This invention relates generally to fluid dispense systems. More particularly, the invention relates to dispense head and drum insert assemblies for use with caustic and high purity fluid containers.
High purity and highly corrosive liquids are often utilized in industries such as semiconductor processing and chemical manufacturing. Due to quality and safety concerns, these liquids generally must be contained in high integrity containers and dispensed using highly reliable dispensing systems.
Conventionally, the containers are drums formed of high purity polyethylene, such as those described in U.S. Pat. No. 6,045,000. Examples of dispensing systems suitable for use with these drums are described in U.S. Pat. Nos. 4,699,298, 5,108,015, 5,957,328, and 5,526,956. The connections, tubing, and fittings for handling these fluids are often formed from inert materials, such as various fluoropolymers. The tubing is commonly formed of Per Fluor Alkoxy (“PFA”), while the fittings and valve components can be formed of components such as PFA, Poly Tetra Fluoro Ethylene (“PTFE”), and other various fluoropolymers.
Conventional drums often include a bung opening and a drum insert connected to an upward and concentric nipple on the bung. A dispense head can be operably coupled with the drum insert and can include a main fluid passageway that connects to and sealingly engages the bung.
In many applications, the fluid that is dispensed from the drum can later be recirculated to the drum. This has been accomplished by using a recirculation passageway in the dispense head. However, these recirculation passageways can be uncontrolled and thus can remain in an open position when the dispense head is not connected to the drum, which can create a potential for spillage.
Also, recirculated fluid can create foam that can cause problems, such as foam entry into the vent lines, potential clogging, contamination of normally dry areas of the dispense head and gas refill line, and difficulty in emptying a drum with low levels of fluid. The foam can be created when fluid is recirculated into the dispense head and further when recirculated fluid is dispensed into the drum.
When using dispense heads to draw high purity, highly corrosive, and highly caustic liquids from drums, it can be important not to connect a dispense head for equipment requiring one type of liquid to a drum containing an incorrect or incompatible different liquid. To inhibit this, coded indexing sections and recesses have been provided in the dispense head and drum insert to enable assembly of the drum insert to the dispense head only when the correct coding exists. However, connecting a coded dispense head to a coded drum insert can require a great amount of force while turning the coding and holding down the dispense head. This process can involve a two-step operation of holding down the dispense head with one hand while rotating the code key with the other.
The fluid dispense system of the present invention provides a valve within the main fluid and recirculation passageways to automatically cut off the flow in the passageways when the dispense head is removed from the drum. The main fluid and recirculation passageways through the dispense head can be controlled by these valve assemblies, which can open when the dispense head is operably coupled with the drum insert and close when the dispense head is removed from the drum insert.
In addition, the fluid dispense system of the present invention decreases the amount of foam created during the recirculation of surfactant fluid into the dispense head and drum. The dispense head can include a recirculated fluid conduit that discharges recirculated fluid into the annular space around the drum insert down tube. A foam reduction diffuser can further reduce or eliminate foam that can be created during this recirculation process.
The fluid dispense system of the present invention also eases connection of a coded dispense head to a coded drum insert can by including a coupling assembly and method for quickly and easily coupling the dispense head to a drum insert.
In an aspect, the present invention relates to a fluid dispense system for use with a drum comprising a drum insert configured to operably couple with a bung included on a drum, the drum insert having an upper portion and a drum insert down tube extending therefrom into an interior of the drum and a dispense head configured to operably couple with the drum insert, the dispense head having a first conduit comprising a first valve assembly and a second conduit comprising a second valve assembly, the first and second valve assemblies in operable communication with the drum insert when the dispense head is operably coupled with the drum insert, such that when the dispense head is operably coupled with the drum insert the first and second valve assemblies can be effected to an open position enabling fluid to flow through the conduits, and when the dispense head is not operably coupled with the drum insert the first and second valve assemblies can be biased to a closed position inhibiting fluid from flowing through the conduits.
The second valve assembly can comprise a poppet valve including a poppet member and a biasing member to bias the poppet member to the closed position. The drum insert can comprise an actuation rib effecting the poppet valve to the open position when the dispense head is operably coupled with the drum insert.
The second conduit can comprise a recirculation fluid conduit enabling fluid to be returned to the interior of the drum through the recirculation fluid conduit. The first fluid conduit can comprise a main fluid conduit in fluid communication with a tube conduit included in the drum insert down tube and the recirculation fluid conduit can be in fluid communication with a media return conduit defined by the drum insert down tube and a diffuser down tube, the diffuser down tube further comprising a deflector proximate a lower end thereof.
