate 125 g/ha




674




675




676




677




678




679




680




681




708




709




710




711




712




713




714




722




736




739




740




741




743




744




745




746




747




748




749




750




751









Postemergence






B. signalgrass




5




4




4




0




0




0




0




0




0




0




5




6




0




3




2




0




0




2




0




0




0




2




0




4




3




2




2




2




3






Barnyardgrass























































































































































Bedstraw









1














0




0




0




0




0









1



















3














3




0




0




0














7




8




6














5






Blackgrass




7




5




6




0




0




0




0




0




0




0




6




7




0




3




7




0




0




3




3




0




5




5




3




7




7




6




5




7




6






Cocklebur




0




3




0




0




0




0




0




0




0




0




0




1




0




2




2




0




0




2




0




0




0




0




0




2




0




0




2




0




2






Corn




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




8




8




7




0




0




0




0




0




0




3




9




8




4




9




9




0




3




9




0









5




4




4




9




9




3




8




9




8






Ducksalad























































































































































Giant foxtail




9




9




8




0




0




0




0




0




2




4




8




8




8




9




6




2




2




9




7




0




7




8




2




8




9




6




5




8




9






Morningglory




2




2




2




2




6




0




1




0




2




0




4




2




4




3









9




6









3




1




3




2




3




8




9




6




3




3




8






Nutsedge




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




2









0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




3




0




5




0




0




0




0




0




0




2




0




4




4




3




2




4




3






Redroot pigweed




3




2




2




2




0




0




0




0




0




5




8




7














8









2




3




2




7




0




0




2




5




4




4




4




7




6






Rice























































































































































S. Flatsedge























































































































































Soybean




3




5




3




0




1




0




0




0




4




3




4




4




5




4




4




0




3




3




3




2




0




3




3




3




4




3




4




6




3






Sugarbeets




0




2




0




0




0




0




0




0




0




0




0




2




3




0




6




0




0




3




0




0




0




0




2




0




0




2




3




3




3






Velvetleaf




6




2




3




0




0




0




0




0




0




4




6




5




5




6




2




0




2




0




0




0




0




0




0




6




4




0




3




3




2






Wheat




0




3




0




0




0




0




0




0




0




0




0




0




0




1




0




0




2




0




0




0




0




0




0




4




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




2




2




0




0




0




0




0




0




2




0




0




0




0




0

















COMPOUND








































Rate 125 g/ha




752




753




754




756




757




758




759




760




761




762




763




764




765




766




767




772




773




774




775




776




777




778




779




780




790




791




792









Postemergence






B. signalgrass




0




0




2




0




0




5




3




0




0




0




3




0




7




2




2




0




0




0




2




0




2




2




3




5




6




0




0






Barnyardgrass













































































































































Bedstraw




0









0




0




0




7














0




0




0




5









0




7




0




0




0




0




3




0




0




0




0




0









7






Blackgrass




2




2




4




0




0




6




5




0




0




0




5




6




5




5




9




0




0




0




0




2




0




4




0




2




5




2




7






Cocklebur




3




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




1






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




1






Crabgrass




3




4




5




0




4




3




4




6









0




5




6




5




6




8




0




0




0




3




2




4




3




4




4









4




9






Ducksalad













































































































































Giant foxtail




9




8




8




0




2




9




5




7




0




0




8




7




8




8




8




0




0




0




7




2




8




8




9




8




9




2




9






Morningglory




2




2




10




7




6




4




3




3




6




2




7




1




6




2




5




0




0




0




5




7




8




4




6




4




4




3




7






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0









0




0




0




0




0




0






Rape




2




0




0




0




0




0




0




1




0









0




0




0




0









0




0




0




0




2




0




2




0




0




0




3




3






Redroot pigweed




5




5




0




0




3




8




0




0









0




0




5




7




6




9




0




0




0




3




2




2




3




2




0




5




6




6






Rice













































































































































S. Flatsedge













































































































































Soybean




5




4




0




2




4




4




3




4




3




2




2




3




3




2




2




0




0




0




5




2




3




3




2




3




3




4




5






Sugarbeets




3




0




0




0




0




0




0




0




3




5




0




0




0




0




3




0




0




0




0




0




3




0




3




0




0




0




1






Velvetleaf




0




0




0




0




2




6




5




0




0




0




0




1




6




3




2




0




0




0




2




3




2




3




2




2




4




2




5






Wheat




5




0




3




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




1




2




0




0




4




0




0






Wild oats




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




2




0




0




0




0




0
















COMPOUND























































Rate 125 g/ha




1




2




3




4




5




6




7




8




9




10




11




12




13




14




15




16




17




18




19




20




21




22




23




24




25




26




27




28




29




30




31




32




33




34




35




36




37




38




39




40




41




42




43




44









Preemergence






B. signalgrass




0




0




0




7




3




0




0




0




0




5




0




0




0




0




0




0




4




0




2




0




0




2




0




4




0




0




0




0




0




0




0




0




0




1




0




8




0




4




0




0




0




0




0




0






Bedstraw




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




0




0




6




3




0




0




0




0




4




0




0




0




0




0




0




2




0




2




1




0




4




1




1




3




0




0




0




0




3




2




2




0




5




2




5




0




6




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0











Corn




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




4




0




0




10




3




7




7









3




7




0




0




2




0




2




2




6




5




5




2




7




4




3




6




8




0




0




7




4




9




9




6




3




7




3




9




0




5




3




4




4




0




0




0






Giant foxtail




7




6




0




9




7




3




2




5




0




6




0




0




3




9




8




2




7




5




2




5




8




4




2




7




7




0




0




5




1




3




8




8




6




6




7




10




0




10




0




9




9




0




0




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




5




6




5




0




4




0




0




0




0




0




0




0




0




10




7




0




2




6




2




0




6




0




0




0




0




0




0




0




0




0




2




0




0




0




10




5




1




1




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




4




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




2




0




2




0




0




2




0




6




0




0




0




0




0




0
















COMPOUND























































Rate 125 g/ha




45




46




47




48




49




51




52




53




54




55




56




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




85




86




87




88




89




90









Preemergence






B. signalgrass




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




3




0




0




0




0




0




0




1




0




0




1




0




0




0




0




0




0




2




2




2




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




1




2




0




4




2




2




4




0




0




0




3




3




4




0




0






Cocklebur




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




1




4




2




6




7




0




1




5




2




0




0




0




0




0




1




4




3




0




0




2




2




4




3




0




0




0




0




5




2




8




4




2




9




7




3




4




0




0




0




8




8




7




0




2






Giant foxtail




10




10




2




9




8




2




5




3




3




0




0




0




0




0




3




7




5




0




0




4




4




7




9




0




0




0




0




7




7




9




9




0




8




8




8




7




0




0




0




9




9




6




0




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




2




0




0




0




0




0




0




2




0




0




0




4




7




0




0




0




0




4




4




10




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




3




0




0




0




0




0




0




3




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




2




2




0




0




0




0




0




2




0




0
















COMPOUND










































Rate 125 g/ha




91




92




93




94




95




96




97




98




99




100




101




102




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120




121









Preemergence






B. signalgrass




10









7




1




0




0




2




0




0




0




0




0




5




0




1




0




7




6




9




7




1




0




9




0




2




8




9




2




7




3




4






Bedstraw




1




0




0




0




0




0




0




0




0









0




0




0




0




0




0




7




5




10




4




0




0




6




0




0




8




0




0




0




0




0






Blackgrass




10




10




10




1




2




3




1




6




3




0




0




0




0




3




7




0




10




7




8




3




0




0




9




8




0




9




8




2




8




3




4






Cocklebur




0









2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0






Corn




6




2




7




2




0




0




0




0




0




0




0




0




0




0




0




0




7




0




3




3




1




0




4




0




0




2




2




0




0




0




0






Crabgrass




10




10




9




3




6




4




0




7




8




0




0




0




6




0




8




0




10




9




10




3




7




6




10




7




4




10




10




9









6




7






Giant foxtail




10




10




10




9




4




2




3




8




10




0




0




4




9




4




10




5




10




10




10




10




9




10




10




9




9




10




10




10




10




9




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




2




2




0




0




0




0




0




2




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




8




9




7




0




0




0




0




0




0




0




0




0




0




0




1




0




8




0




8




1




0




0




7




3




0




9




10




0




6




0




0






Redroot pigweed




9




7




8




0




6




6









4




0




0




0




0




0




0




3




0




10




3




10




6




6




2




8




8




5




10




10




0




10




8




7






Soybean




0




3




2




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




7




5




4




0




8




0




0




7




8




0




0




0




0






Sugarbeets




7




6




7




0




1




0




3




0




2




0




0




0




0




0




1




0




7




3




10




1




0




0




8




6




0




10




8




0




4




2




3






Velvetleaf




6




6




6




0




0




0




0




0




0




0




0




0




0




0




4




0




10




4




7




5




0




2




7




4




0




9




8




0




4




0




0






Wheat




4




6




3




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




5




0




0




0




4




0




0




5




4




0




0




0




0






Wild oats




9




8




8




3




0




0




2




0




3




0




0




0




0




2




3




0




9




9




10




3




0




0




10




7




0




7




6




1




6




2




0
















COMPOUND








































Rate 125 g/ha




122




123




124




125




126




127




128




129




130




131




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149




150









Preemergence






B. signalgrass




0




0




0




0




0




0




0




2




9




8




3




5




2




0




3




5




4




2




0




0




0




0




0




0




9




7




5




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




7




7




0




0




0




0




0




0




0




9




2




0




0




0






Blackgrass




0




0




0




0




0




0




0




0




9




10




6




3




0




0




4




9




9




6




0




0




0




5




1




1




10




8




4




0




0






Cocklebur









0









0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




3




5




0




0




0




0




0




0




3




0




0




0




0




0




0




0




5




7




0




0




0






Crabgrass




4




5




0




0




0




0




0




7




9




7




7




3




6




0




4




10




9




10




6




0




2




7




7




4




8




8




8




0




1






Giant foxtail




9




9




0




0




0




0




0




7




9




10




8




7




9




0




4




9




9




10




8




0




4




9




6




3




10




8




9




0




0






Morningglory




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




1




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




9




10




0




0




0




0




0




4




9




0




0




0




0




3




0




0




10




7




0




0




0






Redroot pigweed




5




4




0




0




0




0




0




2




10




10




6




0




0




3




8




10




10




8




0




0




0




0




0




0




10




8




9




0




8






Soybean




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




3




0




0




0






Sugarbeets




0




3




0




0




0




0




0




3




9




8




5




2




2




0




4




10




10




3




0




0




0




1




0




0




9




2




6




0




0






Velvetleaf




0




0




0




0




0




0




0




0




8




8




4




0




0




0




0




6




8




3




0




0




0




0




0




0




7




4




6




0




0






Wheat




0




0




0




0




0




0




0




0




3




8




0




0




0




0




0




4




5




0




0




0




0




0




0




0




2




6




3




0




0






Wild oats




0




2




0




0




0




0




0




5




8




10




5




2




0




0




0




8




9




7




0




0




0




5




2




0




10




6




6




0




0
















COMPOUND








































Rate 125 g/ha




151




152




153




154




155




156




157




158




159




160




161




162




163




164




165




166




167




168




169




170




171




172




173




174




175




176




177




178




179









Preemergence






B. signalgrass









4




0




0




0




0




0




0




0




0




0




2




2




0




4




0




5




2




7




9




1




5




0




0




0




0




0




7




8






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Blackgrass




9




0




0




0




0




0




0




0




0




0









2




7




0




3




0




0




1




3




10




0




0




0




2




0




0




0




0




0






Cocklebur









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Crabgrass




10




0




0




0




0




4




2




3




0




0




8




8









0




7




4




8




3




8




10




7




8




6




8




6




8




6




2




7






Giant foxtail




10




0




0




0




0




2




6




4




0




0




9




7




8




0




7




5




9




8




10




10




7




9




9




9




7




6




3




4




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0






Rape




8




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




2




8




0




0




0




0




0




0




0




0




0






Redroot pigweed




10




0




0




7




0




4




0




0




0




0




0




0









0




0




0




6




0




6




10




0




6




0




6




0




0




0




0




7






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0






Sugarbeets




8




0




0




0




0




0




0




0




0




0




0




0




3




0




4




0




2




0




0




8




0




2




2




3




0




0




0




0




0






Velvetleaf




8




0




0




0




0




0




0




0




0




0




0




0




2




0




1




0




0




0




2




7




0




0




0




0




0




0




0




0




0






Wheat




2




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0






Wild oats




9




0




0




0




0




0




0




0




0




0




0




0




3




0




4




0




0




0




8




9




2




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




180




181




182




183




184




185




186




187




188




189




190




191




192




193




194




195




196




197




198




199




200




201




202




203




204




205




206




207




208









Preemergence






B. signalgrass




0




0




0




0




5




0




0




0




0









0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0






Blackgrass




0




0




0




0




3




0




0




0




0




4




0




0




5




0




2




1




0




0




0




10




5




0




0




0




2




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




5




6




6




0




0




0




0




3




6




4




9




4




0




0




0




6




2




5




4




0




8




0




0




0




5






Giant foxtail




0




0




0




0




9




5




9




0




2




0




0




8




9




4




8




3




0




0




0




10




4




6




6




0




9




0




3




6




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0









0




0




0




0









0




0




0














0




0




0




0




0




0









0




0









0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




2




0




7




0




0




0




0




7




0




0




0




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




0




2




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




210




211




212




213




214




215




216




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237




238









Preemergence






B. signalgrass




0




0




1




0




0




0




1




0




4




6




7




5




0




0




3




7




6




0




0




0




0




0




0




2




0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




5




4




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




9




4




0









6




2




6




9




10




9




7




0




1




2




10




10




5




0




0




0




0




6




2




0




0




2




0




0






Cocklebur




0




0









0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




4




0




0




4




3




4




4




8




7




8




6




6




5




10




9




10




0




0




1




0




7




6




0




0




3




0




6






Giant foxtail




0




4




4




2




3




3




6




8




9




10




9




9




5




9




7




10




10




10




6




0




2




0




8




7




0




0




7




0




6






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0









0




0









0




0




0



















0




0




0









7









0




0




0




0




0




0





























0






Rape




0




0




0




0




0




0




0




0




0




0




6




6




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




9




4




0




4




0




5




1




4




2




10




0




0




0




7




0




5




0




0




0




0




0




6




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




5




0




0




2




0




0




1




4




6




4




0




0




0




2




3




3




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0









0




0




0




0




1




0




6




3




0




0




0




0




5




5




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




3




0




5




7




2




0




0




0




6




8




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




4









0




0




0




0




0




6




5




5




2




0




0




0




7




3




0




0




0




0




0




0




1




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




239




240




241




242




243




244




245




246




247




248




249




250




251




252




253




254




255




256




257




258




259




260




261




262




263




264




265




266




267









B. signalgrass




0




0




2




9




5




0




7




2




0




0




0




0




3




0




0




0




2




0




0




4




5




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




7




0




0




2




0




0




0









0




0




0




0




0




0




0




0




3




10




0









0




0




0




0




3




0






Blackgrass




3




0




6




10




10




0




10




5




0




0




0




0




8




2




0




0




10




0




0




8




10




0




0




0




0




0









8




2






Cocklebur




0




0




0









0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




3




0




5




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Crabgrass




7




4




7




10




8




0




9




3




0




0




0




4




7




2




0




0




3




2




2




7




4




2




3




2




0




2




2




1




0






Giant foxtail




10




5




10




10




10




0




9




9




0




0




0




8




10




9




0




3




9




5




6




9




9




7




8




3




9




7




8




4




8






Morningglory




0




0




0




2




3




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0









0




10




0




0



















0




0
























0














0









0




0




0




0




0














0




0






Rape




0




0




0




6




5




0




4




2




0




0




0




0




9




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




10




9




0




10




0




0




0




0




3




5




0




0




0




2




0




0




2




0




0




0




0




0




0




0




0




3






Soybean




0




0




0




2




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




7




3




0




8




1




0




0




0




0




10




3




0




2




3




0




0




2




0




0




0




0




0




0




0




5




0






Velvetleaf




0




0




5




8




6




0




7




2




0




0




0




0




4




0




0




0




0




0




0




5




2




0




0




0




0




0




0




0




0






Wheat




0




0




0




7




8




0




6




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0






Wild oats




0




0




5




9




6




0




5




3




0




0




0




0




6




0




0




0




2




0




0




4




2




0




0




0




0




4




0




2




0
















COMPOUND








































Rate 125 g/ha




268




269




270




271




272




273




274




276




277




278




279




280




281




282




283




284




285




286




287




288




289




290




291




292




293




294




295




296




297









Preemergence






B. signalgrass




0




6




0




8




0




0




0




7




9




0




0




0




0




1




10




5




5




3




10




4




7




0




3




0




3




7




6




0




0






Bedstraw




0




0




0




10




0




0




0




0




0




0




0




0




3









0




8




0




0




10




2




4




3




0




0




0




0




0




0




0






Blackgrass




0




2




0




9




0




0




0




6




9




0




0




0




1




1




8




4




4




0




10




2




9




2




8




0




7




3




10




0




0






Cocklebur




0









0




0




0




0




0




0




0




0









0









0




0









0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




2




0




5




0




6




0




4




4




1




0




0




10




1




7




4




8




2




9




2




3




3




0




0




3




9




7




0




2






Giant foxtail




0




6




0




10




5




8




3




10




10




2




3




0




9




8




9




9




9




10




10




9




10




9




9




0




9




9




10




0




0






Morningglory




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0









0




0




0




0









0




0




0




0




0




0




0




6




0




0









0




0




0




0




0




0




0






Rape




0




0




0




4




0




0




0




0




1




0




0




0




0




0









2




0




0




8




0




8




0




0




0




6




0




2




0




0






Redroot pigweed




0




0




0




8




0




0




0




0




0




0




0




0




0




6




6




6




2




0




8




0




6




7




0




0




8




0




6




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




6




0




0




0




1




1




0




0




0




0




0




0




5




0




0




6




0




6




5




0




0




4




0




0




0




0






Velvetleaf




0




0




0




4




0




0




0




0




1




0




0




0




0




0




2




0




2




0




7




0




6




0




0




0




4




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




2




0




0




0




7




0




3




0




0






Wild oats




0




2




0




5




0




0




0




2




7




0




0




0




0




2




1




0




0




0




8




2




8




4




0




0




2




0




8




0




0
















COMPOUND








































Rate 125 g/ha




298




299




300




301




302




303




304




305




306




307




308




309




310




311




312




313




314




315




316




317




318




319




320




321




322




323




324




325




326









Preemergence






B. signalgrass




0




9




0




0




0




0




0




0




0




0




0




0




4




0




0




0




2




2




7




6




0




0




1




0




0




0




0




0




0






Bedstraw




0




10









0




0




0




0









0




0




0




0




3




0




0









0









0









0




0














0




0




0




0











Blackgrass









10




0




0




0




0




0




0




0




0




0




0




10




0




0




0




7




7




10




8




0




0




2




6




0




0




0




1




5






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Crabgrass




0




9




2




0




0




0




4




4




0




0




0




1




5




0




0




0




3




5




8




7




0




0




3




2




2




0




0




0




0






Giant foxtail




0




10




5




0




6




0




4




8




2




8




0




9




10




0




0




0




6




9




10




10




0




7









8




9




0




0




7




2






Morningglory




0




2




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0














0









0




0




0




0




0




0




0




0











Rape




0




8




0




0




0




0




0




0




0




0




0




0




6




0




0




0









0




0




2




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




10




0




0




0




0




0




0




0




0




0




0




10




0




0




0




2




0




6




7




0




0




0




0




6




0




0




0




3






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




8




0




0




0




0




1




0




0




0




0




0




7




0




0




0




2




0




0




4




0




0




0




0




2




0




0




0




0






Velvetleaf




0




7




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




2




6




0




0




0




0




0




0




0




0




0






Wheat




0




7




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Wild oats




0




7




0




0




0




0




0




0




0




0




0




0




9




0




0




0




2




0




4




8




0




0




0




0




0




0




0




0




1
















COMPOUND








































Rate 125 g/ha




327




328




329




330




331




332




333




334




335




336




337




338




339




340




341




342




343




344




345




348




349




350




351




352




353




354




355




356




357









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




3









0




0




6




2




5




2




3




3






Bedstraw









0




0




0









0




0




0




0




0




0




0




0




0




0




0









0




0














10









0




0




0









0




10






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




3




8




0




0




6




2




5




2




10









4




4




6




8






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




5




3




0




0




0




0






Crabgrass




2




0




0




0




0




0




0




0




0




0




0




0




0




3




2




6




9




0




0




7




6




8




10




10




9




9




10




8




9






Giant foxtail




8




5




0




0









1




0




0




4




0




0




0




3




10




9




9




10




2




0




10




9




10




10




10




10




10




10




10




10






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




2






Nutsedge




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




1




0




2




2






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




10




10




3




10




7




7




4




10






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




2




3




2




0




0




0




3






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




3




0




2




3




4




1




5




2




2




5






Wheat









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




4




0




3




0




8




1




4




0




7




10
















COMPOUND








































Rate 125 g/ha




358




359




360




361




362




363




364




365




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388




389









Preemergence






B. signalgrass




3




0




6




4




6




3




0




0




0




6




0




0




2




4




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0






Bedstraw




9




0









0




9




9




0




0




10




2









3









2




0




0




10









0




0









0
























0
















Blackgrass




8




0




9




8




10




10




0




0




7




9




0




8




9




6




3




2




5




0




0




0




0




0




1




0




0




0




0




1




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




3




0




3




0




0




0




0




6




0




2




0




2




0




0




2




0




0




0




0




0




0




0









0




0




0




0






Crabgrass




10




0




10




7




8




7




0




0




9




10




7




8




10




9




7




6




8




0




3




0




7




0




7




8




6




9




6




8




2






Giant foxtail




10




0




10




9




10




10




6




0




10




10




9




10




10




10




8




9




10




0




4




1




8




0




9




7




10




10




3




8




8






Morningglory




0




0




5




0




4




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0









0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




5




3




1




0




0




3




0




0




0




4




5




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




9




0




5




7




10




3




0




0




10




10




4




7




10




10




3




0




10




0




0




0




3




0




0




0




0




7




0




0




0






Soybean




0




0




0




0




1




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




1




0




6




2




7




4




0




0




4




8




0




3




6




4




0




0




2




0




0




0




0




0




0




0




0




1




0




2




0






Velvetleaf




4




0




6




0




6




5




0




0




3




7




0




4




4




5




0




0




3




0




0




0




0




0




0




0




0




0




0




2




0






Wheat




0




0




6




0




8




5




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0






Wild oats




5




0




10




8




10




9




0




0




3




9




0




0




3




7




0




0




4




0




0




0




0




0




0




0




0




2




2




6




0
















COMPOUND








































Rate 125 g/ha




390




391




392




393




394




395




396




397




398




400




401




402




403




404




405




406




407




408




409




410




411




414




415




416




417




418




419




420




421









Preemergence






B. signalgrass




5




0




3




0




5




0




0




6




2




0




0




3




4




4




0




0




0




2




4




5




3




0




3




7




3




3




0




2




8






Bedstraw




0









8














0
























0




3




0














0




0
























0









































Blackgrass




9




0




8




0




8




0




0




9




8




0




0




7




7




7




0




0




0




9




7




8




7




0




5




9









4




0




8




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




3




0




3




0




0




0




0




0




0




0




0




0




2




2




0




0




0




2




8




0




2




0




2




0




0




0




0




0




5






Crabgrass




9




0




10




2




10




0




7




10




10




9




2




9




10




10




1




0




2




10




9




9




10




7




8




10




9




8




1




9




8






Giant foxtail




10




0




10




9




10




0




10




10




10




9




6




10




10




10




8




0




6




10




10




9




10




9




10




10




9




8




1




9




10






Morningglory




3




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




0




1




0




0




4




0




0




0




0




6






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0






Rape




2




0




0




0




2




0




0




9




3




0




0




1




1




4




0




0




0




0




0




0




8




0




6




9




0




0




0




0




10






Redroot pigweed




9




0




7




2




2




0




0




8




5




4




0




2




4




6




0




0




0




6




8




0




8




0




0




9




0




3




0




2




10






Soybean




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




4






Sugarbeets




7




0




3




2




3




0




0




4




4




0




0




0




1




3




0




0




0




4




7




0




8




0




0




4




0




2




0




0




10






Velvetleaf




4




0




3




0




5




0




0




2




2




0




0




0




0




1




0




0




0




1




5




4




5




0




2




3




0




3




0




2




9






Wheat




4




0




3




0




1




0




0




0




0




0




0




0




0




2




0




0




0




0




8




3




4




0




0




4




0




0




0




0




4






Wild oats




6




0




9




0




6




0




0




5




3




0




0




4




4




8




0




0




0




2




5




6




5




0




3




7




0




0




0




2




7
















COMPOUND








































Rate 125 g/ha




422




423




424




425




426




427




428




429




430




431




432




433




434




435




436




437




438




439




440




441




442




443




444




445




446




447




448




449




450









Preemergence






B. signalgrass




0




0




0




8




4




0




0




0




2




0




0




2




0




0




0




0




0




0




4




0




0




0




0




0




6




0




0




0




1






Bedstraw






































































































































0




0











Blackgrass




0




0




0




9




6




0




0




0




3




0




0




2




0




0




0




0




0




0




6




0




0




0




0




0




7




0




0




0




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




10




9




9




7




10




10









5




10




0




2




0




0




6




0




7




0




8




6




5




2




8




3




4




3




7






Giant foxtail




0




0




0




10




9




8




7




10




10




0




2




10




0




2




0




0




7




0




6




0




0




4




9




0




10




3




2




6




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




4




0




0




0




0




0




0




4




0




2




0




0




2




0




4




0




0




0




10




2




10




0




0




0




4






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




3




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0






Velvetleaf




0




0




0




0




2




0




0




0




2




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0






Wheat




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Wild oats




0




0




0




4




7




0




0




0




0




0




0




6




0




0




0




0




0




0




5




0




0




0




0




0




5




0




0




0




0
















COMPOUND








































Rate 125 g/ha




451




452




453




454




455




456




457




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




481









Preemergence






B. signalgrass




0




0




2




0




3




0




0




4




0




0




0




0




0




2




3




0




2




7




0




9




9




0




2




0




2




6




5




4




9






Bedstraw












































0




0









0














2




0







































0









8














0






Blackgrass




0




0




0




0




4




2




0




8




0




0




0




0




0




3




5




2




4




8




0




10




9




0




3




0




1




8




6




5




6






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0









0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




5




6




3




5




6




0




6




7




1




0




0




0









9




6




9




10




7




10




9




2




9




0




8




9




8




8




8






Giant foxtail




0




3




9




9




10




10




0




9




9




6




0




0




0




10




10




7




8




10




0




10




10




3




10




0




6




10




9




10




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4






Rape




0




0




0




0




3




0




0




0




0




0




0




0




0




2




0




7




0




2




0




2




0




0




0




0




0




1




0




0




0






Redroot pigweed




0




0




4




2




10




2




0




3




0




0




0




0




5




9




7




7




4




10




0




10




10




10




3




0




1




8




3









0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




1




2




0




0




0




0




0




0




0




2




0




1




0




8




0




2




2




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




4




0




0




0




0




0




0




0




0




3




0




0




0




5




0




3




3




0




0




0




0




1




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




3






Wild oats




0




0




0




0




3




0




0




2




0




0




0




0




0




0




0




0




0




7




0




4




5




0




3




0




5




7




4




2




6
















COMPOUND








































Rate 125 g/ha




482




483




485




486




487




488




489




490




492




493




494




495




496




497




498




499




500




501




502




503




504




505




506




508




509




510




511




512




513









Preemergence






B. signalgrass




0




0




5




5




3




7




7




5




0




0




0




0




0




0




0




0




9




9




9




8




10









0




7




3




7




0




8




0






Bedstraw









0


































0




0




0









0














0




9




9









5




5




0




0




0




0




0




0




0











Blackgrass




0




0




8




9




3




8




8




8




0




0




0




0




0




0




0




0




9




5




10




9




8




6




0




3




7




6




0




2




4






Cocklebur




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




2




8




5




5




2




0




0




0




0




0




0




0






Crabgrass




8




0




7




9




9




10




10




9




0




0




0




0




4




0




2




6




9




9




10




8




6




6




0




9




7




9




6




7




4






Giant foxtail




6




0




8




10




9




10




10




9




0




3




0




0




8




0




2




5




10




10




10




9




9




9




5




10




9




9









9




6






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




2




2




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




3









0




0




10




0









0




0




0









0






Rape




0




0




0




2




0




7




0




1




0




0




0




0




0




0




0




0




10




0




3




8




10




4




0




0




0




5




0




0




2






Redroot pigweed




0




0




6




8




8




10









7




0




0




0




0




0




0




0




0




10




10




9




10




10




10




8




8




0




9




6




9




7






Soybean




0




0




0




0




0




0




1




0




0




0




1




0




0




0




0




0




3




0




4




3




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




4




2




0




0




0




0




0




0




0




0




0




10




3




2




6




6




3




0




1




4




0




0




0




0






Velvetleaf




0




0




0




0




0




2




2




0




0




0




0




0




0




0




0




0




8




2




5




6




5




2




0




0




6




2




0




0




0






Wheat




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




6




4




3




2




6




7




0




0




0




0




0




2




2






Wild oats




0




0




5




3




0




8




4




7




0




0




0




0




0




0




0




0




9




7




9




10




8




2




2




4




2




6




0




2




3
















COMPOUND








































Rate 125 g/ha




514




515




516




517




518




519




520




521




522




523




524




525




526




527




528




531




532




533




534




535




536




540




541




543




544




545




546




548




549









Preemergence






B. signalgrass




6




8




5




0




3




0




0




0




9




8




0









9




2




0




2




0




3




9




0




0




0




0




4




3




0









2




0






Bedstraw









0




0




0




0




0




0




0




10




0









0




0









0














0




0




0




0




0




0




0




2




0









10




0






Blackgrass




2




5




5




2




8




0




0




0




8




4




4




7




9




2




0




9




0




8




9




0




0




0




0




0




0




0




0




3




4






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Corn




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




7




7




9




4




0




8




9




10




10




10




10




9




10




10




9




10




9




10




10




10




0




9




5




4




9




10




7




9




7






Giant foxtail




10




10




10




3




0




10




10




10




10




10




9




10




10




10




10




10




10




10




9




10




9




9




10




3




10




10




4




9




10






Morningglory




0




0




0




0




0




0




0




0




2




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge









0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




4




1




0




0




0




0




0




2




0




2




0




4




2




0




0




0




0




6




2




0




0




0




0




0




0




0




0




0






Redroot pigweed




8




9









9




2




0




0




0




10




9




8




0




4




4




0




0




0




8




0




2




0




0




0




7




3




8




3




0




6






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




5




4




3




0




2




0




0




0




5




4




3




8




6




6




0




4




2




5




4




4




0




0




0




5




0




0




0




0




0






Velvetleaf




0




0









0




0




0




0




0




6




2




3




3




2




2




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




2




0




0




0




0




0




5









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




4




5




5




4




6




0




0




0




2




0




9









9




0




0




0




0




0




8




0




0




2




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




550




551




552




553




554




555




556




557




558




559




560




561




562




563




564




565




566




567




568




569




570




571




572




573




574




575




576




577




578









Preemergence






B. signalgrass




9




9




8




9




7









7




6




0




10




7




4




8




9




6




0




9




0




6




9




0




3




0




7




7




9




3




3




3






Bedstraw




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









3




0




0




0




0




0




0




0




0




0






Blackgrass




2




7




0




7




4




0




9




6




2




10




6




7




10




8




5




0




9




0




8




0




0




2




0




0




0




6




3




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




3




0




0




3




0




4




0




2




0




4




0




0




0




0




0




0




0




0




2




2






Crabgrass




10




9




9




9




10




9




9




9




9




10




9




9




8




9




8




0




9




9




7




9




9




2




0




9




9




9




4




9




9






Giant foxtail




9




10




10




10




9




10




9




9




9




10




10




6




9




9




9




0




10




9




10




9




0




3




0




9




10




10




4




8




9






Morningglory




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0









3









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




3




0




3




0




0




3




0




0




9




3




2




6




4




0




0




0




0




0




0




0




0




0




2




0




2




0




0




0






Redroot pigweed




9




9




4




7









0




5




0




0




10




8




5




10




9




0




0




9




0




4




9




0




0




0




0




0




9




9




0




4






Soybean




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




6




0




3




0




5




0




3




0




6




0




0




8




3




2




0




4




0




5




0




0




0




0




2




0




0




0




0




2






Velvetleaf




0




0




0




0




0




0




2




0




0




4




2




0




0




3




2




0




0




0




6




0




0




0




0




0




0




0




0




3




2






Wheat




2




0




0




0




3




0




0




0




0




8




5




4




9




8




6




0




6




0




0




0




0




3




0




0




0




0




6




0




0






Wild oats




0




3




0




0




2




0




0




2




0




9




0




2




9




9




0




0




9




0




5




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 125 g/ha




579




580




581




582




584




585




586




587




588




589




590




591




592




593




594




595




596




598




599




600




601




602




603




604




605




606




607




608




609









Preemergence






B. signalgrass




0




6




0




0




7




8




5




0




1




0




0




0




0




0




3




6




0




0




2




0




7




4




0




0




0




0




7




10




6






Bedstraw




0




4




9




0









8









0



















0




0









0




8




0




0




0









0




0














0



















8






Blackgrass




0




3




0




0









8




7




3




3




0




0




0




0




0




5




9




