Hydraulic vessel system having a downwardly feeding separator

Information

  • Patent Grant
  • 6171494
  • Patent Number
    6,171,494
  • Date Filed
    Tuesday, February 17, 1998
    26 years ago
  • Date Issued
    Tuesday, January 9, 2001
    23 years ago
Abstract
A new and improved way of continuously cooking fiber material, wherein temperatures and alkaline levels are controlled to be maintained within specific levels in different zones of the digesting process in order to optimize chemical consumption and heat-economy and at the same time achieve very good pulp properties. The digesting process includes a top separator that separates the transport liquid from the fiber material and permits the fiber material to be exposed to the cooking liquid.
Description




TECHNICAL FIELD




The present invention relates to a novel top separator and a method for producing pulp, preferably sulphate cellulose, with the aid of a continuous digester system.




BACKGROUND AND SUMMARY OF THE INVENTION




Environmental demands has forced our industry to develop improved cooking and bleaching methods. One recent breakthrough within the field of cooking is ITC™, which was developed in 1992-1993. ITC™ is described in WO-9411566, which shows that very good results concerning the pulp quality may be achieved. ITC™ is mainly based on using almost the same temperature (relatively low compared to prior art) in all cooking zones in combination with moderate alkaline levels. The ITC™-concept does not merely relate to the equalization of temperatures between different cooking zones, but a considerable contribution of the ITC™-concept relates to enabling an equalized alkaline profile also in the lower part of the counter-current cooking zone.




Moreover, it is known that impregnation with the aid of black liquor can improve the strength properties of the fibers in the pulp produced. The aim of the impregnation is, in the first place, to thoroughly soak each chip so that it becomes susceptible, by penetration and diffusion, to the active cooking chemicals which, in the context of sulphate cellulose, principally consist of sodium hydroxide and sodium sulphide.




If, as is customary according to prior art, a large proportion of the white liquor is supplied in connection with the impregnation, there will exist no distinct border between impregnation and cooking. This leads to difficulties in optimizing the conditions in the transfer zone between impregnation and cooking.




Now it has been found that surprisingly good results can be achieved when:




1. Keeping a low temperature but a high alkali content in the beginning of a concurrent cooking zone of the digester;




2. Withdrawing a substantial part of a highly alkaline spent liquor that has passed through at least the concurrent cooking zone; and




3. Supplying a substantial portion of the withdrawn spent liquor that has a relatively high amount of rest-alkali, to a point that is adjacent the beginning of an impregnation zone.




This leads to a reduced H-factor demand, reduced consumption of cooking chemicals and better heat-economy. Additionally, the novel method leads to production of pulp that has a high quality and a very good bleachability, which means that bleach chemicals and methods can be chosen with a wider variety than before for reaching desired quality targets (brightness, yield, tear-strength, viscosity, etc.) of the finally bleached pulp.




Furthermore, we have found that these good results can also be achieved when moving in a direction opposite the general understanding of the ITC™-teaching, in connection with digesters having a counter-current cooking zone. Instead of trying to maintain almost the same temperature levels in the different cooking zones, we have found that when using a digester that has both a concurrent and a counter-current cooking zone, big advantages may be gained if the following basic steps are used:




1. Keeping a low temperature but a high alkali content in the concurrent zone of the digester;




2. Keeping a higher temperature but a lower alkali content in the counter-current zone;




3. Withdrawing a substantial part of the highly alkaline spent liquor that has passed through at least one digesting zone; and




4. Preferably supplying almost all of the withdrawn spent liquor, that has a relatively high amount rest-alkali, to a position that is adjacent the beginning of the impregnation zone.




Also, in connection with digesters of the one-vessel type (without a separate impregnation vessel), surprisingly good results are achieved when the basic principles of the invention are used.




Moreover, preliminary results indicate that the preferred manner of using the invention may be somewhat modified also in other respects but still achieving very good result, e.g., by excluding the counter-current cooking zone. Additionally, expensive equipment might be eliminated, e.g., strainers in the impregnation vessel, hanging central pipes, etc., making installations much easier and considerably less expensive.











BRIEF DESCRIPTION OF THE FIGURES





FIG. 1

is a schematic flow diagram of a preferred first embodiment of a digester system according to the present invention;





FIG. 2

is a cross-sectional view of a preferred first embodiment of a top separator to be used in an impregnation vessel or a single vessel digester according to the present invention;





FIG. 2A

is a cross-sectional view of a preferred second embodiment of a top separator to be used in a digester according to the present invention;





FIG. 3

is a schematic flow diagram of a preferred second embodiment of a digester system according to the present invention;





FIG. 4

is a schematic flow diagram of a preferred third embodiment of a digester system according to the present invention;





FIG. 5

is a schematic flow diagram of a preferred fourth embodiment of a digester system according to the present invention;





FIG. 6

is a schematic flow diagram of a preferred fifth embodiment of a digester system according to the present invention;





FIG. 7

is a schematic flow diagram of a preferred sixth embodiment of a digester system according to the present invention;





FIG. 8

is a schematic flow diagram of a preferred seventh embodiment of a digester system according to the present invention;





FIG. 9

is a schematic flow diagram of a preferred eighth embodiment of a digester system according to the present invention;





FIG. 10

is a schematic flow diagram of a preferred ninth embodiment of a digester system according to the present invention;





FIG. 11

is a schematic flow diagram of a preferred tenth embodiment of a digester system according to the present invention;





FIG. 12

is a schematic flow diagram of a preferred eleventh embodiment of a digester system according to the present invention;





FIG. 13

is a schematic flow diagram of a preferred twelfth embodiment of a digester system according to the present invention; and





FIG. 14

is a cross-sectional view of a preferred third embodiment of a top separator of the present invention.











DETAILED DESCRIPTION




The preferred embodiments of the present invention are described with reference to FIGS.


1


-


14


.