A foaming reduction member can be included on the diffuser to reduce foaming of recirculated fluid prior to returning to the drum through the recirculation fluid conduit. The foaming reduction member can comprise a foam reduction chamber such that gas can be separated from the recirculated fluid and the gas can be vented from the chamber and the fluid flows out of the chamber and through the media return conduit.
The dispense head can further comprise a vent conduit enabling gas to enter and leave the drum through the vent conduit and a seal verification conduit in fluid communication with an aperture intermediate two seals at a junction between the operably coupled dispense head and drum insert.
In another aspect, the present invention relates to a method of using a fluid dispense system for use with a drum comprising inserting a drum insert into an access opening of a drum such that a drum insert down tube of the drum insert extends into an interior of the drum, operably coupling an upper portion of the drum insert with the access opening of the drum, providing a dispense head having a first conduit comprising a first valve assembly and a second conduit comprising a second valve assembly, and operably coupling the dispense head to the drum insert such that the first and second valve assemblies can be effected into an open position enabling fluid to flow through the respective first and second conduits.
Fluid can be directed out of the drum via the first conduit when the first valve assembly is in the open position and returned to the drum via the second conduit when the second valve assembly is in the open position.
A foaming reduction member can be provided within the drum insert, the foam reduction member having a foam reduction chamber, such that gas can be separated from recirculated fluid in the foam reduction chamber. Gas can be vented from the foam reduction chamber and liquid enabled to flow out of the foam reduction chamber to an interior of the drum. A vent conduit can be provided on the on the dispense head enabling gas to enter and leave the drum through the vent conduit. A seal verification conduit can be provided on the dispense head, the seal verification conduit in fluid communication with an aperture intermediate two seals positioned at a junction between the dispense head and the drum insert, such that the seal verification conduit can be used to verify an integrity of the seals.
In a further aspect, the present invention relates to a coupling assembly for coupling a dispense head to a drum insert for use in a fluid dispense system, the coupling assembly comprising a retaining ring having a plurality of detents disposed on an inner surface thereof and a collar having a code ring disposed thereon, the retaining ring and collar independently rotatable when the coupling assembly is not in engageable communication with the drum insert, the collar further comprising an internal flange having a flange surface and a plurality of engagement members displaceable between a biased position below the flange surface and an engagement position above the flange surface, and wherein when the coupling assembly is placed into engageable communication with the drum insert, the engagement members can be displaced to the engagement position and engageable with the detents, such that the collar can be rotatably with retaining ring to selectively align the code ring with a coded section disposed on the drum insert.
The coupling assembly can include a first threaded portion on the inner surface of the retaining ring and a second threaded portion on an external surface of the drum insert such that the coupling assembly can be selectively coupled with the drum insert by threading the first threaded portion with the second threaded portion. The coupling assembly can further include a snap member disposed on the collar and a snap receiving notch disposed on the code ring, the code ring and collar selectively engageable by engaging the snap member and snap receiving notch. The retaining ring, collar, and code ring can be constructed of high-density polyethylene (HDPE).
In yet another aspect, the present invention relates to a method of coupling a dispense head to a drum insert in a fluid dispense system comprising providing a coupling assembly comprising a retaining ring having a plurality of detents disposed on an inner surface thereof and a collar having a code ring operably coupled thereto, operably coupling the retaining ring to the dispense head, operably coupling the collar to the dispense head, the collar further comprising an internal flange having a flange surface and a plurality of engagement members movable between a biased position below the flange surface and an engagement position above the flange surface, such that the retaining ring and collar can be independently rotatable when the coupling assembly is not in engageable communication with the drum insert, placing at least a portion of the coupling assembly into communication with the drum insert, effecting a force on the coupling assembly such that the engagement members can be displaced to the engagement position and engage with the detents, such that the collar can be rotatable dependent of the retaining ring, rotating the retaining ring to selectively align the code ring with a coded section disposed on the upper portion of the drum insert, and operably coupling the coupling assembly with the drum insert.
First indicia can be provided on the code ring and second indicia can be included on the coded section on the drum insert, such that step of rotating the retaining ring to selectively align the code ring with the coded section can comprise matching the first indicia with the second indicia.
In another aspect, the present invention relates to a method of reducing foaming while recirculating fluid into a drum through a dispense head, the method comprising inserting a drum insert having a down tube extending therefrom into an access opening of a drum such that the drum insert down tube of the drum insert extends into an interior of the drum, operably coupling an upper portion of the drum insert with the access opening of the drum, operably coupling the dispense head with the upper portion of the drum insert, the dispense head including a main fluid conduit and a recirculation fluid conduit in the dispense head, the main fluid conduit in fluid communication with an interior surface of the drum insert down tube and the recirculation fluid conduit in communication with a media return conduit defined by an external surface of the drum insert down tube and a diffuser down tube, the diffuser down tube comprising a deflector at a lower end thereof, and recirculating fluid into the drum through the recirculation fluid conduit into the media return conduit, such that the recirculating fluid passes over the deflector, the deflector reducing foaming of fluid returning to the drum.