0




0




0




0




8




4




0




0




0




0




7




5




8






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




2




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Crabgrass




7




6




9




0




8




8




9




6




6




1




0




0




0




0




9




9




0




0




3




0




9




8




0




0




3









8




9




7






Giant foxtail




9




9




10




5




8




6




10




8




8




9




0




0




0




0




9




10




0




0




9




0




10




9




0




2




10




6




10




10




10






Morningglory




0




0




2




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




3




0




0




4




8




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




6




5




0






Redroot pigweed




0




10




5




0




8




9




8




0




1




0




0




0




0




0




0




10




0




0




0




0




10




7




0




0




0




0




7




5











Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




6






Sugarbeets




0




0




0




0




2




3




0




0




0




0




0




0




0




0




0




8




0




0




0




0




4




2




0




0




0




0




0




0




3






Velvetleaf




0




0




5




0




0




0




0




0




0




0




0




0




0




0




4




7




0




0




0




0




4




6




0




0




0




0




3




4




8






Wheat




0




0




0




0




0




3




0




0




2




0




0




0




0




0




0




1




0




0




0




0




1




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




2




3




3




2




0




0




0




0




0




0




0




8




0




0




0




0




8




3




0




0




0




0




2




3




7
















COMPOUND








































Rate 125 g/ha




610




611




612




613




614




615




616




617




618




619




620




621




622




623




624




625




627




628




629




630




631




632




633




634




635




636




637




638




639









Preemergence






B. signalgrass




8




7




7




8




0




0




0




0




0




0




0




0




0




0




6




4




5




7




2




3




7




3




3




5




8




9




3




7




0






Bedstraw









1



















0




0




0




0









0




0




0









0









2




7




0




0




0














0




8




5




0
















Blackgrass




9




9




10




8




0




0




0




0




0




0




0




0




2




0




8




3




8




9




8




8




7




4




3




6









4




3




5




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




3




0




0




0




0




0




0




0




0




0




0




0






Corn




3




3




3




3




0




0




0




0




0




0




0




0




0




0




0




0




4




6




2




0




6




4




0




0









0




0




8




0






Crabgrass




10




10




10




10




6




0




0









0




1




0




6




6




0









7




8




8




9




8




7




7




8




8




9




9




9




9




7






Giant foxtail




10




10




10




10




4




0




1




9




2




3




0




7









7




10




9




10




10




10




10




9




10




9




10




9




10




10




10




9






Morningglory




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




5




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




7




6




2




0




4




0




0




0




0




0




0




5




0






Rape




8




3




3




9




0




0




0




0




0




0




0




0




0




0




0




0




3




2




0




0




0




0




0




2




6




2




0




5




0






Redroot pigweed




10




8




10




10




0




0




1




0




0




0




0




0




7




0




0




0




9




9




10




9




9




0




0




4




10




10




9




10




0






Soybean




6




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0






Sugarbeets




7




2




5




5




0




0




0




0




0




0




0




0




0




0




1




0




4




4









4




3




0




0




0




5




0




0




6




0






Velvetleaf




7




6




7




7




0




0




0




0




0




0




0




0




0




0




0




0




8









6




1




7




1




0




0









0




0




5




0






Wheat




2




3




3




3




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




3




0




0




0




0




0




0




0




0






Wild oats




6




7




9




9




0




0




0




0




0




0




0




0




0




0




6




0




3




2




0




3




2




2




2




5




6




0




0




4




0
















COMPOUND








































Rate 125 g/ha




640




641




642




643




644




645




646




647




648




649




650




652




653




654




655




656




657




658




659




660




661




662




663




664




665




666




667




668




669









Preemergence






B. signalgrass




2




0




2




2




0




0




0




7




0




0




0




0




0




0




0




2




8




0




4




1




0




0




0




5




4




3




5




8




8






Bedstraw












































0




0




0




0




0




0




0





































































7






Blackgrass




0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




4




9




7




6




4




2




3




0




6




7




8




8




8




10






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0









0




0




0




0




0




3




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




4




4









9






Crabgrass




3




3




8




3









3




0




8




8




1




8




8




2




3




8




7




10




7




8




7




0




0




0




8




8




8




8




8




9






Giant foxtail




9




9




10




8




2




2




0




10




9









10




9




0




6




9




10




10




9




9




10




6




7




3




10




10




10




10




9




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




1




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




3




0














0




0




0




0




0




0




0




0




0




0




0









0




0











Rape




0









2




0




0




0




0




8




0




0




0




0




0




0




0




0




3




5




0




0




0




0




0




1




6




8




8




5




4






Redroot pigweed




0




0




0




0




0




0




0




10




0




0




7




0




0




0




2




4




10




9




6




5




0




0




0




7




8




10




10




7




10






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




1




2






Sugarbeets




2




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




7




7




0




0




0




0




0




0




3




4




7




6




8






Velvetleaf




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




4




4




0




0




0




0




0




0




0




0




6




6




6




0






Wheat




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




3




2




0




5






Wild oats




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




6




2




0




0




0




0




0




3




5




6




8




7




10
















COMPOUND








































Rate 125 g/ha




670




671




672




673




674




675




676




677




678




679




680




681




682




683




684




685




686




687




689




691




692




693




694




695




696




697




698




699




701









Preemergence






B. signalgrass




9




6




4




6




7




6




0




0




0




0




0




0




6




0




0




7




5




9




4




8




9




0




3




0




10




0




0




9




0






Bedstraw




8









0









0




2





























0




0




0




0




0




0




0




0




9




1




0




0




0




0




0




0









0






Blackgrass




9




7




3




8




8




9




0




0




0




0




0




0




5




3




3




7




7




9




9




9




9




0




8




0




7




0




0




10




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0









0




0




0




0




0









0




0




0






Corn




4




0




0




2




3




3




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




1




0




0




0




0




6




0






Crabgrass




10




8




10




8




9




7




3




3




0




0




0




0




9




8




7




9




9









9




9




9




0




9




9




8




0




3




10




10






Giant foxtail




10




9




10




10




9




10




8




5




0




0




0




0




10




9




9




9




9




6




10




10




9




0




10




10




9




0




0




10




10






Morningglory




7




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




3




0




1




0




2




0




0




0




0




4




0






Nutsedge




5




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0











Rape




9




0




2




2




3




3




0




0




0




0




0




0




0




0




0




0




0




5




0




3




0




0




0




0




0




0




0




2




0






Redroot pigweed




10




2




3




7




7




9




9




4




0




0




0




0




4




2




0




4




6




9




7




3




8




0




4




0




3




0




0




3




0






Soybean




3




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




2




0






Sugarbeets




9




9




4




0




5




7




2




0




0




0




0




0




0




0




0




0




0




5




2




2




0




0




0




0




0




0




0




4




0






Velvetleaf




8




7




3




3




7




7




4




0




0




0




0




0




0




0




0




0




0




5




3




0




1




0




0




0




0




0




0




2




0






Wheat




9




0




0




0




5




2




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




3




0






Wild oats




9




0




4









3




5




0




0




0




0




0




0




0




0




0




3




1




9




9




6




9




0




0




0




0




0




0




10




0
















COMPOUND








































Rate 125 g/ha




702




703




704




706




707




708




709




710




711




712




713




714




715




716




718




719




720




721




722




723




724




725




726




727




728




729




730




732




733









Preemergence






B. signalgrass




2




3




5




8




7




0




0




8




2




5




7




9




8




0




2




7




9




8




0




0




0




3




7




6




8




10




0




0




6






Bedstraw




0




0




0




0




7




0




0




3




3




0




0




8




0




0




0




0




10




10




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




2




3




6




8




10




2




0




9




6




6




8




8




9




0




9




8




9




10




0




0




0




4




8




7




9




10




9




0




7






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




3




0




0




0




0




0




0




0




0




3




0




0






Crabgrass




10




8




8




5




9




7




3




10




9




9




10




10




9




0




10




3




9




9




0




2




3




6




9




8




6




9




9




0




5






Giant foxtail




10




7




7




6




10




7




4




10




10




10




10




10




10




0




10




5




10




10




0




7




0




8




9




7




7




9




10




0




6






Morningglory




0




0




0




1




3




0




0




0




1




0




0




2




1




0




0




1




0




2




2




0




0




1




0




0




0




0




0




0




1






Nutsedge




0




0




0









0




0




0




0









0




0




0




0




0









0




0




0









0




0




0




0




0




0




0




0









0






Rape




0




0




0




0




8




0




0




8




6




2




4




3




8




0




0




0




7




9




0




0




0




0




0




0




3




2




0




0




0






Redroot pigweed




5




4




5




8




10




3




0




8




7




8




7




9




9




0




4




7




9




10




0




0




0




0




4




5




7




9




9




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




3




4




6




0




0




6




6




4




4




4




5




0




0




4




6




7




0




0




0




0




0




0




0




0




2




0




0






Velvetleaf




0




0




0




1




5




0




0




6




6




3




5




5




5




0




0




0




2




5




0




0




0




0




0




0




0




2




2




0




0






Wheat




0




0




0




4




2




0




0




6




6




0




0




4




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




7




8




0




0




9




7




3




5




4




9




0




2




6




8




8




0




0




0




2




7




3




4




7




4




0




2
















COMPOUND








































Rate 125 g/ha




734




735




736




737




738




739




740




741




742




743




744




745




746




747




748




749




750




751




752




753




754




755




756




757




758




759




760




761




762









Preemergence






B. signalgrass




9




8




3




4




9














0




0




3




8




9




9




8




3




2




10














7




3




0




0




0




6




3




3




0




0






Bedstraw




0




0




0




0




0




10




0




0




0




0




0














0




0




0




0




2




10




0




0




0




0




0




1




0




0




0




0






Blackgrass




9




10




2




9




10




3




6




0




0




8




9




6




9




8




3




2




8




10




9




9




9




0




2




2




8




5




4




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0









0




0






Corn




5




6




2




2




4




0




0




0




0




0




0




0




3




2




0




0




3




4




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




9




10




3




9




9




2




4




5




0




9




9




10




10




10




10




10




9




10




9




9




9




0




9




9




9




7




7




3




4






Giant foxtail




10




10




8




10




9




9




9




2




0




9




9




10




10




10




10




10




10




10




10




9




9




0




9




9




9




9




9




0




10






Morningglory




2




0




0




2




1




0




0




0




0




0




0




0




4




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0









0




0









0




0




0




0









0









3




2




0




0




0




0




0




0




3









0




0




0




0




0




0




0






Rape




2




6




0




0




5




0




3




0




0




5




6




5




9




9




0




0




0




6




3




5




4




0




0




0




4




0




0




0




0






Redroot pigweed




7




7




0




3




7




2




9




0




0




9




8




9




10









10




5




9




10




2




8




8




0




0




0




8




2




7




0




2






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




2




2




0




5




6




2









0




0




2




2




4




7




6




0




2




3




2




0




0




0




0




0




0




7




0




3




0




0






Velvetleaf




3




0




0




0




1




0




0




3




0




2




0




0




6




6




0




0




0




8




0




0




1




0




0




0




4




0




0




0




0






Wheat




7




0




3




0




4




0




0




0




0




0




0




0




7









0




0




4




4




0




0




3




0




0




0




5




2




0




0




0






Wild oats




8




8




2




6




9




0




0




0




0




5




8




6




10









2




0




5




8




0




4




6




0




0




0




8




4




0




0




0

















COMPOUND






























Rate 125 g/ha




763




764




765




766




767




772




773




774




775




776




777




778




779




780




790




791




792









Preemergence






B. signalgrass




9




7









8









0




0




0





























6




9




0




0






Bedstraw




6




5









9




0




0




0




0




0




0




0




0




0




0




3




0




0






Blackgrass




9




7









7




10




0




0




0




5




0




2




9




9




6




9




0




4






Cocklebur




0









0




0




0




0




0




0




0









0




0




0




0




0




0











Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




2




7




0




2






Crabgrass




9




10




10




9




10




0




0




0




9




8




10




10




10




10




10




6




10






Giant foxtail




9




10




10




9




10




0




0




0




9




9




10




10




10




10




10




10




10






Morningglory




0









0




3




0




0




0




0




0




2




1




0




0




0




0




0




0






Nutsedge









0









0




0




0




0




0




0









0




0




0




0




0




0




0






Rape




5




0









5




6




0




0




0




0




0




0




0




0




0




4




0




0






Redroot pigweed




9




10









10




10




0




0




0




0




0




2




2




2




3




6




0




9






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0






Sugarbeets




0




0









6




6




0




0




0




0




0




0




2




2




2




2




0




3






Velvetleaf




1




5




4




5




0




0




0




0




0




0




0




0




2




3




2




0




3






Wheat




0




3









4




5




0




0




0




0




2




0




0




0




6




2




0




0






Wild oats




8




3









7









0




0




0




2




2




3




0




3




0




6




0




0
















COMPOUND










































Rate 62 g/ha




18




69




70




71




72




129




131




146




165




166




180




181




182




183




184




185




186




187




189




190




191




192




193




194




195




196




197




198




200




201




202









Pre-emergence






Barnyardgrass




2




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




203




204




205




206




207




208




210




211




212




213




214




215




216




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




233




234




235




236




237




238




239




240




241




242




243




245




246




249




250




251




252




253




254




255




256




257




258




259




264




265




266




267




268









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




269




270




271




272




273




274




276




277




278




281




282




283




284




285




286




287




288




289




290




291




293




294




295




296




297




298




299




300




301









Pre-emergence






Barnyardgrass




0




0




4




0




0




0




1




2




0




0




7




0




0




0




0




0




0




0




3




2




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




303




304




305




310




311




312




313




314




315




316




318




319




320




321




323




324




325




326




327




328




329




330




334




335




336




337




338




339




340









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




4




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




7






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




341




346




350




351




353




354




358




366




367




368




369




370




371




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388




389









Pre-emergence






Barnyardgrass




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0











S. Flatsedge




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




390




391




392




393




394




395




401




402




403




404




405




406




407




408




409




410




411




414




437




438




439




441




442




443




444




445




446




449




450









Pre-emergence






Barnyardgrass




2




0




0




0




0




0




0




5




2




4




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




1




0




0




0




1




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




451




452




453




454




455




456




457




458




459




460




461




462




463




465




466




467




468




469




470




471




472




473




474




476




477




478




479




480




482









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




483




485




486




487




488




489




490




492




493




494




495




496




498




499




509




521




528




529




531




532




538




539




546




550




552




556




558




560




561









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0














0




0









0









0









0









0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




567




568




570




577




580




586




588




589




590




591




592




593




594




595




596




598




601




602




603




604




605




606




607




608




609




610




611




612




613









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




614




615




618




619




620




621




622




624




625




627




628




629




630




631




632




633




634




636




637




638




639




640




641




642




643




644




645




646




647









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




649




650




651




655




656




657




658




659




660




661




663




664




665




666




667




668




671




674




675




676




692




694




695




696




697




699




701




702




705









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




0




4




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




3




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9




0




0




0




0




6




0




0




0

















COMPOUND























Rate 62 g/ha




706




715




720




721




724




740




741




758




765




793









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




6






Rice




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




6
















COMPOUND























































Rate 62 g/ha




4




10




11




14




15




16




17




18




19




20




21




22




23




24




25




26




27




28




29




30




31




32




33




34




35




36




37




38




39




40




41




42




43




44




45




46




47




48




49




50




51




52




53




54









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0









0














0




0




0




0




0




0









0









0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0




2




2




3




0




1




0




2




4




0




0




3




0




0




0




0




0




4




0




0




0




0









0




0




0




0




0




3




0




0




0




0









0




1




2




0






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




1




0




0




4




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Crabgrass




0




3




0




0




0




0




1




0




0




0




0




0




0




2




2




0




0




3




0




1




0




0




1




0




0




3




0




0




0




0




0




0




1




0




0




0




0




0




0









0




1




1




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0














0




0




0




0




0




0









0









0




0




0




0




0






Giant foxtail




0




2




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1









0




0




0




3






Morningglory




0




0




0




1




2




1




3




1




0




4




2




0




1




9




1




1




0




2




0




1




0




6




3




1




4




4




0




0




0




3




1




0




2




0




0




0




1




0




0









0




1




1




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




1




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




1




0




0




0




0




0




0









0




0




1




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0














0




0




0




0




0




0









0









0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0














0




0




0




0




0




0









0









0




0




0




0




0






Soybean




2




3




0




2




2




1




2




2




2




3




2




3




3




3




2




1




1




3




2




1




1




2




2




0




1




5




0




0




3




3




3




0




2




0




1




1




2




1




1









0




2




3




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0









0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0
















COMPOUND























































Rate 62 g/ha




55




56




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




84




85




86




87




88




89




90




91




92




93




94




95




96




97




98









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0









0




0




0




0




0




0




4




3




3




0




0




0




0




0






Barnyardgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0














0




0




0




0




0




5






Bedstraw




0




0




0




0




0









2




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0









0




2




2




3




0




0
























0




0




0




0






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




2




2




0




0









0




0




0




2




0




0




8




7




7




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0









0




0




0




0




1




1




3




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




2




0




3




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




3




2









0




0









0




2




2




0




0




1




5




6




7




3




0




1




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0














0




0




0




0




0




0






Giant foxtail




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




3




0




0




0




0




0




0




0









0




0




0




0




0




0




8




8




6




0




0




0




0




0






Morningglory




1




0




1




0




0




1




2




2




0




0




0




0




0




2




0




0




0




0




3




2




1




0




0




7




5




7




2




4




0









0




4




4




8




0




3




7




7




6




10




1




1




1




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0









0




0




0




0




0




0




2




2




2




1




0




0




0




0






Redroot pigweed




0




0




0




0




0




2




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




2




0




0




0









0




0




0




3




0




2




1




2




2




0




2




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




2




0




0




0




0




0




0




0




0




0




0




0




0









0




0














0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0
























0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0














0




0




0




0




0




0






Soybean




1




2




1




1




1




2




1




1




2




0




1




1




0




1




2




0




0




0




0




0




1




0




0




1




0




0




0




0




0









0




2




2




1




0




4




3




3




4




5




1




1




0




1






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




3









0




0




0









0




0




0




3




0




0




3




1




2




2




2




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




3




0




3




0




0




0




0




0




0




0




0




2




0




0




0




2




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




1




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




1




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




99




100




101




102




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120




121




122




123




124




125




126




127









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




7




0




7




0




0




0




4




0




0




8




6




0




0




0




0




0




0




0




0




0




0






Barnyardgrass




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0






Bedstraw




3




0









0














0




0




2




0




6




2




5




0




1




3




0




0




0




0




0


































0




0






Blackgrass




3




0




0




0




0




0




2




0




7




4




7




1




0




0




8




0




4




9




8




0




2




0




0




0




2




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




2




0




0




0




1




0




0




0




0




0




0




1




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0









0




8




4




8




2




1




0




9




2




0




9




9




1




2




5




4




0




0




0




0




0




0






Ducksalad




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0






Giant foxtail




0




0




0




0




0




3




2




0




8




5




8




0




2




2




9




5




0




9




9




1




8




3




1




2




3




0




0




0




0






Morningglory




1




0




0




0




8




10









6




3




0




3




4




4




8




5




1




3




2




2




1




3




4




5




1




8




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




5




2




0




0




0




0




0




0




0




0




0




0






Rape




2




0




0




0




0




0




0




0




0




0




3




2




3




2




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




3




0




0




0




0




1




0




0




0




0




3




3




3




2




3




0




0




0




0




0




0




0




2




0




0




0




0




0




0






Rice




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




0




0




0




0




0




0




0






S. Flatsedge




0









0




0














0




0









0




0




0




0




0




0




0




0




0




0














0




3




0




0




0




0




0




0






Soybean




2




0




2




0




4




4




1




0




3




1




4




3




3




4




6




3




1




3




2




1




1




2




5




3




2




0




0




0




0






Sugarbeets




2




0




0




0




1




0




0




0




0




0




3




0




2




2




4




3




2




2




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




4




2




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




2




0




0




0




0




0




1




0




0




0




2




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




3




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




128




129




130




131




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149




150




151




152




153




154




155




156









Postemergence






B. signalgrass




0




0




1




4




0




0




0




0




0




0




5




2




0




0




0




0




0




0




4




7




0




0




0




3




0




0




0




0




0






Barnyardgrass







































0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




7




0




0




4




0




2




4




2









4




2




2




5




2




0




2




2




2




0




0




3




0




0




0




0




0






Blackgrass




0




0




3




8




0




0




0




0




0




5




7




2




3




0




0




3




0




0




8




7




5




0




0




8




0




0




0




0




0






Cocklebur




0




0




0




2




0




2




0




0




1




0




0




0




0




0




0




1




0




0




2




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0






Crabgrass




0




2




5




5




5




0




0




0




1




7




8




8




0




0




3




1




2




2




8




9




8




0




0




8




0




0




0




1




0






Ducksalad







































0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0






Giant foxtail




0




4




8




8




8




0




0




0




0




8




9




6




0




0




0




0




0




0




8




8




5




0




0




7




0




0




0




1




0






Morningglory




0




4




2




7




3




2




5




0




6




7




5




3




4




1




3




3




0




6




3




3




3




0




0




4




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Rape




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




1




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




2




0




0




0




0




3




2




3




3




0




0




0




3




0




0




4




0




2




0




0




3




0




0




0




0




0






Rice







































0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge







































0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Soybean




0




1




1




5




3




1




1




2




3




5




2




1




3




3




2




3




3




3




3




5




4




0




1




3




0




0




2




1




1






Sugarbeets




0




0




0




2




0




0




0




0




3




3




0




0




0




0




0




1




0




0




1




0




2




0




0




2




0




0




0




0




0






Velvetleaf




0




0




0




0




2




0




0




0




0




0




2




2




0




0




0




2




0




0




0




0




0




0




0




3




0




0




0




0




0






Wheat




0




0




0




3




0




0




0




0




0




0




3




2




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




2




0




0




0




0




0




1




0




2




0




0




0




0




0




0




2




2




0




0




0









0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




157




158




159




160




161




162




163




164




165




166




167




168




169




170




171




172




173




174




175




177




178




179




180




181




182




183




184




185




186









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass









0




0




0



















0
























0




0




0
























0



















































Bedstraw




0




0




0




0




0




0




0




0




0




0




0




3




2




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




1




0




0




0




0




2




0




0




0




0




0




2




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




6




0




2




0




0




0




2




8




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0






Ducksalad









0




0




0



















0
























0




0




0
























0



















































Giant foxtail




0




0




0




0




0




0




6




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Morningglory




0




0




0




0




4




6




2




0




3




1




2




7




1




0




0




2




7




3




1




0




2




4




0




0




0




0




0




1




1






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice









0




0




0



















0
























0




0




0
























0



















































S. Flatsedge









0




0




0



















0
























0




0




0
























0



















































Soybean




0




3




0




0




2




3




2




0




2




0




2




1




1




2




1




2




2




2




1




1




1




1




0




0




0




0




1




2




1






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0






Velvetleaf




0




0




0




0




0




3




3




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




187




188




189




190




191




192




193




194




195




196




197




198




199




200




201




202




203




204




205




206




207




208




210




211




212




213




214




215




216









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Barnyardgrass
































































0






















































































Bedstraw




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




1




0




0




0




0




0




0




0




4




0




0




0




0




0






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




6




0




1




0




0






Cocklebur




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




2




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




1




0




0






Ducksalad
































































0






















































































Giant foxtail




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0






Morningglory




0




0




0




0




1




1




0




0




0




0




3




0




4




0




1




2




0




3




0




1




0




1




2




4




2




6




2




0




3






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




2




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




2




0




5




0




0




0






Rice
































































0






















































































S. Flatsedge
































































0






















































































Soybean




0




1




0




0




3




3




0




0




2




0




0




0




2




2




1




2




0




1




0




0




1




1




1




3




1




1




0




0




1






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




3




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




217




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237




238




239




240




241




242




243




244




245









Postemergence






B. signalgrass




0




0




0




2




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




1






Barnyardgrass























































































































































Bedstraw




0




6




6




6




2




3




3




3




0




0




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




3






Blackgrass




3




5




5




5




2




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




8




7




0




4






Cocklebur




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




1




3




3




2




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




8




3




0




2






Ducksalad























































































































































Giant foxtail




1




1




6




5




2




0




0




0




8




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




7




3




0




5






Morningglory




0




3




6




5




0




1




1




2




2




5




4




2




0




0




1




3




3




0




2




4




2




2




1




5




3




0




5




0




5






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




5




0




6




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




2




0




3






Rice























































































































































S. Flatsedge























































































































































Soybean




1




3




5




5




2




2




3




2




2




2




1




0




0




0




0




3




3




0




0




1




0




1




1




0




1




4




3




0




2






Sugarbeets




0




2




4




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




1




0




0




2




3




0




0




3






Wheat




0




0




5




3




0




0




0




0




3




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




2




0




4






Wild oats




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




246




248




249




250




251




252




253




254




255




256




257




258




259




260




261




262




263




264




265




266




267




268




269




270




271




272




273




274




276









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




7




0




0




0




2




0




0




0




0




0




0




2




0




6




0




0




0




0




0




0




0




0









0




4




0




0




0




0






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




2




4




3




0




0




0




0




3




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0






Ducksalad























































































































































Giant foxtail




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0






Morningglory




8




0




0




4




6




2




0




7




3




8




6




3




6




2




3




3




2




7




6




4




1




1




3




0




2




0




0




0




3






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




3




0




2




0




0




1




0




0




2




2




0




0




3




0




3




0




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




1




0




2




1




2




1




0




0




2




3




3




3




3




1




2




1




0




0




3




5




2




0




1




0




4




1




2




2




3






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




277




278




281




282




283




284




285




286




287




288




289




290




291




292




293




294




295




296




297




298




299




300




301




303




304




305




306




307




308









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




5




0









5




0




2




0




2




4




0




0




0




0




0




0




3




0




0




0




0




2




0




0









0









0




0




0






Blackgrass




2




0




0




0




2




3




0




0




8




0




5




0




1




0




5




0




2




0




0




0




7




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




1




0




0




0




0




0




0




0




2




0




3




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad























































































































































Giant foxtail




2




0




0




0




0




0




0




0




7




0




2




0




0




0




5




0




0




0




0




0




7




0




0




0




0




0




0




0




0






Morningglory




7




3




2




6




8




7




3




1




2




7




3




4




4




0




1




6




1




0




0




0




3




0




0




0




3




0




2




0




0






Nutsedge




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




2




2




1




0




0




0




1




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0






Redroot pigweed




1




0




0




4




4




3




0




0




2




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




3




3




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




3




1




2




3




4




4




2




1




1




0




2




2




1




0




1




2




2




0




2




0









1




0




2




3




4




1




0




1






Sugarbeets




1




0




0




2




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Velvetleaf




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




5




0




2




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




309




310




311




312




313




314




315




316




317




318




319




320




321




322




323




324




325




326




327




328




329




330




332




333




334




335




336




337




338









Postemergence






B. signalgrass




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




4




0




0




5




2




0









2




0




0




0




0




0




0




0




2









7




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




5




0




0




0




2




0




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




8




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Ducksalad























































































































































Giant foxtail




0




7




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Morningglory




1




4




0




0




2




2




0




3




1




0




2




1




2




4




0




0




4




5




7




7




0




0




0




0




0




0




0




0




0






Nutsedge




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




2




0




0




0




3




2




2




0




0




0




3




4




2




0




0




0




0




0




0




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




2




4




2




2




1




2




3




3




3




0




0




2




2




1




0




0




2




3




5









1




1




2




2




1




1




1




1




1






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




339




340




341




342




343




344




345




348




349




350




351




352




353




354




355




356




357




358




359




360




361




362




363




364




367




368




369




370




371









Postemergence






B. signalgrass




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0






Barnyardgrass



















0




0




0




0




2




2




0




0




0









0




1









0




2




0




2



















0














0




0











Bedstraw




0




3




0




4




0




0




0









2














0














0




0




0




0




0




0




7




5




4




0









0





















Blackgrass




0




0




0




0




3




0




0




2




1




4




0




8




0




3




3




3




3




2




0




5




5




8




5




0




0




7




0




2




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




1




0




0




1




0




1




0




1




0




0




0




0




2




0




0




2




0




3




1




0




0




6




0




3




3






Ducksalad



















0




0




0




0




0




0




0




0




0









0




0









0




0




0




0



















0














0




0











Giant foxtail




0




0




0




0




7




0




0




3




0




5




0




2




0




0




2




2




8




3




0




8




1




6




4




0




0




8




0




6




5






Morningglory




2




2




7




7




2




0




0




2




5




3




3




0




3




0




2




4




2




3




0




4




1




1




1




0




5




2




7




10




7






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




2




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




1




0




0




2




0




0




0




0




0




0




0




0






Redroot pigweed




0




2




0




2




0




0




0




0




0




0




0




0




2




2




0




0




0




3




0




0




3




2




0




0




0




2




0




0




0






Rice



















0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0



















0














0




0











S. Flatsedge



















0




0




0




0




4




0




0




0




2









5




0









0




0




0




2



















0














0




2











Soybean




1




1




1




3




1




2




0




1




1




1




1




2




4




3




1




2




2




4




0




1




2




4




4




0




0




4




0




1




1






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




2




2




0




0




0




1




0




0




0




0




0




0




0






Wheat




0




0




0




0




2




0




0




2




0




0




0




0




0




0




0




2




4




2




0




3




0




2




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




2




3




0




0




3




0




3




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




372




373




374




375




376




378




379




380




381




382




383




384




385




387




388




389




390




391




392




393




394




395




396




397




398




400




401




402




403









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




2




0




1




0




0




0




0




0




0




0




0




0




0






Barnyardgrass




0













































































































0




0




0




0





















Bedstraw


































0









0














0









0







































0





























3




0






Blackgrass




4




0




0




2




0




0




0




0




0




0




0




3




0




3









0




8









7




0




2




0




0




6




0




0




0









6






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




2




0




0




0




0




0




0




0




0




0




0




1




6




0




4




0




2




0




2




0




2




0




0




2




2




0




0




3




2






Ducksalad




3













































































































0




0




0




0





















Giant foxtail




4




0




0




0




0




0




0




1




0




0




0




4




7




2




7




0




9




0




7




5









0




0




8