FIG. 1

shows a preferred first embodiment of a two vessel hydraulic digester for producing chemical pulp according to the present invention. The main components of the digesting system consist of an impregnation vessel


1


and a hydraulic digester


6


. It is to be understood that both the digester and the impregnation vessel may be hydraulic vessels that are totally filled with, among other things, a liquid.




The impregnation vessel


1


, which normally is totally liquid filled, includes a feeding-in device


2


at the top. The feeding-in device may be of a conventional type, i.e., a top separator having a screw-feeding device that feeds the chips in a downward direction at the same time as a transport liquid is drawn off. Other types of top separators may also be used. At the bottom, the impregnation vessel


1


has a feeding-out device


3


comprising a bottom scraper. In addition to this, there is a conduit


17


that extends from the digester


6


to the impregnation vessel


1


for adding hot black liquor. As seen in

FIG. 1

, the black liquor is preferably supplied to the top of the impregnation vessel


1


. In contrast to conventional impregnation vessels, no draw-off screen is located inside the impregnation vessel. However, such draw-off screen may be provided if desired.




The chips are fed from the chip bin


20


A, through the steaming vessel


20


B and the chip chute


20


C. A feeding preferably a high-pressure feeder


19


, feeds the chips suspended in a transport liquid via a conduit


18


to the top of the impregnation vessel


1


. The feeder


19


is cooperating with the chute


20


C, and is connected to the necessary liquid circulations and replenishment.




A conduit


21


, for transporting chips and a transport liquid D, extends from the bottom of the impregnation vessel


1


up to the top


5


of the digester


6


. Conduit


21


opens up at the top of a top separator


7


which feeds by means of a screw in an downwardly moving direction.




The screen of the separator may be used to draw off the transport liquid D (which is then returned in line


15


) together with which the chips are transported from the impregnation vessel


1


up to the top


5


of the digester. Below the top separator


7


there are inlet openings


37


defined that are in operative engagement with a conduit


24


which (preferably via a heat-exchanger


13


) leads to a cooking liquor supply such as a white-liquor container (not shown). The heat-exchanger


13


is connected to a high pressure steam conduit


102


and heats up the white liquor to a suitable temperature before the white liquor enters the top


5


. As best seen in

FIG. 1

, approximately 95% of the total supply of the white liquor in the conduit


24


is supplied to the top


5


of the digester and the remaining 5% is supplied to the high pressure feeder


19


via a conduit


132


and a conduit


134


to lubricate the high pressure feeder


19


. About 90% of the white liquor in the conduit


24


is supplied to the top of the digester, the remaining 10% is supplied to the counter-current zone D via a conduit


123


.




A first screen girdle section


8


may be arranged in conjunction with a step-out approximately in the middle of the digester


6


. If the digester


6


is an MCC digester, the screen section may be used to withdraw spent liquor that is conducted to a recovery unit. Draw-off from this screen girdle section


8


can also be conducted directly via the conduit


17


to the impregnation vessel


1


. A second screen girdle section


104


may be arranged below the first screen girdle section


8


(in an MCC digester, the screen girdle section


104


would normally be called the MCC screen). Draw-off from the second screen section


104


, such as spent liquor, i.e., black liquor, may be conducted via a conduit


106


to a first flash tank


108


to recover steam and let pressure off before the liquor is conducted to a recovery unit


110


. Preferably, the spent liquor is also conducted through a second flash tank


112


via a conduit


114


to further reduce the pressure and temperature of the spent liquor before the liquor is conducted to the recovery unit


110


. In the preferred embodiment, a conduit


124


conducts the spent liquor from the return conduit


15


(preferably at least 3 m


3


/ADT) to the second flash tank


112


. The spent liquor from both flash tanks


108


,


112


is then conducted with a conduit


126


to the recovery unit


110


. Conduits


128


and


130


may be connected to the flash tanks


108


,


112


, respectively, to supply steam to the chip bin


20


A and the steaming vessel


20


B.




At the bottom


10


of the digester, there is a feeding-out device including one scraping element


22


. A third lower screen girdle section


12


is disposed at the bottom


10


of the digester


6


. The girdle section


12


may, for example, include three rows of screens for withdrawing liquid, which is heated and to which some white liquor, preferably about 10% of the total amount of the white liquor in conduit


24


, is added via a branch conduit


117


before it is recirculated by means of a central pipe


123


, which opens up at about the same level as the lowermost strainer girdle


12


.




The draw-off from the screen girdles


12


and the white liquor from the branch conduit


117


are preferably conducted via a heat exchanger


120


back to the bottom


10


of the digester


6


. The temperature of this draw off is about 140° C. since it is a mix of washing liquid and black liquor. The white liquor is supplied in a counter-current direction via the central pipe


123


to the screen girdle section


12


. The white liquor provides fresh alkali and, in the form of counter-current cooking, further reducing the Kappa number. A conduit


122


is connected to the high pressure steam conduit


102


to provide the heat exchanger with steam to regulate the temperature of the liquid supplied via the standpipe


123


. A blow line


26


is connected to the bottom


10


of the digester for conducting the digested pulp away from the digester


6


.




A preferred installation according to the present invention, as shown in

FIG. 1

, may function as follows. The chips are fed in a conventional manner into the chip bin


20


A and are subsequently steamed in the vessel


20


B and, thereafter, conveyed into the chute


20


C. The high-pressure feeder


19


, which is supplied with a minor amount of white liquor (approximately 5% of the total amount to lubricate the feeder), feeds the chips into the conduit


18


together with the transport liquid. The slurry of chips and transport liquid are fed to the top of the impregnation vessel


1


and may have a temperature of about 110° C. to 120° C. when entering the impregnation vessel (excluding recirculated transport liquor).




