Embodiments herein relate to filter media, filter media packs, and filter elements.
High efficiency filtration, including high efficiency particulate air (HEPA) filtration, is desirable for many applications, in particular for applications where removal of various small particulates (including, but limited to, particles from engine combustion, fires, dust, microbes and other pathogens, viruses, etc.) is desirable in various environments (such as interior and exterior spaces, including within buildings and aircraft). For example, it is often desirable to have HEPA filtration of air circulating within an aircraft cabin.
Although various HEPA filtration products exist, there remains a need for improved HEPA filtration media, media packs, and filter elements.
The present application is directed to filter media, filter media packs, and filter elements. In an embodiment, a filtration media pack has a plurality of layers of single facer media wherein the layers of single facer media include a fluted sheet, a facing sheet, and a plurality of flutes extending between the fluted sheet and the facing sheet. The flutes have a flute length extending from a first face of the filtration media pack to a second face of the filtration media pack. A first portion of the plurality of flutes is closed to unfiltered fluid (such as air) flowing into the first portion of the plurality of flutes, and a second portion of the plurality of flutes is closed to unfiltered fluid flowing out of the second portion of the plurality of flutes so that fluid passing into one of the first face or the second face of the media pack and out the other of the first face or the second face of the media pack passes through media to provide filtration of the fluid. The fluted sheet and facing sheet are formed of multilayer media that can include a polytetrafluoroethylene (PTFE) layer supported by a polymeric scrim layer. The facing sheet is typically not fluted, but in some embodiments the facing sheet is also fluted. The polymeric scrim can be, for example, a spunbond material with high uniformity in the media, such as uniformity of fiber diameter (thickness) or fiber distribution.
Generally, it is desirable that the polymeric scrim layer be relatively uniform in terms of surface irregularities (such as peak height of fibers relative to surrounding fibers), in terms of fiber diameter, and in terms of fiber distribution. This relative uniformity allows for improved support of the PTFE layer without undue damage to the PTFE layer, which is typically quite thin and relatively fragile.
In an embodiment, a filtration media pack is included having (a) a plurality of layers of single facer media wherein the layers of single facer media include a fluted sheet, a facing sheet, and a plurality of flutes extending between the fluted sheet and the facing sheet and having a flute length extending from a first face of the filtration media pack to a second face of the filtration media pack, (b) a first portion of the plurality of flutes being closed to unfiltered fluid flowing into the first portion of the plurality of flutes, and a second portion of the plurality of flutes being closed to unfiltered fluid flowing out of the second portion of the plurality of flutes so that fluid passing into one of the first face or the second face of the media pack and out the other of the first face or the second face of the media pack passes through media to provide filtration of the fluid, wherein the fluted sheet and facing sheet are formed of multi-layer media can include a polytetrafluoroethylene (PTFE) layer supported by a polymeric scrim layer, wherein the polymeric scrim has a fiber diameter standard deviation of less than 4 μm.
The polymeric scrim generally has a relatively small deviation in fiber diameter. The fiber diameter can be measured, for example, on the face of the scrim that does not have a PTFE layer laminated to it (so opposite the PTFE layer). In an embodiment, the polymeric scrim has a fiber diameter standard deviation of less than 3 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of less than 2.5 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of less than 2 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of 1 to 3 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of 1 to 4 μm.
Further, the overall size of the scrim fibers can be controlled to improve performance, in particular to preserve filtration performance, as the filter media is converted from flat sheets into fluted sheets. In an embodiment, the polymeric scrim has a mean fiber diameter of less than 30 μm. In an embodiment, the polymeric scrim has a mean fiber diameter of less than 25 μm. In an embodiment, the polymeric scrim has a mean fiber diameter of less than 20 μm. In an embodiment, the polymeric scrim has a mean fiber diameter of greater than 10 μm. In an embodiment, the polymeric scrim has a mean fiber diameter of greater than 15 μm. In an embodiment, the polymeric scrim has a mean fiber diameter of 5 to 30 μm. In an embodiment, the polymeric scrim has a mean fiber diameter of 10 to 25 μm. In an embodiment, the polymeric scrim has a mean fiber diameter of 15 to 20 μm.
Minimum fiber size can vary. In an embodiment, the polymeric scrim has a minimum fiber diameter of 8 μm. In an embodiment, the polymeric scrim has a minimum fiber diameter of 10 μm. In an embodiment, the polymeric scrim has a minimum fiber diameter of 12 μm.