3




5




0




8




3






Morningglory




5




8









1




0




5




5




5




2




0




0




0




1




0




1




2




2




0




5




0




0




0




0




0




2




0




3




3




2






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0









7




0




0









0




0




0




0




0




0




0




1




2






Redroot pigweed




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




2




0






Rice




0













































































































0




0




0




0





















S. Flatsedge




2













































































































0




0




0




0





















Soybean




1




3




2




1




0




0




1




0




1




1




2




1




2




0




1




2




2




0




1




1




3




0




2




3




3




1




0




4




4






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




404




405




406




407




408




409




410




411




414




415




416




417




418




419




420




421




422




423




424




425




426




427




428




429




430




431




432




433




434









Postemergence






B. signalgrass




2




0




0




0




0




3




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Barnyardgrass

















































0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Bedstraw
























6




0





























0









0




0



















0

















































0






Blackgrass




5




0




0




0




0




6














0




0




6




0




2




0




0




8




0




0




0




2




3




0




0




0




2




0




0




2




0






Cocklebur




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




3




6




4




4




1




0




2




0




0




0




2




4




0




0




0




4




1




0




0




0




1




0




0




2




0






Ducksalad

















































0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Giant foxtail




5




0




0




0




9




8




8




6




3




5




7




0




0




0




7




8




0




0




0




6




3




0




0




0




6




0




0




4




0






Morningglory









2




0




6




1




4




4




6




1




2




4




3




3




2




4




2




0




2




0




2




6




0




0




1




1




0




1




2




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




2




0




0




0




0




0




2




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




2




0




0




0




0




0




0




0




0




0




1




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice

















































0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge

















































0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Soybean




4




2




1




0




1




4




4




3




2




3




5




3




3




2




2




4




2




2




0




1




4




0




1




1









1




1




1




0






Sugarbeets




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




435




436




437




438




439




440




441




442




443




444




445




446




449




450




451




452




453




454




455




456




457




458




459




460




461




462




463




465




466









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Barnyardgrass




0




0



















0

























































































































Bedstraw




0




0




0




0



















0




0














0














0





























0
























0














4






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




6




4




0




0




0




2




0




0




0




0




8






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




2




0




1




0




0




0




2




0




5




0




0




0




3




0




2




4




4




0




2




0




3




0




0




0




1




9






Ducksalad




0




0



















0

























































































































Giant foxtail




0




0




0




5




0




0




0




0




0




4




0




6




0




2




0




2




3




2




7




2




0




7




0




0




0




0




0




2




9






Morningglory




1




0




0




4




0




2




0




4




2




0




3




2




2




0




1




1




0




7




3




3




0




0




6




7




3




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




2






Rice




0




0



















0

























































































































S. Flatsedge




0




0



















0

























































































































Soybean




0




0




0




1




0




5




0




0




1




1




1




1




0




1




0




1




1




1




1




1




0




0




3




3




2




0




1




1




4






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




467




468




469




470




471




472




473




474




476




477




478




479




480




481




482




483




485




486




487




488




489




490




492




493




494




495




496




497




498









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




2




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw














0




0



















6














0




0




0




0




0









0




0




0




0




0



















0














0











Blackgrass




0




0




7




0




0




0




0




7




0




0




0




0




0




0




0




0




3




0




0




1




1




2




0




0




0




0




2




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




3




3




0




1




7




1




2




0




1




2




2




2




0




0




0




3




0




0









2




3




0




0




0




0




0




0




0






Ducksalad























































































































































Giant foxtail




0




1




8




0




0




7




1




3




0




2




3




0




3




2




0




0




5




2




0




5




2




2




0




0




0




0




0




0




0






Morningglory




3




2




9




0




3




3




0




1




0




6




3




7




2




0




5




0




8




1




2




1




2




2




0




0




0




1




8




0




1






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed









0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




0




1




0




0




2




2




1




3




0




1




2




1




2




4




1




0




2




4




3




4




3




4




0









0




0




2




0




1






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




499




500




501




504




505




506




508




509




510




511




512




513




514




515




516




517




518




519




520




521




522




523




524




525




526




527




528




531




532









Postemergence






B. signalgrass




0




3




2




0




0




0




0




0




2




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw



























































6









6









4









0














0




0



















0




0




0




0






Blackgrass




0




3




3




6




2




0




0




2




5




0




2




4




0




0




0




0




4




0




0




2




8




0




0




4




3




0




0




0




0






Cocklebur




0




3




0




2




0




0




0




0




3




0




0




3




0




0




2




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Corn




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Crabgrass




0




6




7




8




7




0




9




3




3




3




2




1




7




4




3




7




0




0




2




2




8




3




3




6




6




4




3




2




4






Ducksalad























































































































































Giant foxtail




0




7




8




8




8




2




8




3




4




3




2




1




6




8




0




8




0




4




2




4




8




2




4




5




3




5




0




0




0






Morningglory




3




3




0




4




5




0




3









4




4




5




3




2




2




2




2




5




0




3




3




3




2




0




2




6




3




2




2




0






Nutsedge




0




0









0




0




0









0









0




0




0




0




0




0




0




0









0




0




0




0









0




0




0









0




4






Rape




0




3




2




1




0




0




1




0




1




0




0




0




6




4




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




7




0




7




0




0




3




0




7




5




1




3




0




3




4




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




0




3




4




3




1




2




4




1




4




1




4




1




6




4




4




0




4




3




2




4




4




4




3




3




2




3




3




3




0






Sugarbeets




0




6




5




5




3




2




0




0




2




0




0




2




3




3




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0






Velvetleaf




0




4




0




1




0




0




0




2




4




0




0




3




2




2




3




0









2




3




0




2




0




0




2




4




3




0




0




0






Wheat




0




0




2




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




533




534




535




536




540




541




543




544




545




546




548




549




550




551




552




553




554




555




556




557




558




559




560




561




562




563




564




565




566









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0









0




0




0




2






Barnyardgrass























































































































































Bedstraw
























0




0




0




0




0




0




0




0




0




0




2




0




5




2




0




0














0




0









0




0




0











Blackgrass









0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




7




2




2




3




0




0




0




0






Cocklebur




2




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




2






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3









5




0




5




0




0




0




0




1









2









0




3




0




0




0




0




0




0




5




0




2




7




9




2




0




2






Ducksalad























































































































































Giant foxtail




8









5




0




0




0




0




0




0




0




0




2




2




0




0




0




2




0




4




0




2




9




2




2




7




6




2




0




0






Morningglory




4




2




4




2




2




0




1




3




4




0




5




4




1




1




1




0




1




1




0




5




10




9




4




1




4




4




5




3




5






Nutsedge




0




0




0




0




0




0




0




0




0



















0









0




0




0




0




0




0




0




0




3




0









0




0









0






Rape




0




0




0




0




0




0




0




0




0




0









0




0




3




2




2




0




4




0




0




0




0




0




4




0




0




0




0




0






Redroot pigweed




9




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




2




0




9




0




3




0




3






Rice























































































































































S. Flatsedge























































































































































Soybean




4









3




2




1




0




0




0




1




1




2




2




2




2




2




1




2




1




0




0




3




4




2




2




3




5




0




2




4






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0









0




0




0









0




0




0




0




0




0




0




0




3




0




0




3




3






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0




0




2




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




567




568




569




570




571




572




573




574




575




576




577




578




579




580




581




582




584




585




586




588




589




590




591




592




593




594




595




596




598









Postemergence






B. signalgrass




0




1




0




0




0




0




0




0




0




0




0




0




0




0




5




0




3




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




0




0




0









0


































0




3




0









5




0




0




0












































0






Blackgrass




0




8




0




0




0




0




0




2




0




0




0




0




0




2




4




3




5




3




0




0




0




0




0




0




0









3




0




0






Cocklebur




0




1




0




0




0




0




0




0




0




0




0




0




0




3




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




8




0




0




0




0




6




0




0




2




0




0




0




0




3




0




1









2




0




0




0




0




0




0




5




5




0




0






Ducksalad























































































































































Giant foxtail




0




7




0




0




0




0




2




2









2




0




0




0




0




7




3




7




6




2




0




0




0




0




0




0




6




8




0




0






Morningglory




0




7




3




4




4




3




10




10




4




2




6




9




10




7




4




9




1




4




6




7




3




2




0




1




0




0




1




0




0






Nutsedge




4




0




0




0




0




0




0




0









0




0














0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




2




0




0




0




0




0




2




0




4




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




3




0




0




5




0




0









0




0




0




0




0




0




0









0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




0




4




0




0




2




2




2




4




3




2




2




3




2




2




0




1




2









2




2




2




1




1




1




0




0




0




1




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




3




0




0




0




0




0




0




0




0




2




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




601




602




603




604




605




606




607




608




609




610




611




612




613




614




615




618




619




620




621




622




624




625




627




628




629




630




631




632




633









Postemergence






B. signalgrass




0




0




0




0




0




0




0




3




0




0




0




1




1




0




0




0




0




0




0




0




4




0




3




2




0




0




1




0




0






Barnyardgrass























































































































































Bedstraw
























0




0




0









0




0









3




8









0









0




0









0




0




0









0




3




0









0




0






Blackgrass









4




0




0




0




0




0




4




5




8




7




7




8




0




0




0




0




0




0




0




4




0




8




6




3




0




1




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




5




0




0






Crabgrass




3




2




0




1




0




0




5




3




5




9




8




4




8




0




0




0




0




1




0




2




6




1




8




8




1




1




8




0




0






Ducksalad























































































































































Giant foxtail




7




1




0




1




0




0




6




5




6




8




8




7




5




0




0




0




0




0




0




0




4




0




9




8




3




2




8




3




0






Morningglory




1




0




0




0









6




6




0




8




8




7




5




7




2




0




0




0




2




1




0




1




0




3




1




2




1




0




1




1






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0






Rape




0




0




0




0




0









0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




2




0




0




0




0




0




3




0




0




0




0




1




0




0




0




0




0




0




0




0




0




2




3




0




0




0




0




0






Rice























































































































































S. Flatsedge























































































































































Soybean




4




3




0




0




2




1




3




3




5




5




5




4




4




3




1




0




1




1




1




4




2




0




2




4




4




4




5




1




2






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




3




0




0




2




0




0




0




0




0




0




0




0




0




0




3




6




0




0




4




0




0






Wheat




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0






Wild oats




0




0




0




0




2




0




0




3




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




634




635




636




638




639




640




641




642




643




644




645




646




647




648




649




650




652




653




654




655




656




657




658




659




660




661




663




664




665









Postemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass























































































































































Bedstraw




0




5




7







































0




0




0






















































0




0














0











Blackgrass




2




2




0




0




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




6




6




0




1




0




0




0




4




3






Cocklebur




1




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0






Crabgrass




0




4




3




2




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




1




0




3




0




1




0




0




0




0




1






Ducksalad























































































































































Giant foxtail




4




5




2




5




0




0




0




0




0




0




0




0




8




0




0




0




0




0




0




1




3




5




0




5




3




2




0




2




2






Morningglory




1




1




2




0




0




0




0




0




0




0




0




0




0




6




4




4




3




0




3




9




1




2




7




4




1




0




0




0




4






Nutsedge




0




0




0




0




0




0




0




0




0









0




0




0




0




0




2









0




0




0




0









0




0




0




0




0




0











Rape




0




2




2




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




1




0




0




0




3




0









0




0




2




0




0




0




0




0




2




0




0




0




1




0




0




6




0




2




0




0




0




3






Rice























































































































































S. Flatsedge























































































































































Soybean




3




3




2




1




0




0




0




2




1




0




1




0




2




0




2




2




0




0




0




2




2




1




2




2




2




1









3




2






Sugarbeets




0




3




2




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




3




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




1




1




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




1




1




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




666




667




668




670




671




672




674




675




676




708




709




710




711




712




713




714




722




739




740




741




743




744




745




746




747




748




749




750




751









Postemergence






B. signalgrass




0




0




1




3




0




0




3




1




0




0




0




5




4




0




0




2




0




0




0




0




0




0




0




3




1




2




2




0




3






Barnyardgrass























































































































































Bedstraw









0





























0









0







































3




0




0




0



















8




5




3




5




0






Blackgrass




6




6




7




2




0




0




4




5




2




0




0




5




3




0




1




7




0




0




3




0




3




5




3




5




5




5




5




4




6






Cocklebur




0




2




0




2




0




0




0




0




0




0




0




0




1




0




1




0




0




2




0




0




0




0




0




0




0




0




0




0




0






Corn




0




4




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




6




6




9




1




5




6




6




4




0




2




8




4




1




2




4




0




4




0




9




2




3




4




7




3




2




4




7




7






Ducksalad























































































































































Giant foxtail




2




5




8




9




5




3




7




8




4




0




3




8




6




3




4




6




0




7




2




0




7




6




2




6




8




2




3




9




8






Morningglory




0




2




1




3




1




4




2




1




0




0









4




2




3




2




0




4




6




2









5




2




3




4




2




0




2




3




8






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




2




0




0




0




0




0




0




0




0




0




0




2




0




5




0




0




0




0




0




0




0




4




4




0




2




0




2






Redroot pigweed




0




2




3




7




0




7




0




2




0




0




5




8




3




3




2




5




8




0




0




3




0




0




2




6




4




2




4




4











Rice























































































































































S. Flatsedge























































































































































Soybean




4




2




2




3




2




2




2




4




2




3




1




3




1




2




3




2




0




3




2




2




0




2




3




2




4




3




3




2




2






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




1




1




0




0




0




3




0




0




0




0




2




0




0




0




1




0




3






Velvetleaf




0




5




0




5




0




6




4




0




0




0




4




5




3




0




3




2




0




0




0




0




0




0




0




2




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0

















COMPOUND





































Rate 62 g/ha




752




753




754




756




757




758




759




760




761




762




763




764




765




766




767




772




773




774




776




779




780




790




791




792









Postemergence






B. signalgrass




0




0




0




0




0




4




0




0




0




0




0




0




3




0




2




0




0




0




0




2




0




2




0




0






Barnyardgrass






























































































































Bedstraw




0














0














0














0









0









0




7




0




0




0




0




0




0




0




0











Blackgrass




0




0




2




0




0




3




4




0




0




0




5




3




3




0




9




0




0




0




2




0




0




4




0




4






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




0




5




0




3




2




2




5









0




2




0




3




2




8




0




0




0




2




3




3




9




1




2






Ducksalad






























































































































Giant foxtail









3




4




0




2




8




3




0




0









6




3




5




0




8




0




0




0




2




8




7




9




0




2






Morningglory




2









10




4




6




2




3




3




0




0




2




1




5




2




5




0




0




0




7




5




4




2




3




6






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




2




0




0




0




0




0




0




2




0




0




0




0




0




0









0




0




0




2




0




0




0




3




3






Redroot pigweed




0




4









0




1




7




0




0




0




0




0




0




6




5




6




0




0




0




2




2




0




0




2




0






Rice






























































































































S. Flatsedge






























































































































Soybean




4




1




0




2




3




4




3




4




2




2




2




1




2




2




1




0




0




0




2




2




3




2




4




4






Sugarbeets




3




0




0




0




0




0




0




0




2




0




0




0




0




0




3




0




0




0




0




2




0




0




0




0






Velvetleaf




0




0




0




0




0




5




2




0




0




0




0




0




6




0




2




0




0




0




3




2




0




4




2




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND























































Rate 62 g/ha




4




10




11




14




15




16




17




18




19




20




21




22




23




24




25




26




27




28




29




30




31




32




33




34




35




36




37




38




39




40




41




42




43




44




45




46




47




48




49




51




52




53




54




55









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0






Blackgrass




0




1




0




0




0




0




0




2




0




0




0




0




0




0




3




0




0




0




0




3




0




1




0




3




0




4




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




2




0




0




0




0




0




6




3




1




4




3




3




0




5




0




0




3




3




3




9




4




3




7




3




8




0




2




0




2




3




0




0




0




0




1




0




1




2




0




0




3




2




0






Giant foxtail




9




3




0




6




6




0




3




2




0




3




8




3




2




6




5




0




0




2




0




2




6




4




4




2




3




10




0




10




0




9




4




0




0




0




7




10




0




6




8




0




3




3




2




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




2




0




0




0




0




0




3




4




0




0




6




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0

















COMPOUND
























































Rate 62 g/ha




56




57




58




59




60




61




62




63




64




65




66




67




68




69




70




71




72




73




74




75




76




77




78




79




80




81




82




83




85




86




87




88




89




90




91




92




93




94




95




96




97




98




99









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




7




10









0




0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




2




2




1




0




0




10




9




9




0




0




0




0




2




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




3




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




2




0




0




0




0




2




2




0




0




0




0




1




2




3




3




0




7




2




3




1




0




0




0




5




5




5




0




0




10




8




7




3




2




1




0




4




5






Giant foxtail




0




0




0




0




3




3




5




0




0




3




4




3




5




0




0




0




0




2




3




6




4




0




8




4




6




2




0




0




0




8




8




4




0




4




10




10




10




8




2




2




0




5











Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




4




3




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




2




4




9




0




0




6




2




9




0




5









0




4




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




7




2




6




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




4




5




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




3




3




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




7




8




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




100




101




102




103




104




105




106




107




108




109




110




111




112




113




114




115




116




117




118




119




120




121




122




123




124




125




126




127




128









Preemergence






B. signalgrass




0




0




0




1




0




0




0




5




4




9




3




0




0




7




0




2




4




6




0




5




0




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0




2




0




8




0




0




0




4




0




0




2




0




0









0




0




0




0




0




0




0




0




0






Blackgrass




0




0




0




0




0




5




0




9




5




8




0




0




0




8




6




0




9




8




0




5




0




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0









0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




4




0




0




2




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




2




0




2




0




10




7




10




3




6




5




7




2




4




8




9




7




7




6




2




4




4




0




0




0




0




0






Giant foxtail




0




0




2




8




0




10




2




10




10




10




10




8




8




9




5




9




10




10




9




9




8




8




7




7




0




0




0




0




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




3




0




7




0




0




0




4




0




0




6




6




0




4




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




10









10




3




3




0




8




5




5




10




9




0




10




7




4




0




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




1




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




4




3




8




0




0




0




7




4




0




9




0




0




3




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




7




3




5




0




0




0




6




4




0




8




6




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




3




2




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




2




0




9




9




8




0




0




0




6




5




0




7




3




0




5




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




129




130




131




132




133




134




135




136




137




138




139




140




141




142




143




144




145




146




147




148




149




150




151




152




153




154




155




156




157









Preemergence






B. signalgrass




0




6




7




0




0




0




0




3




3




2




0




0




0




0




0




0




0




9




6




0




0




0




4




0




0




0




0




0




0






Bedstraw




0




0









0




0




0














4




5




0




0




0




0




0




0




0




9




1




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




5




10




3




3




0




0




0




7




9




4




0




0




0




4




0




0




8




8




4




0




0




8




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0









0




0









0




0




0









0




0




0




0




0




0




0




0




0






Corn




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




6




0




0




0




0




0




0




0




0




0




0






Crabgrass




6




6




2




7




1




2




0




0




8




9




7




4




0




0




3




4




0




8




8




5




0




0




10




0




0




0




0




0




0






Giant foxtail




7




7




10




8




3




6




0




0




8




7




10




1




0




0




3




3




0




10




7




7




0




0




9




0




0




0




0




0




3






Morningglory




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




4




8




0




0




0




0




0




0




7




0




0




0




0




0




0




0




2




1




0




0




0




2




0




0




0




0




0




0






Redroot pigweed




0




6




7




2




0




0









7




9




9




6




0




0




0









0




0




10




6




7




0




4




10




0




0




6




0




0




0






Soybean




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




2




7




7




2




0




0




0




4




6




9




3




0




0




0




0




0




0




8




2




4




0




0




1




0




0




0




0




0




0






Velvetleaf




0




5




7




3




0




0




0




0




3




5




2




0




0




0




0




0




0




7




3




0




0




0




6




0




0




0




0




0




0






Wheat




0




2




2




0




0




0




0




0




0




3




0




0




0




0




0




0




0




2




5




0




0




0




2




0




0




0




0




0




0






Wild oats




3




7




10




3




0




0




0




0




5




5




3




0




0




0




0




0




0




9




2




6




0




0




8




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




158




159




160




161




162




163




164




165




166




167




168




169




170




171




172




173




174




175




177




178




179




180




181




182




183




184




185




186




187









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




2




0




7




2




0




2




0




0




0




0




6




7




0




0




0




0




5




0




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




0




0




3




0




7




0




0




0




0




0




3




10




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




0




0




4




6




8




0




4




4




7




0




8




8




2




7




2




2




5




1




0




6




0




0




0




0




0




2




2




0






Giant foxtail




3




0




0




4




7




8




0




6




3




8




6




10




9




5




8




6




8




5




3




4




6




0




0




0




0




0




0




5




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0









0




0




0




0




0




6




10




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




2




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




3




0




4




0




0




0




8




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




188




189




190




191




192




193




194




195




196




197




198




199




200




201




202




203




204




205




206




207




208




210




211




212




213




214




215




216




217









Preemergence






B. signalgrass




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




1




0




0




5




0




0




0




0




0




0




6




0




0




0




0




0




0




0




0




0




0




6




4




0




0




4




0




6






Cocklebur




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




2









4




3




0




0




0




6




0




0




3




0




6




0




0




0




4




0




0




0




0




0




3




0




3






Giant foxtail




0




0




0




3




8




2




3




3




0




0




0




7




0




2




2




0




7




0




0




3




2




0




3




2




0




2




3




0




6






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0









0




0




0




0









0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




5




0




0




0




0




7




0




0




0




0




0




0




0




0




0




0




0




9




0




0




4




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




218




219




220




221




222




223




224




225




226




227




228




229




230




231




232




233




234




235




236




237




238




239




240




241




242




243




244




245




246









Preemergence






B. signalgrass




0




4




7




5




0




0




0




1




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




4




0




3




0






Bedstraw




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0






Blackgrass




8




7




8




5




0




0




2




2




10




2




0




0




0




0




2




2




0




0




0




0




0




0




0




6




9




8




0




10











Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




3




0






Crabgrass




4




5




7




6




0




4




2




9




5




1




0




0




1




0




5




5




0




0




2




0




2









2




3




9




7




0




9




3






Giant foxtail




9




10




9




5




0




7




3




8




9




9









0




2




0




6




7




0




0




7




0




5




4




5




10




10




10




0




9




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0






Nutsedge



















0









0




0




7









0




0




0




0




0




0




0
























0




0














10




0




0
















Rape




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0






Redroot pigweed




6




0




0




9




0




0




0




6




0




3




0




0




0




0




0




3




0




0




0




0




0




0




0




0




9




6




0




8




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




3




5




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




2




0




3




0






Velvetleaf




0




3




1




0




0




0




0




4




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




6




4




0




7




0






Wheat




0




3




6




0




0




0




0




5




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




5




0




6




0






Wild oats




5




2




3




2




0









0




4




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




7




3




0




3




2
















COMPOUND








































Rate 62 g/ha




248




249




250




251




252




253




254




255




256




257




258




259




260




261




262




263




264




265




266




267




268




269




270




271




272




273




274




276




277









Preemergence






B. signalgrass




0




0




0




2




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




8




0




0




0




4











Bedstraw




0




0




0




0




0




0




0




0




0




0




0




7




0









0




0




0




0




0




0




0




0




0




3




0




0




0




0











Blackgrass




0




0




0




6




0




0




0




10




0




0




6




2




0




0




0




0




0




0




8




0




0




0




0




8




0




0




0
















Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




2




3




0




0




0




0




0




0




3




4




0




2




0




0




0




1




0




2




0




0




0




3




0




2




0




3




4






Giant foxtail




0




0




8




8




3




0




0




8




0




3




8




9




3




8




0




2




2




6




0




8




0




3




0




8




2




7




0




9




10






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0






Nutsedge




0




0
























0
























0




0









0




0









0









0




0




0




0




0




0









0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0











Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0











Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




6




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0











Velvetleaf




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0











Wild oats




0




0




0




0




0




0




0




0




0




0




2




2




0




0




0




0




2




0




0




0




0




0




0




2




0




0




0




0





















COMPOUND








































Rate 62 g/ha




278




281




282




283




284




285




286




287




288




289




290




291




292




293




294




295




296




297




298




299




300




301




303




304




306




307




308




309




310









Preemergence






B. signalgrass




0




0




0




6




5




2




0




6




0




7




0




0




0




2




0




6




0




0




0




6




0




0




0




0




0




0




0




0




4






Bedstraw









0




0




0




0




0




0




9




0




0




0




0




0




0




0




0




0














10









0




0




0




0




0




0




0




2






Blackgrass




0




0




0




7




0




0




0




10




0




8




2




0




0




7




0




5




0




0




0




9




0




0




0




0




0




0




0




0




10






Cocklebur




0














0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




2




1




2




4




4




0




8




1




2




1




0




0




1




1




2




0




0




0




6




0




0




0




3




0




0




0




0




5






Giant foxtail




0




7




8




8




9




8




8




10




5




10




8




8




0




9




7




8




0




0




0




9




0




0




0




0




2




6




0




5




10






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Nutsedge









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




2




0




0




4




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




5






Redroot pigweed




0




0




1




2




5




0




0




5




0




5




2




0




0




6




0




3




0




0




0




9




0




0




0




0




0




0




0




0




9






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




2




0




0




3




0




2




2




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




5






Velvetleaf




0




0




0




0




0




0




0




6




0




3




0




0




0




4




0




0




0




0




0




6




0




0




0




0




0




0




0




0




2






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




3




0




0




0




0




0




0




0




0




2






Wild oats




0




0




0




0




0




0




0




8




0




1




0




0




0




1




0




2




0




0




0




2




0




0




0




0




0




0




0




0




8
















COMPOUND








































Rate 62 g/ha




311




312




313




314




315




316




317




318




319




320




321




322




323




324




325




326




327




328




329




330




332




333




334




335




336




337




338




339




340









Preemergence






B. signalgrass




0




0




0




0




2




6




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Bedstraw




0




0




0




0




0




0




0









0




0




0




0




0




0




0














0




0









0




0




0




0




0




0




0




0




0






Blackgrass




0




0




0




5




4




8




3




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Cocklebur




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




1




2




6




6




0




0




2




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Giant foxtail




0




0




0




3




7




9




9




0




6




0




4




6




0




0




3




0




7




0




0




0




0




0




0




2




0




0




0




1




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




4




2




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




4




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




341




342




343




344




345




348




349




350




351




352




353




354




355




356




357




358




359




360




361




362




363




364




367




368




369




370




371




372




373









Preemergence






B. signalgrass




0




0




3




0




0














0




0




2




0




1




0




0




1




1




0




5




3




4




3




0




0




1




0




0




0




0




0






Bedstraw




0




0









0




0














10









0




0




0




0




0




10




0




0









0




9




9




0




10




0









0









0




0






Blackgrass




0




0




7




0




0




4




2




4




0




9




2




3




2




5




7




4




0




9




3




9




8




0




2




8




0




6




5




5




1






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0









0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




2




0






Crabgrass




2




4




6




0




0




7




3




8




7




9




7




9




4




7




9




9




0




9




2




5




3




0




6




10




5




7




8




8




4






Giant foxtail




9




8




10




0




0




9




8




10




10




10




9




10




10




10




10




10




0




10




7




10









3




10




10




8




9




10




10




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




5




0






Redroot pigweed




0




0




10




0




0




0




0




4




10









7




5









0




7




7




0




5




1




8




2




0




10




10




0




5




4




6




0






Soybean




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




2




2




2




0




0




0




0




2




0




0




2




0




5




0




0




2




6




0




2




0




2




0






Velvetleaf




0




0




5




0




0




3




0




2




0




2




0




1




0




1




4




3




0




3




0




4




1




0




3




4




0




2




0




3




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




3




0




7




3




0




0




0




0




0




0




0




0






Wild oats




0




0




2




0




0




3




0




0




0




8




0




0




0




5




9




4




0




3




7




7




5




0




0




4




0




0




0




4




0
















COMPOUND








































Rate 62 g/ha




374




375




376




378




379




380




381




382




383




384




385




387




388




389




390




391




392




393




394




395




396




397




398




400




401




402




403




404




405









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




2




0




2




0




0




3




0




0




0




0




3




2




0






Bedstraw




0




6









0




0









0









0









0




0





























0









0
























0




2




0




0











Blackgrass




0




3




0




0




0




0




0




0




0




0




0




0




0




0




6




0




6




0




7




0




0




7




3




0




0




3




2




6




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




6




7




0




0




0




1




0




6




6




6




3




0




6




1




8




0




10




0




9




0




0




10




9




6




0




9




10




10




0






Giant foxtail




8




10




0




4




0




2




0




9




0




9




3




3




8




2




10




0




10




1




9




0




2




10




10




9




0




10




10




10




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




1




0






Redroot pigweed




0




10




0




0




0




0




0




0




0




0




2




0




0




0




8




0




2




0




1




0




0




8




2




3




0




0




0




2




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




1




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




3




0




3




0




2




0




4




0




0




2




0




0




0




1




0




3




0
















COMPOUND








































Rate 62 g/ha




406




407




408




409




410




411




414




415




416




417




418




419




420




421




422




423




424




425




426




427




428




429




430




431




432




433




434




435




436









Preemergence






B. signalgrass




0




0




0




0




1




0




0




2




7




2




0




0




2




7




0




0




0




3




4




0




0




0




1




0




0




2




0




0




0






Bedstraw




0




0
























0




















































































0































Blackgrass




0




0




6




4




3




6




0




5




8




3




4




0




4




8




0




0




0




7




4




0




0




0




0




0




0




2




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




7




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




9




9




7




9




2




8




7




6




6




0




7




8




0




0




0




9




8




5




2




7




9




0




3




9




0









0






Giant foxtail




0




0




10




9




9




10




2




9




8




4




7




0




5




9




0




0




0




10




9




7




0