In addition to the actual fibers in the wood, the latter also conveys its own moisture (the wood moisture), which normally constitutes about 50% of the original weight, to the impregnation vessel


1


. Over and above this, some condense is present from the steaming, i.e., at least a part of the steam (principally low-pressure steam) which was supplied to the steaming vessel


20


B is cooled down to such a low level that it condenses and is then recovered as liquid together with the wood and the transport liquid.




Inside the top of the impregnation vessel


1


, the screw feeder


2


pushes the chips in a downward direction. No liquid is necessarily recirculated within the impregnation vessel


1


. Instead, spent liquor, such as black liquor, from the screen girdle section


8


is preferably supplied to the impregnation vessel


1


. However, it is to be understood that liquid may be recirculated within the impregnation vessel


1


.




The chips which are fed out from the bottom of the top screen


2


of the impregnation vessel


1


then move slowly downwards in a plug flow through the impregnation vessel


1


in a liquid/wood ratio between 2/1-10/1 preferably between 3/1-8/1, more preferred of about 4/1-6/1. Hot black liquor, which is drawn off from the screen girdle section


8


, may be added, via the conduit


17


, to the top of the impregnation vessel


1


. The black liquor may also be added to other sections of the impregnation vessel such as to an intermediate section of the impregnation vessel. The high temperature of the black liquor (100° C. to 160° C.), preferably exceeding 130° C., more preferred between 130° C. to 160° C., ensures rapid heating of the chips flowing through the impregnation vessel


1


. In addition, the relatively high pH, exceeding pH 10, of the black liquor neutralizes acidic groups in the wood and also any acidic condensate accompanying the chips, thereby, i.e., counteracting the formation of encrustation, so-called scaling.




An additional advantage of the method of the present invention is that the black liquor supplied into the impregnation vessel


1


has a high content of rest alkali, (effective alkali EA as NaOH), at least 13 g/l, preferably about or above 16 g/l and more preferred between 13-30 g/l at the top of the impregnation vessel


1


. This alkali mainly comes from the black liquor due to the high amount of alkali in the concurrent zone B of the digester


6


. Furthermore, the strength properties of the fibers are positively affected by the impregnation because of the high amount of sulphide. A major portion of the black liquor may be directly (or via one flash) fed into the impregnation vessel


1


. A minor amount of the black liquor (not shown) may be used for transferring the chips from the high pressure feeder


19


to the inlet of the impregnation vessel


1


.




The minor flow of the black liquor should be cooled (not shown) before it is entered into the feeder


19


. The two flows of black liquor are preferably used to regulate the temperature within an impregnation zone A disposed inside the impregnation vessel


1


. In the preferred embodiment, the temperature should not exceed 140° C. However, it should be understood that the temperature may exceed 140° C. The total supply of black liquor to the impregnation vessel


1


may exceed 80% of the amount drawn off from the draw-off strainers


8


, preferably more than 90% and most preferred about 100% of the total flow, which normally is about 8-12 m


3


/ADT.




The retention time in the impregnation zone A should be at least 20 minutes, preferably at least 30 minutes and more preferred at least 40 minutes. However, a shorter retention time than 20 minutes, such as 15-20 minutes may also be used. The volume of the impregnation vessel


1


may be larger than 1/11, preferably larger than 1/10 of the volume of the digester


6


. Additionally, in the preferred embodiment, the volume V of the impregnation vessel


1


should exceed 5 times the value of the square of the maximum digester diameter, i.e., V=5D


2


, where D is the maximum diameter of the digester


6


.




From tests made in lab-scale, we have found indications that it is desirable to keep the alkaline level at above at least 2 g/l, preferably above 4 g/l, in the impregnation vessel


1


in connection with black liquor, which would normally correspond to a pH of about 11. If not, it appears that dissolved lignin precipitates and even condenses.




The chips, which have been thoroughly impregnated and partially delignified in the impregnation vessel


1


, may be fed to the top of the digester


6


and conveyed into the downwardly-feeding top separator


7


. The chips are thus fed downwards through the screen, meanwhile free transport liquid may be withdrawn outwardly through the separator screen. Before the chips enter the concurrent cooking zone B, the chips pieces are drained with cooking liquor, such as white liquor, which is supplied by means of the annular openings


37


at the top separator


7


that are defined in a cylindrical portion


39


of the digester


6


(see FIG.


2


).




The digester


6


also has a large diameter portion


41


disposed below the cylindrical portion


39


. The quantity of white liquor that is added at the top separator


7


depends on how much white liquor possibly is added else where, but the total amount corresponds to the quantity of white liquor that is required to achieve the desired delignification of the wood chips. Preferably, a major part of the white liquor is added here, i.e., more than 60%, which also improves the diffusion velocity, since it increases in relation to the concentration difference (chip-surrounding liquid). The thoroughly impregnated chips very rapidly assimilate the active cooking chemicals by diffusion, since the concentration of alkali (EA as NaOH) is relatively high, at least 20 g/l, preferably between 30 g/l and 50 g/l and more preferred about 40 g/l.




The chips then move down in the concurrent zones B, C through the digester


6


at a relatively low cooking temperature, i.e., between 130 ° C. to 160° C., preferably about 140° C. to 150° C. The major part of the delignification takes place in the first and second concurrent cooking zones B, C.




The liquid-wood ratio should be at least 2/1 and should be below 7/1, preferably in the range of 3/1-5.5/1, more preferred between 3.5/1 and 5/1. (The liquid wood-ratio in the counter-current cooking zone should be about the same as in the concurrent cooking zones.)




The temperature in a lower counter-current zone D is preferably higher than in the concurrent zones B, C, i.e., preferably exceeding 140° C., preferably about 145° C. to 165° C. in order to dissolve remaining lignin. The alkali content in the lowermost part of the concurrent cooking zone C should preferably be lower than in the beginning of the concurrent zone B, above 5 g/l, but below 40 g/l. Preferably less than 30 g/l and more preferred between 10-20 g/l. Expediently, the conduit


116


may be charged with about 5-20%, preferably 10-15%, white liquor from the conduit


24


via the conduit


117


. Below the draw-off screen section


104


is the counter-current zone D that is defined between the section


104


and the section


12


.