Maximum fiber size can also be controlled and is generally less than 50 μm. In an embodiment, the polymeric scrim has a maximum fiber diameter of 40 μm. In an embodiment, the polymeric scrim has a maximum fiber diameter of 35 μm. In an embodiment, the polymeric scrim has a maximum fiber diameter of 30 μm. In an embodiment, the polymeric scrim has a maximum fiber diameter of 25 μm.
In an embodiment, the polymeric scrim layer includes polyethylene terephthalate (PET) fibers. The polymeric scrim can be composed entirely of PET fibers, or can be formed of PET fibers mixed w/other fibers, or formed entirely of non-PET fibers.
In an embodiment, the polymeric scrim layer has a basis weight of less than 2 ounces per square yard, or optionally the polymeric scrim layer has a basis weight of 1 to 2 ounces per square yard. In an embodiment, the polymeric scrim layer has a thickness of less than 11 μm. In an embodiment, the polymeric scrim layer has a thickness of less than 10 μm. In an embodiment, the polymeric scrim layer has a thickness of less than 9 μm. In an embodiment, the polymeric scrim layer has a thickness of greater than 5 μm. In an embodiment, the polymeric scrim layer has a thickness of greater than 6 μm. In an embodiment, the polymeric scrim layer has a thickness of greater than 7 μm. In an embodiment, the polymeric scrim layer has a thickness of 5 to 11 μm. In an embodiment, the polymeric scrim layer has a thickness of 6 to 10 μm. In an embodiment, the polymeric scrim layer has a thickness of 7 to 9 μm.
In an embodiment, the polymeric scrim layer has an air perm of less than 300 cfm/ft2. In an embodiment, the polymeric scrim layer has an air perm of less than 250 cfm/ft2.
In an embodiment, the polymeric scrim layer has an air perm of greater than 150 cfm/ft2. In an embodiment, the polymeric scrim layer has an air perm of greater than 200 cfm/ft2. In an embodiment, the polymeric scrim layer has an air perm of greater than 225 cfm/ft2. In an embodiment, the polymeric scrim layer has an air perm of 200 to 300 cfm/ft2. In an embodiment, the polymeric scrim layer has an air perm of 225 to 275 cfm/ft2.
In an embodiment, the polymeric scrim layer has an external maximum peak height, SP, measured between the highest peak and the mean plane, of less than 5 μm.
In an embodiment, the polymeric scrim layer has fibers having a mean diameter of 10 μm to 20 μm and a standard deviation of less than 3 μm. In an embodiment, the polymeric scrim layer has fibers having a mean diameter of 12 μm to 18 μm and a standard deviation of less than 2 μm.
In an embodiment, the multi-layer media has air permeability of greater than 4.0 cubic feet per minute (CFM).
In an embodiment, the filter pack has an efficiency of at least 99.97 percent of 0.3 μm particles at a face velocity of 10 feet per minute.
In an embodiment, the polymeric scrim layer has a Frazier air permeability of greater than 900 cfm/ft2 at 0.5 inches of water.
In an embodiment, the PTFE has a basis weight of 1.5 to 2.5 ounces per square yard. In an embodiment, the PTFE has a basis weight of less than 3.0 ounces per square yard.
In an embodiment, an filtration media pack as described herein has (a) a plurality of layers of filter media wherein the layers of filter media include a folded sheet and a facing sheet with spaces between the layers, (b) a first portion of the spaces between the layers of filter media being closed to unfiltered fluid flowing into the first portion of the spaces between the layers, and a second portion of the spaces between the layers being closed to unfiltered fluid flowing out of the second portion of the spaces between the layers, so that fluid passing into one face of the media pack and out another face of the media pack passes through media to provide filtration of the fluid, and (c) wherein the folded sheets include first peaks and second peaks, and at least a portion of the folded sheets have a crease aligned so that it approaches toward a first peak and away from a second peak, wherein the fluted sheet and facing sheet are formed of multi-layer media that includes a polytetrafluoroethylene (PTFE) layer supported by a polymeric scrim layer.
In an embodiment, the polymeric scrim has a fiber diameter standard deviation of less than 4 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of less than 3 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of less than 2.5 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of less than 2 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of 1 μm to 3 μm. In an embodiment, the polymeric scrim has a fiber diameter standard deviation of 1 μm to 4 μm.