3




10




0




0




10




0




0




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




2




0




2




7




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




4




7




0




3




0




0




7




0




2




0




0




8




0




0




0




0




2




0




0




0




0




0




0




0




0




2




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




2




2




0




5




0




0




3




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




2




3




2




0




0




0




0




0




0




0




8




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0






Wheat




0




0




0




4




0




0




0




0




2




0




0




0




0




4




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




3




0




0




0




6




0




0




0




0




6




0




0




0




2




2




0




0




0




0




0




0




2




0




0




0
















COMPOUND








































Rate 62 g/ha




437




438




439




440




441




442




443




444




445




446




449




450




451




452




453




454




455




456




457




458




459




460




461




462




463




465




466




467




468









Preemergence






B. signalgrass




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0






Bedstraw






















































0

















































0




0









0



















0











Blackgrass




0




0




0




2




0




0




0




0




0




5




0




0




0




0




0




0




3




0




0




6




0




0




0




0




0




2




2




0




3






Cocklebur




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




3




0




7




0




7




5




4




0




8




0




2




0




5




5




2




5




6




0




6




5




0




0




0




0




2




6




5




9






Giant foxtail




0




2




0




6




0




0




3




9




0




9




2




2




0




2




7




6




10




5




0




9




8




0




0




0




0




7




9




0




6






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0






Redroot pigweed




0




2




0




0




0




0




0




10




0




6




0




0




0




0




0




0




7




0




0




0




0




0




0




0




2




3




1




7




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




469




470




471




472




473




474




476




477




478




479




480




481




482




483




485




486




487




488




489




490




492




493




494




495




496




497




498




499




500









Preemergence






B. signalgrass




3




0




6




3




0




0




0




0




4




0




0




7




0




0




3




5




3




4




6




3




0




0




0




0




0




0




0




0




9






Bedstraw





























0




0




0



















0




0




0


































0




0




0









0




0









0




8






Blackgrass




6




0




9




9




0




3




0




0




4




2




3




6




0




0




4




7




2




5




7




7




0




0




0




0




0




0




0




0




9






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0









0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




9




1




9




9









6




0




8




8









7




7




3




0




6




8




6




8




9




8




0




0




0




0




0




0




0




4




7






Giant foxtail




9




0




10




10




2




7




0




6




9




7




10




9




1




0




7




9




9




9




9




9




2




3




0




0




2




0




0




3




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0









0




0




0









0




0




0




0




0




0




0




0




0









0




0




0




0




0









0






Rape




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




2




0




1




0




0




0




0




0




0




0




0




0




0




9






Redroot pigweed




5




0




10




10




2




1




0




0




8




0




2




0




0




0




1




6




1




4




0




5




0




0




0




0




0




0




0




0




10






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




6




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




9






Velvetleaf




4




0




2




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




5






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Wild oats




7




0




2




2




0




0




0




0




2




0




0




4




0




0




2




0




0




3




0




6




0




0




0




0




0




0




0




0




7
















COMPOUND








































Rate 62 g/ha




501




502




503




504




505




506




508




509




510




511




512




513




514




515




516




517




518




519




520




521




522




523




524




525




526




527




528




531




532









Preemergence






B. signalgrass




8




6




6




7




0




0




4




2




7




0




3




0




6




2




1




0




0




0




0




0




10




4




0




9




8




2




0




2




0






Bedstraw




2




10




5




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0









0




0




0




0




0




0






Blackgrass




5




10




10




6




0




0




1




5




6




0




0




1




2




3




3




2




7




0




0




0




4




2




4




8




7




0




0




2




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn









0




3




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0






Crabgrass




8




10




8




6









0




6




3




5




5




3




4




5




6




6




4




0




7




9




10




9




9




9




9




9




9




7




8




9






Giant foxtail




9




10




9




9




9




0




10




9




9




5




5




2




9




10




10




2




0




10




9




10




10




10




9




9




9




9




9




9




10






Morningglory




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0






Nutsedge




0




0




0




2




3




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




2




4




5




4




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




4




0




0




0




0






Redroot pigweed




9




9




8




10




9




2




7




0




7




4




3




7




7




8




7




8




2




0




0




0




10




2




8




0




4




0




0




0




0






Soybean




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




2




4




3




0




1




0




0




0




0




0




0




0




1




0




0




0




0




0




5




3




0




5




4




0




0




0




0






Velvetleaf




0




0




6




1




0




0




0




3




1




0




0




0




0




0




0




0




0




0




0




0




2




0




0




2




0




0




0




0




0






Wheat




4




0




0




2




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0






Wild oats




0




9




6




6




2




0




3




0




4




0




2




3




3




3




0




4




4




0




0




0




10




0




7




5




7




0




0




0




0
















COMPOUND








































Rate 62 g/ha




533




534




535




536




540




541




543




544




545




546




548




549




550




551




552




553




554




555




556




557




558




559




560




561




562




563




564




565




566









Preemergence






B. signalgrass




2




9









0




0




0




0




3




0




0




0




0




6




4




4




6




7




6




6




4




0




8




4




4




5




3




2




0




9






Bedstraw




0




0




0




0




0




0









0




0




0




8




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




4




8









0




0




0




0




0




0




0




0




0




0




3




0




7









0




6




6




2




9




4




5




4




2




0




0




3






Cocklebur




0




0




0




0




0














0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




2




0




0






Crabgrass




9




9




10




0




8




5




4




9




8




7




9




3




4




9




9




10




9




9




9




9




8




9




9




9




8




8




7




0




9






Giant foxtail




9




9




10




7




9




7




3




9




10









9




9




7




10




9




10




9




9




9




9




8




10




10




0




4




9




9




0




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0














0




0




0




0




0









0




0




0




0




0




0




0




0




0









0









0




0




0




0




0






Rape




0




2




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




2




0




0




0




0




0






Redroot pigweed




8




0




2




0




0




0




7




3




3









0




6




7




8




0




0




9




0




0




0




0




7




3




3




10




4




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




3




3




4




0




0




0




4




0




0




0




0




0




0




2




0




0




0




2




0




2




0




3




0




0




6




2




2




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




3




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









3




0




0




0




0




3




3




0




3




3




0




0




0






Wild oats




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




4




2




0




0




3
















COMPOUND








































Rate 62 g/ha




567




568




569




570




571




572




573




574




575




576




577




578




579




580




581




582




584




585




586




588




589




590




591




592




593




594




595




596




598









Preemergence






B. signalgrass




0




3




0




0




0




0




7




4




6




0




0




0




0




2




0




0




7




3




0




0




0




0




0




0




0




3




2




0




0






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0




0




0




8




0




9




7



















0




0




0




0




0




0




0




0






Blackgrass




0




5




0




0




0




0




0




0




2




0




0




0




0




0




0




0




9




3




3




0




0




0




0




0




0




5




6




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0














0




0






Corn




0




0




0




0




0




0




0




0




0




0




2




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




7




7




9




2




0




3




2




8




0




7




0




7




6




4




0




8




5




9




3




0




0




0




0




0




9




7




0




0






Giant foxtail




3




9




9




0




3




0




9




9




8




2




7




2




8




9




4




0




9




7




9




7




3




0




0




0




0




9




10




0




0






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0






Rape




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




3




3




0




0




0




0




0




0




0




0




4




0




0






Redroot pigweed




0




2




7




0




0




0




0




0




9




0




0




2




0




9









0




7




6




0




0




0




0




0




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




0




0






Velvetleaf




0




5




0




0




0




0




0




0




0




0




4




0




0




0




5




0




0




0




0




0




0




0




0




0




0




2




7




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0
















COMPOUND








































Rate 62 g/ha




601




602




603




604




605




606




607




608




609




610




611




612




613




614




615




618




619




620




621




622




624




625




627




628




629




630




631




632




633









Preemergence






B. signalgrass




3




0




0




0




0




0




4




1




3




6




7




4




7




0




0




0




0




0




0




0




3




0




5




3




0




0




6




0




0






Bedstraw




0




0














0



















4









1














0




0




0









0




0




0




0









2




6




0




0




0
















Blackgrass









0




0




0




0




0




4




2




7




8




9




8




8




0




0




0




0




0




0




1




1




0




8




6




4




5




6




2




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




2




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




2




0




2




0




2




0




0




0




0




0




0




0




0




0




3




3




1




0




5




0




0






Crabgrass




6




7




0




0




0




0




7




7




7




9




9




10




9




0




0




0




0




0




5




6




7




2




7




8




7




7




7




2




5






Giant foxtail




10




9




0




0




2




0




9




9




10




9




10




10




10




0




0




2




0




0




0




4




10




6




9




10




8




9




9




8




6






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




6




5




0




0




0




0




0






Nutsedge




0




0




0




0




0




0














0




0




0




0




0









0









0




0




0




0




0




0




7




3




0




0




0




0




0






Rape




0




0




0




0




0




0




0




1




0




3




3




0




7




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0






Redroot pigweed




4




2




0




0




0




0




4




5




8




10




6




8




10




0




0




0




0




0




0




4




0




0




9




8




2




2




7




0




0






Soybean




0









0




0




0




0




0




0




4




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




3




2




3




3




0




0




0




0




0




0




0




0




0




5




3




2




0




0




0




0






Velvetleaf




1




0




0




0




0




0




0




0




7




7




6




6




7




0




0




0




0




0




0




0




0




0




7




7




3




0




6




0




0






Wheat




0




0




0




0




0




0




0




0




0




2




1




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0






Wild oats




3




0




0




0




0




0




0




0




3




5




5




5




7




0




0




0




0




0




0




0




2




0




0









0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




634




635




636




637




638




639




640




641




642




643




644




645




646




647




648




649




650




652




653




654




655




656




657




658




659




660




661




663




664









Preemergence






B. signalgrass




1




4




3




0




4




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




2




0




2




0




0




0




1






Bedstraw









9









0












































0









0




0




0




0




0




0




0














































Blackgrass




4




9




2




2




4




0




0




0




0




0




0




0




0




7




0




0




0




0




0




0




0




4




5




3




3




0




0




0




5






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




7




9




8




9




9




7




3




0




6




0




2




2









8




0




0




3




4




0




0









7




3




3




8




4




0




0




4






Giant foxtail




9




9




9




9




10




7




9




5




8




6




0




1




0




9




5




0




7




8




0




0




3




4




10




9




9




8




2




0




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




6




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




3




2




0




0




0




0




0






Redroot pigweed




0




10




10




4




7




0




0




0




0




0




0




0




0




10




0




0




1




0




0




0




0




0




7




2




6




0




0




0




2






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




3




0




0




0




0




0




0




0




0




0




0




0




7




0









0




0




0




0




0




0




7




3




0




0




0




0




0






Velvetleaf




0




0




0




0




3




0




0




0




0




0




0




0




0




6




0




0




0




0




0




0




0




2




3




0




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




2




2




0




0




4




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0
















COMPOUND








































Rate 62 g/ha




665




666




667




668




669




670




671




672




673




674




675




676




682




683




684




685




686




687




689




691




692




693




694




695




696




699




700




701




702









Preemergence






B. signalgrass




1




2




3




5




8




8




4




2




4




6




4




0




2




0




0




5




2




6




2




0




2




0




3




0




0




8




4




0




0






Bedstraw
























0




8









0




3




0




0









0




0




0









0




0




0




0




0




0




0









0




0




0




0




0






Blackgrass




5




6




8




6




9




8




5




1




3




6




5




0




3




1




1




5




4




8




9




4




8




0




7




0




6




8




4




0




2






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




2




2




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




3




0




0




0






Crabgrass




6




7




8




8




9




10




4




8




4




8




6




0




5




6




3




9




8




4




9




9




9




0




8




8




8




10




10




0




9






Giant foxtail




9




9




10




9




9




10




8




9




9




6




9




8




9




8




7




9




9




6




10




9




9




0




9




8




8




10




10




6




10






Morningglory




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




2




0




0




1




0




0




0




0




2




0




0




0






Nutsedge




0




0




0




0




0









0




0




0




0




0




0




0




0




0









0









0




0




0









0




0









0









0




0






Rape




4




0




7




0




2




8




0




0




1




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




7




8




10




0




6




9




0




0




6




7




5




4




4




0




0




0




0




8




3




2




7




0




0




0




3




3




0




0




2






Soybean




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




5




0




6




8




1




3




0




2




5




2




0




0




0




0




0




4




0




0




0




0




0




0




0




3




0




0




0






Velvetleaf




0




5




6




3




0




6




2




0




0




6




6




4




0




0




0




0




0




2




2




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




2




0




6




7




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




3




5




4




2




10




7




0




0




5




1




4




0




0




0




0




0




0




7




7




2




0




0




0




0




0




9




4




0





















COMPOUND








































Rate 62 g/ha




703




704




706




707




708




709




710




711




712




713




714




715




716




717




718




719




720




721




722




725




726




727




728




729




730




732




733




734




735









Preemergence






B. signalgrass




2




2




2




6




0




0




8




2




3




5




7




8




0




4




0




3




8




7




0




0




4




0




5




5




0




0




6




9




7






Bedstraw




0




0




0




7




0




0




3




2




0




0




0




0




0




0




0




0









3




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




0




2




8




9




0




0




9




6




3




5




7




9




0




9




8




6




9




9




0




2




7




0




0




6




6




0




4




7




8






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




5




5




5




5




6




2




10




8




8




10




10




9




0




10




9









9




9




0




6




9




3




6




7




9




0




2




9




10






Giant foxtail




5




4




6




6




5




2




10




10




10




10




10




10




0




10




10









9




9




0




7




9




7




4




9




10




0




3




9




9






Morningglory




0




0




1




3




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




1




0




0




0




0




0




0




1




2




0






Nutsedge




0




0




0




0









0









0




0




0




0




0




0




0




0




0









0




0




0




0









0




0




0




0




0




0




0






Rape




0




0




0




8




0




0




7




1




0




4




2




2




0




0




0




0




6




1




0




0




0




0




0




0




0




0




0




0




1






Redroot pigweed




0




0




8









0




0




8




7




6




6




10




8




0




6




0




7




8




9




0




0




0




0




0




7




6




0




0




2




5






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




6




0




0




6




5




0




3




2




4




0




0




0




4




4




3




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




3




0




0




5




4




0




2




6




0




0




0




0




0




1




0




0




0




0




0




0




0




0




0




0




2




0






Wheat




0




0




0




2




0




0




5




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




4




8




0




0




8




7




0




2




0




9




0




9




2




2




7




6




0




0




1




0




0




2




0




0




2




3




6
















COMPOUND








































Rate 62 g/ha




737




738




739




740




741




742




743




744




745




746




747




748




749




750




751




752




753




754




755




756




757




758




759




760




761




762




763




764




765









Preemergence






B. signalgrass




4




6














0




0




0




5




8




7




7




0




0




5














2




3




0




0




0




6




3




2




0




0




0




8




5






Bedstraw




0




0




0




0




0




0




0




0




0




8




0









0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0






Blackgrass




6




8




2




3




0




0




8




6




3




9




8




0




0




7




9




4




5




7




0




0




1




6




4




0




0




0




8




7




7






Cocklebur




0




0




0




0




0




0




0




0




0









0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




8




8




2




4




5




0




9




9




7




9




10




9




9




9




10




9




9




8




0




4




6




9




7




2




3









9




10




9






Giant foxtail




9




8




9




4




0




0




9




9




10




10




10




9




9




9




10




10




9




8




0




7




9




9




9




8




0




5




9




10




9






Morningglory




1




1




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0









0




0




0




0




0









0




0




0




0




0




0




0




0




0




3




0









0




0




0




0




0




0




0




0




0






Rape




0




2




0




0




0




0




5




4




0




2




7




0




0




0




4




0




2




0




0




0




0




0




0




0




0




0




0




0




2






Redroot pigweed




2




6




2




3




0




0




7




4




7




10




8




4




0




7




10




0




6




8




0




0




0




8




0




7




0




2




8




9




8






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




1




3




2




0




0




0




0




0




0




5




4




0




0




1




2




0




0




0




0




0




0




5




0




3




0




0




0




0




6






Velvetleaf




0




0




0




0




0




0




0




0




0




4




4




0




0




0




7




0




0




0




0




0




0




2




0




0




0




0




0




3




0






Wheat




0




2




0




0




0




0




0




0




0




6




0




0




0




2




0




0




0




0




0




0




0




4




0




0




0




0




0




0




3






Wild oats




5




4




0




0




0




0




5




3




2




7




3




0




0




0




3




0




0




0




0




0




0




5




0




0




0




0




2




0




4

















COMPOUND
























Rate 62 g/ha




766




767




772




773




774




776




779




780




790




791




792









Preemergence






B. signalgrass




6









0




0




0














6




8




0




0






Bedstraw




4









0




0




0




0




0




0




0









0






Blackgrass




0




10




0




0




0




0




2




2




8




0




1






Cocklebur




0




0




0




0




0









0




0




0




0




0






Corn




0




0




0




0




0




0




0




2




2




0




0






Crabgrass




9




10




0




0




0




5




9




10




10




6




10






Giant foxtail




9




10




0




0




0




9




9




10




10




10




10






Morningglory




2




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0






Rape




2




4




0




0




0




0




0




0




2




0




0






Redroot pigweed




9




10




0




0




0




0




0




0




2




0




7






Soybean




0




0




0




0




0




0




0




0




0




4




0






Sugarbeets




2




2




0




0




0




0




0




2




1




0




0






Velvetleaf




5




0




0




0




0




0




2




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0






Wild oats




3




9




0




0




0




2




0




0




0




0




0

















COMPOUND


































Rate 31 g/ha




196




200




217




221




285




287




288




289




290




291




295




296




318




324




392




442




450




483




614




644




656









Pre-emergence






Barnyardgrass




0




0




0




0




0




0




0




0




6




2




0




0




0




0




0




0




0




0




0




0




0






Ducksalad




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






S. Flatsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0
















COMPOUND













































Rate 31 g/ha




4




14




22




23




26




27




28




29




30




31




32




33




87




98




100




137




138




139




146




155




156




200




213




217




221




225




244




250




252




256




264




285




287




288









Postemergence






B. signalgrass




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Barnyardgrass




0




0




0




0












































0




3









0




0




0




0




0




0







































































Bedstraw




0









0




0




0




0




3




0




0




0




0




0









0




0



















0




0




0




0




0




0




2









0




0




0




0




0




0




0




0






Blackgrass




0









0




0




0




0




0




0




0




0




0




3









0




0



















4




0




0




0




0




0




2




0




0




0




0




0




0




0




8




0






Cocklebur




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0









0




0




0




0




1




0




0




0




0




0









0




0



















5




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0






Ducksalad




0




0




0




0












































0




0









0




0




0




0




0




0







































































Giant foxtail




0









0




0




0




0




1




0




0




0




0




0









0




0



















3




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0






Morningglory




0









0




0




0




0




0




0




1




0




6




3









0




0



















2




0




0




0




5




0




0




2




0




4




2




6




6




1




2




3






Nutsedge




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0






Rape




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Rice




0




0




0




0












































0




0









0




0




0




0




0




0







































































S. Flatsedge




0




0




0




0












































0




0









0




0




0




0




0




0







































































Soybean




1









3




3




1




1




3




1




1




0




2




2









1




0



















2




1




1




1




1




1




1




1




0




1




1




3




0




0




1




0






Sugarbeets




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0






Wild oats




0









0




0




0




0




0




0




0




0




0




0









0




0



















0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0

















COMPOUND


































Rate 31 g/ha




289




290




291




295




296




318




324




362




392




442




450




481




483




518




548




614




644




656




722




776




779









Postemergence






B. signalgrass




0




0




0




0




0




0




0




1




0




0




0




0




0




3




0




0




0




0




0




0




2






Barnyardgrass















































































































Bedstraw




0




0




0




0




0




0




0




5









0




0



















0
























0




0






Blackgrass




2




0




0




0




0




0




0




8




7




0




0




0




0




4




0




0




0




6




0




2




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0




0




0




0




0




3




1




0




0




0




0




0




0




0




0




0




0




2




3






Ducksalad















































































































Giant foxtail




2




0




0




0




0




0




0




5




7




0




0




0




0




0




0




0




0




0




0




2




5






Morningglory




2




4




1




1




0




0




0




0




3




1




0




0




0




5




1




0




0




0




3




4




5






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0




0




2






Rice















































































































S. Flatsedge















































































































Soybean




0




1




1




1




0




0




0




4




1




0




0




4




0




4




1




2




0




1




0




1




2






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




2




2






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




2




0




0
















COMPOUND












































Rate 31 g/ha




4




22




23




26




27




28




29




30




31




32




33




98




100




146




155




156




200




213




217




221




225




244




250




252




256




264




285




287




288




289




290




291




295









Preemergence






B. signalgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




2




0




0




0




0




0




0




0




3




0




2




0




0




3






Bedstraw




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0




0




0




0









0




0




0




0




0




0




4




0




0




0




0




0






Blackgrass




0




0




0




0




0




0




0




0




0




0




0




0




0




7




0




0




0




0




0




5




0




0




0




0




0




0




0




7




0




6




0




0




4






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0









0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




3




3




0




0




0




2




0




2




2




0




3




2




0




5




0




0




0




0




0




2




2




0




0




0




0




0




0




2




0




1




0




0




2






Giant foxtail




8




3




1




0




0




0




0




2




1




1




3




4




0




9




0




0




0




0




3




5




8




0




7




3




0




0




7




9




0




9




2




8




8






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0









0




0




0




0



















0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




4




0




0




0




0




0






Redroot pigweed




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




7




6




0




0




0




0




0




0




4




0




5




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




0




0




0




0




0




0




0




0




0




0




5




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




3




0




0




0




0




0






Wheat




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




0




0




0




0




0




0




0




0




0




0




1




0




0




0




0




0




2




0




0




0




0




0




0




0




1




0




0




0




0




0

















COMPOUND
































Rate 31 g/ha




296




318




324




362




392




442




450




481




483




518




548




614




644




656




716




722




727




776




779









Preemergence






B. signalgrass




0




0




0




2




0




0




0




7




0




0




0




0




0




0




0




0




0
















Bedstraw




0









0




8




0














0




0




0




9




0














0




0




0




0




0






Blackgrass




0




0




0




8




2




0




0




3




0




4




0




0




0




2




0




0




0




0




0






Cocklebur




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Corn




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Crabgrass




0




0




0









8




5




0




7




0




0




4




0




2




6




0




0




3




5




8






Giant foxtail




0




0




0









10




0




0




8




0




0




9




0




0




4




0




0




5




5




9






Morningglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Rape




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed




0




0




0




3




0




0




0




0




0




2




0




0




0




0




0




0




0




0




0






Soybean




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sugarbeets




0




0




0




3




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Velvetleaf




0




0




0




2




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wheat




0




0




0




4




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Wild oats




0




0




0




7




2




0




0




4




0




4




0




0




0




0




0




0




0




2




0

















COMPOUND
















Rate 16 g/ha




287




290




291









Pre-emergence






Barnyardgrass




0




0




0






Ducksalad




0




0




0






Rice




0




0




0






S. Flatsedge




0




0




0

















COMPOUND

















Rate 16 g/ha




287




290




291




779









Postemergence






B. signalgrass




0




0




0




0






Barnyardgrass


























Bedstraw




0




0




0




0






Blackgrass




0




0




0




0






Cocklebur




0




0




0




0






Corn




0




0




0




0






Crabgrass




0




0




0




2






Ducksalad


























Giant foxtail




0




0




0




2






Morningglory




2




3




1




5






Nutsedge




0




0




0




0






Rape




0




0




0




0






Redroot pigweed




0




0




0




2






Rice


























S. Flatsedge


























Soybean




1




1




1




2






Sugarbeets




0




0




0




2






Velvetleaf




0




0




0




2






Wheat




0




0




0




0






Wild oats




0




0




0




0

















COMPOUND

















Rate 16 g/ha




287




290




291




779









Preemergence






B. signalgrass




0




0




0











Bedstraw




0




0




0




0






Blackgrass




0




0




0




0






Cocklebur




0




0




0




0






Corn




0




0




0




0






Crabgrass




0




0




0




3






Giant foxtail




8




2




7




3






Morningglory




0




0




0




0






Nutsedge




0




0




0




0






Rape




0




0




0




0






Redroot pigweed




0




0




0




0






Soybean




0




0




0




0






Sugarbeets




0




0




0




0






Velvetleaf




1




0




0




0






Wheat




0




0




0




0






Wild oats




0




0




0




0














Test C




Compounds evaluated in this test were formulated in a non-phytotoxic solvent mixture which included a surfactant and applied to plants that were grown for various periods of time before treatment (postemergence application). A mixture of sandy loam soil and greenhouse potting mix in a 60:40 ratio was used for the postemergence test.




Plantings of these crops and weed species were adjusted to produce plants of appropriate size for the postemergence test. All plant species were grown using normal greenhouse practices. Crop and weed species include arrowleaf sida (


Sida rhombifolia


), barnyardgrass (


Echinochloa crus


-


galli


), cocklebur (


Xanthium strumarium


), common ragweed (


Ambrosia elatior


), corn (


Zea mays


), cotton (


Gossypium hirsutum


), eastern black nightshade (


Solanum ptycanthum


), fall panicum (


Panicum dichotomiflorum


), field bindweed (


Convolvulus arvensis


), giant foxtail (


Setaria faberii


), hairy beggarticks (


Bidens pilosa


), ivyleaf morningglory (


Ipomoea hederacea


), johnsongrass (


Sorghum halepense


), ladysthumb smartweed (


Polygonum persicaria


), lambsquarters (


Chenopodium album


), large crabgrass (


Digitaria sanguinalis


), purple nutsedge (


Cyperus rotundus


), redroot pigweed (


Amaranthus retroflexus


), soybean (


Glycine max


), surinam grass (


Brachiaria decumbens


), velvetleaf (


Abutilon theophrasti


) and wild poinsettia (


Euphorbia heterophylla


).




Treated plants and untreated controls were maintained in a greenhouse for approximately 14, to 21 days, after which all treated plants were compared to untreated controls and visually evaluated. Plant response ratings, summarized in Table C, were based upon a 0 to 100 scale where 0 was no effect and 100 was complete control. A dash response (−) means no test result.














TABLE C













COMPOUND


























80




93




94




103




107




109




113




116




117




131




132




138




146




242





























Rate 1120 g/ha




















Postemergence






Arrowleaf sida




30




60




80









85




95




95




90




50




60




80




70




90




90






Barnyardgrass




20




95




65




80




95




95




95




90




90




95




95




85




95




95






Cocklebur




50














0














50




50




0




10




0




0




70




20






Common ragweed




5




20




5




5




50




20




20




0




50




0




0









30




80






Corn




0




45




0




0




60




55




60




20




85




40




10




60




50




20






Cotton




40




85




80




80




90




70




80









60




65




40




70




70




70






E. blacknightsh




60




85




95




0




95




95




95




50




80




80




0




70




85




90






Fall panicum




10




90




70




30




85




95




85




90




80




90




50




90




90




90






Field bindweed




0




50




0




0




60




10




50




50




40




60




70




50




0




0






Giant foxtail




20




95




40




40




95




85




80




85




80




80




0




85




85




85






H. beggarticks




10




70




20




5




95




85




50









0




70









80




85




90






I. morningglory




50




70









10




95




70




50




20




0




50




0




0




50




0






Johnsongrass




0




90




0




0




90




95




95




80




85




70




60




90




90




90






Ladysthumb




70









90




10









95




85









































Lambsquarters




20




40




30




20




40




70




50




0




0




0




0




20




50




0






Large crabgrass




10




95









10




95




90




95




90




80




85




80




85




80




85






Purple nutsedge




0




10




0




0




10




0




10




10




80




80




0




70




0




80






Redroot pigweed




80




85




0




85




80




85




90




20




30




30




30




70




20




50






Soybean









85




55




35




85




85




85




40




60




45




40




40




85




65






Surinam grass




10




85




10




5




95




95




90




90




90




90




30




90




95




90






Velvetleaf




20




70




40




45




75




75




75




80




60




70




0




80




60




60






Wild poinsettia




5




70




85




60




80




90




95









0




80




0




70




70




85






Rate 560 g/ha






Postemergence






Arrowleaf sida









60




80




0




75




85




70




85




0




30




10









85




70






Barnyardgrass




20




90




30




10




90




85




85




90




90




95




80




85




85




90






Cocklebur




50




40









0









60




50




0




0




0




0




0




70




0






Common ragweed




5




10




5




0




50




10









0




20




0




0




0




30




80






Corn




0




0




0




0




55




5




45




15




40




5




0




50




5




0






Cotton




40




70




70




40




80




70




50




50




30




40




20




40




65




45






E. blacknightsh




50









75




0




70














10




70




50




0




70




85




60






Fall panicum




0




90




10




0




85




80




85




85




40




90




50




60




90




90






Field bindweed




0




0




0




0




30




10




50




50




30




0




40




0




0




0






Giant foxtail




0




80




10




0




95




80




80




60




75




60




0




80




80




80






H. beggarticks




10




5




5




0




70




70




30




90









40














85











I. morningglory




30




10




90




0




30




50




50




0




0




20




0




0




20




0






Johnsongrass




0




85




0




0




90




60




60




60




40




60




0




60




60




60






Ladysthumb




70




80




85




10




30




30




85





























85











Lambsquarters




20




10




10




5




40




30




20




0




0









0




10




10




0






Large crabgrass




10




50




70




0




95




90




95




30




60




70




40




85




60




85






Purple nutsedge




0




0




0




0




10




0




0




10




10




0




0




50




0




10






Redroot pigweed




50




10




0




70




80




70




0




0




0




20









40









10






Soybean




60




80




30




35




85




85




85




30




40




30




30




30




60




25






Surinam grass




0




50




0




0




80




50




90









40




85




0




85




50




85






Velvetleaf




20




40




20




10




70




50




60




40




20




10




0




70




40




40






Wild poinsettia




5




30




60




10




40




50




80




0




0




30




0




0




50




0






Rate 280 g/ha






Postemergence






Arrowleaf sida




5




10




10




0




30




70




40









0




10




0









45




30






Barnyardgrass




10




90




0




0




85




85




80




85




80




70




50




70




80




85






Cocklebur




10




35




0




0




50




30




50









0




0




0




0




40




0






Common ragweed




0




10




0




0




50




10




5




0




0




0




0




0









10






Corn




0




0




0




0




5




0




40




0




0




0




0




20




0




0






Cotton




35




30




70




20




60




50




15




50




10




10




10




30




65




20






E. blacknightsh




5




40




40




0




50




80




50




0




0




10




0




10




30




40






Fall panicum




0




80




0




0




60




50




80




60









40




30




0




60




85






Field bindweed




0




0




0




0




0




0




0




0




30




0




0




0




0











Giant foxtail




0




55




0




0




70




80




70




60




60




40




0




15




40




60






H. beggarticks









0




0




0




60




5




30



















0




10




20











I. morningglory




10




10




10




0




30




50




50




0




0




0




0




0




20




0






Johnsongrass




0




5




0




0




50




10




20




40




35




40




0




20




30




45






Ladysthumb




10




0




10




0









10




0





























10











Lambsquarters




15




10




5




5




0




10














0




0




0




0




5




0






Large crabgrass




0




30




0




0




85




60




85




0




20




20




10




10




60




30






Purple nutsedge




0




0




0




0




0




0




10




0




0




0




0




0




0




0






Redroot pigweed




0














60




75




40




0




0




0




10




10




10









0






Soybean




20




60




15




30




70




70




70




10




35




25




20




30




50




25






Surinam grass




0




45




0




0




70




5




40




0




0




80




0




40




5




40






Velvetleaf




5




5




5




5




60




20




0




0









0




0




60




40




0






Wild poinsettia




0




0




0




0




15




30




50




0




0




10




0




0




40




0






Rate 140 g/ha






Postemergence






Arrowleaf sida




0














0









60




30




0




0









0




0




40




10






Barnyardgrass




0




70




0




0




70




60




80




55




70




70




50




40




60




80






Cocklebur




5




0




0




0




0




30




5




0




0




0




0




0




40




0






Common ragweed




0




5




0




0




0




5




5




0




0




0




0




0




10




0






Corn




0




0




0




0




0




0




0




0




0




0




0









0




0






Cotton




20




15




20




0




45




10




10




10




5




10




5




5




40




0






E. blacknightsh




0




10




0




0




50




50




50




0




0




0




0




0




0




0






Fall panicum




0




0




0




0




50




50




60




10




0




0




0




0




50




30






Field bindweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Giant foxtail




0




10




0




0









50




20









0




10




0




0




0




40






H. beggarticks




0









0




0




5









5




80









0




0









10











I. morningglory




0




5




0




0




10




0




10




0




0




0




0




0




0




0






Johnsongrass




0




0




0




0




35




0




0




10




10




15




0




0




0




45






Ladysthumb




10




0




5




0




0









0





























0











Lambsquarters




0




10




0




0




0




10




0




0




0




0




0




0




0




0






Large crabgrass




0




0




0




0




70




10




0




0




0




0




0




0




0




10






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Redroot pigweed









5









0









0




0




0




0




10




0




0




0




0






Soybean




5




40




15




30




45




35




40




10




10




20




5




10




40




20






Surinam grass




0




0




0




0




10




0




0




0




0




0




0




10




0




0






Velvetleaf




5




0




5




0




5




10




0




0




0




0




0




0




0




0






Wild poinsettia




0




0




0




0




0




10




10




0




0




0




0




0




0




0














Test D




Seeds, tubers, or plant parts of Alexandergrass (


Brachiaria plantaginea


), bermuda-grass (


Cynodon dactylon


), common pursiane (


Portulaca oleracea


), common ragweed (


Ambrosia elatior


), common groundsel (


Senecio vulgaris


), dallisgrass (


Paspalum dilatatum


), goosegrass (


Eleusine indica


), guineagrass (


Panicum maximum


), itchgrass (


Rottboellia exaltata


), Johnson grass (


Sorghum halepense


), large crabgrass (


Digitaria sanguinalis


), pitted morningglory (


Ipomoea lacunosa


), purple nutsedge (


Cyperus rotundus


), sandbur (


Cenchrus echinatus


), sourgrass (


Trichachne insularis


), Spanishneedles (


Bidens bipinnata


), surinam grass (


Brachiaria decumbens


) and tall mallow (


Malva sylvestris


) were planted into greenhouse pots of flats containing greenhouse planting medium. Plant species were grown in separate pots or individual compartments. Preemergence applications were made within one day of planting the seed or plant part.




Test chemicals were formulated in a non-phytotoxic solvent mixture which included a surfactant and applied preemergence to the surface of the pot containing seeds in a sandy loam soil. Untreated control pots and treated pots were placed in the greenhouse for growth and visually evaluated for injury 14 to 21 days after herbicide application. Plant response ratings, summarized in Table C, are based on a 0 to 100 scale where 0 is no injury and 100 is complete control. A dash (−) response means no test result.