The temperature of the liquid which is recirculated via the pipe


123


up to the screen girdle section


12


is regulated with the aid of the heat exchanger


120


so that the desired cooking temperature is obtained at the lowermost part of the counter-current cooking zone D.




At the lowermost part of the digester, cool wash liquid is added in order to displace, in counter-current, hot liquid which is subsequently withdrawn at the lowermost screen girdle


12


.





FIG. 2

shows a preferred embodiment of a separator that may be used together with an impregnation vessel that is part of a digester system, such as the digester system shown in

FIG. 1

, where there is a need for a heat seal. The advantage of providing the heat seal in the separator is to enable the injection of hot black liquor below the separator without risking to operate the high pressure feeder at too high of a temperature. The heat seal reduces or even eliminates the risk of any hot liquor being inadvertently conducted back to the high pressure feeder which may damage the feeder. It is to be understood that the separator may also be used in an impregnation vessel that is connected to a steam/vapor phase digester and the separator may be used in a single-vessel hydraulic digester.




Only a portion of a an impregnation vessel


1


is shown. The non-impregnated slurred fiber material is transferred to the top of the digester by means of the transfer line


21


and enters an in-let space


30


of a screw-feeder


31


. The screw-feeder


31


is attached to a shaft


32


connected to a drive-unit


33


which is attached to a mounting-plate


34


at the top of the digester shell


6


. The drive-shaft


32


is rotated in a direction so as to force the screw to feed the chips and the transport fluid in a downward direction.




A cylindrical screen-basket


35


surrounds the screw-feeder


31


. The screen-basket


35


is arranged within the digester shell


6


so as to define a liquid collecting space


36


between the digester shell and the outer surface of the screen-basket


35


. The liquid collecting space


36


, which preferably is annular, communicates with a conduit


15


for withdrawing liquid from the liquid collecting space


36


, which in turn is replenished by liquid from the slurry within the screen basket


35


. The major part of the free liquid within the slurry entering the screen basket is withdrawn into the liquid collecting space


36


, but a small portion of free liquid, at least about 0.5 m


3


/ADT should not be withdrawn from the slurry.




A set of level sensors


60


are positioned along a side wall of the digester


6


to sense the level in the digester. The level sensors are disposed below the screw-feeder


31


but above the pair of liquid supply devices


37


. A top section


62


of the digester


6


has a diameter (d) that is less than a diameter (D) of the digester at a mid-portion and bottom portion thereof. The diameter (d) is small to reduce or even avoid any substantial heat transfer to the T-C lines so that the T-C lines may maintain a temperature that is slightly above 100° C. In this way, a heat lock zone


64


is formed between the liquid supply devices


37


and the top of the level sensors


60


. Preferably, the heat lock zone


64


has a length h that is greater than the diameter d where h is the distance between the lower edge of the screen


35


and the transition zone and d is the diameter of the separator at its upper end, as described earlier. It is to be understood that the heat lock zone may have any other suitable length.




The liquid supply device


37


preferably comprises an annular distribution ring


38


which has a number of supply conduits


37


disposed between the ring and the impregnation vessel


1


. The supply conduits


37


open up into the chips pile for supply of liquid into the fiber material moving down into the impregnation vessel


1


. The annular distribution ring


38


is replenished by means of the conduit


24


wherein a desired amount of liquid is supplied. The liquid supplied through the liquid supply device


37


and ring


38


may be hot black liquor having a relatively high amount of effective alkaline, in order to provide for the possibility of establishing a concurrent impregnation zone (B) having a desired temperature of about 120° C. to 145° C., and a desired content of effective alkaline, of about 10-20 g/l.




In

FIG. 2A

, there is shown a simpler separation device intended for a two-vessel hydraulic digester. If the separator shown in

FIG. 2A

is used in an impregnation vessel (that is part of a two vessel steam/vapor phase digester system) the separator works exactly in the same way. The heat-seal eliminates any risk of obtaining any hot return-liquid in return line


15


which could cause problems with the operation of the high pressure feeder. Only a part of the top of the digester


6




s


is shown. The slurred fiber material is transferred to the top of the digester by means of a transfer line


21




s


and enters an in-let space


30




s


of a screw-feeder


31




s


. The screw-feeder


31




s


is attached to a shaft


32




s


connected to a drive-unit


33




s


which is attached to a mounting-plate


34




s


on the top of the digester shell


6




s


. The drive-shaft


32




s


is rotated in a direction so as to force the screw to feed in a down-ward direction.




A cylindrical screen-basket


35




s


surrounds the screw-feeder


31




s


. The screen-basket


35




s


is arranged within the digester shell


6




s


so as to form a liquid collecting space


36




s


between the digester shell and the outer surface of the screen-basket


35




s


. The liquid collecting space


36




s


, which preferably is annular, communicates with a conduit


15




s


for withdrawing liquid from the liquid collecting space


36




s


, which in turn is replenished by liquid from the slurry within the screen basket


35




s


. The major part of the free liquid within the slurry entering the screen basket is withdrawn into the liquid collecting space


36




s


, but a small portion of free liquid, at least about 0.5 m


3


/ADT should not be withdrawn from the slurry.




Below the outlet end of the screen basket


35




s


there is arranged a pair of liquid supply devices


37




s


, each preferably comprising an annular distribution ring which opens up into the chips pile for supply of liquid into the fiber material moving down into the digester


6




s


. The liquid supply devices


37




s


are replenished by means of lines


24




s


wherein a desired amount of liquid is supplied. If it is a two-vessel hydraulic digester system, the liquid supplied through the liquid supply devices


37




s


would be hot cooking liquor having a relatively high amount of effective alkaline, in order to provide for the possibility of establishing a concurrent cooking zone (B) having a desired temperature of about 145-150° C., and a desired content of effective alkaline, e.g. about 45 g/l.