In an embodiment, the polymeric scrim layer has an external maximum peak height Sp, measured between the highest peak and the mean plane, of less than 80 μm. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 60 μm. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 50 μm. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 40 μm. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 30 μm. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 20 μm.
In an embodiment, the polymeric scrim layer has an external root mean square height Sq, of less than 100 μm according to the formula:
In an embodiment, the polymeric scrim layer has an external root mean square height Sq, of less than 75 μm; of less than 50 μm; of less than 40 μm; of less than 35 μm; or less than 20 μm.
In an embodiment, the polymeric scrim layer has an external arithmetical mean height Sa of less than 100 μm according to the following formula:
In an embodiment, the polymeric scrim layer has an external arithmetical mean height Sa of less than 75 μm; the polymeric scrim layer has an external arithmetical mean height Sa of less than 60 μm; the polymeric scrim layer has an external arithmetical mean height Sa of less than 50 μm; the polymeric scrim layer has an external arithmetical mean height Sa of less than 40 μm; the polymeric scrim layer has an external arithmetical mean height Sa of less than 30 μm; or the polymeric scrim layer has an external arithmetical mean height Sa of less than 20 μm;
It is typically desirable to have the fibers of the polymeric scrim layer be relatively uniformly distributed. In an embodiment, the polymeric scrim layer has fibers having a uniformity of distribution of measured variance from the mean density of −1.0 to −0.25 as measured by the following formula:
according to “Nonwoven Uniformity-Measurements using Image Analysis by Rajev Chhabra, 50 INJ Spring 2003, incorporated herein by reference.
In an embodiment, the polymeric scrim layer has fibers having a uniformity of distribution of −1 to −0.5. In embodiments the polymeric scrim layer has fibers having a uniformity of distribution of more than −1.5; alternatively, the polymeric scrim layer has fibers having a uniformity of distribution of more than −2.0; alternatively, the polymeric scrim layer has fibers having a uniformity of distribution of greater than −3.0.
In embodiments, the polymeric scrim layer has fibers having a uniformity of contact points of less than 2.0, of less than 1.5, of less than 1.0, or less than 1.0. In an embodiment, the polymeric scrim layer has fibers having a uniformity of contact points of 0.5 to 2.5. In an embodiment, the polymeric scrim layer has fibers having a uniformity of contact points 1.0 to 2.0. Uniformity of Contact Points can be measured in accordance with MEASUREMENT OF THE UNIFORMITY OF THERMALLY BONDED POINTS IN POLYPROPYLENE SPUNBONDED NON-WOVENS USING IMAGE PROCESSING AND ITS RELATIONSHIP WITH THEIR TENSILE PROPERTIES by Mina Emadi et al., AUTEX Research Journal, Vol. 18, No. 4, December 2018 (incorporated herein by reference).
In an embodiment, the multi-layer media has air permeability of 2.0 to 3.0 cubic feet per minute (CFM); in an embodiment, the multi-layer media has air permeability of 1.5 to 4.0 cubic feet per minute (CFM); in an embodiment, the multi-layer media has air permeability of 1.0 to 5.0 cubic feet per minute (CFM); in an embodiment, the multi-layer media has air permeability of 0.5 to 6.0 cubic feet per minute (CFM); in an embodiment, the multi-layer media has air permeability of greater than 2.0 cubic feet per minute (CFM); in an embodiment, the multi-layer media has air permeability of greater than 2.5 cubic feet per minute (CFM), in an embodiment, the multi-layer media has air permeability of greater than 3.0 cubic feet per minute (CFM); in an embodiment, the multi-layer media has air permeability of greater than 4.0 cubic feet per minute (CFM); and in an embodiment, the multi-layer media has air permeability of greater than 5.0 cubic feet per minute (CFM).
In an embodiment, the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 1200 cfm through the media pack. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 800 cfm through the media pack. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 1600 cfm through the media pack. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 2400 cfm through the media pack. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 3000 cfm through the media pack.
In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 5 to 25 feet per minute. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 5 feet per minute. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 10 feet per minute. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 15 feet per minute. In an embodiment, the filter pack has an efficiency of 99.97 percent of 3 μm particles at a face velocity of 20 feet per minute. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 25 feet per minute. In an embodiment, the filter pack has an efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 30 feet per minute.