TABLE D









COMPOUND




















































Rate 500 g/ha




146




147




299









Postemergence






Alexandergrass




65




75




100






Bermudagrass




35




40




100






C. purslane




20




10




0






C. ragweed




40




0




100






Com. groundsel




0




0




100






Dallisgrass




80




85




100






Goosegrass




80




65




100






Green foxtail














100






Guineagrass




60




60




100






Itchgrass




65




65




100






Johnsongrass




65




70




100






Large crabgrass




65




60




100






P. morninglory




65




30




0






Purple nutsedge




35




60




100






Sandbur




80




90




100






Sourgrass




80




80











Spanishneedles




20




20




100






Surinam grass




80




70




100






Tall Mallow




50




20




100









Rate 500 g/ha




4




24




30




36




46




78




93




94




103




105




107




108




109




110




112




115




117




131




138




146




147




151




170




242









Preemergence






Alexandergrass




100




98




90




98




80




100




100




80




95




100




100




100




100




100




100




100




98




100




100




100




100




100




100




100






Bermudagrass




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




100




0




0




0




10




0






C. ragweed




0




0




0




10




0




0




80




10




0




0




100




80




55




0




0




20




65




100




100




75




0




20




45




100






Com. groundsel









0




100




100




0




0




100




100




0




80




100




100




0




20




10




98




100




100




100




100




0




100




100











Dallisgrass




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






Goosegrass




100




100




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






Green foxtail














100




100




100




100




100




100




100




100




100




100




100




100




0




100




100




100




100




100









100




100




100






Guineagrass




100




100




98




100




85




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






Itchgrass




80




40









80




10




20




100




40




0




85




100




100




100




40




80




50




100




100




100




100




85




100




50




100






Johnsongrass




30




85




40




0




60




20




85




20




40




90




100




85




100




45




50




90




100




100




100




95




95




100




95




100






Large crabgrass




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




0




0




0




0




0




0




20




0




0




0




100




0




100




0




10




10




40




100




65




20




30




20




85




100






Purple nutsedge




0




0




0




0




0




0




100




50




10




75




85




30




85




0




40




0




100




85




80




100




85




70




65




60






Sandbur




100




100




100




100




0




80




100




100




100




100




100




100




100




98




100




100




100




100




100




100




80




100




98




100






Sourgrass




100




100




















































































100




100





















Spanishneedles




0




0




0




10




20




0




45




0




20




0




100




20




30




0




10




10




0




90




75




100




30




40




85




40






Surinam grass




98




65




85




85




30




98




100




90




40




100




100




100




100




85




98




85




100




100




100




100




100




100




100




100






Tall Mallow




30




0




0




0




10




0




98




20




0




75




100




98




100




0




20




0




100




100




100




100




70




85




45




85









Rate 250 g/ha




131




146




147




241




242




243




299




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




100




40




50




100




100




100




100




80




100




100




90




100




100




100




100






Bermudagrass




100




0




20




100




100




100




100




100




100




100




100




100




100




100




100






C. purslane




0




20




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




100




30




0




100




100




60




100




100




90




20




20




100




50




70




30






Com. groundsel




100




0




0




100




100




100




100




0




100




100




50




100




100




40




100






Dallisgrass




100




60




85




100




100




100




100




100




100




100




90




100




100




100




100






Goosegrass




100




30




50




100




100




100




100




100




100




100




90




100




100




100




100






Green foxtail




100














100




100




100




100




100




100




100




100




100




100




100




100






Guineagrass




100




35




50




100




100




100




100




90




100




80




40




100




100




100




100






Itchgrass




100




50




50




100




100




100




50




0




30




100




0




60




50




100




30






Johnsongrass




100




50




60




0




90




100




100




0




100




90




40




80




90




100




70






Large crabgrass




100




50









100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




100




50




30




0




0




40




0




0




0




0




0




0




0




0




10






Purple nutsedge




100




0




35




0




100




100




0




0




0




0




0




0




50




10




20






Sandbur




100




85




35




90




100




100




100




0




50




100




80




100




100




90




100






Sourgrass




—80




80


































































Spanishneedles




60




10




0




10




100




100




20




0




20




0




0




30




20




0




20






Surinam grass




100









80




100




100




100




100




40




100




100




60




100




100




50




100






Tall Mallow




100




0




0




40




100




60




70




10




30




40




0




20




100




80




90









Rate 250 g/ha




4




24




28




30




34




46




78




93




103




105




107




108




109




110




112




115




119




131




138




146




147




151




170




242









Preemergence






Alexandergrass




90




65




75




80




60




75




75




100




85




98




100




100




100




100




80




85




100




100




98




100




90




100




98




100






Bermudagrass




98




100




100




98




100




100




100




100




100




100




100




100




100




100




98




100




100




100




100




90




100




100




100




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




100




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




100




0




10




0




0




20




0




100




60




60




0




20




40




100






Com. groundsel









0




0




0




0




0




0




0




0




0




100




100




0




20




0




10




100




100




100




85




0




100




45











Dallisgrass




98




98




100




80




100




100




100




100




98




100




100




100




100




100




100




98




98




100




100




100




100




100




100




100






Goosegrass




98




98




100




85




98




98




98




100




98




100




100




100




100




100




100




100




100




100




100




100




100




100




98




100






Green foxtail



















100









100




100




100




100




100




100




100




100




100




98




100




100




100




100




100









100




100




100






Guineagrass




100




98




98




98




98




65




100




100




90




100




100




100




100




100




90




98




98




100




100




100




100




100




100




100






Itchgrass




80




40




40




75




20




0




10




90




0




85




100




98




100




40




0




50




75




100




100




100




75




100




45




98






Johnsongrass




30




85




0




0




30




40




20




95




0




75




98




85




100




20




0




75




85




98




100




90




95




50




100




98






Large crabgrass




100




100




100




98




100




100




100




100




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




75




0




85




0




0




0




0




85




65




0




0




0




65




20






Purple nutsedge




0




0




0




0




0




0




0




30




0




0




85




10




75




0




0




0




0




85




75




75




40




65




65




60






Sandbur




90




20




0




40




40




0




75




100




75




98




100




98




100




98




0




50




100




100




98




100




85




100




40




100






Sourgrass




100




100




100









100










































































100




100





















Spanishneedles




0




0




75




0




40




10




0




0




20




0




100




0




30




0




0




10




10




75




70




90




30




85




100




100






Surinam grass




85




10




75




85




20




10




85




98




0




98




100




98




100




70




0




75




98




100




30




100




10




0




40




10






Tall Mallow




30




0




0




0




0




10




0




90




0




75




98




45




98




0




0




0




0




90




98




100




90




100




40




60









Rate 125 g/ha




131




146




147




241




242




243




299




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




100




20




35




100




100




100




100




70




100




100




70




100




100




90




100






Bermudagrass




100




0




0




100




100




100




100




100




100




100




100




100




100




100




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




90




0




0




100




90




10




50




0




60




0




0




20




0




70




30






Com. groundsel




100




0




0




100




90




100




100




0




100




100




20




100




100









100






Dallisgrass




100




30




70




90




100




100




100




90




90




100




60




100




100




100




100






Goosegrass




100




35




50




100




100




100




100




100




90




100




100




100




100




100




100






Green foxtail




100














100




100




100




100




60




100




100




80




100




100




100




100






Guineagrass




100




10




30




100




100




100




80




50




50




100




0




80




70




100




100






Itchgrass




100




30




50




100




80




10




10




0




20




0




0




20




30




0




20






Johnsongrass




60




35




50




0




30




30




60




0




20




20




10




40




60




0




50






Large crabgrass




100




20




60




100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




0




40




0




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




30




0




0




0




0




10




0




0




0




0




0




0




0




0




10






Sandbur




100









0




100




100




30




100









50




60




20




100




0




100




100






Sourgrass









50




30


































































Spanishneedles




70




10




0




0




0




20




0




0




0




0




0




40




10




0




0






Surinam grass




100









20




100




100




100




100




30




70




80




10




70




100




50




90






Tall Mallow




90




0




0




10




90




40




90




0




0




20




0




30




50




70




60









Rate 125 g/ha




4




18




24




28




30




34




46




78




93




94




103




105




107




108




109




113




114




115




117




119




131




138




146




147




151




170




242









Preemergence






Alexandergrass




80




30




10




60




50




30




65




75




85




50




40




98




100




98




100




98




98




75




90




98




100




80




98




85




98




85




98






Bermudagrass




30




100




98




100




98




100




100




98




100




90




80




100




100




100




100




100




100




100




100




100




100




100




90




98




100




100




98






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




30




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




10




0




0




0




85




0




10




0




0




10




0




0




30




30




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




35




75




0




0




100




100




0




100




85




10




75




100




100




100




75




0




100




45











Dallisgrass




98




100




98




85




60




98




100




100




98




98




65




100




100




100




100




100




100




98




95




90




100




100




100




98




100




85




98






Goosegrass




98




85




98




98




85




85




85




98




100




85




85




98




100




100




100




100




100




98




100




100




100




100




100




98




100




75




100






Green foxtail









85














85









40




100




100




90




100




100




100




100




100




100




100




100




100




100




100




100




100









100




100




100






Guineagrass




90




65




90




75




75




85




30




85




100




0




85




98




100




98




100




100




100




85




100




98




100




100




100




90




100




100




100






Itchgrass




0




0




40




40




75




0




0




0




75




0




0




20




98




40




75




60




20




50




75




60




90




80




90




65




85




30




80






Johnsongrass




0




0




0




0




0




20




40




0




75




0




0




20




90




40




98




90




0




60




90




75




90




65




80




85




50




75




85






Large crabgrass




100




100




100




100




98




100




98




100




100




98




95




100




100




100




100




100




100




100




98




100




100




100




100




100




100




100




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0




30




0




65




10




0




0




20




0




50




65




0




0




0




40




20






Purple nutsedge




0




0




0




0




0




0




0




0




0




50




0




0




65




10




40




30




20




0




0




0




60




65




70




30




30




0




40






Sandbur




30




0




20




0




40




30




0




0




65




20




0




0




98




98




100




100




85




40




0




98




100




65




100




0




100




40




90






Sourgrass




100









100




100









100















































































100




100





















Spanishneedles




40




0




0




75




0




0




10




0




10




0




0




0




20




0




10




0




0




0




0




10




60




10




90




10




0




0




10






Surinam grass




90




20




10




65




40




0




0




30




90




80




0




40




100




98




98




100




75




75




100




85




100




85




100




85




100




75




90






Tall Mallow




0




0




0




0




0




0




10




0




30




0




0




40




90




10




85




30




10




0




65




0




80




40




80




0




75




30




0









Rate 64 g/ha




131




146




147




169




241




242




243




299




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




100




10




20




65




10




90




20




90




0




50




70




40




80




100




100




50






Bermudagrass




100




0




0




100




100




100




100




90




90




60




100




70




100




100




100




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




20




30




10




100




0




0




0




0




20




0




—30






Com. groundsel




100




0




0




65




0




90




0




100









100




50









50




100




0




0






Dallisgrass




100









10




90




50




90




70




100




0




90




90




0




80




100




100




100






Goosegrass




100




0




0




100




100




100




100




90




90




90




100




100




100




100




100




100






Green foxtail




100














100




10




100




100




100




0




100




100




10




100




100




100




100






Guineagrass




100




10




0




100




80




0




20




0




80




0




0




20




60




20




100






Itchgrass




20




30




0




0




0




40




0




0




0




20




0




0




0




0




0




0






Johnsongrass




30




20




0




0




0




40




0




0




0




20




0




0




0




0




0




0






Large crabgrass




100




20




10




100




100




100




100




100




40




90




100




70




100




100




100




100






P. morninglory




0




30




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sandbur




100




0




0




40




20




50




30




90




0




0




20




0




70




0




100




50






Sourgrass









50




0







































































Spanishneedles




0




10




0




0




0




0




50




0




0




0




0




0




0




10




0




0






Surinam grass




60














65




60




100




90




50




20




20




20




0




30




80




0




100






Tall Mallow




40




0




0




0




0




50




30




30




0




0




0




0




30




20




50




40









Rate 64 g/ha




4




18




24




28




30




34




46




78




93




103




105




107




108




109




112




113




115




117




119




130




131




132




138




139




146




147




151




170




242









Preemergence






Alexandergrass




80




0




10




0




40




20




40




30




30




0




85




100




85




98




0




98




50




90




75




98




98




98




80




60




95




75




98




30




100






Bermudagrass




0




85




95




100




98




98




98




90




90




60




98




100




100




100




85




100




98




98




100




100




100




100




100




98




95




95




90




100




85






C. purslane




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




30




30




0




10




0




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




0




0




0




98




85




0




0




100




10




0




100




0




85




0




40




0




0




0




0




0











Dallisgrass




90




85




30




75




50




80




40




75




98




45




98




100




100




100




70




100




75




85




85




100




100




98




100




90




98




80




100




85




98






Goosegrass




95




85




50




85




70




75




75




85




98




65




98




100




98




100




85




100




90




85




98




100




100




98




98




98




100




98




100




75




95






Green foxtail









85














85









30




85




100




50




100




100




100




100




85




100




85




100




90




100




100




100




100




98




100









100




100




100






Guineagrass




50




30




75




65




40




80




30




65




100




0




98




100




98




100




40




100




30




100




85




100




100




85




100




65




100




85




100




98




98






Itchgrass




75




0




40




20




40




0




0




0




60




0




20




85




30




75




0




50




40




40




50




80




90




10




30




20




90




20




75




0




70






Johnsongrass




30




0




0




0




0




0




0




0




40




0




0




90




20




75




0




80




40




90




65




65




65




35




40




10




60




20




40




0




40






Large crabgrass




98




98




70




98




85




98




40




98




98




85




100




100




100




100




10




100




85




98




98




100




100




100




100




90




100




98




100




100




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




30




0




0




0




10




0




0




0




65




0




0




65




30




0




0




0




20




10






Purple nutsedge




0




0




0




0




0




0




0




0




20




0




0




20




0




40




0




20




0




0




0




0




40




0




30




0




65




0




0




0




0






Sandbur




65




0




20




0




0




0




0




0




65




0




0




65




30




98




0




75




0




0




65




100




85




0




65




40




100




0




90




40




0






Sourgrass




90




100




85









100




















































































100




98





















Spanishneedles




0




0




0




60




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




60




40




0




10




20




85




0




0




0




0






Surinam grass




65




0




10




0




40




0




0




20




85




0




0




100




65




85




0




98




65




80




50




80




85




30




40




20




60




75




85




30




85






Tall Mallow




0




0




0




0




0




0




0




0




0




0




0




0




0




60




0




0




0




40




0




85




80




40




40




20




50




0




0




30




0









Rate 32 g/ha




131




241




242




243




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




50




10




50




0




0




0




0




0




60




20




0




60






Bermudagrass




90




30




100




60




30




80




20




40




80




100




90




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




30




0




0




0




0




0




0









0




0






Com. groundsel




100




0




100




0




0




40














0




40




0











Dallisgrass




60




40




90




50




0




30




50




0




70




20




30




40






Goosegrass




100




100




100




80




30




80




90




20




90




100




20




100






Green foxtail




60




10




100




100




0




100




20




0




100




30




30




70






Guineagrass




20




0




100




0




0




0




0




0




0




0




0




100






Itchgrass




0




0




0




0




0




0




0




0




0




0




0




0






Johnsongrass




0




0




0




0




0




0




0




0




0




0




0




0






Large crabgrass




100




70




100




70




0




30




60




0




100




100




40




80






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0






Sandbur




0




40




30




20




0




0




0




0




90




0




20




90






Sourgrass


































































Spanishneedles




0




0




0




50




0




0




0




0




0




10




0











Surinam grass




40




0




30




20




0




20




0




0




0




20




0




0






Tall Mallow




30




0




0




20




0




0




0




0




0




10




30




0









Rate 32 g/ha




4




18




24




28




30




34




46




78




93




103




105




107




108




109




112




113




115




119




131




146




147




151




170




242









Preemergence






Alexandergrass




20




0




10




0




0




0




0




0




10




0




30




90




20




90




0




85




20




50




90




85




0




40




20




85






Bermudagrass




0




60




75




85




65




85




85




85




80




30




98




100




98




100




75




100




98




65




100




100




85




90




90




85






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




0




0




0




75




75




0




0




65




0




98




75




0




0




0




0











Dallisgrass




85




0




30




30




0




0




40




0




98




20




98




85




50




98




65




95




75




65




95




90




60




85




0




85






Goosegrass




85




0




50




0




40




0




20




10




98




30




98




98




85




98




40




100




85




85




98




98




65




85




65




85






Green foxtail









0














50









0




75




75




0




85




100




100




100




0




98




70




75




100














100




75




100






Guineagrass




20




0




60




40




30




30




0




20




75




0




85




75




85




100




0




100




30




75




100




95




0




90




85




85






Itchgrass




0




0




40




0




20




0




0




0




60




0




0




75




20




65




0




40




40




10




50




90




0




0




0




65






Johnsongrass




0




0




0




0




0




0




0




0




0




0




0




85




20




0




0




60




40




0




40




60




0




0




0




40






Large crabgrass




100




0




70




85




40




85




20




40




98




0




98




98




100




100




10




100




75




90




100




100




98




98




85




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




0




20




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




40




0




0




0




0






Sandbur




0




0




20




0




0




0




0




0




0




0




0




30




0




0




0




65




0




0




60




85




0




20




0




0






Sourgrass




65









40




60









98





































































98




75





















Spanishneedles









0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




75




0




0




0




0






Surinam grass




0




0




10




0




40




0




0




0




0




0




0




75




65




30




0




90




20




0




75




60




0




30




0




85






Tall Mallow




0




0




0




0




0




0




0




0




0




0




0




0




0




20




0




0




0




0




30




40




0




0




30




0









Rate 16 g/ha




131




241




242




243




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




0




0




0




0




0




0




0




0




0




0




0




20






Bermudagrass




30




0




90




20




20




0




0




0




0




90




0




0






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




50




0









0




0




0




0




0




0






Com. groundsel




90









0




0









0




30



















0











Dallisgrass




20




0




60




0




0




0




0




0




0




0




0




0






Goosegrass




90




0




90




70




20




40




50




0




0




90




0




20






Green foxtail




0




0




30




10




0




0




0




0




0




10




0




0






Guineagrass




0




0




0




0




0




0




0




0




0




0




0




0






Itchgrass




0




0




0




0




0




0




0




0




0




0




0




0






Johnsongrass




0




80




0




0




0




0




0




0




0




0




0




0






Large crabgrass




90




0




0




0




0




0




20




0




0




100




0




0






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0






Sandbur




0




0




20




10




0




0




0




0




0




0




0




0






Sourgrass





























































Spanishneedles




0




0




0




0




0




0




0




0




0




10




0




0






Surinam grass




0




0




0




0




0




0




0




0




0




0




0




0






Tall Mallow




0




0




0




50




0




0




0




0




0




10




0




0









Rate 16 g/ha




4




18




30




46




78




93




103




105




107




108




109




112




113




115




119




131




146




147




151




170




242









Preemergence






Alexandergrass




20




0




0




0




0




0




0




0




0




20




40




0




65




0




0




20




65




0




40




20




65






Bermudagrass




0




40




50




65




75




80




30




85




85




85




98




60




98




75




50




100




65




0




90




80




80






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




40




65




0




0




0




0




85




75




65




0




0




0











Dallisgrass




75




0




0




20




0




60




10




60




30




40




40




30




0




0




30




85




80




0




100




0




65






Goosegrass




70




0




30




0




10




65




0




85




85




60




85




40




90




20




30




75




90




0




85




50




75






Green foxtail









0




0




0




0




65




0




75




100




40




98




0




80




0




10




90














100




65




80






Guineagrass




20




0




30




0




20




65




0




40




65




0




90




0




85




0




65




0




90




0




85




0




70






Itchgrass




0




0




20




0




0




50




0




0




40




0




0




0




10




40




0




30




85




0




0




0




65






Johnsongrass




0




0




0




0




0




0




0




0




20




0




0




0




0




0




0




10




60




0




0




0




10






Large crabgrass




100




0




40




0




0




90




0




40




85




85




85




10




85




75




85




100




90




50




98




30




90






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




0




20




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




40




0




0




0




0






Sandbur




0




0




0




0




0




0




0




0




30




0




0




0




0




0




0




0




0




0




0




0




0






Sourgrass




50



























































































Spanishneedles




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Surinam grass




0




0









0




0




0




0




0




30




0




0




0




85




0




0




20




40




0




30




0




20






Tall Mallow




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




30




40




0




0




30




0









Rate 500 g/ha




146




147




299









Postemergence






Alexandergrass




65




75




100






Bermudagrass




35




40




100






C. purslane




20




10




0






C. ragweed




40




0




100






Com. groundsel




0




0




100






Dallisgrass




80




85




100






Goosegrass




80




65




100






Green foxtail














100






Guineagrass




60




60




100






Itchgrass




65




65




100






Johnsongrass




65




70




100






Large crabgrass




65




60




100






P. morninglory




65




30




0






Purple nutsedge




35




60




100






Sandbur




80




90




100






Sourgrass




80




80











Spanishneedles




20




20




100






Surinam grass




80




70




100






Tall Mallow




50




20




100









Rate 500 g/ha




4




24




30




36




46




78




93




94




103




105




107




108




109




110




112




115




117




131




138




146




147




151




170




242









Preemergence






Alexandergrass




100




98




90




98




80




100




100




80




95




100




100




100




100




100




100




100




98




100




100




100




100




100




100




100






Bermudagrass




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






C. purslane




0




0




0




10




0




0




80




10




0




0




100




80




55




0




0




20




65




100




100




0




0




0




10




0






C. ragweed




0




0




0




10




0




0




80




10




0




0




100




80




55




0




0




20




65




100




100




75




0




20




45




100






Com. groundsel









0




100




100




0




0




100




100




0




80




100




100




0




20




10




98




100




100




100




100




0




100




100











Dallisgrass




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






Goosegrass




100




100




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






Green foxtail














100




100




100




100




100




100




100




100




100




100




100




100




0




100




100




100




100




100









100




100




100






Guineagrass




100




100




98




100




85




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






Itchgrass




80




40









80




10




20




100




40




0




85




100




100




100




40




80




50




100




100




100




100




85




100




50




100






Johnsongrass




30




85




40




0




60




20




85




20




40




90




100




85




100




45




50




90




100




100




100




95




95




100




95




100






Large crabgrass




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




0




0




0




0




0




0




20




0




0




0




100




0




100




0




10




10




40




100




65




20




30




20




85




100






Purple nutsedge




0




0




0




0




0




0




100




50




10




75




85




30




85




0




40




0




100




85




80




100




85




70




65




60






Sandbur




100




100




100




100




0




80




100




100




100




100




100




100




100




98




100




100




100




100




100




100




80




100




98




100






Sourgrass




100




100

























































































100




100





















Spanishneedles




0




0




0




10




20




0




45




0




20




0




100




20




30




0




10




10




0




90




75




100




30




40




85




40






Surinam grass




98




65




85




85




30




96




100




90




40




100




100




100




100




85




98




85




100




100




100




100




100




100




100




100






Tall Mallow




30




0




0




0




10




0




98




20




0




75




100




98




100




0




20




0




100




100




100




100




70




85




45




85









Rate 250 g/ha




131




146




147




241




242




243




299




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




100




40




50




100




100




100




100




80




100




100




90




100




100




100




100






Bermudagrass




100




0




20




100




100




100




100




100




100




100




100




100




100




100




100






C. purslane




0




20




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




100




30




0




100




100




60




100




100




90




20




20




100




50




70




30






Com. groundsel




100




0




0




100




100




100




100




0




100




100




50




100




100




40




100






Dallisgrass




100




60




85




100




100




100




100




100




100




100




90




100




100




100




100






Goosegrass




100




30




50




100




100




100




100




100




100




100




90




100




100




100




100






Green foxtail




100














100




100




100




100




100




100




100




100




100




100




100




100






Guineagrass




100




35




50




100




100




100




100




90




100




80




40




100




100




100




100






Itchgrass




100




50




50




100




100




100




50




0




30




100




0




60




50




100




30






Johnsongrass




100




50




60




0




90




100




100




0




100




90




40




80




90




100




70






Large crabgrass




100




50









100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




100




50




30




0




0




40




0




0




0




0




0




0




0




0




10






Purple nutsedge




100




0




35




0




100




100




0




0




0




0




0




0




50




10




20






Sandbur




100




85




35




90




100




100




100




0




50




100




80




100




100




90




100






Sourgrass









80




80


































































Spanishneedles




60




10




0




10




100




100




20




0




20




0




0




30




20




0




20






Surinam grass




100









80




100




100




100




100




40




100




100




60




100




100




50




100






Tall Mallow




100




0




0




40




100




60




70




10




30




40




0




20




100




80




90









Rate 250 g/ha




4




24




28




30




34




46




78




93




103




105




107




108




109




110




112




115




119




131




138




146




147




151




170




242









Preemergence






Alexandergrass




90




65




75




80




60




75




75




100




85




98




100




100




100




100




80




85




100




100




98




100




90




100




98




100






Bermudagrass




98




100




100




98




100




100




100




100




100




100




100




100




100




100




98




100




100




100




100




90




100




100




100




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




100




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




100




0




10




0




0




20




0




100




60




60




0




20




40




100






Com. groundsel









0




0




0




0




0




0




0




0




0




100




100




0




20




0




10




100




100




100




85




0




100




45











Dallisgrass




98




98




100




80




100




100




100




100




98




100




100




100




100




100




100




98




98




100




100




100




100




100




100




100






Goosegrass




98




98




100




85




98




98




98




100




98




100




100




100




100




100




100




100




100




100




100




100




100




100




98




100






Green foxtail



















100









100




100




100




100




100




100




100




100




100




98




100




100




100




100




100









100




100




100






Guineagrass




100




98




98




98




98




65




100




100




90




100




100




100




100




100




90




98




98




100




100




100




100




100




100




100






Itchgrass




80




40




40




75




20




0




10




90




0




85




100




98




100




40




0




50




75




100




100




100




75




100




45




98






Johnsongrass




30




85




0




0




30




40




20




95




0




75




98




85




100




20




0




75




85




98




100




90




95




50




100




98






Large crabgrass




100




100




100




98




100




100




100




100




98




100




100




100




100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




75




0




85




0




0




0




0




85




65




0




0




0




65




20






Purple nutsedge




0




0




0




0




0




0




0




30




0




0




85




10




75




0




0




0




0




85




75




75




40




65




65




60






Sandbur




90




20




0




40




40




0




75




100




75




98




100




98




100




98




0




50




100




100




98




100




85




100




40




100






Sourgrass




100




100




100









100










































































100




100





















Spanishneedles




0




0




75




0




40




10




0




0




20




0




100




0




30




0




0




10




10




75




30




100




10




0




40




10






Surinam grass




85




10




75




85




20




10




85




98




0




98




100




98




100




70




0




75




98




100




98




100




90




100




100




100






Tall Mallow




30




0




0




0




0




10




0




90




0




75




98




45




98




0




0




0




0




90




70




90




30




85




40




60









Rate 125 g/ha




131




146




147




241




242




243




299




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




100




20




35




100




100




100




100




70




100




100




70




100




100




90




100






Bermudagrass




100




0




0




100




100




100




100




100




100




100




100




100




100




100




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




90




0




0




100




90




10




50




0




60




0




0




20




0




70




30






Com. groundsel




100




0




0




100




90




100




100




0




100




100




20




100




100









100






Dallisgrass




100




30




70




90




100




100




100




90




90




100




60




100




100




100




100






Goosegrass




100




35




50




100




100




100




100




100




90




100




100




100




100




100




100






Green foxtail




100














100




100




100




100




60




100




100




80




100




100




100




100






Guineagrass




100




10




30




100




100




100




80




50




50




100




0




80




70




100




100






Itchgrass




100




30




50




100




80




10




10




0




20




0




0




20




30




0




20






Johnsongrass




60




35




50




0




30




30




60




0




20




20




10




40




60




0




50






Large crabgrass




100




20




60




100




100




100




100




100




100




100




100




100




100




100




100






P. morninglory




0




40




0




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




30




0




0




0




0




10




0




0




0




0




0




0




0




0




10






Sandbur




100









0




100




100




30




100









50




60




20




100




0




100




100






Sourgrass




50




30





























































Spanishneedles




70




10




0




0




0




20




0




0




0




0




0




40




10




0




0






Surinam grass




100









20




100




100




100




100




30




70




80




10




70




100




50




90






Tall Mallow




90




0




0




10




90




40




90




0




0




20




0




30




50




70




60









Rate 125 g/ha




4




18




24




28




30




34




46




78




93




94




103




105




107




108




109




113




114




115




117




119




131




138




146




147




151




170




242









Preemergence






Alexandergrass




80




30




10




60




50




30




65




75




85




50




40




98




100




98




100




98




98




75




90




98




100




80




98




85




98




85




98






Bermudagrass




30




100




98




100




98




100




100




98




100




90




80




100




100




100




100




100




100




100




100




100




100




100




90




98




100




100




98






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




30




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




10




0




0




0




85




0




10




0




0




10




0




0




30




30




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




35




75




0




0




100




100




0




100




85




10




75




100




100




100




75




0




100




45











Dallisgrass




98




100




98




85




60




98




100




100




98




98




65




100




100




100




100




100




100




98




95




90




100




100




100




98




100




85




98






Goosegrass




98




85




98




98




85




85




85




98




100




85




85




98




100




100




100




100




100




98




100




100




100




100




100




98




100




75




100






Green foxtail









85














85









40




100




100




90




100




100




100




100




100




100




100




100




100




100




100




100




100









100




100




100






Guineagrass




90




65




90




75




75




85




30




85




100




0




85




98




100




98




100




100




100




85




100




98




100




100




100




90




100




100




100






Itchgrass




0




0




40




40




75




0




0




0




75




0




0




20




98




40




75




60




20




50




75




60




90




80




90




65




85




30




80






Johnsongrass




0




0




0




0




0




20




40




0




75




0




0




20




90




40




98




90




0




60




90




75




90




65




80




85




50




75




85






Large crabgrass




100




100




100




100




98




100




98




100




100




98




95




100




100




100




100




100




100




100




98




100




100




100




100




100




100




100




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0




30




0




65




10




0




0




20




0




50




65




0




0




0




40




20






Purple nutsedge




0




0




0




0




0




0




0




0




0




50




0




0




65




10




40




30




20




0




0




0




60




65




70




30




30




0




40






Sandbur




30




0




20




0




40




30




0




0




65




20




0




0




98




98




100




100




85




40




0




98




100




65




100




0




100




40




90






Sourgrass




100









100




100









100




















































































100




100





















Spanishneedles




40




0




0




75




0




0




10




0




10




0




0




0




20




0




10




0




0




0




0




10




60




10




90




10




0




0




10






Surinam grass




90




20




10




65




40




0




0




30




90




80




0




40




100




98




98




100




75




75




100




85




100




85




100




85




100




75




90






Tall Mallow




0




0




0




0




0




0




10




0




30




0




0




45




90




10




85




30




10




0




65




0




80




40




80




0




75




30




0









Rate 64 g/ha




131




146




147




169




241




242




243




299




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




100




10




20




65




10




90




20




90




0




50




70




40




80




100




100




50






Bermudagrass




100




0




0




100




100




100




100




90




90




60




100




70




100




100




100




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




20




30




10




100




0




0




0




0




20




0









30






Com. groundsel




100




0




0




65




0




90




0




100









100




50









50




100




0




0






Dallisgrass




100









10




90




50




90




70




100




0




90




90




0




80




100




100




100






Goosegrass




100




0




0




100




100




100




100




90




90




90




100




100




100




100




100




100






Green foxtail




100














100




10




100




100




100




0




100




100




10




100




100




100




100






Guineagrass




100




10




0




0




100




80




0




20




0




80




0




0




20




60




20




100






Itchgrass




20




30




0




0




0




40




0




0




0




20




0




0




0




0




0




0






Johnsongrass




30




20




0




0




0




40




0




0




0




20




0




0




0




0




0




0






Large crabgrass




100




20




10




100




100




100




100




100




40




90




100




70




100




100




100




100






P. morninglory




0




30




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Sandbur




100




0




0




40




20




50




30




90




0




0




20




0




70




0




100




50






Sourgrass









50




0







































































Spanishneedles




0




10




0




0




0




0




50




0




0




0




0




0




0




10




0




0






Surinam grass




60














65




60




100




90




50




20




20




20




0




30




80




0




100






Tall Mallow




40




0




0




0




0




50




30




30




0




0




0




0




30




20




50




40









Rate 64 g/ha




4




18




24




28




30




34




46




78




93




103




105




107




108




109




112




113




115




117




119




130




131




132




138




139




146




147




151




170




242









Preemergence






Alexandergrass




80




0




10




0




40




20




40




30




30




0




85




100




85




98




0




98




50




90




75




98




98




98




80




60




95




75




98




30




100






Bermudagrass




0




85




95




100




98




98




98




90




90




60




98




100




100




100




85




100




98




98




100




100




100




100




100




98




95




95




90




100




85






C. purslane




0




0




0




0




0









0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




30




30




0




10




0




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




0




0




0




98




85




0




0




100




10




0




100




0




85




0




40




0




0




0




0




0











Dallisgrass




90




85




30




75




50




80




40




75




98




45




98




100




100




100




70




100




75




85




85




100




100




98




100




90




98




80




100




85




98






Goosegrass




95




85




50




85




70




75




75




85




98




65




98




100




98




100




85




100




90




85




98




100




100




98




98




98




100




98




100




75




95






Green foxtail









85














85









30




85




100




50




100




100




100




100




85




100




85




100




90




100




100




100




100




98




100









100




100




100






Guineagrass




50




30




75




65




40




80




30




65




100




0




98




100




98




100




40




100




30




100




85




100




100




85




100




65




100




85




100




98




98






Itchgrass




75




0




40




20




40




0




0




0




60




0




20




85




30




75




0




50




40




40




50




80




90




10




30




20




90




20




75




0




70






Johnsongrass




30




0




0




0




0




0




0




0




40




0




0




90




20




75




0




80




40




90




65




65




65




35




40




10




60




20




40




0




40






Large crabgrass




98




98




70




98




85




98




40




98




98




85




100




100




100




100




10




100




85




98




98




100




100




100




100




90




100




98




100




100




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




30




0




0




0




10




0




0




0




65




0




0




65




30




0




0




0




20




10






Purple nutsedge




0




0




0




0




0




0




0




0




20




0




0




20




0




40




0




20




0




0




0




0




40




0




30




0




65




0




0




0




0






Sandbur




65




0




20




0




0




0




0




0




65




0




0




65




30




98




0




75




0




0




65




100




85




0




65




40




100




0




90




40




0






Sourgrass




90









100




85









100






























































































100




98





















Spanishneedles




0




0




0




60




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




60




40




0




10




20




85




0




0




0




0






Surinam grass




65




0




10




0




40




0




0




20




85




0




0




100




65




85




0




98




65




80




50




80




85




30




40




20




60




75




85




30




85






Tall Mallow




0




0




0




0




0




0




0




0




0




0




0




0




0




60




0




0




0




40




0




85




80




40




40




20




50




0




0




30




0









Rate 32 g/ha




131




241




242




243




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




50




10




50




0




0




0




0




0




60




20




0




60






Bermudagrass




90




30




100




60




30




80




20




40




80




100




90




100






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




30




0




0




0




0




0




0









0




0






Com. groundsel




100




0




100




0




0




40














0




40




0











Dallisgrass




60




40




90




50




0




30




50




0




70




20




30




40






Goosegrass




100




100




100




80




30




80




90




20




90




100




20




100






Green foxtail




60




10




100




100




0




100




20




0




100




30




30




70






Guineagrass




20




0




100




0




0




0




0




0




0




0




0




100






Itchgrass




0




0




0




0




0




0




0




0




0




0




0




0






Johnsongrass




0




0




0




0




0




0




0




0




0




0




0




0






Large crabgrass




100




70




100




70




0




30




60




0




100




100




40




80






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0






Sandbur




0




40




30




20




0




0




0




0




90




0




20




90






Sourgrass


































































Spanishneedles




0




0




0




0




0




0




0




0




0




10




0











Surinam grass




40




0




30




20




0




20




0




0




0




20




0




0






Tall Mallow




30




0




0




20




0




0




0




0




0




10




30




0









Rate 32 g/ha




4




18




24




28




30




34




46




78




93




103




105




107




108




109




112




113




115




119




131




146




147




151




170




242









Preemergence






Alexandergrass




20




0




10




0




0




0




0




0




10




0




30




90




20




90




0




85




20




50




90




85




0




40




20




85






Bermudagrass




0




60




75




85




65




85




85




85




80




30




98




100




98




100




75




100




98




65




100




100




85




90




90




85






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




0




0




0




75




75




0




0




65




0




98




75




0




0




0




0











Dallisgrass




85




0




30




30




0




0




40




0




98




20




98




85




50




98




65




95




75




65




95




90




60




85




0




85






Goosegrass




85




0




50




0




40




0




20




10




98




30




98




98




85




98




40




100




85




85




98




98




65




85




65




85






Green foxtail









0



















0




75




75




0




85




100




100




100




0




98




70




75




100














100




75




100






Guineagrass




20




0




60




40




30




30




0




20




75




0




85




75




85




100




0




100




30




75




100




95




0




90




85




85






Itchgrass




0




0




40




0




20




0




0




0




60




0




0




75




20




65




0




40




40




10




50




90




0




0




0




65






Johnsongrass




0




0




0




0




0




0




0




0




0




0




0




85




20




0




0




60




40




0




40




60




0




0




0




40






Large crabgrass




100




0




70




85




40




85




20




40




98




0




98




98




100




100




10




100




75




90




100




100




98




98




85




100






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




0




20




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




40




0




0




0




0






Sandbur




0




0




20




0




0




0




0




0




0




0




0




30




0




0




0




65




0




0




60




85




0




20




0




0






Sourgrass




65









40




60









98





































































98




75





















Spanishneedles









0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




75




0




0




0




0






Surinam grass




0




0




10




0




40




0




0




0




0




0




0




75




65




30




0




90




20




0




75




60




0




30




0




85






Tall Mallow




0




0




0




0




0




0




0




0




0




0




0




0




0




20




0




0




0




0




30




40




0




0




30




0









Rate 16 g/ha




131




241




242




243




342




343




348




349




352




357




358




360









Postemergence






Alexandergrass




0




0




0




0




0




0




0




0




0




0




0




20






Bermudagrass




30




0




90




20




20




0




0




0




0




90




0




0






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




50




0









0




0




0









0




0




0






Com. groundsel




90









0




0









0




30



















0











Dallisgrass




20




0




60




0




0




0




0




0




0




0




0




0






Goosegrass




90




0




90




70




20




40




50




0




0




90




0




20






Green foxtail




0




0




30




10




0




0




0




0




0




10




0




0






Guineagrass




0




0




0




0




0




0




0




0




0




0




0




0






Itchgrass




0




0




0




0




0




0




0




0




0




0




0




0






Johnsongrass




0




80




0




0




0




0




0




0




0




0




0




0






Large crabgrass




90




0




0




0




0




0




20




0




0




100




0




0






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0






Sandbur




0




0




20




10




0




0




0




0




0




0




0




0






Sourgrass


































































Spanishneedles




0




0




0




0




0




0




0




0




0




10




0




0






Surinam grass




0




0




0




0




0




0




0




0




0




0




0




0






Tall Mallow




0




0




0




50




0




0




0




0




0




10




0




0









Rate 16 g/ha




4




18




30




46




78




93




103




105




107




108




109




112




113




115




119




131




146




147




151




170




242









Preemergence






Alexandergrass




20




0




0




0




0




0




0




0




0




20




40




0




65




0




0




20




65




0




40




20




65






Bermudagrass




0




40




50




65




75




80




30




85




85




85




98




60




98




75




50




100




65




0




90




80




80






C. purslane




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






C. ragweed




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




100






Com. groundsel









0




0




0




0




0




0




0




40




65




0




0




0




0




85




75




65




0




0




0











Dallisgrass




75




0




0




20




0




60




10




60




30




40




40




30




0




0




30




85




80




0




100




0




65






Goosegrass




70




0




30




0




10




65




0




85




85




60




85




40




90




20




30




75




90




0




85




50




75






Green foxtail









0




0




0




0




65




0




75




100




40




98




0




80




0




10




90














100




65




80






Guineagrass




20




0




30




0




20




65




0




40




65




0




90




0




85




0




65




0




90




0




85




0




70






Itchgrass




0




0




20




0




0




50




0




0




40




0




0




0




10




40




0




30




85




0




0




0




65






Johnsongrass




0




0




0




0




0




0




0




0




20




0




0




0




0




0




0




10




60




0




0




0




10






Large crabgrass




100




0




40




0




0




90




0




40




85




85




85




10




85




75




85




100




90




50




98




30




90






P. morninglory




0




0




0




0




0




0




0




0




0




0




0




0




10




0




0




0




0




0




0




20




0






Purple nutsedge




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




40




0




0




0




0






Sandbur




0




0




0




0




0




0




0




0




30




0




0




0




0




0




0




0




0




0




0




0




0






Sourgrass




50










































































90




0





















Spanishneedles




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0






Surinam grass




0




0









0




0




0




0




0




30




0




0




0




85




0




0




20




40




0




30




0




20






Tall Mallow




0




0




0




0




0




0




0




0




0




0




0




0




0




0




0




30




40




0




0




30




0














Test E




Compounds evaluated in this test were formulated in a non-phytotoxic solvent mixture which included a surfactant and applied to plants that were in the 1- to 4-leaf stage (postemergence application). A mixture of sandy loam soil and greenhouse potting mix in a 60:40 ratio was used for the postemergence test.




Plantings of these crops and weed species were adjusted to produce plants of appropriate size for the postemergence test. All plant species were grown using normal greenhouse practices. Crop and weed species include annual bluegrass (


Poa annua


), blackgrass (


Alopecurus myosuroides


), black nightshade (


Solanum nigra


), chickweed (


Stellaria media


), common poppy (


Papaver rhoeas


), deadnettle (


Lamium amplexicaule


), downy brome (


Bromus tectorum


), field violet (


Viola arvensis


), galium (


Galium aparine


), green foxtail (


Setaria viridis


), Italian ryegrass (


Lolium multiflorum


), jointed goatgrass (


Aegilops cylindrica


), kochia (


Kochia scoparia


), lambsquarters (


Chenopodium album


), littleseed canarygrass (


Phalaris minor


), rape (


Brassica napus


), redroot pigweed (


Amaranthus retroflexus


), Russian thistle (


Salsola kali


), scentless chamomile (


Matricaria inodora


), spring barley (


Hordeum vulgare


), sugar beet (


Beta vulgaris


), sunflower (


Helianthus annuus


), ivyleaf speedwell (


Veronica hederaefolia


), spring wheat (


Triticum aestivum


), winter wheat (


Triticum aestivum


), wild buckwheat (


Polygonum convolvulus


), wild mustard (


Sinapis arvensis


), wild oat (


Avena fatua


), windgrass (


Apera spica


-


venti


) and winter barley (


Hordeum vulgare


).




Treated plants and untreated controls were maintained in a greenhouse for approximately 21 to 28 days, after which all treated plants were compared to untreated controls and visually evaluated. Plant response ratings, summarized in Table E, are based upon a 0 to 100 scale where 0 is no effect and 100 is complete control. A dash response (-) means no test result.

















TABLE E













Rate 2000 g/ha




COMPOUND 177




Rate 2000 g/ha




COMPOUND 177











Postemergence





Preemergence







Annual bluegras









Annual bluegras












Barley (winter)









Barley (winter)




80







Blackgrass









Blackgrass




60







Blk nightshade









Blk nightshade












Chickweed









Chickweed












Common poppy









Common poppy












Deadnettle









Deadnettle












Downy brome









Downy brome












Field violet









Field violet












Galium









Galium












Green foxtail









Green foxtail




100







I. Ryegrass









I. Ryegrass




65







Jointed goatgra









Jointed goatgra












Kochia









Kochia












Lambsquarters









Lambsquarters












LS canarygrass









LS canarygrass












Rape









Rape












Redroot pigweed









Redroot pigweed












Russian thistle









Russian thistle












Scentless chamo









Scentless chamo












Spring Barley









Spring Barley












Spring Wheat









Spring Wheat












Sugar beet









Sugar beet












Sunflower









Sunflower












Veronica hedera









Wheat (winter)




70







Wheat (winter)




70




Wild buckwheat












Wild buckwheat









Wild mustard












Wild mustard









Wild oat




70







Wild oat









Windgrass












Windgrass






















COMPOUND








































Rate 1000 g/ha




4




30




40




46




67




75




86




88




94




103




115




123




157




161




162




163




165




167




169




172




173




174




176




177




202




204




207




208




212









Postemergence






Annual bluegras























































































































