The method can further include recirculating fluid through a foam reduction chamber disposed proximate an upper end of the diffuser down tube, the foam reduction chamber separating gas from fluid and discharging the gas through vents that can be connected to a venting port included on the dispense head, while the recirculating fluid flows downwardly through the media return conduit. The deflector can be positioned below the liquid level of fluid in the drum.
In a further aspect, the present invention relates to a fluid dispense system for use with a drum comprising a drum insert configured to couple an access opening of a drum, the drum insert having an upper portion and a drum insert down tube extending therefrom into an interior of the drum and a dispense head comprising means for coupling the dispense head to the drum insert, the dispense head having a first fluid conduit comprising a first valve means and a second conduit comprising a second valve means, the first and second valve means in communication with the drum insert when the dispense head is operably coupled with the drum insert, such that when the dispense head is operably coupled with the drum insert the first and second valve means can be in an open position enabling fluid to flow through the conduits, and when the dispense head is not operably coupled with the drum insert the first and second valve means can be biased to a closed position inhibiting fluid from flowing through the conduits.
In yet another aspect, the present invention relates to a fluid dispense system for use with a drum comprising a drum insert configured to couple a bung included on a drum, the drum insert having an upper portion and a drum insert down tube extending therefrom into an interior of the drum and a dispense head configured to couple the drum insert, the dispense head having a first fluid conduit comprising a first valve assembly and a seal verification port in fluid communication with a seal verification conduit and an aperture intermediate two seals at a junction between the dispense head and the drum insert, the aperture being substantially transverse the seal verification conduit, such that an integrity of a sealing between the dispense head and drum insert can be verified by forcing air into the seal verification port. The two seals can be O-rings, which can be encapsulated with polytetrafluoroethylene (PTFE).
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The drum 20 can be constructed of single or multiple layers, such as polymer layers, and can be formed in a blow molding process. While the drum can be constructed of a blow molded polymer, such as blow molded polyethylene, those skilled in the art will recognize that other polymer materials and forming processes can be used. Examples of drums 20 that can be employed with the various embodiments of the present invention are disclosed in U.S. Pat. No. 6,045,000 and U.S. Patent Application Publication No. 2002/0050494, both of which are incorporated herein by reference.
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In operation, the diffuser 44 can receive recirculated fluid that has first moved through the dispense head 24 and then through a plurality of annular recirculation conduits 69 (
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The deflector 51 is depicted as a peripheral flange and can scatter the dispensed recirculated fluid outwardly and generally laterally to provide better recirculation and reduce the formation of foam as the recirculated fluid is introduced into the drum 20. The deflector 51 can be positioned such that the recirculated fluid is returned to the drum 20 through the media return conduit 43 and out of the deflector 51 or an exiting portion of the down tube 31 below or above the liquid level in the drum, thus inhibiting the foaming of the recirculated fluid as it is reintroduced into the drum 20. As a result, the diffuser 44 can inhibit turbulent flow of the fluid, which can be present in conventional system as fluid is discharged directly into a drum and into the top level of the fluid in the drum 20. The deflector 51 can be positioned at any point along the down tube 31.
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The ports 62, 64 can provide connection to a main fluid conduit 66 and main recirculation conduit 68, respectively, and both conduits 66, 68 can run from the upper body section 52 to the lower body section 54. In addition, other ports and conduits for venting 65 and seal verification 63 can be implemented and employed in the dispense head 24.
The recirculation port 64 can be connected to the recirculation conduit 66 with corresponding threaded sections on the port 64 and conduit 68. By having multiple ports in a single dispense head 24, extra bungs 21 on a drum 20 can be freed for other uses, such as including a mixer on an additional bung that can be used to mix various slurries within the drum to inhibit settling of the solids in the drum.
The lower body section 54 of the dispense head 24 can include a plurality of O-rings 82a, 82b, and 82c and a main valve assembly 84. As depicted in
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The retaining ring 102 of the coupling assembly 80 includes a body portion 108, a threaded portion 110, and a plurality of interior drive apertures or detents 111 that are spaced on an interior surface of the retaining ring 102. In one embodiment, the body portion 108 also can include a plurality of gripping members 109 on an exterior surface of the retaining ring 102 to enable ease of gripping and rotating the coupling assembly 80.