In an embodiment, the multi-layer media has a thickness of 6 to 9 mils. In an embodiment, the multi-layer media has a thickness of 5 to 10 mils. In an embodiment, the multi-layer media has a thickness of 4 to 11 mils. In an embodiment, the multi-layer media has a thickness of 3 to 15 mils. In an embodiment, the multi-layer media has a thickness of less than 22 mils; less than 15 mils, less than 12 mils, less than 9 mils, less than 7 mils, less than 6 mils, or less than 5 mils.
In an embodiment, the multi-layer media has a bubble point of 6 to 10 psi. In an embodiment, the multi-layer media has a bubble point of 5 to 11 psi. In an embodiment, the multi-layer media has a bubble point of 4 to 12 psi.
In an embodiment, the PTFE includes expanded PTFE (ePTFE).
In an embodiment, the PTFE has an average pore size of 1.0 to 5.0 μm.
In an embodiment, the polymeric scrim includes spunbond fibers. In an embodiment, the spunbond fibers include polyester fibers.
In an embodiment, the fibers are substantially uniformly distributed.
In an embodiment, the polymeric scrim layer has a basis weight of 0.5 to 1.0 ounces per square yard. In an embodiment, the polymeric scrim layer has a basis weight of 0.6 to 0.9 ounces per square yard. In an embodiment, the polymeric scrim layer has a basis weight of greater than 0.5 ounces per square yard. In an embodiment, the polymeric scrim layer has a basis weight of less than 1.5 ounces per square yard. In an embodiment, the polymeric scrim layer has a basis weight of less than 2.0 ounces per square yard.
In an embodiment, the polymeric scrim layer has a thickness of 6 mils. In an embodiment, the polymeric scrim layer has a thickness of 4 to 8 mils. In an embodiment, the polymeric scrim layer has a thickness of 3 to 10 mils. In an embodiment, the polymeric scrim layer has a thickness of less than 12 mils. In an embodiment, the polymeric scrim layer has a thickness of less than 14 mils. In an embodiment, the polymeric scrim layer has a thickness of less than 16 mils.
In an embodiment, the polymeric scrim layer has a Frazier air permeability of 800 to 900 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 700 to 1,000 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 600 to 1,100 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 550 to 1,050 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 500 to 1.500 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of greater than 500 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of greater than 700 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of greater than 900 cfm/ft2 at 0.5 inches of water.
In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.5 to 1.0. In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.6 to 0.9. In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.7 to 0.8. In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.25 to 1.0.
In an embodiment, the filter media can further include an additional layer between the PTFE layer and polymeric scrim layer. In an embodiment, the additional layer includes polypropylene or polyethylene. In an embodiment, the polymeric scrim layer further includes cellulose.
In an embodiment, the PTFE has a thickness of 6 to 10 mils. In an embodiment, the PTFE has a thickness of 4 to 12 mils. In an embodiment, the PTFE has a thickness of 7 to 9 mils. In an embodiment, the PTFE has a thickness of 2 to 14 mils. In an embodiment, the PTFE has a thickness of 5 to 10 mils. In an embodiment, the PTFE has a thickness of greater than 4 mils. In an embodiment, the PTFE has a thickness of greater than 5 mils. In an embodiment, the PTFE has a thickness of greater than 6 mils. In an embodiment, the PTFE has a thickness of greater than 7 mils.
In an embodiment, the PTFE has a thickness of less than 9 mils. In an embodiment, the PTFE has a thickness of less than 10 mils. In an embodiment, the PTFE has a thickness of less than 12 mils. In an embodiment, the PTFE has a thickness of less than 15 mils. In an embodiment, the PTFE has a thickness of less than 20 mils.
In an embodiment, the PTFE has an air perm of 200 to 300 cfm/ft2. In an embodiment, the PTFE has an air perm of 150 to 350 cfm/ft2. In an embodiment, the PTFE has an air perm of 100 to 400 cfm/ft2. In an embodiment, the PTFE has an air perm of 500 to 500 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 100 cfm/ft2.
In an embodiment, the PTFE has an air perm of greater than 125 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 150 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 200 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 225 cfm/ft2. In an embodiment, the PTFE has an air perm of less than 275 cfm/ft2; an air perm of less than 300 cfm/ft2; an air perm of less than 350 cfm/ft2; an air perm of less than 400 cfm/ft2; an air perm of less than 500 cfm/ft2; or an air perm of less than 1000 cfm/ft2.
In some embodiments the PTFE has a Mullen burst of 25 to 75 psi; alternatively, in some embodiments the PTFE has a Mullen burst of 10 to 90 psi; a Mullen burst of 10 to 100 psi; a Mullen burst of less than 125 psi; a Mullen burst of less than 150 psi; or a Mullen burst of less than 200 psi.