Barley (winter)























































































































































Blackgrass























































































































































Blk nightshade























































































































































Chickweed























































































































































Common poppy























































































































































Deadnettle























































































































































Downy brome























































































































































Field violet























































































































































Galium























































































































































Green foxtail























































































































































I. Ryegrass























































































































































Jointed goatgra























































































































































Kochia























































































































































Lambsquarters























































































































































LS canarygrass























































































































































Rape























































































































































Redroot pigweed























































































































































Russian thistle























































































































































Scentless chamo























































































































































Spring Barley























































































































































Spring Wheat























































































































































Sugar beet























































































































































Sunflower























































































































































Veronica hedera























































































































































Wheat (winter)




0




0




0




70




40




70




60




10




0




10




40




65




40




50




50




70




85




50




65




50




60




50




40




65




60




30




50




60




75






Wild buckwheat























































































































































Wild mustard























































































































































Wild oat























































































































































Windgrass


































































































































































COMPOUND





































Rate 1000 g/ha




232




233




236




238




246




269




271




273




274




277




281




282




283




284




285




288




290




291




297




309




328




340




341




369









Postemergence






Annual bluegras






























































































































Barley (winter)






























































































































Blackgrass






























































































































Blk nightshade






























































































































Chickweed






























































































































Common poppy






























































































































Deadnettle






























































































































Downy brome






























































































































Field violet






























































































































Galium






























































































































Green foxtail






























































































































I. Ryegrass






























































































































Jointed goatgra






























































































































Kochia






























































































































Lambsquarters






























































































































LS canarygrass






























































































































Rape






























































































































Redroot pigweed






























































































































Russian thistle






























































































































Scentless chamo






























































































































Spring Barley






























































































































Spring Wheat






























































































































Sugar beet






























































































































Sunflower






























































































































Veronica bedera






























































































































Wheat (winter)




60




60




10




40




0




55




0




60




60




10




80




50




75




85




30




40




70




55




70




80




80




60




65




70






Wild buckwheat






























































































































Wild mustard






























































































































Wild oat






























































































































Windgrass








































































































































COMPOUND








































Rate 1000 g/ha




4




18




30




40




46




67




75




86




88




94




103




115




123




157




161




162




163




165




167




169




172




173




174




176




177




202




204




207




208









Preemergence






Annual bluegras























































































































































Barley (winter)




10




50




10




50




50




40




60




70




0




50




50




30




50




30




40




40




50




50




20




50




20




40




10




50




70




70




30




80




50






Blackgrass




100




85




30




70




70




40




85




65




50




60




70




60




65




50




55




55




50




100




80




55




80




98




55




75




60




30




95




85




85






Blk nightshade























































































































































Chickweed























































































































































Common poppy























































































































































Deadnettle























































































































































Downy brome























































































































































Field violet























































































































































Galium























































































































































Green foxtail




100




70




60




90




80




60




60




100




85




100




100




90




40




50




90




85




100




65




100




95




100




100




85




100




85




100




100




100




70






I. Ryegrass




85




70




50




70




70




50




50




60




50




60




70




80




50




50




85




70




60




70




80




90




80




98




40




98




60




60




65




30




95






Jointed goatgra























































































































































Kochia























































































































































Lambsquarters























































































































































LS canarygrass























































































































































Rape























































































































































Redroot pigweed























































































































































Russian thistle























































































































































Scentless chamo























































































































































Spring Barley























































































































































Spring Wheat























































































































































Sugar beet























































































































































Sunflower























































































































































Wheat (winter)




0




20




0




40




50




20




65




65




10




40




30




20




20




40




45




40




55




70




30




65




30




50




40




50




50




70




50




70




30






Wild buckwheat























































































































































Wild mustard























































































































































Wild oat




50




50




20




60




70




50




10




70




20




50




70




60




55




50




60




60




70




70




50




40




50




50




50




50




80




80




50




70




50






Windgrass


































































































































































COMPOUND






































Rate 1000 g/ha




212




232




233




236




238




246




269




271




273




274




277




281




282




283




284




285




288




290




291




297




309




328




340




341




369









Preemergence






Annual bluegras



































































































































Barley (winter)




50




55




60




50




30




60




60




60




80




55




50




80




70




80




60




20




10




70




20




60




70




70




50




80




60






Blackgrass




65




50




85




70




75




100




40




100




100




65




100




50




70




85




70




70









95




50




50




75




40




85




90




100






Blk nightshade



































































































































Chickweed



































































































































Common poppy



































































































































Deadnettle



































































































































Downy brome



































































































































Field violet



































































































































Galium






























































































































Green foxtail




100




100




100




100




100




100




100




100




60




40




100




100




100




100




100




65




100




85




100




60




100




100




100




85




100






I. Ryegrass




70




55




60




55




85




100




70




100




60




50




100




60




70




98




85




70




60




90




90




40




70




70




65




55




70






Jointed goatgra



































































































































Kochia



































































































































Lambsquarters



































































































































LS canarygrass



































































































































Rape



































































































































Redroot pigweed



































































































































Russian thistle



































































































































Scentless chamo



































































































































Spring Barley



































































































































Spring Wheat



































































































































Sugar beet



































































































































Sunflower



































































































































Wheat (winter)




60




50




60




20




50




50




50




75




60




50




50




80




70




80




80




50




55




50




60




70




70




70




60




85




70






Wild buckwheat



































































































































Wild mustard



































































































































Wild oat




70




60




60




50




50




85




70




60




80




60




70




80




80




70




70




40




50




70




60




70




70




60




60




80




75






Windgrass













































































































































COMPOUND








































Rate 500 g/ha




4




18




30




38




40




46




67




75




86




94




98




103




105




109




114




115




116




118




131




132




146




147




157




158




161




162




163




165




167









Postemergence






Annual bluegras





































































50




60









75









70









65














































Barley (winter)





































































10




20









10









20









20














































Blackgrass





































































70




65









80









75









40














































Blk nightshade





































































60




80









60









70









70














































Chickweed





































































10




10









50









50









30














































Common poppy





































































10




20









10









0









10














































Deadnettle





































































30




70









50









50









20














































Downy brome





































































0




30









60









70









5














































Field violet





































































40




15









0









0









10














































Galium





































































50




85









70









50









60














































Green foxtail





































































80




90









75









75









80














































I. Ryegrass





































































65




20









0









40









50














































Jointed goatgra





































































30




50









50









60









40














































Kochia





































































50




30









0









0









40














































Lambsquarters





































































30




40









0









0









50














































LS canarygrass





































































65




60









50









50









65














































Rape





































































60




55









30









0









60














































Redroot pigweed





































































15




20









0









0









50














































Russian thistle





































































0




0









0









0









0














































Scentless chamo





































































10




0









40









50









10














































Spring Barley





































































20




35









0









20









20














































Spring Wheat





































































10




30









10









40









20














































Sugar beet





































































30




50









0









0









40














































Sunflower





































































40




15









0









0









50














































Veronica hedera





































































70




70









70









20









70














































Wheat (winter)




0




65




0




10




0




70




30




75




70




0




55




0




20




0




20




20




10




70




20




80




20




80




30




30




35




40




50




65




40






Wild buckwheat





































































10




30









0









0









50














































Wild mustard





































































20




70









40









30









60














































Wild oat





































































10




0









70









70









10














































Windgrass





































































95




90









80









100









100
























































COMPOUND








































Rate 500 g/ha




169




172




173




174




176




177




191




192




202




207




208




211




212




218




219




232




233




236




241




242




243




246




267




269




271




273




274




276




277









Postemergence






Annual bluegras



































































































80



















































Barley (winter)



































































































20



















































Blackgrass



































































































50



















































Blk nightshade



































































































75



















































Chickweed



































































































50



















































Common poppy



































































































0



















































Deadnettle



































































































50



















































Downy brome



































































































40



















































Field violet



































































































40



















































Galium



































































































40



















































Green foxtail



































































































70



















































I. Ryegrass



































































































60



















































Jointed goatgra



































































































40



















































Kochia



































































































20



















































Lambsquarters



































































































0



















































LS canarygrass



































































































50



















































Rape



































































































50



















































Redroot pigweed



































































































40



















































Russian thistle



































































































0



















































Scentless chamo



































































































20



















































Spring Barley



































































































20



















































Spring Wheat



































































































20



















































Sugar beet



































































































30



















































Sunflower



































































































20



















































Veronica hedera























































































































































Wheat (winter)




50




40




40




40




50




70




60




50




55




30




50




40




70




85




60




50




55




0




50




90




80




0




70




40




0




50




50




20




0






Wild buckwheat



































































































0



















































Wild mustard



































































































5



















































Wild oat



































































































20



















































Windgrass



































































































95






























































COMPOUND







































Rate 500 g/ha




281




282




283




284




285




288




290




291




293




297




309




315




317




328




340




341




350




351




353




354




369




370




371




372




375




388









Postemergence






Annual bluegras








































































































































Barley (winter)








































































































































Blackgrass








































































































































Blk nightshade








































































































































Chickweed








































































































































Common poppy








































































































































Deadnettle








































































































































Downy brome








































































































































Field violet








































































































































Galium








































































































































Green foxtail








































































































































I. Ryegrass








































































































































Jointed goatgra








































































































































Kochia








































































































































Lambsquarters








































































































































LS canarygrass








































































































































Rape








































































































































Redroot pigweed








































































































































Russian thistle








































































































































Scentless chamo








































































































































Spring Barley








































































































































Spring Wheat








































































































































Sugar beet








































































































































Sunflower








































































































































Veronica hedera








































































































































Wheat (winter)




70




30




50




20




40




30




60




40




50




60




70




80




95




70




55




65




40




75




40




50




70




85




80




80




50




65






Wild buckwheat








































































































































Wild mustard








































































































































Wild oat








































































































































Windgrass


















































































































































COMPOUND








































Rate 500 g/ha




4




18




30




38




40




46




67




75




86




94




98




103




105




109




114




115




116




118




131




132




146




147




157




158




161




162




163




165




167









Preemergence






Annual bluegras





































































75




60









100









100









90














































Barley (winter)




10




30




10




0




40




40




40




20




80




50




30




40




10




5




40




20




80




50




100




60




95




45




10




30




40




30




40




55




40






Blackgrass




90




25









35




60




55




20




40




55




60




55




50




50




90




100




50




100




100




100




75




70




65




40




50




50




60




40




60




60






Blk nightshade





































































90




90









100









90









100














































Chickweed





































































100




100









100









100









70














































Common poppy








































































































100














































Deadnettle





































































30




20









80









100









50














































Downy brome





































































60




50









70









100









60














































Field violet





































































20




10









90









40









50














































Galium





































































100




70









100









100









95














































Green foxtail




100




50




60




100




90




85




55




60




55




90




65




70




100




85




85




70









65









100




100




65




40




50




70




65




100




55




85






I. Ryegrass




50




60




40




80




70




65




30




30




50




60




60




50




85




70




95




50




100




60




100




100




90




50




30




50




65




65




50




55




65






Jointed goatgra





































































70




50









65









95









50














































Kochia





































































100




30









70









100









75














































Lambsquarters





































































100




100









100









100









100














































LS canarygrass





































































50




80









100









100









85














































Rape





































































65




50









100









90









60














































Redroot pigweed





































































100




100









100









95









100














































Russian thistle





































































0




0









50









0









10














































Scentless chamo





































































30




10





























80














































Spring Barley





































































50




20









100









85









90














































Spring Wheat





































































50




20









100









100









100














































Sugar beet





































































70




50









95









90









80














































Sunflower





































































5




5









70









20









30














































Wheat (winter)




0




10




0




10




30




70




10




20




40




30




40




30




10




10




0




10




100




70




95




60




100




70




30









20




15









50




20






Wild buckwheat





































































90




80









95









100









100














































Wild mustard





































































80




90









65









100









100














































Wild oat




25




40




10




20




50




60




40









60




40




50




50




55




80




70




50




80




70




100




65




85




0




30




60




50




50




60




60




40






Windgrass





































































100




100









100









100









100
























































COMPOUND








































Rate 500 g/ha




169




172




173




174




176




177




191




192




201




202




207




208




211




212




218




219




232




233




236




241




242




243




246




267




269




271




273




274




276









Preemergence






Annual bluegras








































































































100














































Barley (winter)




30




40




40




0




40




60




20




30




20




40




70




40




10




40




65




70




20




50




40




60




85




70




50




70




50




50




65




60




50






Blackgrass




60




60




70




50




50




60




30




50




50




50




80




85




50




50




100




70




50




60




60




98




98




100




100




60




30




80




80




30




50






Blk nightshade








































































































95














































Chickweed























































































































































Common poppy























































































































































Deadnettle








































































































100














































Downy brome








































































































100














































Field violet








































































































100














































Galium








































































































100














































Green foxtail




70




85









50




70




60




50




65




65




85




90




60




20




65




85




70




90




100




100




90




100




100




100




100




70




100




30




30




98






I. Ryegrass




80




65




45




20




60




60




30




60




60




60




55




60




10




70




70




70




50




50




40




100




100




100




90




50




60




85




55




30




50






Jointed goatgra








































































































90














































Kochia








































































































60














































Lambsquarters








































































































100














































LS canarygrass








































































































100














































Rape








































































































85














































Redroot pigweed








































































































100














































Russian thistle








































































































50














































Scentless chamo























































































































































Spring Barley








































































































85














































Spring Wheat








































































































100














































Sugar beet








































































































65














































Sunflower








































































































60














































Wheat (winter)




40




20




30




50




30




70




50




40




40




40




70




30




30




30




50




60




30




50




10




60




95




75









70




40




50




60




50




50






Wild buckwheat








































































































100














































Wild mustard








































































































70














































Wild oat




30




40




45




40




50




80




50




55




40




60




70




60




40




70




70




60




50




60




30




55




100




90




65




70




70




65




70




50




60






Windgrass








































































































100

























































COMPOUND








































Rate 500 g/ha




277




281




282




283




284




285




288




290




291




293




297




309




315




317




328




340




341




350




351




353




354




369




370




371




372




375




388









Preemergence






Annual bluegras













































































































































Barley (winter)




65




70




50




75




30




10




5




60




30




50




55




20




80




70




50




40




60




25




80




30




40




50




70




70




70




30




70






Blackgrass




70









60




60









55




50




70




40




50




20




60




85




60




50




60




60




60




100




55




30




70




100




100




100




65




40






Blk nightshade













































































































































Chickweed













































































































































Common poppy













































































































































Deadnettle













































































































































Downy brome













































































































































Field violet













































































































































Galium













































































































































Green foxtail




100




100




100




100




100




60




60




70




85




60




60




100




100




100




85




60




55




85




85




100




100




85




100




85




100




70




85






I. Ryegrass




95




60




70




90




70




70




50




70




100




50




50




60




85




95




60




60




55




85




60




90




90




65




90




90




85




65




60






Jointed goatgra













































































































































Kochia













































































































































Lambsquarters













































































































































LS canarygrass













































































































































Rape













































































































































Redroot pigweed













































































































































Russian thistle













































































































































Scentless chamo













































































































































Spring Barley













































































































































Spring Wheat













































































































































Sugar beet













































































































































Sunflower













































































































































Wheat (winter)




10




65




60




65




70




25




30




30




50




55




60




65




85




60




70




50




50




50




70




60




60




55




60




65




70




50




60






Wild buckwheat













































































































































Wild mustard













































































































































Wild oat




65




65




70




50




60




20




30




70




50




50




60




50




70




70




50




50




70




65




80




85




40




70




90




90




80




70




30






Windgrass























































































































































COMPOUND








































Rate 250 g/ha




4




18




30




38




40




46




67




75




86




88




93




94




98




103




105




107




108




109




110




111




112




113




114




115




116




117




118




119




123









Postemergence






Annual bluegras






















































50
























50




50




10
























30









70


























Barley (winter)






















































0
























10




15




20
























10









10


























Blackgrass






















































40
























85




10




10
























20









80


























Blk nightshade






















































50
























60




50




40
























40









50


























Chickweed






















































0
























0




0




0
























0









20


























Common poppy






















































0
























5




0




10
























10









0


























Deadnettle






















































0
























50




30




30
























10









20


























Downy brortie






















































0
























0




0




0
























0









30


























Field violet






















































0
























0




20




20
























0









0


























Galium






















































0
























30




50




30
























50









40


























Green foxtail






















































0
























85




75




65
























50









75


























I. Ryegrass






















































0
























30




40




10
























20









70


























Jointed goatgra






















































0
























10




10




5
























5









40


























Kochia






















































0
























15




30




30
























30









0


























Lambsquarters






















































0
























5




20




30
























30









0


























LS canarygrass






















































0
























60




70




50
























30









40


























Rape






















































0
























50




50




50
























50









0


























Redroot pigweed






















































0
























20




30




15
























10









0


























Russian thistle






















































0
























0




0




0
























0









0


























Scentless chamo






















































0
























10




10




0
























0









0


























Spring Barley






















































0
























30




25




20
























30









10


























Spring Wheat






















































0
























10




20




20
























20









10


























Sugar beet






















































0
























40




20




35
























55









0


























Sunflower






















































0
























30




35




30
























10









0


























Veronica hedera






















































0
























10




40




50
























50









0


























Wheat (winter)




0




55




0




10




0




60




20




60




55




0




0




0




50




0




10




0




40




75




0




0




10




70




60




10




45




25




65




20




55






Wild buckwheat






















































0
























10




10




20
























30









0


























Wild mustard






















































10
























40




80




50
























50









40


























Wild oat






















































0
























0




20




0
























0









30


























Windgrass






















































80
























90




100




90
























85









75




































COMPOUND








































Rate 250 g/ha




131




132




137




138




146




147




148




157




158




161




162




163




165




167




169




170




172




173




174




176




191




199




201




202




204




207




208




211




212









Postemergence






Annual bluegras




40














10




10






























































































































Barley (winter)




0














0




10






























































































































Blackgrass




60














0




15






























































































































Blk nightshade




60














60




40






























































































































Chickweed




20














0




0






























































































































Common poppy




0














40




0






























































































































Deadnettle




30














50



































































































































Downy brome




50














2




0






























































































































Field violet




0














30




0






























































































































Galium




0














50




15






























































































































Green foxtail




50














70




70






























































































































I. Ryegrass




30














0




10






























































































































Jointed goatgra




0














0




10






























































































































Kochia




0














0




10






























































































































Lambsauarters




0














30




10






























































































































LS canarygrass




20














10




30






























































































































Rape




0














0




50






























































































































Redroot pigweed




0














10




10






























































































































Russian thistle




0














0




0






























































































































Scentless chamo




20














0




10






























































































































Spring Barley




0














5




10






























































































































Spring Wheat




0














0




10






























































































































Sugar beet




0














10




30






























































































































Sunflower




0














0




40






























































































































Veronica hedera




0



















40






























































































































Wheat (winter)




0




50




20




80




60




80




80




20




40




30




30




40




40




30




40












































































Wild buckwheat




0














0




10






























































































































Wild mustard




0














0




40






























































































































Wild oat




20














0




0






























































































































Windgrass




90














95




95








































































































































COMPOUND








































Rate 250 g/ha




218




219




225




232




233




236




238




241




242




243




246




267




269




271




273




274




276




277




281




282




283




284




285




287




288




290




291




293




295









Postemergence






Annual bluegras












































10










































































































Barley (winter)












































10










































































































Blackgrass












































10










































































































Blk nightshade












































50










































































































Chickweed












































0










































































































Common poppy












































20










































































































Deadnettle












































10










































































































Downy brome












































30










































































































Field violet












































0










































































































Galium












































30










































































































Green foxtail












































60










































































































I. Ryegrass












































70










































































































Jointed goatgra












































0










































































































Kochia












































0










































































































Lambsquarters












































0










































































































LS canarygrass












































15










































































































Rape












































0










































































































Redroot pigweed












































0










































































































Russian thistle












































0










































































































Scentless chamo












































0










































































































Spring Barley












































20










































































































Spring Wheat












































10










































































































Sugar beet












































40










































































































Sunflower












































0










































































































Veronica hedera























































































































































Wheat (winter)