A major advantage with both kinds of the shown separation devices is that they provide for establishing a distinguished change of zones (they enable almost a total exchange of free liquid at this point), which means that the desired conditions in the beginning of the concurrent zone (B) can easily be established.





FIG. 3

illustrates an second embodiment of the hydraulic digester system of the present invention. This embodiment is almost identical to the embodiment shown in FIG.


1


. Only the main differences are therefore described. It relates to a two-vessel hydraulic digester which, but with a cupped gable at the top of the digester in which the downwardly feeding separator is positioned. A screen girdle section


38




a


(which normally would have existed prior to converting the system according to the present invention) is disposed at the bottom of an impregnation vessel


1




a


. Spent liquor is withdrawn at the girdle section


38




a


and conducted via a conduit


34




a


to a second flash tank


112




a


to be further conducted to a recovery unit, as described in

FIG. 1. A

conduit


36




a


extends between a return conduit


15




a


and a conduit


24




a


so that a portion of the white liquor in the conduit


24




a


is conducted via the conduit


36




a


to the return line


15




a


. Instead of conducting the white liquor in the conduit


24




a


up to the top of a digester


6




a


, the conduit


24




a


is connected to the conduit


116




a


so that about 90% of the white liquor in the conduit


24




a


is conducted to the conduit


116




a


. The remaining parts of this embodiment operates in a way that is very similar to the embodiment described in FIG.


1


.





FIG. 4

also shows a hydraulic digester, being the third embodiment of the present invention. Only the new features of this embodiment compared to the first embodiment are described. A conduit


106




b


attached to a digester


6




b


conducts spent liquor that has been withdrawn from a screen section


104




b


to the top of an impregnation vessel


1




b


. A portion of the spent liquor withdrawn in the conduit


106




b


is diverted via a conduit


107




b


to a first flash tank


108




b


and then via a conduit


114




b


to a second flash tank


112




b


. It should be noted that the third embodiment does not have a screen girdle section at the upper end of the digester


6




b.







FIG. 5

describes a fourth embodiment of the present invention. A digester


6




c


has a first screen girdle section


8




c


disposed therein. Spent liquor is withdrawn from the girdle section


8




c


via a conduit


109




c


to a second flash tank


112




c


. The spent liquor withdrawn from the girdle section


8




c


has a low effective alkali value that is below 12 g/l.




The digester


6




c


also has a second screen girdle section


11




c


immediately below the first screen girdle section


208




d


. Liquor is withdrawn from the second screen girdle section via a conduit


113




c


. A conduit


24




c


conducts white liquor so that approximately 5% to 15% of the white liquor in the conduit


24




c


is diverted via a conduit


117




c


to a conduit


116




c


that is connected to a lower screen girdle section


12




c


. The remaining amount of white liquor in the conduit


24




c


is conducted up to the conduit


113




c


. The liquor withdrawn from the screen girdle section


11




c


together with the white liquor from the conduit


24




c


is via a central pipe conducted back into the digester at about the same level as the screen girdle section


8




c


. With this embodiment, the impregnation zone is prolonged to also include the upper zone of the digester, i.e., to the screen


8




c


. Below the screen


8




c


, the cooking zone commences at the point there the conduit


113




c


opens up. The cooling liquor is then radially, uniformly displaced/mixed into the chips column by means of withdrawing and recirculating liquor with the screen


11




c.






In the preferred fourth embodiment, the conduit


113




c


is associated with a heat exchanger


115




c


to regulate the temperature of the black liquor and the white liquor which is to be reintroduced by the conduit


113




c


. The heat exchanger is adapted to receive steam via a conduit


217




c


that is connected to a main high pressure steam conduit


102




c


. Similar to the embodiment shown in

FIG. 1

, spent liquor is also withdrawn from a screen girdle section


104




c


and conducted back to an impregnation vessel


1




c


via a conduit


17




c


. The effective alkali of the spent liquor that is conducted in the conduit


17




c


is about 13 g/l.





FIG. 6

illustrates an fifth embodiment of the present invention. White liquor is supplied to a digester


6




d


via a conduit


24




d


. The temperature of the white liquor may be regulated by a heat exchanger


13




d


that is adapted to receive steam from a high pressure steam conduit


102




d


. About 5% to 15% of the total amounts of the white liquor in the conduit


24




d


is diverted via a conduit


117




d


to a conduit


116




d


. The remaining portion is conducted up to a top portion of the digester


6




d


. Spent liquor may be withdrawn from a screen girdle section


11




d


via a conduit


113




d


. A major portion of the spent liquor in the conduit


113




d


is diverted and conducted via a conduit


121




d


back to an impregnation vessel


1




d


. The addition of a small amount of black liquor to the top of the digester


6




d


prevents the white liquor from flowing back into the separator. Accordingly, the black liquor addition takes place above the white liquor addition so that the black liquor creates a barrier between the white liquor and the separator.





FIG. 7

describes a sixth embodiment of the present invention. In general, the sixth embodiment is very similar to the fifth embodiment shown in FIG.


6


. The sixth embodiment has the advantage of including a liquid exchanger to completely eliminate the risk of any undesirable back flow of white liquor that is particularly difficult problem with most hydraulic digesters. However, the separator shown in

FIG. 2

has features to reduce the risk of back flow.