In an embodiment the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 60/48. In an embodiment, the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 40 to 80/40 to 60; alternatively, in an embodiment, the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 30 to 90/30 to 70; and alternatively, in an embodiment the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 20 to 100/20 to 80.
In an embodiment, the PTFE has a basis weight of 1.0 to 3.0 ounces per square yard; alternatively, in an embodiment, the PTFE has a basis weight of 1.5 to 2.5 ounces per square yard. In an embodiment, the PTFE has a basis weight of 0.5 to 3.0 ounces per square yard; alternatively, the PTFE has a basis weight of greater than 0.5 ounces per square yard. In an embodiment, the PTFE has a basis weight of greater than 1.0 ounces per square yard; of greater than 1.5 ounces per square yard; of less than 3.0 ounces per square yard; of less than 4.0 ounces per square yard; or less than 5.0 ounces per square yard.
This summary is an overview of some of the teachings of the present application and is not intended to be an exclusive or exhaustive treatment of the present subject matter. Further details are found in the detailed description and appended claims. Other aspects will be apparent to persons skilled in the art upon reading and understanding the following detailed description and viewing the drawings that form a part thereof, each of which is not to be taken in a limiting sense. The scope herein is defined by the appended claims and their legal equivalents.
Aspects may be more completely understood in connection with the following figures (FIGS.), in which:
While embodiments are susceptible to various modifications and alternative forms, specifics thereof have been shown by way of example and drawings, and will be described in detail. It should be understood, however, that the scope herein is not limited to the particular aspects described. On the contrary, the intention is to cover modifications, equivalents, and alternatives falling within the spirit and scope herein.
Now, in reference to the drawings,
Measurement of fiber diameter can be undertaken by selecting a region, such as region A, region B, or region C, and then measuring the number of fibers in that region and the diameter of each fiber to obtain a mean fiber diameter, and also allow for other statistical measures, such as median fiber diameter, mode fiber diameter, standard deviations, etc. The size of the regions used for these measures can be adjusted, but in general should be big enough to allow for a statistically meaningful sample size. Typically, at least 20 fibers should be shown in a measurement region, more typically at least 30 fibers, at least 40 fibers, or at least 50 fibers. It is possible to also use higher sample sizes, such as 50 to 500 fibers, 50 to 250 fibers, or 50 to 100 fibers. Also, it is possible to take multiple measurements across multiple regions and then combine the results, such as combining regions A, B, and C and averaging the results. Generally, it is desirable to try to have a large enough sample size to properly characterize the overall media properties.
Note that it is often desirable to measure the fiber sizes from the non-laminated side of the media, in other words from the side of the media that does not contain the PTFE, since this non-laminated side of the media will have visible fibers that are not obscured by the PTFE. Also, it is possible to deconstruct an element and take samples from exposed areas of the media, such as portions of the flat sheet forming the media, or portions of the corrugated media that have been flattened out. It will be appreciated that not all portions of the media in a media pack or element need to meet the fiber diameter (or other parameters) requirement, but only a portion of the media must meet the requirement. Generally, the majority of the media will meet the requirement, and in some cases all of the media will meet the requirements, but in some cases less than the majority of the media will meet the requirements.
In an embodiment, the polymeric scrim layer has fibers having a uniformity of distribution of −1 to −0.5. In an embodiment, the polymeric scrim layer has fibers having a uniformity of distribution of greater than −1.5; in an embodiment, the polymeric scrim layer has fibers having a uniformity of distribution of greater than −2.0; in an embodiment, the polymeric scrim layer has fibers having a uniformity of distribution of greater than −3.0; and in an embodiment, the polymeric scrim layer has fibers having a uniformity of contact points of less than 3.0.
In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 100μ. In an embodiment, the polymeric scrim layer has an external maximum peak height Sp, measured between the highest peak and the mean plane, of less than 80p. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 60μ. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 50μ. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 40μ. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 30μ. In an embodiment, the polymeric scrim layer has an external maximum peak height SP, measured between the highest peak and the mean plane, of less than 20μ.