70




50




70




40




50




0




60




60




10




75




0




70




50




10




30




30




10




0




55




20




60




60




20




50




35




50




30




30




50






Wild buckwheat












































10










































































































Wild mustard












































20










































































































Wild oat












































20










































































































Windgrass












































95





















































































































COMPOUND



































Rate 250 g/ha




297




299




309




310




314




315




317




328




340




341




350




351




353




354




367




369




370




371




372




375




387




388









Postemergence






Annual bluegras




















































































































Barley (winter)




















































































































Blackgrass




















































































































Blk nightshade




















































































































Chickweed




















































































































Common poppy




















































































































Deadnettle




















































































































Downy brome




















































































































Field violet




















































































































Galium




















































































































Green foxtail




















































































































I. Ryegrass




















































































































Jointed goatgra




















































































































Kochia




















































































































Lambsquarters




















































































































LS canarygrass




















































































































Rape




















































































































Redroot pigweed




















































































































Russian thistle




















































































































Scentless chamo




















































































































Spring Barley




















































































































Spring Wheat




















































































































Sugar beet




















































































































Sunflower




















































































































Veronica hedera




















































































































Wheat (winter)




50




70




50




80




70




80




95




65




30




70




30




70




30




40




40




60




80




65




70




35




30




30






Wild buckwheat




















































































































Wild mustard




















































































































Wild oat




















































































































Windgrass






























































































































COMPOUND








































Rate 250 g/ha




4




18




30




38




40




46




67




75




86




88




93




94




98




103




105




107




108




109




110




111




112




113




114




115




116




117




118




119




123









Preemergence






Annual bluegras






















































65
























85




60




90
























50









85


























Barley (winter)




10




20




10




0




30




30




20




10




70




0




50




40




10




30




0




15




10




20




5




0




10




85




10




10




70




30




65




10




30






Blackgrass




50




10




30




45




40




40




10




20




60




50




75




60




20




30




50




80




90




65




60




0




50




85




50




30




45




60




80




50




30






Blk nightshade






















































80
























95




90




90
























60









90


























Chickweed






















































100



















85




50




30





























50









100


























Cornmon poppy























































































































































Deadnettle






















































85
























85




40




30
























20









80


























Downy brome






















































20
























75




70




80
























60









50


























Field violet






















































30
























20




20




15
























0









40


























Galium






















































100
























100




95




100
























60









100


























Green foxtail




55




30




30




90




70




60




30




60




40




60









80




60




70




90




95




90




100




85




10




50




85




100




65




100




80




55




60




20






I. Ryegrass




20




40




20




20




30




50




40




20




30




10




100




40




50




50




30




95




95




100




20




0




20




100




100




45




60




85




60




60




40






Jointed goatgra






















































60
























50




60




65
























65









100


























Kochia






















































20
























80




40




50
























30









85


























Lambsquarters






















































100
























100




90




100
























100









100


























LS canarygrass






















































60
























80




70




60
























60









80


























Rape






















































10
























100




50




55
























20









100


























Redroot pigweed






















































90
























100




90




100
























65









100


























Russian thistle






















































0
























10




15




0
























0









0


























Scentless chamo















































































90




80




30
























30




































Spring Barley






















































60
























70




5




20
























0









75


























Spring Wheat






















































80
























85




30




40
























10









80


























Sugar beet






















































5
























100




60




60
























40









85


























Sunflower






















































20
























40




10




10
























0









40


























Wheat (winter)




0




0




0




0




20




40




10




10




60




0




100




30




40




20




0




40




10




55




0




0




0




60




0




5




30




90




50




30




10






Wild buckwheat






















































40
























95




80




85
























50









60


























Wild mustard






















































80
























100




65




85
























40









85


























Wild oat




20




20




10




20




40




55




30




0




70




10




60




40




46




40




50




80




75




50




10




0




0




60




70




40




95




60




70




30




50






Windgrass






















































100
























100




100




100
























100









100




































COMPOUND








































Rate 250 g/ha




131




132




137




138




146




147




148




157




158




161




162




163




165




167




169




170




172




173




174




176




191




199




201




202




204




207




208




211




212









Preemergence






Annual bluegras




80














70




80






























































































































Barley (winter)




100




50




20




90




10




20




10




0




30




30




30




30




20




40




30




70




40




30




0




30




30




70




0




20




50




65




30




20




20






Blackgrass




60




60




30




70




90




55




50




20




50




30




55




30




40




50




30




85




50




50




30




40




20




60




30




30




55




30




40




0




20






Blk nightshade




85














95




10






























































































































Chickweed




100



















80






























































































































Common poppy
























100






























































































































Deadnettle




60














70




40






























































































































Downy brome




80














90




0






























































































































Field violet




20














70




30






























































































































Galium




50














70




50






























































































































Green foxtail




100




98




50




75




65




65




55




30




20




60




60




100




50




60




60




100




60




85




30




50




40




100




50




70




75




80




40




10




55






I. Ryegrass




100




100




50




80




60




55




30




20




50




60




50




30




60




30




75




70




30




35




0




50




0




70




50




30




50




40




50




0




60






Jointed goatgra




70














80




50






























































































































Kochia




10














40




50






























































































































Lambsquarters




100














100




100






























































































































LS canarygrass




70














85




75






























































































































Rape




75














95




80






























































































































Redroot pigweed




100














90




100






























































































































Russian thistle




0














20




0






























































































































Scentless chamo
























100






























































































































Spring Barley




70














90




10






























































































































Spring Wheat




100














100




80






























































































































Sugar beet




60














50




60






























































































































Sunflower




20














60




30






























































































































Wheat (winter)




60




40




30




80




0




30




0




20




30




10




30




30




40




10




10




70




10




20




60




20




30




50




40




50




30




60




30




35




10






Wild buckwheat




70














100




85






























































































































Wild mustard




100














55




95






























































































































Wild oat




60




50




10




65




50




0




40




50




50




50




50




50




55




30




50




70




30




50




50




30




40




80




50




50




50




65




50









60






Windgrass




100














100




100








































































































































COMPOUND








































Rate 250 g/ha




218




219




225




232




233




236




238




241




242




243




246




267




269




271




273




274




276




277




281




282




283




284




286




287




288




290




291




293




295









Preemergence






Annual bluegras












































100





































































































Barley (winter)




50




30




60




20




30




20




40




50




60




60




40




30




30




45




70




50




30




50




70




50




60




50




5




35




0




55




10




40




30






Blackgrass




70




20




80




30




50




60




50




100




100




85




60




50




40




100




55




0




50




100




50




60




50




65




10




60




50




60




30









10






Blk nightshade












































95










































































































Chickweed























































































































































Cornmon poppy























































































































































Deadnettle












































70










































































































Downy brome












































100










































































































Field violet












































65










































































































Galium












































100










































































































Green foxtail




55




60




60




95




100




85




70




90




98




100




100




100




60




100




20




20




100




100




100




80




100




100




55




90




50




65




55




70




100






I. Ryegrass




60




55




90




40




40




20




50




70




98




85




80




50




50




100




30




20




60




75




60




70




70




85




40




60




30




60




70




50




50






Jointed goatgra












































80










































































































Kochia












































50










































































































Lambsquarters












































100










































































































LS canarygrass












































100










































































































Rape












































60










































































































Redroot pigweed












































100










































































































Russian thistle












































30










































































































Scentless chamo























































































































































Spring Barley












































70










































































































Spring Wheat












































60










































































































Sugar beet












































50










































































































Sunflower












































70










































































































Wheat (winter)




40




60




70




30




50




0




40




50




55




70




50




55




60




60




50




30




30




20




60




60




50




70




40




50




40




10




35




50




60






Wild buckwheat












































70










































































































Wild mustard












































65










































































































Wild oat




65




50




60




55




55




20




50




60




98




55




50




55




70




60




80




40




60




60




70




70




65




70




10




60




20




60




20




10




10






Windgrass












































100





















































































































COMPOUND



































Rate 250 g/ha




297




299




309




310




314




315




317




328




340




341




350




351




353




354




367




369




370




371




372




375




387




388









Preemergence






Annual bluegras




















































































































Barley (winter)




50




50




50




70




60




70




50




40




50




70




10




70




20




30




30




70




60




60




70









15




20






Blackgrass




40




100




60




85




50




60




100




50




50




40




30




85




50




55




30




85




70




100




60




60




20




0






Blk nightshade




















































































































Chickweed




















































































































Common poppy




















































































































Deadnettle




















































































































Downy brome




















































































































Field violet




















































































































Galium




















































































































Green foxtail




60




100




65




100




85




100




100




100




30




25




55




90




100




80




50




50




100




60




60




60




20




40






I. Ryegrass




60




85




50




70




55




70




85




65




55




50




90




60




90




60




60




50




85




70




70




70




10




40






Jointed goatgra




















































































































Kochia




















































































































Lambsquarters




















































































































LS canarygrass




















































































































Rape




















































































































Redroot pigweed




















































































































Russian thistle




















































































































Scentless chamo




















































































































Spring Barley




















































































































Spring Wheat




















































































































Sugar beet




















































































































Sunflower




















































































































Wheat (winter)




30




65




70




70




70




70




50




40




40




40




40




60




40




50




40




60




40




60




50




40




55




50






Wild buckwheat




















































































































Wild mustard




















































































































Wild oat




70




70




50




70




70




60




60




70




50




60




60




70




55




30




50




65




75




85




60




60




0




20






Windgrass






























































































































COMPOUND








































Rate 125 g/ha




4




38




93




98




105




107




108




109




110




111




112




113




114




116




117




119




131




132




137




138




146




147




148




151




158




170




191




192




199









Postemergence






Annual bluegras














20














5




15




10
























0




50














40














0




10














































Barley (winter)














0














5




10




40
























5




10














0














0




10














































Blackgrass














30














80




5




30
























0




40














20














20




25














































Blk nightshade














0














30




30




40
























50




50














50














20




50














































Chickweed














0














0




0




0
























10




0














10














0




0














































Comnion poppy














0














0




0




30
























0




0














0














20




10














































Deadnettle














0














5




20




0
























20




0














30














0




10














































Downy brome














0














10




0




0
























0




0














0














0




10














































Field violet














0














25




0




10
























0




0














0














10




0














































Galium














0














30




10




50
























10




40














10














20




0














































Green foxtail














0














30




15




30
























20




70














70














15




20














































I. Ryegrass














0














50




5




10
























10




50














0














0




10














































Jointed goatgra














0














10




10




10
























15




20














0














0




15














































Kochia














0














20




40




30
























20




0














0














15




10














































Lambsquarters














0














15




20




20
























30




30














0














10




20














































LS canarygrass














0














20




20




25
























0




30














0














10




30














































Rape














0














30




40




50
























55




0














0














10




40














































Redroot pigweed














0














10




20




20
























15




0














0














20




20














































Russian thistle














0














0




0




0
























0




0














0














0




0














































Scentless chamo














0














0




0




0
























0




0














0














20




10














































Spring Barley














0














0




20




30
























20




0














0














0




10














































Spring Wheat














0














5




10




30
























10




0














0














0




10














































Sugar beet














0














10




10




30
























50




0














0














30




20














































Sunflower














0














20




30




30
























10




0














0














0




40














































Veronica hedera














0














0




10




20
























10




0














0



















60














































Wheat (winter)




0




10




65




30




10




30




20




55




0




0




0




30




10




10




10




10




60




20




10




70




40




70




10




70




15




75




30




30




55






Wild buckwheat














0














0




20




10
























20




0














0














0




0














































Wild mustard














0














90




10




40
























75




20














0














0




50














































Wild oat














0














5




5




0
























0




0














0














0




5














































Windgrass














70














90




90




90
























85




70














60














90




90
























































COMPOUND








































Rate 125 g/ha




211




218




219




225




241




242




243




245




271




276




277




285




287




293




295




299




310




314




315




317




350




351




353




354




367




370




371




372




375









Postemergence






Annual bluegras





























20

























































































































Barley (winter)





























0

























































































































Blackgrass





























0

























































































































Blk nightshade





























30

























































































































Chickweed





























30

























































































































Common poppy





























40

























































































































Deadnettle





























10

























































































































Downy brome





























30

























































































































Field violet





























60

























































































































Galium





























20

























































































































Green foxtail





























30

























































































































I. Ryegrass





























0

























































































































Jointed goatgra





























0

























































































































Kochia





























60

























































































































Lambsquarters





























0

























































































































LS canarygrass





























10

























































































































Rape





























10

























































































































Redroot pigweed





























0

























































































































Russian thistle





























0

























































































































Scentless chamo





























40

























































































































Spring Barley





























20

























































































































Spring Wheat





























20

























































































































Sugar beet





























50

























































































































Sunflower





























10

























































































































Veronica hedera























































































































































Wheat (winter)




20




65




20




75




20




10




70




0




10




10




0




20




40




50




30




60




80




65




70




70




50




60




20




30




50




70




70




65




35






Wild buckwheat





























10

























































































































Wild mustard





























20

























































































































Wild oat





























0

























































































































Windgrass





























95




































































































































COMPOUND















Rate 125 g/ha




387




388









Postemergence






Annual bluegras
















Barley (winter)
















Blackgrass
















Blk nightshade
















Chickweed
















Common poppy
















Deadnettle
















Downy brome
















Field violet
















Galium
















Green foxtail
















I. Ryegrass
















Jointed goatgra
















Kochia
















Lambsquarters
















LS canarygrass
















Rape
















Redroot pigweed
















Russian thistle
















Scentless chamo
















Spring Barley
















Spring Wheat
















Sugar beet
















Sunflower
















Veronica hedera
















Wheat (winter)




20




30






Wild buckwheat
















Wild mustard
















Wild oat
















Windgrass





















































Rate 125 g/ha




4




38




93




98




105




107




108




109




110




111




112




113




114




116




117




119




131




132




137




138




146




147




148




151




158




170




191




192




199









Preemergence






Annual bluegras














50














80




60




40
























50




60














70



















60














































Barley (winter)




10




0




50




20




0




20




20




10




0




0




10




10




5




30




20




10




65




10




20




60




10




10




10




20




20




60




10




20




70






Blackgrass




30




25




70




30




20




85




75




65




50




0




20




30




50




50




50




10




50




20




20




60




85




20




50




75




20




60




10




40




65






Blk nightshade














65














95




85




75
























20




80














70














85




85














































Chickweed














20














50




40




40
























15




100














100



















30














































Common poppy








































































































100














































Deadnettle














10














60




10




20
























20




95














30














65




40














































Downy brome














60














60




30




0
























10




60














85














90




60














































Field violet














10














30




0




50
























0




50














20














50




10














































Galium














15














70




50




100
























100




100














60














50




40














































Green foxtail




50




80




80




60




55




100









85




60




0




20




70




100




50




60




50




100




60




15




70




50




55




30




80




10




100




30




50




100






I. Ryegrass




20




0




70




50




30




98




45




100




0




0




0




50




30




30




45




35




100




20




20




70




50




20




20




50




20




70




0




20




60






Jointed goatgra














70














50




40




20
























20




30














50














65




45














































Kochia














0














60




50




0
























25




0














0














20




0














































Lambsquarters














100














100




100




60
























50




100














100














100




100














































LS canarygrass














80














80




50




50
























50




70














70














70




40














































Rape














0














70




60




10
























0




60














70














30




60














































Redroot pigweed














100














100




90




70
























50




100














100














90




70














































Russian thistle














0














0




0




0
























0




0














10














10




0














































Scentless chamo





























80




60




0
























30







































15














































Spring Barley














10














70




10




5
























0




40














20














60




20














































Spring Wheat














50














75




20




20
























0




15














70














55




50














































Sugar beet














10














100




40




0
























20




50














80














0




60














































Sunflower














5














30




0




0
























0




15














20














55




20














































Wheat (winter)




0




10




40




30




10




30




10




30




0




0




0




50




10




55




60




20




35




30




20




70




10




20




0




10




10




70




10




10




70






Wild buckwheat














30














90




100




20
























20




40














30














50




70














































Wild mustard














65














85




90




30
























50




75














60














40




60














































Wild oat




10




0




60




50




30




60




30




30




0




0




0




30




40




30




20




10




50




35




20




60




30




0




15




20




50




70




30




30




70






Windgrass














100














100




100




100
























100




100














100














100




100
























































COMPOUND








































Rate 125 g/ha




211




218




219




225




241




242




243




245




271




276




277




285




287




293




295




299




310




314




315




317




350




351




353




354




367




370




371




372




375









Preemergence






Annual bluegras





























100

























































































































Barley (winter)




10




40




20




50




40




40




30




70




35




50




30




0




30




40




20




40




60




50




55




40




5




70




10




20




20




60




40




60




35






Blackgrass




0




65




0




60




60




95




65




50




30




30




60




20




50




40




0




60




85




40




50




50




50




35




10




50




60




50




85




70




20






Blk nightshade





























70

























































































































Chickweed























































































































































Common poppy























































































































































Deadnettle























































































































































Downy brome





























70

























































































































Field violet





























50

























































































































Galium





























0

























































































































Green foxtail




0




30




65




50




65




70




75




100




70




60




95




20




60




55




50




100




100




60




90




100




65




40




70




85




70




70




35




60




50






I. Ryegrass









55




30




50




60




95




70




60




60




30




65




20




55




30




40




70




70




50




55




60




60




55




40




50




60




55




60




60




50






Jointed goatgra





























65

























































































































Kochia





























35

























































































































Lambsquarters





























100

























































































































LS canarygrass





























100

























































































































Rape





























50

























































































































Redroot pigweed





























90

























































































































Russian thistle





























20

























































































































Scentless chamo























































































































































Spring Barley





























60

























































































































Spring Wheat





























55

























































































































Sugar beet





























30

























































































































Sunflower





























55

























































































































Wheat (winter)




50




50




35




65




40




65




50




50




30




20




30




30




45




40




40




50




40




65




55




50




40




50




20




30




60




50




60




60




30






Wild buckwheat





























60

























































































































Wild mustard





























65

























































































































Wild oat




20




70




30




50




50




60




60




30




50




50




50




10




70




0




0




65




50




70




65




60




40




70




30




0




55




60




70




50




55






Windgrass





























100




































































































































COMPOUND















Rate 125 g/ha




387




388









Preemergence






Annual bluegras
















Barley (winter)




20




10






Blackgrass




0




0






Blk nightshade
















Chickweed
















Common poppy
















Deadnettle
















Downy brome
















Field violet
















Galium
















Green foxtail




10




30






I. Ryegrass




0




30






Jointed goatgra
















Kochia
















Lambsquarters
















LS canarygrass
















Rape
















Redroot pigweed
















Russian thistle
















Scentless chamo
















Spring Barley
















Spring Wheat
















Sugar beet
















Sunflower
















Wheat (winter)




50




50






Wild buckwheat
















Wild mustard
















Wild oat




0




20






Windgrass



























COMPOUND







































Rate 62 g/ha




91




93




107




108




109




110




111




112




113




114




116




117




119




131




138




146




148




151




158




170




199




225




242




245




287




310









Postemergence






Annual bluegras









20




20




0


































100














55









85


































95





















Barley (winter)









0




5




10


































0














5









5


































20





















Blackgrass









10




5




5


































0














85









70


































60





















Blk nightshade









0




10




20


































10














50









50


































60





















Chickweed









0




10




10


































0














60









30


































0





















Common poppy









0




0




10


































30














65









60


































55





















Deadnettle









0




0




10


































0














30









50


































100





















Downy brome









0




0




0


































0














55









55


































30





















Field violet









0




0




0


































60














60









50


































30





















Galium









0




5




0


































30














50









50


































0





















Green foxtail









0




20




10


































20














55









70


































60





















I. Ryegrass









0




0




20


































0














50









50


































50





















Jointed goatgra









0




0




10


































30














30









55


































55





















Kochia









0




5




20


































0














45









30


































20





















Lambsquarters









0




15




10


































20














0









50


































10





















LS canarygrass









0




15




0


































10














50









30


































65





















Rape









0




20




60


































10














10









60


































20





















Redroot pigweed









0




20




5


































0














5









30


































0





















Russian thistle









0




0




0


































40














10









20


































50





















Scentless chamo









0




10




10


































50














55









20


































55





















Spring Barley









0




20




10


































5














5









20


































5





















Spring Wheat









0




0




10


































5














5









10


































15





















Sugar beet









0




10




5


































0














0









0


































50





















Sunflower









0




10




20


































20














10









0


































10





















Veronica hedera









0




10




0




















































































































Wheat (winter)




10




20




40




0




0




0




0




0




15




0




20




0




10




50




60




20




0




10




10




80




50




60




65




10




30




75






Wild buckwheat









0




0




0


































0














50









20


































50





















Wild mustard









0




5




5


































70














30









60


































0





















Wild oat









0




5




0


































20














40









20



















































Windgrass









60




85




80


































70














85









85


































90
































COMPOUND







































Rate 62 g/ha




91




93




107




108




109




110




111




112




113




114




116




117




119




131




138




146




148




151




158




170




199




225




242




245




287




310









Preemergence






Annual bluegras









10




70




20




















































































































Barley (winter)




40




50




20




10




10




0




0




0




10




0




10




25




5




40




30




10




10




10




10




60




70




50




30




50




20




50






Blackgrass




60




50




60




40




30




20




0




10




60




30




40




50




20




60




50




70




20




45




10




60




60




50




70




60




30




85






Blk nightshade









60




70




50




















































































































Chickweed









60




80




30




















































































































Common poppy








































































































































Deadnettle









10




50




10




















































































































Downy brome









40




50




30




















































































































Field violet









0




70




15




















































































































Galium









10




50




95




















































































































Green foxtail




80




70




80




65




50




30




0




10




55




45




65




50




10




60




60




55




20




30




0




100




100




60









100




60




100






I. Ryegrass




40




50




55




20




20




0




0




0




50




20




50




50




10




70




60




40




20




30




10




60




70




30




70




40




50




70






Jointed goatgra









15




40




30




















































































































Kochia









0




50




50




















































































































Lambsquarters









100




100




80




















































































































LS canarygrass









40




50




60




















































































































Rape









0




60




40




















































































































Redroot pigweed









100




100




70




















































































































Russian thistle









0




0




0




















































































































Scentless chamo














70




50




















































































































Spring Barley









5




30




10




















































































































Spring Wheat









30




60




10




















































































































Sugar beet









0




70




60




















































































































Sunflower









10




20




0




















































































































Wheat (winter)




40




40




50




0




20




0




0




0




40




0




30




30




0




50




60




0




0




0




0




70




60




30




40




20




30




60






Wild buckwheat









30




60




60




















































































































Wild mustard









30




100




50




















































































































Wild oat




60




50




50




15




20




0




0




0




20




20




20




20




20




50




50




25




10




10




50




65




60




40




60




40




30




70






Windgrass









100




100




100

































































































































COMPOUND





COMPOUND
































Rate 31 g/ha




91




93




107




146




151




225




242




245




287




Rate 31 g/ha




91




93




107




146




151




225




242




245




287









Postemergence













Preemergence






Annual bluegras

















































Annual bluegras



















































Barley (winter)

















































Barley (winter)




20




20




10




20




10




0




30




40




30






Blackgrass

















































Blackgrass




20




0




30




20




30




30




55




60




30






Blk nightshade

















































Blk nightshade



















































Chickweed

















































Chickweed



















































Common poppy

















































Common poppy



















































Deadnettle

















































Deadnettle



















































Downy brome

















































Downy brome



















































Field violet

















































Field violet



















































Galium

















































Galium



















































Green foxtail

















































Green foxtail




60




30




55




50




20




30




50




60




30






I. Ryegrass

















































I. Ryegrass




40




30




40




50




20




20




65




20




20






Jointed goatgra

















































Jointed goatgra



















































Kochia

















































Kochia



















































Lambsquarters

















































Lambsquarters



















































LS canarygrass

















































LS canarygrass



















































Rape

















































Rape



















































Redroot pigweed

















































Redroot pigweed



















































Russian thistle

















































Russian thistle



















































Scentless chamo

















































Scentless chamo



















































Spring Barley

















































Spring Barley



















































Spring Wheat

















































Spring Wheat



















































Sugar beet

















































Sugar beet



















































Sunflower

















































Sunflower



















































Veronica hedera

















































Wheat (winter)




10




20




0




20




0




10




30




20




40






Wheat (winter)




0




0




50




30




10




50




55




0




30




Wild buckwheat



















































Wild buckwheat

















































Wild mustard



















































Wild mustard

















































Wild oat




40




40




20




40




10




30




50




30




0






Wild oat

















































Windgrass



















































Windgrass



























































Test F Protocol






Abutilon theophrasti


(ABUTH),


Chenopodium album


(CHEAL),


Amaranthus rudis


(AMATA),


Setaria faberii


(SETFA),


Panicum dichotomiflorum


(PANDI), and


Digitaria sanguinalis


(DIGSA) were grown from seed in pots of an artificial potting mixture in a greenhouse. Compounds of the present invention were applied at 70 and 105 g ai/ha preemergence. Rimsulfuron was applied at 8.8 and 17.5 g ai/ha. Mixtures of the compounds of the present invention and rimsulfuron were also applied.




Following application, the plants were maintained by watering as needed. A fertilizer solution of Peter's 20-20-20 (10 pounds/5 gallons of water) plus Sprint 330, a Iron Chelate micronutrient, (113.5 grams/5 gallons of water) was injected into the water with an Anderson fertilizer injection system to provide approximately 219 ppm of nitrogen with each watering. Artificial lighting was used to supplement natural light to produce a 14 hour photoperiod and: an additional one hour light period was used between 1:00 am to 2:00 am for a night interruption. Greenhouse temperatures were targeted for 27° C. in the day and 21° C. at night. At 21 days after treatment, all plants were evaluated for injury as compared to control plants that were sprayed only with non-phytotoxic solvent. Mean plant response ratings, summarized in Table F, are based upon a 0 to 100 scale where 0 is no effect and 100 is complete control.




Colby's equation was used to calculate the expected additive herbicidal effect of the mixtures of Compound 21 and the mixture partners listed above. Colby's equation (Colby, S. R. “Calculating Synergistic and Antagonistic Responses of Herbicide Combinations,”


Weeds


, 15(1), pp 20-22 (1967)) calculates the expected additive effect of herbicidal mixtures, and for two active ingredients is of the form:








P




a+b




=P




a




+P




b


−(


P




a




P




b


/100)






wherein




P


a+b


is the percentage effect of the mixture expected from additive contribution of the individual components,




P


a


is the observed percentage effect of the first active ingredient at the same use rate as in the mixture, and




P


b


is the observed percentage effect of the second active ingredient at the same use rate as in the mixture.




Combinations of Compound 113, Compound 131, and Compound 242 with rimsulfuron are surprisingly found to provide better control of certain weeds than expected by calculation from the Colby's equation, thus demonstrating synergism. Weeds other than those specifically listed are also controlled by mixtures of compounds of the present invention and rimsulfuron. Different ratios of compounds of the present invention with rimsulfuron, and different formulation types, also provide useful weed control from the combination of the two herbicides.















TABLE F











Cmpd.





ABUTH




CHEAL
















113




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone







 70




0




45









15











105




0




65









35











 0




8.8




20









25











 0




17.5




40









60











Mixtures






 70




8.8




75




56




60




36






 70




17.5




85




67




95




66






105




8.8




90




72




100




51






105




17.5




80




79




100




74

















Cmpd.





AMATA




SETFA
















113




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




35









60











105




0




25









65











 0




8.8




10









75











 0




17.5




15









90











Mixtures






 70




8.8




15




23




95




90






 70




17.5




70




45




100




96






105




8.8




25




33




100




91






105




17.5




90




36




100




97

















Cmpd.





PANDI




DIGSA
















113




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




100









95











105




0




95









70











 0




8.8




75









95











 0




17.5




95









100











Mixtures






 70




8.8




90




100




100




100






 70




17.5




100




100




100




100






105




8.8




100




99




90




99






105




17.5




85




99




100




100

















Cmpd.





ABUTH




CHEAL
















131




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




40









60











105




0




60









95











 0




8.8




20









25











 0




17.5




40









60











Mixtures






 70




8.8




50




52




95




70






 70




17.5




85




64




100




84






105




8.8




80




68




95




96






105




17.5




75




76




100




98

















Cmpd.





AMATA




SETFA
















131




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




50









35











105




0




40









65











 0




8.8




10









75











 0




17.5




15









90











Mixtures






 70




8.8




95




54




85




84






 70




17.5




100




58




100




93






105




8.8




95




46




95




91






105




17.5




85




49




100




97

















Cmpd.





PANDI




DIGSA
















131




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




100









100











105




0




95









100











 0




8.8




75









95











 0




17.5




95









100











Mixtures






 70




8.8




75




100




100




100






 70




17.5




95




100




100




100






105




8.8




100




99




100




100






105




17.5




100




100




100




100

















Cmpd.





ABUTH




CHEAL
















242




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




50









30











105




0




70









100











 0




8.8




20









25











 0




17.5




40









60











Mixtures






 70




8.8




85




60




100




48






 70




17.5




80




81




85




72






105




8.8




85




76




100




100






105




17.5




80




82




100




100

















Cmpd.





AMATA




SETFA
















242




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




20









60











105




0




55









75











 0




8.8




10









75











 0




17.5




15









90











Mixtures






 70




8.8




70




28




90




90






 70




17.5




85




32




100




96






105




8.8




35




60




75




94






105




17.5




65




62




100




97

















Cmpd.





PANDI




DIGSA
















242




Rimsulfuron




Observed




Expected†




Observed




Expected†









Alone






 70




0




60









100











105




0




80









100











 0




8.8




75









95











 0




17.5




95









100











Mixtures






 70




8.8




95




90




100




100






 70




17.5




100




98




100




100






105




8.8




100




85




100




100






105




17.5




100




99




100




100











*Data are reported as percent control.










†Expected from the Colby Equation













Test G Protocol




In soil-containing pots were planted seeds of maize hybrid P33G26 that was previously treated with dichlomid, fenchlorazole-ethyl, and naphthalic anhydride (or no safener). The soil surface was then treated with several rates of Compound 131 or Compound 146 dissolved in a non-phytotoxic solvent using a flat-fan sprayer calibrated to deliver 310 L/ha. Treatmemtes were replicated 4 or 5 times. The treated and untreated plants were allowed to grow in a greenhouse using supplementary artificial lighting with a day-length of 14 hours, with the temperature maintained at about 27° C. during the day and 24° C. during the night. Plants were kept watered with a dilute balanced fertilizer solution.




At 28 days after application, the treated plants were compared with untreated controls and vissually evaluated. Mean plant response ratings, summarized in Table G, are based upon a 0 to 100 scale where 0 is no effect and 100 is complete control.














TABLE G*













Safener

















Rate






Fenchlorazole-




naphthalic






Compd




(g ai/ha)




None




Dichlormid




ethyl




anhydride



















131




560




95




40




96




ND†






131




280




91




3




92




ND†






131




140




88




3




91




 0






131




70




80




3




85




ND†






146




1120




85




4




85




35






146




560




80




4




78




ND†






146




280




73




1




74




ND†






146




140




49




1




3




 0











*Data are reported as percent control.










†naphthalic anhydride treatment severely inhibited corn germination. Where corn did satisfactorily emerge, it was safened against the herbicide damage.













As can be seen from Table F, in the absence of any safener, both Compound 131 and Compound 14 at rates ranging from 70 to 560 g/ha, and 140 to 1120 g/ha respectively, were severely injurious to maize. With the exception of Compound 131 at the rate of 560 g/ha (entry 1 in Table F), the presence of dichlormid reduced the injury to an insignificant level from which the corn would be expected to recover with no long-term deleterious effects. The presence of fenchlorazole-ethyl, however, did not provide safening effects except for low rate of Compound 146 (Entry 8 in Table F). The dramatic safening effects observed here were unexpected and surprising. Based on this discovery, it is anticipated that other compounds known to safen herbicides on corn, soybeans or other crops are useful in safening compounds of the present invention on corn, soybeans or other crops.