A conduit


24




e


conducts white liquor to a return line


15




e


. The temperature of the white liquor may be controlled by a heat exchanger


13




e


that is adapted to receive steam from a high pressure steam conduit


102




e


. The temperature of the white liquor may be about 140-150° C. depending on the type of wood pulp that is used. The return line


15




e


terminates at a liquid exchanger


31




e


, which fulfills the same function as a top separator, i.e., it provides a very distinct exchange of treatment zones by almost totally withdrawing a first liquid from the chips and, subsequently, adding a second liquid so that any undesired mixing is avoided, the liquid changer


31




e


, in turn, has a mid-portion that is connected via a return line


33




e


to a bottom portion of an impregnation vessel


1




e


. A slurry of the chips and transport liquid may be conducted from the bottom portion of the impregnation vessel


1




e


via a conduit


35




e


to a bottom end of the liquid exchanger


31




e


after exchange of liquid the chips are transported in a conduit


21




e


to the top of a digester


6




e


. A portion of the spent liquor in the return line


33




e


is diverted and conducted to a second flash tank


114




e


via a conduit


137




e


for recovery.




Black liquor is withdrawn from a girdle section


8




e


of the digester


6




e


and conducted via a conduit


17




e


back to a top portion of the impregnation vessel


1




e


. Spent liquor is also drawn off from a screen girdle section


104




e


and is conducted to a first flash tank


108




e


via a conduit


106




e.







FIG. 8

shows a seventh embodiment of the present invention. This embodiment is similar to the sixth embodiment. In some instances, the seventh embodiment is preferred over the sixth embodiment because there is often no need for a screen between the top of the digester and the draw-off screen girdle


104


. This is because the liquid exchanger and the transport to the digester often provide sufficient and homogenous mixing of the cooking liquor so that a perfect condition can be established in the long concurrent cooking zone. If the conditions are optimally adjusted in the seventh embodiment, almost all or all the black liquor withdrawn from the screen


104


may be supplied to the impregnation vessel and therefore all or almost all of the liquid for the recovery may be taken from the liquid that is separated in the liquid exchanger.




Only some of the most important differences compared to the other embodiments are described. This embodiment has a digester


6


f that does not have a screen girdle section at the top of the digester. Most of the spent liquor is therefore withdrawn from the digester


6




f


at a screen girdle section


104




f


and a portion of the spent liquor withdrawn is conducted via a conduit


17




f


back to an impregnation vessel


1




f


. The remaining portion of the spent liquor is conducted to a first flash tank


108




f


via a conduit


106




f.







FIG. 9

illustrates a eighth embodiment of the present invention. This embodiment is similar to the embodiment shown in FIG.


7


. Only some of the main differences are described. In general, when a liquid exchanger is used, there is no longer any need for a heat seal at the top of the impregnation vessel (contrary to the embodiments shown in FIGS.


6


-


8


). In fact, even less expensive cupped gables can be used in the impregnation vessel. Therefore, the eighth embodiment may be an attractive way of retrofitting existing two vessel hydraulic digester systems. Also, the slurry of pulp and transport liquid is heated to a cooking temperature before the introduction into the digester by heating the transport liquid in the return line that is associated with a heat exchanger. It is to be understood that several advantages are gained by not only eliminating the heat seal in the impregnation vessel but also design the separator so that there is no back flow in the digester because a simple and inexpensive cupped gable design may be used at the top of both the impregnation vessel and the digester.




A high pressure feeder


19




g


feeds a slurry of chips to a bottom portion of a liquid exchanger


31




g


. The object of this liquid exchanger is to ensure safe operation of the high pressure feeder at the same time as a high temperature (e.g., 130° C.) is maintained at the top of an impregnation vessel


1




g


, which is achieved by supplying hot black liquor to a conduit


21




g


via a conduit


17




g


. After exchange of liquid, the slurry is further conducted to a top of the impregnation vessel


1




g


via a conduit


18




g


. Relatively cool transport fluid is returned to the high pressure feeder


19




g


via a conduit


23




g


. The temperature of the transport liquid can be kept low thanks to the total exchange of free liquid.





FIG. 10

illustrates a ninth embodiment of a single vessel hydraulic digester system of the present invention. The chips are fed from a chip bin


20


Ah, through a steaming vessel


20


Bh and a chip chute


20


Ch. A feeding device, preferably a high-pressure feeder


19




h


feeds the chips suspended in a transport liquid D via a conduit


18




h


to the top of a digester


6




h


. The feeder


19




h


is cooperating with the chute


20


Ch, and is connected to the necessary liquid circulations and replenishment.




The conduit


18




h


extends from the feeder


19




h


up to a top


5




h


of the digester


6




h


. The conduit


18




h


may open up at the top of a top separator


7




h


that feeds by means of a screw in a downwardly moving direction. The separator


7




h


is preferably identical or very similar to the top separator


7


that is shown in FIG.


2


and described in detail above. The screen of the separator may be used to draw off the transport liquid D (which is then returned in a return line


15




h


) together with which the chips are transported from the feeder


19




h


up to the top


5




h


of the digester


6




h


. A first screen girdle section


8




h


may be arranged in conjunction with a step-out approximately in the middle of the digester


6




h


. Draw-off of spent liquor from this screen girdle section


8


may be conducted via the conduit


17




h


to an impregnation zone A that is defined between the screen girdle section


8




h


and the top


5




h


of the digester


6




h


. A portion of the spent liquor may be withdrawn from the screen girdle section


8




h


via a conduit


111




h


that conducts the spent liquor to a second flash tank


112




h.






A cooking liquor conduit


24




h


is operatively attached to the conduit


17




h


to supply a major part of the cooking liquor, such as white liquor, to the conduit


17




h


. A heat-exchanger


13




h


may heat up the white liquor and the spent liquor to a suitable temperature before the liquor enters the top


5




h


. The heat exchanger


13




h


may be in operative engagement with a high pressure steam line


102




h


. The effective alkali of the liquor in the conduit


17




h


is at least about 35 g/l; more preferably at least about 40 g/l; and, most preferably, between about 45 g/l and about 55 g/l.




Approximately 95% of the total supply of the white liquor in conducted in the conduit


24




h


and the remaining 5% is supplied to the high pressure feeder


19




h


via a conduit


132




h


and a conduit


134




h


to lubricate the high pressure feeder


19




h.