In an embodiment, the polymeric scrim layer has an external root mean square height Sq, of less than 100μ according to the formula:
In an embodiment, the polymeric scrim layer has an external root mean square height Sq, of less than 75μ; of less than 50μ; of less than 40μ; of less than 35μ; or of less than 20μ. In an embodiment, the polymeric scrim layer has an external arithmetical mean height Sa of less than 100μ according to the following formula:
In an embodiment, the polymeric scrim layer has an external arithmetical mean height Sa of less than 75μ; the polymeric scrim layer has an external arithmetical mean height Sa of less than 60μ; the polymeric scrim layer has an external arithmetical mean height Sa of less than 50μ; the polymeric scrim layer has an external arithmetical mean height Sa of less than 40μ; the polymeric scrim layer has an external arithmetical mean height Sa of less than 30μ; or the polymeric scrim layer has an external arithmetical mean height Sa of less than 20μ.
In an embodiment, a filtration media pack is included having (a) a plurality of layers of single facer media wherein the layers of single facer media include a fluted sheet, a facing sheet, and a plurality of flutes extending between the fluted sheet and the facing sheet and having a flute length extending from a first face of the filtration media pack to a second face of the filtration media pack, (b) a first portion of the plurality of flutes being closed to unfiltered fluid flowing into the first portion of the plurality of flutes, and a second portion of the plurality of flutes being closed to unfiltered fluid flowing out of the second portion of the plurality of flutes so that fluid passing into one of the first face or the second face of the media pack and out the other of the first face or the second face of the media pack passes through media to provide filtration of the fluid, wherein the fluted sheet and facing sheet formed of multi-layer media can include a polytetrafluoroethylene (PTFE) layer supported by a polymeric scrim layer.
In an embodiment, the multi-layer media has air permeability of 2.0 to 3.0 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of 1.5 to 4.0 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of 1.0 to 5.0 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of 0.5 to 6.0 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of greater than 2.0 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of greater than 2.5 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of greater than 3.0 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of greater than 4.0 cubic feet per minute (CFM). In an embodiment, wherein the multi-layer media has air permeability of greater than 5.0 cubic feet per minute (CFM).
In an embodiment, the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 1200 cfm through the media pack. In an embodiment, the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 800 cfm through the media pack. In an embodiment, the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 1600 cfm through the media pack. In an embodiment, the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 2400 cfm through the media pack. In an embodiment, wherein the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a flow rate of 3000 cfm through the media pack. In an embodiment, wherein the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 5 to 25 feet per minute.
In an embodiment, the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 5 feet per minute. In an embodiment, wherein the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 10 feet per minute. In an embodiment, wherein the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 15 feet per minute. In an embodiment, wherein the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 20 feet per minute. In an embodiment, wherein the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 25 feet per minute.
In an embodiment, wherein the filter pack has efficiency of 99.97 percent of 0.3 μm particles at a face velocity of 30 feet per minute. In an embodiment, wherein the multi-layer media has a thickness of 6 to 9 mils. In an embodiment, wherein the multi-layer media has a thickness of 5 to 10 mils. In an embodiment, wherein the multi-layer media has a thickness of 4 to 11 mils. In an embodiment, wherein the multi-layer media has a thickness of 3 to 15 mils. In an embodiment, wherein the multi-layer media has a thickness of less than 20 mils. In an embodiment, wherein the multi-layer media has a thickness of less than 20 mils. In an embodiment, wherein the multi-layer media has a thickness of less than 15 mils.
In an embodiment, wherein the multi-layer media has a thickness of less than 12 mils. In an embodiment, wherein the multi-layer media has a thickness of less than 9 mils. In an embodiment, wherein the multi-layer media has a thickness of less than 7 mils. In an embodiment, wherein the multi-layer media has a thickness of less than 6 mils. In an embodiment, wherein the multi-layer media has a thickness of less than 5 mils. In an embodiment, wherein the multi-layer media has a bubble point of 6 to 10 psi. In an embodiment, wherein the multi-layer media has a bubble point of 5 to 11 psi. In an embodiment, wherein the multi-layer media has a bubble point of 4 to 12 psi.
In an embodiment, the PTFE includes expanded PTFE (ePTFE).
In an embodiment, the PTFE has an average pore size of 1.0 to 5.0 μm.
In an embodiment, wherein the polymeric scrim includes spunbond fibers. In an embodiment, wherein the spunbond fibers include polyester fibers.
In an embodiment, wherein the fibers are substantially uniformly distributed. In an embodiment, wherein the polymeric scrim layer has a basis weight of 0.5 to 1.0 ounces per square yard. In an embodiment, the polymeric scrim layer has a basis weight of 0.6 to 0.9 ounces per square yard. In an embodiment, the polymeric scrim layer has a basis weight of greater than 0.5 ounces per square yard. In an embodiment, the polymeric scrim layer has a basis weight of less than 1.5 ounces per square yard.