Test H Protocol




Mixtures of the herbicide and safeners were applied to pots of a soil mixture previously sown with corn. Pioneer hybrid P33G26 corn was sown in pots containing a sterile mix of 60% sassafras soil and 40% Metro Mix 360® growing medium (pH 6.7, O.M. 2%). Test compounds were dissolved in AGWT (a mixture of 0.25% Tween 20 surfactant, 5% water, 5% glycerin and 89.75% acetone) and sprayed on the soil as pots passed under a stationary 8002E nozzle. Treatments were applied at a 33 gal/acre rate of the AGWT carrier. After treatment, the test pots were placed in the greenhouse and watered. There were two replications for each treatment. Each pot contained eight corn seeds. The pots within each replication were placed in random positions on greenhouse benches. Test plants were fertilized as they were watered with approximately 200 ppm of N (as water soluble 20-20-20 fertilizer) which was metered into the water lines with a fertilizer injector. Daytime temperatures was 23-30° C. and night time temperature was 18-25° C. The test plants were supplemented with artificial lighting. The lights were activated whenever the natural light intensity dropped below the programmed threshold. Day length was maintained for approximately 14 hours.




The test was evaluated approximately 12 days after treatment. Treated plants were visually compared to untreated controls and rated on a scale from 0 to 100 where 0 is no effect and 100 is plant death. The results summarized in Table H are the averages from the two replications for each treatment.

















TABLE H












Rate





Dichlormid




Dichlormid




Dichlormid






Compd




(g ai/ha)




None




70 g/ha




140 g/ha




280 g/ha









113




 70




18




 0




 0




 0






113




140




25




20




 0




 0






113




280




53




35




28




33










Rate





Benoxacor




Benoxacor




Benoxacor






Compd




(g ai/ha)




None




70 g/ha




140 g/ha




280 g/ha









113




 70




18




 0




 0




 0






113




140




25




 0




 0




 8






113




280




53




38




18




20














As shown in Table H, both dichlormid and benoxacor functioned very effectively as safeners for Compound 113. Without safener, Compound 113 at rates from 70 to 280 g/ha produced corn injury of 18 to 53%. In the presence of dichlormid or benoxacor at rates from 70 to 280 g/ha, corn injury was reduced to from 0 to 38%. The dramatic and unexpected safening by dichlormid and benoxacor demonstrates the potential utility of mixtures of these compounds with Compound 113, or other similar compounds of this invention, for the control of undesired vegetation in corn production.



Claims
  • 1. A compound selected from Formula 1, an N-oxide or an agriculturally suitable salt thereof, whereinQ is H; or C1-C12 alkyl, C3-C10 cycloalky, C6-C14 bicycloalkyl, C3-C12 alkenyl, C3-C10 cycloalkenyl, C6-C14 bicycloalkenyl or C3-C12 alkynyl, each optionally substituted with one or more R21; or Q is a 3- to 7-membered fully saturated or 5- to 7-membered partially saturated heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)n, then only one X may be present and (b) when two X are present in the ring, they cannot be bonded directly to each other; or Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R16; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom; or Q is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R16, phenoxy and Z; or Q is Q is —C(R14)(═NOR15), —C(O)R19, —C(O)OR19, —C(O)SR19, —C(S)R19, —C(S)OR19, —C(S)SR19, —C(O)NR23R24, —C(S)NR23R24, —OR19, —NR19R20, —S(O)nR19 or —S(O)nNR19R20; each X is —O—, —S(O)n—, —N═, —NR10— or —Si(R11)2—; Y is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered carbocyclic ring optionally substituted with one or more C1-C4 alkyl groups; or Y is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered heterocyclic ring which contains one or two X and is optionally substituted with one or more R12, provided that when said heterocyclic ring contains two X, then one X is other than O; Z is phenyl or a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each phenyl and heterocyclic ring system is optionally substituted with one or more R16; R1 is C1-C6 alkyl, C1-C6 haloalkyl, C3-C6 alkenyl, C3-C6 haloalkenyl, C3-C6 alkynyl, C3-C6 haloalkynyl, C1-C6 alkoxy, C2-C6 alkoxyalkyl or C2-C6 haloalkoxyalkyl; or R1 is C3-C7 cycloalkyl or C3-C7 cycloalkenyl, each optionally substituted with one or more R5; or R1 is phenyl optionally substituted with one or more R13; or R1 is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R16; R2 is C1-C6 alkyl, C1-C6 haloalkyl, C3-C7 cycloalkyl, C3-C6 alkenyl, C3-C6 haloalkenyl, C3-C6 alkynyl, C3-C6 haloalkynyl, C1-C6 alkoxy, C2-C6 alkoxyalkyl, C2-C6 haloalkoxyalkyl or NR3R4; or R2 is R1 and R2 are taken together as —CH2CH2—, —CH2CH2CH2—, —CH2CH2CH2CH2—, —CH2CH2CH2CH2CH2— or —CH2CH2OCH2CH2—; R3 is C1-C6 alkyl, C1-C6 haloalkyl, C3-C6 alkenyl, C3-C6 haloalkenyl, C3-C6 alkynyl, C3-C6 haloalkynyl; or R3 is C3-C7 cycloalkyl or C3-C7 cycloalkenyl, each optionally substituted with one or more R5; or R3 is a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing 1 to 2 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, and each heterocyclic ring is optionally substituted with one or more R5; or R3 is phenyl optionally substituted with one or more R26 groups; or R1 and R3 are taken together with the two nitrogen atoms to which they are attached to form a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing an optional third heteroatom selected from the group consisting of oxygen, sulfur and nitrogen, and said heterocyclic ring is optionally substituted with one or more R9; or R2 and R13, together with the two atoms to which they are attached and the atom between them, form a fully saturated 5-, 6- or 7-membered carbocyclic or heterocyclic ring containing one oxygen, one sulfur or one or two nitrogen atoms, said heterocyclic ring is optionally substituted with one or more R12 provided that when said heterocyclic ring contains two nitrogen atoms, they are other than bonded directly to each other; R4 is H or C1-C4 alkyl; or R3 and R4 are taken together with the nitrogen atom to which they are attached to form a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing an optional second heteroatom selected from the group consisting of oxygen, sulfur and nitrogen, and said heterocyclic ring is optionally substituted with 1-4 R9; each R5 is independently halogen, C1-C4 alkyl or C1-C4 alkoxy; or when two R5 are attached to the same carbon, then said two R5 groups are taken together as (═O); each R6 and, R7 are independently H or C1-C4 alkyl; R8 is independently C1-C4 alkyl, C1-C4 haloalkyl or C1-C4 alkoxy; each R9 is independently C1-C4 alkyl or C1-C4 alkoxy; or when two R9 are attached to the same carbon, then said two R9 groups are taken together as (═O); W is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)n, then only one X may be present; (b) when two X are present in the ring, they cannot be bonded directly to each other; and (c) said heterocyclic ring is bonded to the group (CR17R18)q through other than X; R10 is H, C1-C4 alkyl, C1-C4 haloalkyl, C3-C4 alkenyl, C3-C4 alkynyl, C2-C4 alkoxycarbonyl or C2-C4 alkylcarbonyl; or R10 is phenyl optionally substituted with C1-C3 alkyl, halogen, cyano, nitro or C2-C4 alkoxycarbonyl; each R11 is C1-C4 alkyl; each R12 is independently halogen, C1-C4 alkyl, C1-C4 haloalkyl, C1-C4 alkoxy, C1-C4 haloalkoxy, C1-C4 alkylthio, C1-C4 haloalkylthio, C1-C4 alkylsulfinyl, C1-C4 alkylsulfonyl or C2-C4 alkoxycarbonyl; each R13 is independently halogen, C1-C3 alkyl, C1-C3 haloalkyl, C1-C3 alkoxy, C1-C3 haloalkoxy, C3-C6 alkenyloxy, C3-C6 alkynyloxy, C1-C4 alkylthio, C1-C4 haloalkylthio, C1-C4 alkylsulfinyl, C1-C4 alkylsulfonyl, cyano, amino, nitro or C2-C4 alkoxycarbonyl; R14 is H, C1-C6 alkyl, C1-C6 haloalkyl or C2-C6 alkoxyalkyl; or R14 and R6, together with the carbon atoms to which they are bonded, form a 5- or 6-membered saturated carbocyclic ring optionally substituted with one or more C1-C4 alkyl groups; R15 is H, C1-C6 alkyl, C1-C6 haloalkyl, C3-C4 alkenyl or C3-C4 alkynyl; each R16 is independently halogen, nitro, cyano, C1-C4 alkyl, C1-C4 haloalkyl, C3-C4 alkenyl, C3-C4 alkynyl, OR22, NR23R24 or S(O)nR19; each R17 and R18 are independently H or C1-C4 alkyl; each R19 and R20 are independently C1-C12 alkyl, C3-C8 cycloalkyl, C3-C12 alkenyl, C3-C8 cycloalkenyl or C3-C12 alkynyl, each optionally substituted with one or more R21; each R21 is halogen, C4-C8 trialkylsilylalkyl, CN, NO2, —OR22, —NR23R24, —S(O)nR22, —S(O)nNR23R24, —C(O)R22, —C(S)R22, —C(O)OR22, —C(S)OR22, —C(S)SR22, —C(O)NR23R24, —C(S)NR23R24, —CHR2, COR22, —CHR25P(O)(OR22)2, —CHR25P(S)(OR22)2, —CHR25C(O)NR23R24, —CHR25C(O)NH2, —CHR25CO2R22, phenyl optionally substituted with one or more R26 groups or benzyl optionally substituted with one or more R26 groups; each R22 is C1-C8 alkyl, C3-C8 cycloalkyl, C3-C8 alkenyl, C3-C8 alkynyl, C1-C8 haloalkyl, C2-C8 alkoxyalkyl, C2-C8 alkylthioalkyl, C2-C8 alkylsulfinylalkyl, C2-C8 alkylsulfonylalkyl, C4-C8 alkoxyalkoxyalkyl, C4-C8 cycloalkylalkyl, C4-C8 alkenoxyalkyl, C4-C8 alkynyloxyalkyl, C6-C8 cycloalkoxyalkyl, C4-C8 alkenyloxyalkyl, C4-C8 alkynyloxyalkyl, C3-C8 haloalkoxyalkyl, C4-C8 haloalkenoxyalkyl, C4-C8 haloalkynyloxyalkyl, C6-C8 cycloalkylthioalkyl, C4-C8 alkenylthioalkyl, C4-C8 alkynylthioalkyl, C1-C4 alkyl substituted with phenoxy or benzyloxy, each ring optionally substituted with halogen, C1-C3 alkyl or C1-C3 haloalkyl, C4-C8 trialkylsilylalkyl, C3-C8 cyanoalkyl, C3-C8 halocycloalkyl, C3-C8 haloalkenyl, C5-C8 alkoxyalkenyl, C5-C8 haloalkoxyalkenyl, C5-C8 alkylthioalkenyl, C3-C8 haloalkynyl, C5-C8 alkoxyalkynyl, C5-C8 haloalkoxyalkynyl, C5-C8 alkylthioalkynyl, C2-C8 alkyl carbonyl, C2-C8 alkoxy carbonyl, phenyl optionally substituted with halogen, CN, C1-C2 haloalkyl and C1-C2 haloalkoxy or benzyl optionally substituted with halogen, C1-C3 alkyl and C1-C3 haloalkyl; each R23 is H or C1-C4 alkyl; each R24 is C1-C4 alkyl or phenyl optionally substituted with one or more R26 groups; R23 and R24 may be taken together as —(CH2)5—, —(CH2)4— or —CH2CH2OCH2CH2—, each ring optionally substituted with C1-C3alkyl, phenyl or benzyl; each R25 is H or C1-C4 alkyl; each R26 is C1-C3 alkyl, C1-C3 haloalkyl, C1-C3 alkoxy, C1-C3 haloalkoxy, C1-C3 alkylthio, C2-C5 alkylcarbonyl, C2-C5 alkoxycarbonyl, halogen, amino, cyano or nitro; R28 is H or C1-C4 alkyl; X1 and X2 are independently O or S; X3 is O, S or NR28; m is 0, 1, 2, 3 or 4; each n is independently 0, 1 or 2; p is 0 or 1; each q is independently 0, 1 or 2; and t is 0, 1 or 2; provided that when Q is unsubstituted phenyl, X1, X2 and X3 are O, q is 0 and R2 is methyl, then R1 is other than methyl; provided that when q is 0, and X1, X2 and X3 are O, and R1 and R2 are CH3, then Q is other than ethyl.
  • 2. The compound of claim 1 whereinQ is H; or C1-C12 alkyl, C3-C10 cycloalkyl, C6-C14 bicycloalkyl, C3-C12 alkenyl, C3-C10 cycloalkenyl, C6-C14 bicycloalkenyl or C3-C12 alkynyl, each optionally substituted with one or more R21; or Q is a 3- to 7-membered partially saturated or 5- to 7-membered partially saturated heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)n, then only one X may be present and (b) when two X are present in the ring, they cannot be bonded directly to each other; or Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R16; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom; or Q is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R16, phenoxy and Z.
  • 3. The compound of claim 2 whereinQ is H; or C1-C12 alkyl, C3-C10 cycloalkyl, C6-C14 bicycloalkyl, C3-C12 alkenyl, C3-C10 cycloalkenyl, C6-C14 bicycloalkenyl or C3-C12 alkynyl, each optionally substituted with one or more R21.
  • 4. The compound of claim 2 whereinQ is a 3- to 7-membered fully saturated or 5- to 7-membered partially saturated heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)n, then only one X may be present and (b) when two X are present in the ring, they cannot be bonded directly to each other; or Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R16; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom.
  • 5. The compound of claim 2 whereinQ is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R16, phenoxy and Z.
  • 6. The compound of claim 3 whereinQ is C1-C6 alkyl optionally substituted with one or more R21, C3-C7 cycloalkyl, C3-C7 alkenyl or C3-C6 alkynyl.
  • 7. The compound of claim 4 whereinQ is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R16; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom.
  • 8. The compound of claim 5 whereinQ is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R16.
  • 9. The compounds of claim 3, claim 4 or claim 5 wherein X1, X2 and X3 are O.
  • 10. The compound of claim 8 whereinQ is phenyl with substituents on the 2-, and 6-position independently selected from the group consisting of R16.
  • 11. The compound of claim 6 wherein q is 0 or 1.
  • 12. The compound of claim 7 wherein q is 0 or 1.
  • 13. The compound of claim 8 wherein q is 0 or 1.
  • 14. The compound of claim 1 whereinR1 is phenyl substituted with one or more R13.
  • 15. The compound of claim 1 whereinR2 is C2-C6 alkyl, C2-C6 haloalkyl or C2-C6 alkoxyalkyl.
  • 16. The compound of claim 1 which is selected from the group consisting of:(a) N-(4-fluorophenyl)-N-(1-methylethyl)-4-(2-methylphenyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide; (b) 4-(2,6-dimethylphenyl)-N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide; (c) 4-(2,6-dimethylphenyl)-N-(1-methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamide; (d) 4-cyclohexyl-N-(1-methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamide; (e) 4-cyclohexyl-N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-2-carboxamide; (f) N,4-bis(1-methylethyl)-3,5-dioxo-N-phenyl-1,2,4-oxadiazolidine-2-carboxamide; (g) N-(4-fluorophenyl)-N-(1-methylethyl)-3,5-dioxo-4-(cyclopropyl)-1,2,4-oxadiazolidine-2-carboxamide; and (h) N-(4-fluorophenyl)-N,4-bis(1-methylethyl)-3,5-dioxo-1,2,4-oxadiazolidine-carboxamide.
  • 17. A process for preparing a compound of Formula 1wherein Q, R6, R7, q, X1, X2, X3, R1 and R2 are as defined for Formula 1 in claim 1, comprising:(a) contacting a compound of Formula 5 wherein R27 is —(CR6R7)q—Q, with a compound of Formula 4 Q—(CR6R7)q—X4  4  wherein X4 is halogen or mesylate, in the presence of a base to provide a compound of Formula 3(b) contacting the compound of Formula 34 with a carbamoyl or thiocarbamoyl chloride of Formula 2
  • 18. A process for preparing a compound of Formula 1wherein Q, R6, R7, q, X1, X2, X3, R1 and R2 are as defined for Formula 1 in claim 1, comprising:(a) contacting a compound of Formula 5 wherein R27 is —(CR6R7)q—Q with an alcohol of Formula 6 Q—(CR6R7)q—OH  6  under reaction conditions involving a tertiary phosphine and an azo compound to provide a compound of Formula 3(b) contacting the compound of Formula 3 with a carbamoyl or thiocarbamoyl chloride of Formula 2.
  • 19. A process for preparing a compound of Formula 1wherein Q, R6R7, q, X1, X2, X3, R1 and R2 are as defined for Formula 1 in claim 1, comprising:(a) concting a compound of Formula 5 wherein R27 is —(CR6R7)q—Q, with a carbamoyl thiocarbamoyl chloride of Formula 2 in the presence of a base to provide the compound of Formula 1 directly or a compound of Formula 7(b) contacting the compound of Formula 7 with an alcohol of Formula 6 Q—(CR6R7)q—OH  6  under reaction conditions involving a tertiary phosphine and an azo compound or with a compound of Formula 4 O—(CR6R7)q—X4  4  in the presence of a base.
  • 20. A process for preparing a compound of Formula 1wherein Q, R6, R7, q, X2, X3, R1 and R2 are as defined for Formula 1 in claim 1, and X1 is O, comprising:(a) contacting a compound of Formula 19 with phosgene or thiophosgene to provide a compound of Formula 20(b) contacting the compound of Formula 20 with hydroxylamine, following by treatment with a base, and then an acid, to provide a compound of Formula 8(c) contacting the compound of Formula 8 with a compound of Formula 2
  • 21. A process for preparing a compound of Formula 1wherein Q, R6, R7, q, X1, X2, X3, R1 and R2 are as defined for Formula 1 in claim 1, comprising:(a) contacting a compound of Formula 2 with hydroxylamine in the presence of a base to provide a compound of Formula 22(b) contacting the compound of Formula 22 with a compound of Formula 23 in the presence of a base to provide a compound of Formula 7(c) contacting the compound of Formula 7 with an alcohol of Formula 6 Q—(CR6R7)q—OH  6  under reaction conditions involving a tertiary phosphine and an azo compound or with a compound of Formula 4 Q—(CR6R7)q—X4  4  in the presence of a base.
  • 22. A process for preparing a compound of Formula 1wherein Q, R6, R7, q, X1, X2, X3, R1 and R2 are as defined for Formula 1 in claim 1, comprising contacting a compound of Formula 7with an orthoformate of Formula 24(R27O)3CH  24 wherein R27 is —(CR6R7)q—Q, in the presence of a base.
  • 23. A process for preparing a compound of Formula 1wherein Q, R6, R7, q, X1, X2, X3, R1 and R2 are as defined for Formula 1 in claim 1, comprising:(a) contacting a compound of Formula 8 with a compound of Formula 26 to provide a compound of Formula 25 or a compound of Formula 27 in the presence of a catalyst such as hexamethylguanidinium chloride; and (c) contacting the compound of Formula 25 or Formula 27 with an amine of Formula 13 in the presence of a base.
  • 24. A herbicidal composition comprising a herbicidally effective amount of a compound selected from Formula 1, an N-oxide or an agriculturally suitable salt thereof, whereinQ is H; or C1-C12 alkyl, C3-C10 cycloalky, C6-C14 bicycloalkyl, C3-C12 alkenyl, C3-C10 cycloalkenyl, C6-C14 bicycloalkenyl or C3-C12 alkynyl, each optionally substituted with one or more R21; or Q is a 3- to 7-membered fully saturated or 5- to 7-membered partially saturated heterocyclic ring containing one or two X, provided that (a) when X is other than O, or S(O)n, then only one X may be present and (b) when two X are present in the ring, they cannot be bonded directly to each other; or Q is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R16; and when Q is a 5- or 6-membered aromatic heterocyclic ring system containing a nitrogen, then Q is bonded through any available carbon or nitrogen atom by replacement of a hydrogen on said carbon or nitrogen atom; or Q is phenyl optionally substituted with one or more substituents independently selected from the group consisting of R16, phenoxy and Z; or Q is Q is —C(R14)(═NOR15), —C(O)R19, —C(O)OR19, —C(O)SR19, —C(S)R19, —C(S)OR19, —C(S)SR19, —C(O)NR23R24, —C(S)NR23R24, —OR19, —N19R20, —S(O)nR19 or —S(O)nNR19R20; each X is —O—, —S(O)n—, —N═, —NR10— or —Si(R11)2—; Y is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered carbocyclic ring optionally substituted with one or more C1-C4 alkyl groups; or Y is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered heterocyclic ring which contains one or two X and is optionally substituted with one or more R12, provided that when said heterocyclic ring contains two X, then one X is other than O; Z is phenyl or a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each phenyl and heterocyclic ring system is optionally substituted with one or more R16; R1 is C1-C6 alkyl, C1-C6 haloalkyl, C3-C6 alkenyl, C3-C6 haloalkenyl, C3-C6 alkynyl, C3-C6 haloalkynyl, C1-C6 alkoxy, C2-C6 alkoxyalkyl or C2-C6 haloalkoxyalkyl; or R1, is C3-C7 cycloalkyl or C3-C7 cycloalkenyl, each optionally substituted with one or more R5; or R1 is phenyl optionally substituted with one or more R13; or R1 is a 5- or 6-membered aromatic heterocyclic ring system containing 1 to 3 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, provided that the heterocyclic ring system contains no more than one oxygen and no more than one sulfur, and each heterocyclic ring system is optionally substituted with one or more R16; R2 is C1-C6 alkyl, C1-C6 haloalkyl, C3-C7 cycloalkyl, C3-C6 alkenyl, C3-C6 haloalkenyl, C3-C6 alkynyl, C3-C6 haloalkynyl, C1-C6 alkoxy, C2-C6 alkoxyalkyl, C2-C6 haloalkoxyalkyl or NR3R4; or R2 is R1 and R2 are taken together as —CH2CH2—, —CH2CH2CH2—, —CH2CH2CH2CH2—, —CH2CH2CH2CH2CH2— or —CH2CH2OCH2CH2—; R3 is C1-C6 alkyl, C3-C6 haloalkyl, C3-C6 alkenyl, C3-C6 haloalkenyl, C3-C6 alkynyl, C3-C6 haloalkynyl; or R3 is C3-C7 cycloalkyl or C3-C7 cycloalkenyl, each optionally substituted with one or more R5; or R3 is a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing 1 to 2 heteroatoms independently selected from the group consisting of nitrogen, oxygen and sulfur, and each heterocyclic ring is optionally substituted with one or more R5; or R3 is phenyl optionally substituted with one or more R26 groups; or R1 and R3 are taken together with the two nitrogen atoms to which they are attached to form a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing an optional third heteroatom selected from the group consisting of oxygen, sulfur and nitrogen, and said heterocyclic ring is optionally substituted with one or more R9; or R2 and R13, together with the two atoms to which they are attached and the atom between them, form a fully saturated 5-, 6- or 7-membered carbocyclic or heterocyclic ring containing one oxygen, one sulfur or one or two nitrogen atoms, said heterocyclic ring is optionally substituted with one or more R12, provided that when said heterocyclic ring contains two nitrogen atoms, they are other than bonded directly to each other; R4 is H or C1-C4 alkyl; or R3 and R4 are taken together with the nitrogen atom to which they are attached to form a saturated or partially saturated 5-, 6- or 7-membered heterocyclic ring containing an optional second heteroatom selected from the group consisting of oxygen, sulfur and nitrogen, and said heterocyclic ring is optionally substituted with 1-4 R9; each R5 is independently halogen, C1-C4 alkyl or C1-C4 alkoxy; or when two R5 are attached to the same carbon, then said two R5 groups are taken together as (═O); each R6 and R7 are independently H or C1-C4 alkyl R8 is independently C1-C4 alkyl, C1-C4 haloalkyl or C1-C4 alkoxy; each R9 is independently C1-C4 alkyl or C1-C4 alkoxy; or when two R9 are attached to the same carbon, then said two R9 groups are taken together as (═O); W is, together with the carbons to which it is attached, a fully or partially saturated 5-, 6- or 7-membered heterocyclic ring containing one or two X, provided that (a) when X is other than O or S(O)n, then only one X may be present; (b) when two X are present in the ring, they cannot be bonded directly to each other; and (c) said heterocyclic ring is bonded to the group (CR17R18)q through other than X; R10 is H, C1-C4 alkyl, C1-C4 haloalkyl, C3-C4 alkenyl, C3-C4 alkynyl, C2-C4 alkoxycarbonyl or C2-C4 alkylcarbonyl; or R10 is phenyl optionally substituted with C1-C3 alkyl, halogen, cyano, nitro or C2-C4 alkoxycarbonyl; each R11 is C1-C4 alkyl; each R12 is independently halogen, C1-C4 alkyl, C1-C4 haloalkyl, C1-C4 alkoxy, C1-C4 haloalkoxy, C1-C4 alkylthio, C1-C4 haloalkylthio, C1-C4 alkylsulfinyl, C1-C4 alkylsulfonyl or C2-C4 alkoxycarbonyl; each R13 is independently halogen, C1-C3 alkyl, C1-C3 haloalkyl, C1-C3 alkoxy, C1-C3 haloalkoxy, C3-C6 alkenyloxy, C3-C6 alkynyloxy, C1-C4 alkylthio, C1-C4 haloalkylthio, C1-C4 alkylsulfinyl, C1-C4 alkylsulfonyl, cyano, amino, nitro or C2-C4 alkoxycarbonyl; R14 is H, C1-C6 alkyl, C1-C6 haloalkyl or C2-C6 alkoxyalkyl; or R14 and R6, together with the carbon atoms to which they are bonded, form a 5- or 6-membered saturated carbocyclic ring optionally substituted with one or more C1-C4 alkyl groups; R15 is H, C1C6 alkyl, C1-C6 haloalkyl, C3-C4 alkenyl or C3-C4 alkynyl; each R16 is independently halogen, nitro, cyano, C1-C4 alkyl, C1-C4 haloalkyl, C3-C4 alkenyl, C3-C4 alkynyl, OR22, NR23R24 or S(O)nR19; each R17 and R18 are independently H or C1-C4 alkyl; each R19 and R20 are independently C1-C12 alkyl, C3-C8 cycloalkyl, C3-C12 alkenyl, C3-C8 cycloalkenyl or C3-C12 alkynyl, each optionally substituted with one or more R21; each R21 is halogen, C4-C8 trialkylsilylalkyl, CN, NO2, —OR22, —NR23R24, —S(O)nR22, —S(O)nNR23R24, —C(O)R22, —C(S)R22, —C(O)OR22, —C(S)OR22, —C(S)SR22, —C(O)NR23R24, —C(S)NR23R24, —CHR25COR22, —CHR25P(O)(OR22)2, —CHR25P(S)(OR22)2, —CHR25C(O)NR23R24, —CHR25C(O)NH2, —CHR25CO2R22, phenyl optionally substituted with one or more R26 groups or benzyl optionally substituted with one or more R26 groups; each R22 is C1-C8 alkyl, C3-C8 cycloalkyl, C3-C8 alkenyl, C3-C8 alkynyl, C1-C8 haloalkyl, C2-C8 alkoxyalkyl, C2-C8 alkylthioalkyl, C2-C8 alkylsulfinylalkyl, C2-C8 alkylsulfonylalkyl, C4-C8 alkoxyalkoxyalkyl, C4-C8 cycloalkylalkyl, C4-C8 alkenoxyalkyl, C4-C8 alkynyloxyalkyl, C6-C8 cycloalkoxyalkyl, C4-C8 alkenyloxyalkyl, C4-C8 alkynyloxyalkyl, C3-C8 haloalkoxyalkyl, C4-C8 haloalkenoxyalkyl, C4-C8 haloalkynyloxyalkyl, C6-C8 cycloalkylthioalkyl, C4-C8 alkenylthioalkyl, C4-C8 alkynylthioalkyl, C1-C4 alkyl substituted with phenoxy or benzyloxy, each ring optionally substituted with halogen, C1-C3 alkyl or C1-C3 haloalkyl, C4-C8 trialkylsilylalkyl, C3-C8 cyanoalkyl, C3-C8 halocycloalkyl, C3-C8 haloalkenyl, C5-C8 alkoxyalkenyl, C5-C8 haloalkoxyalkenyl, C5-C8 alkylthioalkenyl, C3-C8 haloalkynyl, C5-C8 alkoxyalkynyl, C5-C8 haloalkoxyalkynyl, C5-C8 alkylthioalkynyl, C2-C8 alkyl carbonyl, C2-C8 alkoxy carbonyl, phenyl optionally substituted with halogen, CN, C1-C2 haloalkyl and C1-C2 haloalkoxy or benzyl optionally substituted with halogen, C1-C3 alkyl and C1-C3 haloalkyl; each R23 is H or C1-C4 alkyl; each R24 is C1-C4 alkyl or phenyl optionally substituted with one or more R26 groups; R23 and R24 may be taken together as —(CH2)5—, —(CH2)4— or —CH2CH2OCH2CH2—, each ring optionally substituted with C1-C3 alkyl, phenyl or benzyl; each R25 is H or C1-C4 alkyl; each R26 is C1-C3 alkyl, C1-C3 haloalkyl, C1-C3 alkoxy, C1-C3 haloalkoxy, C1-C3 alkylthio, C2-C5 alkylcarbonyl, C2-C5 alkoxycarbonyl, halogen, amino, cyano or nitro; R28 is H or C1-C4 alkyl; X1 and X2 are independently O or S; X3 is O, S or NR28; m is 0, 1, 2, 3 or 4; each n is independently 0, 1 or 2; p is 0 or 1; each q is independently 0, 1 or 2; and t is 0, 1 or 2; provided that when Q is unsubstituted phenyl, X1, X2 and X3 are O, q is 0 and R2 is methyl, then R1 is other than methyl; and at least one of a surfactant, a solid diluent or a liquid diluent.
  • 25. A method for controlling the growth of undesired vegetation comprising contacting the vegetation or its environment with a herbicidally effective amount of a compound of claim 1.
Parent Case Info

This application claims the benefit of Provisional Application Ser. No. 60/117,210 filed Jan. 25, 1999.

PCT Information
Filing Document Filing Date Country Kind
PCT/US00/01283 WO 00
Publishing Document Publishing Date Country Kind
WO00/43377 7/27/2000 WO A
US Referenced Citations (2)
Number Name Date Kind
3950367 Botta Apr 1976 A
5356865 Miller et al. Oct 1994 A
Foreign Referenced Citations (3)
Number Date Country
1259871 Feb 1968 DE
0477646 Apr 1992 EP
1168721 Oct 1969 GB
Non-Patent Literature Citations (5)
Entry
Database Crossfire Online—Beilstein Institut zur Foerderung der Chemischen Wissenschaften; XP002141082 Beilstein Registry No. 5973265, 5944839, 5942772, 5940606, 5927572 & Arch. Pharm., vol. 314, No. 4, 1981, pp. 294-302.
Database Crossfire Online—Beilstein Institut zur Foerderung der Chemischen Wissenschaften; XP992141083 Beilstein Registry No. 513318, 611515, 519232, 509077, 510600, 511401 & Arch. Pham. Ber. DTSCH. Pharm. GES., vol. 303, 1970, pp. 139-144.
Database Crossfire Online Beilstein Institut zur Foerderung der Chemischen Wissenschaften; XP002141084 Beilstein Registry No. 972970, 973571, 974317, 975960, 981328 & Arch Pharm Ber. DTSCH. Pharm GES., vol. 303, 1970, pp. 385-390.
Database Crossfire Online Bellstein Institut zur Foerderung der Chemischen Wissenschaften; XP002141085 Beilstein Registry No. 519889, 521425, 5222254, 534767, 4937992 & Chem. Ber., vol. 98, 1965, pp. 144-154.
Chemical Abstracts, vol. 80, No. 19, May 13, 1974 Columbus, Ohio, US; abstract No. 108148v, Zinner G et al: “Hydroxylamine derivatives. 56. Synthesis and acylations of 1,1-Dialkyl-3-hydroxyureas” p. 383; XP0021164 cited in the application abstract & Arch. Pharm., vol. 307, No. 1, 1974, pp. 7-12, Weinheim, DE Arch. Pharm (1974), 307, 7-12.
Provisional Applications (1)
Number Date Country
60/117210 Jan 1999 US