A second screen girdle section


104




h


may be arranged below the first screen girdle section


8




h


. Draw-off from the second screen section


104




h


, such as spent liquor, i.e., black liquor, may be conducted via a conduit


106




h


back to a top portion of the impregnation zone A. The effective alkali of the spent liquor conducted in the conduit


106




h


is about 10-20 g/l. A portion of the black liquor in the conduit


106




h


may be conducted to a first flash tank


108




h


via a conduit


107




h


to cool the spent liquor before the liquor is conducted to a recovery unit


110




h


. Preferably, the spent liquor is also conducted through a second flash tank


112




h


via a conduit


114




h


to further reduce the temperature and pressure of the spent liquor before the liquor is conducted to the recovery unit


110




h


. The spent liquor from both flash tanks


108




h


,


112




h


are then conducted with a conduit


126




h


to the recovery unit


110




h


. Conduits


128




h


and


130




h


may be connected to the flash tanks


108




h


,


112




h


, respectively, to provide steam that is sent to the chip bin


20


Ah and the steaming vessel


20


Bh.




At a bottom


10




h


of the digester


6




h


, there is a feeding-out device including a scraping element


22




h


. A third lower screen girdle section


12




h


is disposed at the bottom


10




h


of the digester


6




h


. The girdle section


12




h


may, for example, include three rows of screens for withdrawing liquid, which is heated and to which some white liquor, preferably about 10% of the total amount of the white liquor in the conduit


24




h


, is added via a branch conduit


117




h


before it is recirculated by means of a central pipe


123




h


, which opens up at about the same level as the lowermost strainer girdle


12




h.






The draw-off from screen girdles


12




h


and the white liquor from the branch conduit


117




h


are preferably conducted via a heat exchanger


120




h


back to the bottom


10




h


of the digester


6




h


. The high pressure steam conduit


102




h


is connected to the heat exchanger


120




h


to provide the heat exchanger


120




h


with steam to regulate the temperature of the white liquor in the conduit


116




h


. The temperature of this draw off is about 130-150° C. The temperature may depend on how much washing-liquor that has penetrated to the screen is withdrawn. The white liquor is supplied in a counter-current direction via the central pipe


123




h


to the screen girdle section


12




h


. The white liquor provides fresh alkali and, in the form of counter-current cooking, further reducing the kappa number. A blow line


26




h


may be connected to the bottom


10




h


of the digester for conducting the digested pulp away from the digester


6




h.






A preferred installation according to the present invention, as shown in

FIG. 10

, may be described as follows. The chips are fed into the chip bin


20


Ah and are subsequently steamed in the vessel


20


Bh and, thereafter, conveyed into the chute


20


Ch. The high-pressure feeder


19




h


, which is supplied with a minor amount of white liquor (approximately 5% of the total amount to lubricate the feeder), feeds the chips into the conduit


18




h


together with the transport liquid. The slurry of chips and the liquid are fed to the top of the digester


6




h


and may have a temperature up to 110-120° C. when entering the digester


6




h


(excluding recirculated transport liquor).




Inside the top of the digester


6




h


, there is the top separator


7




h


that pushes chips in a downward direction then the chips move slowly downwards in a plug flow through the impregnation zone A in a liquid/wood ratio between 2/1-10/1 preferably between 3/1-8/1, more preferred of about 4/1-6/1. Hot black liquor, which is drawn off from the screen girdle section


104




h


, may be added, via the conduit


106




h


, to the top of the impregnation zone A of the digester


6




h


. The black liquor may also be added to other sections of the digester such as to an intermediate section thereof. The high temperature of the black liquor (100-160° C.), preferably exceeding 130° C., more preferred between 130-160° C., ensures rapid heating of the chips flowing through the impregnation zone A. In addition, the relatively high pH, exceeding pH 10, of the black liquor neutralizes acidic groups in the wood and also any acidic condensate accompanying the chips, thereby, i.e., counteracting the formation of encrustation, so-called scaling.




An additional advantage of the method of the present invention is that the black liquor supplied into the impregnation zone A has a high content of rest alkali, (effective alkali EA as NaOH), at least 13 g/l, preferably about or above 16 g/l and more preferred between 13-30 g/l in the top of the impregnation zone A. This alkali mainly comes from the black liquor due to the high amount of alkali in the concurrent zone B of the digester


6




h


. Furthermore, the strength properties of the fibers are positively affected by the impregnation because of the high amount of sulphide. A major portion of the black liquor may directly (or via one flash tank) be fed into the impregnation zone A.




The total supply of black liquor to the impregnation zone A may exceed 80% of the amount drawn off from the draw-off screen girdle section


104




h


, preferably more than 90% and optimally about 100% of the total flow, which normally is about 8-12 m


3


/ADT.




The retention time in the impregnation zone A should be at least 20 minutes, preferably at least 30 minutes and more preferred at least 40 minutes. However, a shorter retention time than 20 minutes, such as 15-20 minutes may also be used. The volume of the impregnation zone A may be larger than 1/11, preferably larger than 1/10 of the volume of the digester


6




h


. Additionally, in the preferred embodiment, the volume V of the impregnation zone A should exceed 5 times the value of the square of the maximum digester diameter, i.e., V=5D


2


, where D is the maximum diameter of the digester


6




h.






The chips, which have been thoroughly impregnated and partially delignified in the impregnation zone A, may be fed to the top of the digester


6




h


and conveyed into the downwardly-feeding top separator


7




h


. The chips are thus fed upwards through the screen, meanwhile free transport liquid may be withdrawn outwardly through the separator screen and finally the chips fall down into the digester


6




h


. Before or during their free fall, the chips pieces are drained with cooking liquor, such as white liquor, which is supplied at the top separator


7




h.






The quantity of white liquor that is added at the top separator


7


depends on how much white liquor possibly is added else where. The thoroughly impregnated chips very rapidly assimilate the active cooking chemicals by diffusion, since the concentration of alkali (EA as NaOH) is relatively high, at least 20 g/l, preferably between 30 g/l and 50 g/l and more preferred about 40 g/l.