In an embodiment, the polymeric scrim layer has a basis weight of less than 2.0 ounces per square yard.
In an embodiment, the polymeric scrim layer has a thickness of 6 mils.
In an embodiment, the polymeric scrim layer has a thickness of 4 to 8 mils. In an embodiment, the polymeric scrim layer has a thickness of 3 to 10 mils. In an embodiment, the polymeric scrim layer has a thickness of less than 12 mils. In an embodiment, the polymeric scrim layer has a thickness of less than 14 mils. In an embodiment, the polymeric scrim layer has a thickness of less than 16 mils.
In an embodiment, the polymeric scrim layer has a Frazier air permeability of 800 to 900 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 700 to 1,000 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 600 to 1,100 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 550 to 1,050 cfm/ft2 at 0.5 inches of water. In an embodiment, the polymeric scrim layer has a Frazier air permeability of 500 to 1.500 cfm/ft2 at 0.5 inches of water. In an embodiment, wherein the polymeric scrim layer has a Frazier air permeability of greater than 500 cfm/ft2 at 0.5 inches of water. In an embodiment, wherein the polymeric scrim layer has a Frazier air permeability of greater than 700 cfm/ft2 at 0.5 inches of water. In an embodiment, wherein the polymeric scrim layer has a Frazier air permeability of greater than 900 cfm/ft2 at 0.5 inches of water.
In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.5 to 1.0. In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.6 to 0.9. In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.7 to 0.8. In an embodiment, the fibers are substantially uniformly distributed such that the standard deviation of fiber spacing is from 0.5 to 1.0. In an embodiment, further can include an additional layer between the PTFE layer and polymeric scrim layer. In an embodiment, the additional layer includes polypropylene or polyethylene.
In an embodiment, wherein the polymeric scrim layer further includes cellulose.
In an embodiment, the PTFE has a thickness of 6 to 10 mils. In an embodiment, the PTFE has a thickness of 4 to 12 mills. In an embodiment, the PTFE has a thickness of 7 to 9 mils. In an embodiment, the PTFE has a thickness of 2 to 14 mils. In an embodiment, the PTFE has a thickness of 6 to 10 mils. In an embodiment, the PTFE has a thickness of greater than 4 mils. In an embodiment, the PTFE has a thickness of greater than 5 mils.
In an embodiment, the PTFE has a thickness of greater than 6 mils. In an embodiment, wherein the PTFE has a thickness of greater than 7 mils. In an embodiment, the PTFE has a thickness of less than 9 mils. In an embodiment, the PTFE has a thickness of less than 10 mils.
In an embodiment, the PTFE has a thickness of less than 12 mils. In an embodiment, the PTFE has a thickness of less than 15 mils. In an embodiment, the PTFE has a thickness of less than 20 mils. In an embodiment, the PTFE has an air perm of 200 to 300 cfm/ft2. In an embodiment, the PTFE has an air perm of 150 to 350 cfm/ft2. In an embodiment, the PTFE has an air perm of 100 to 400 cfm/ft2. In an embodiment, the PTFE has an air perm of 500 to 500 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 100 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 125 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 150 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 200 cfm/ft2. In an embodiment, the PTFE has an air perm of greater than 225 cfm/ft2. In an embodiment, the PTFE has an air perm of less than 275 cfm/ft2. In an embodiment, the PTFE has an air perm of less than 300 cfm/ft2. In an embodiment, the PTFE has an air perm of less than 350 cfm/ft2. In an embodiment, the PTFE has an air perm of less than 400 cfm/ft2. In an embodiment, the PTFE has an air perm of less than 500 cfm/ft2. In an embodiment, the PTFE has an air perm of less than 1000 cfm/ft2. In an embodiment, the PTFE has a Mullen burst of 25 to 75 psi. In an embodiment, the PTFE has a Mullen burst of 10 to 90 psi. In an embodiment, the PTFE has a Mullen burst of 10 to 100 psi. In an embodiment, the PTFE has a Mullen burst of less than 125 psi. In an embodiment, the PTFE has a Mullen burst of less than 150 psi. In an embodiment, the PTFE has a Mullen burst of less than 200 psi. In an embodiment, the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 60/48.