The spring collar 104 of the coupling assembly 80 includes a retaining ring flange 112 having a flange surface 113, a plurality of snap members 114, and a plurality of drive lugs 116 having spring fingers 118. The spring collar 104 can be operably connected to the retaining ring 102 such that the retaining ring 102 spins freely on the retaining ring flange 112 when the dispense head 24 is not connected to the drum insert 22.
The key code ring 106 of the coupling assembly 80 includes a plurality of key sections 119. Examples of key code rings can be seen in U.S. Pat. No. 5,108,015, which is hereby incorporated by reference in its entirety. The key code ring 106 of the coupling assembly 80 in the various embodiments of the present invention can further include a plurality of snap receiving notches 122 spaced to correspond with the snap members 114 on the spring collar 104, and indicia 120 located on or intermediate the key sections 119. The key code ring 104 can be connected to the spring collar 104 by slidably engaging the key code ring 106 with the spring collar 104 until the snap members 114 engage the snap receiving notches 122.
To inhibit the key code ring 106 from rotating with respect to the spring collar 104, the key code ring 106 and spring collar 104 are provided with retaining tabs 115 and retaining grooves 117. A first retaining tab 115a can be provided on the spring collar 104 and corresponds with a first retaining groove 117a on the key code ring 106. A second retaining tab 115b can be provided on the key code ring 106 and corresponds with a second retaining groove 117b on the spring collar 104. The retaining tabs 115 engage the retaining grooves 117 when the key code ring 106 is connected to the spring collar 104, thus inhibiting the key code ring 106 from rotating with respect to the spring collar 104.
The retaining ring 102 and spring collar 104 are operably engaged or attached prior to coupling the dispense head 24 to the drum insert 22. In this position, the retaining ring 102 can spin freely on the retaining ring flange 112 of the retaining ring 102, and therefore the retaining ring 102 can spin freely with respect to the key code ring 106. In this position, the drive lugs 116 are below the flange surface 113 and therefore not engageable with the interior drive detents 111.
The coupling assembly 80 enables much easier connection of a coded dispense head 24 to a coded drum insert 22 than required by prior systems. To assemble the fluid dispense system 10, the dispense head 24, including the coupling assembly 80, can be first placed onto the drum insert 22. As the coupling assembly 80 is pushed downwardly, the key code ring 106 abuts against a top portion of the insert 72, causing the key code ring 106 to push on the spring fingers 118 so that the drive lugs 116 are forced above the flange surface 113. In this position, the drive lugs 116 are then engageable with the interior drive detents 111. When the drive lugs 116 engage with the interior drive detents 111, the drive lugs 116 inhibit the retaining ring 102 from spinning freely with respect to the key code ring 106 when the retaining ring 102 is rotated in a clockwise motion. Therefore, by rotating the retaining ring 102 in a clockwise motion, one can control the rotation of the key code ring 106 to align the key code ring 106 into alignment with a matching coded drum insert 22.
Once the key code ring 106 is rotated into alignment with a matching coded drum insert 22, the spring fingers 118 drive the key code ring 106 into the matching coded drum insert 22, causing the key code ring 106 to fall into position in the drum insert 22. In this position, the spring fingers 118 are relaxed and the drive lugs 116 fall below the flange surface 113 and thus out of reach of the interior drive detents 111, such that the retaining ring 102 can again spin freely on the retaining ring flange 112. By continuing to rotate the retaining ring 102 in a clockwise motion, the threaded portion 110 of the retaining ring 102 mates with the cap thread portion 32 of the upper portion 26 of the drum insert 22. This threading action continues to pull the dispense head 24 into the drum insert 22 to complete the sealing connection of the dispense head 24 to the drum insert 22.
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In order to verify that there is an adequate seal between the dispense head 24 and drum insert 22, air (such as compressed air) can be forced into the seal verification port 63. If there is a drop in pressure greater than a predetermined amount, this indicates that there is not an adequate seal between O-rings 82a, 82b, and thus between the dispense head 24 and drum insert 22, and adequate remedial measures must generally be taken to ensure that there is a proper seal. Otherwise, the seal is sufficient and dispensing of liquids from the drum is possible.
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The invention has been described above with reference to several embodiments thereof. It will be apparent to those skilled in the art that alterations may be made in the embodiments described without departing from the scope of the invention. Thus, the scope of the present invention should not be limited by the embodiments described herein, but rather by the language of the claims and the equivalents of those structures.
The present application claims the benefit of U.S. Provisional Application No. 60/669,945, filed Apr. 8, 2005, which is incorporated herein in its entirety by reference.
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