In an embodiment, the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 40 to 80/40 to 60. In an embodiment, the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 30 to 90/30 to 70. In an embodiment, the PTFE has a strip tensile strength (MD/CD, kg/5 cm) of 20 to 100/20 to 80.
In an embodiment, the PTFE has a basis weight of 1.0 to 3.0 ounces per square yard. In an embodiment, the PTFE has a basis weight of 1.5 to 2.5 ounces per square yard. In an embodiment, the PTFE has a basis weight of 0.5 to 3.0 ounces per square yard. In an embodiment, the PTFE has a basis weight of greater than 0.5 ounces per square yard. In an embodiment, the PTFE has a basis weight of greater than 1.0 ounces per square yard. In an embodiment, the PTFE has a basis weight of greater than 1.5 ounces per square yard. In an embodiment, the PTFE has a basis weight of less than 3.0 ounces per square yard. In an embodiment, the PTFE has a basis weight of less than 4.0 ounces per square yard. In an embodiment, the PTFE has a basis weight of less than 5.0 ounces per square yard.
Example media was produced using two different spunbond materials. The first media produced filter elements with HEPA performance, while the second media produced filter elements with non-HEPA performance. Thus the first media is an example of media made in accordance with HEPA properties, while the second media is a comparative example of media that does not demonstrate HEPA properties.
The PTFE used in the examples had a basis weight of 0.054 oz/yd2 and a perm of 3.0 CFM. The substrate material had properties as provided below in Table 1. Fiber sizing was analyzed using SEM images and Scandium® software program. A minimum of 30 measurements over a minimum of 5 different areas were averaged for results. For SEM, the samples were mounted on aluminum stubs, sputter coated with 60:40 Au:Pd, and imaged on the JSM-7100F.
Further aspects of the present subject matter include the following:
It should be noted that, as used in this specification and the appended claims, the singular forms “a,” “an,” and “the” include plural referents unless the content clearly dictates otherwise. It should also be noted that the term “or” is generally employed in its sense including “and/or” unless the content clearly dictates otherwise.
It should also be noted that, as used in this specification and the appended claims, the phrase “configured” describes a system, apparatus, or other structure that is constructed or configured to perform a particular task or adopt a particular configuration. The phrase “configured” can be used interchangeably with other similar phrases such as arranged and configured, constructed and arranged, constructed, manufactured and arranged, and the like.
All publications and patent applications in this specification are indicative of the level of ordinary skill in the art to which this invention pertains. All publications and patent applications are herein incorporated by reference to the same extent as if each individual publication or patent application was specifically and individually indicated by reference.
As used herein, the recitation of numerical ranges by endpoints shall include all numbers subsumed within that range (e.g., 2 to 8 includes 2.1, 2.8, 5.3, 7, etc.).
The headings used herein are provided for consistency with suggestions under 37 CFR 1.77 or otherwise to provide organizational cues. These headings shall not be viewed to limit or characterize the invention(s) set out in any claims that may issue from this disclosure. As an example, although the headings refer to a “Field,” such claims should not be limited by the lang34uage chosen under this heading to describe the so-called technical field. Further, a description of a technology in the “Background” is not an admission that technology is prior art to any invention(s) in this disclosure. Neither is the “Summary” to be considered as a characterization of the invention(s) set forth in issued claims.
The embodiments described herein are not intended to be exhaustive or to limit the invention to the precise forms disclosed in the following detailed description. Rather, the embodiments are chosen and described so that others skilled in the art can appreciate and understand the principles and practices. As such, aspects have been described with reference to various specific and preferred embodiments and techniques. However, it should be understood that many variations and modifications may be made while remaining within the spirit and scope herein.
This application is being filed as a PCT International Patent application on Sep. 22, 2022 in the name of Donaldson Company, Inc., a U.S. national corporation, applicant for the designation of all countries and Rakesh K. Yadav, Daniel L. Tuma, Robert R. Levac, Byron G. Griffin, Jonathan M. Beckett, Anil Suthar and Robert J. Pannepacker, Jr., all Citizens of the U.S., inventors for the designation of all countries and claims priority to U.S. Provisional Patent Application No. 63/248,270, filed Sep. 24, 2021, the content of which is herein incorporated by reference in its entirety.
Filing Document | Filing Date | Country | Kind |
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PCT/US2022/044395 | 9/22/2022 | WO |
Number | Date | Country | |
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63248270 | Sep 2021 | US |