The chips then move down in the concurrent zone B through the digester


6




h


at a relatively low cooking temperature, i.e., between 130-160° C., preferably about 140-150° C. The major part of the delignification takes place in the first concurrent cooking zone B.




The liquid-wood ratio should be at least 2/1 and should be below 7/1, preferably in the range of 3/1-5.5/1, more preferred between 3.5/1 and 5/1. (The liquid wood-ratio in the counter-current cooking zone should be about the same as in the concurrent cooking zone.)




The temperature in the lower counter-current zone C is preferably higher than in the concurrent zone B, i.e., preferably exceeding 140° C., preferably about 145-165° C., in order to dissolve remaining lignin. The alkali content in the lowermost part of the counter-current cooking zone C should preferably be lower than in the beginning of the concurrent zone B, above 5 g/l, but below 40 g/l. Preferably less than 30 g/l and more preferred between 10-20 g/l. In the preferred case, the aim is to have a temperature difference of about 10° C. between the concurrent zone B and the counter-current cooking zone C. Expediently, the conduit


116




h


may be charged with about 5-20%, preferably 10-15%, white liquor from the conduit


24




h


via the conduit


117




h.






The temperature of the liquid which is recirculated via the pipe


123




h


up to the screen girdle section


12




h


is regulated with the aid of the heat exchanger


120




h


so that the desired cooking temperature is obtained at the lowermost part of the counter-current cooking zone.




From tests made in lab-scale, we have found indications that it is desirable to keep the alkaline level at above at least 2 g/l, preferably above 4 g/l, in the impregnation zone A in connection with black liquor, which would normally correspond to a pH of about 11. If not, it appears that dissolved lignin precipitates and even condenses.





FIG. 11

illustrates a tenth embodiment of the present invention. This embodiment is substantially similar to the embodiment shown in FIG.


10


. Chips and a transport fluid is pumped up in a conduit


18




i


and a conduit


119




i


to a top section


5




i


of a digester


6




i


via a liquid exchanger


33




i


. The operation of the liquid exchanger is similar to the liquid exchanger


33




i


described for the sixth embodiment shown in FIG.


7


and its function is similar to the eighth embodiment shown in FIG.


9


. As described earlier, liquid is exchanged in the liquid exchanger


33




i


before the chips enter the top section


5




i


of the digester


6




i.






A portion of the transport liquid may be returned in return line


15




i


that leads from the top portion


5




i


to a mid-section of the liquid exchanger


33




i


and then back to a feeder


19




i


via a conduit


25




i


. The conduit


106




i


conducts the spent liquor withdrawn from a screen girdle section


104




i


to the liquid from


117




i


and to the conduit


15




i


. A portion of the liquor in the conduit


106




i


may be sent to a flash tank


108




i.







FIG. 12

shows a eleventh embodiment of the present invention. The eleventh embodiment is similar to the ninth embodiment shown in FIG.


10


. Some of the more important differences are described herein. The eleventh embodiment has a digester


6




j


having a return line


15




j


attached to a top portion


5




j


of the digester


6




j


. A recirculation line


101




j


is in fluid communication with the return line


15




j


so that a portion of the liquid in the return line


15




j


may be diverted back to the top portion


5




j


via the line


101




j


. The temperature of the liquid in the recirculation line


101




j


may be regulated with a heat exchanger


113




j


that is operatively engaged with a high pressure steam line


102




j


. The recirculation line is used to heat the liquid from the return line


15




j


before the liquid is introduced. The temperature in the return line


15




j


must not exceed about 100° C. to avoid undesirable flashing in the high pressure feeder.




Similar to the above described embodiments, a flash tank


108




j


is in fluid communication via a conduit


106




j


to a screen girdle section


104




j


so that spent liquor from the section


104




j


may be conducted to the flash tank


108




j


. A bottom portion of the flash tank


108




j


has a conduit


103




j


connected thereto to conduct a portion of the spent liquor back to a conduit


134




j


that carries some white liquor from the cooking liquor conduit


24




j.







FIG. 13

describes a twelfth embodiment of the present invention. This embodiment is similar to the embodiment shown in

FIG. 12

but it does not have the recirculation line


101




j


that is associated with the return line. Instead the twelfth embodiment includes a digester


6




k


having an additional screen girdle section


200




k


that is disposed immediately below a top section


5




k


. The girdle section


200




k


has a recirculation line


201




k


in fluid communication therewith. The recirculation line


201




k


withdraws cooking liquor from the girdle section


200




k


and recirculates it back up to a point that is immediately below a top separator


7




k


disposed inside the top portion


5




k


. The temperature of the liquor in the line


201




k


may be controlled by a heat exchanger


203




k


that is in operative engagement with a high pressure steam line


102




k


. The main reason for using the recirculation line


201




k


is to improve the distribution of the white liquor that is withdrawn from the girdle section


200




k


. The method of recirculating the cooking liquor is often called quench circulation. The remaining sections of this twelfth embodiment are similar to the embodiments shown in FIGS.


10


-


12


.





FIG. 14

is a cross-sectional view of a preferred third embodiment of a top separator


300


of the present invention. In contrast to previously downwardly feeding top separators, this third embodiment is peripherally supplied with chips/slurry. The top separator


300


has a rotating source


333


that is attached to a top of the top separator


300


. The rotating source


333


may rotate a rotor


332


that is in operative engagement therewith and disposed inside the top separator


300


. A plate or lid


334


is disposed adjacent the top of the top separator. The lid may be made of a suitable material such as a standard steel plate. The lid


334


extends diametrically across the top separator


300


and has a central opening defined therein to receive the rotor


332


. A screen


335


is disposed below the lid


334


inside the top separator


300


. The screen


335


extends vertically from about a mid-point of the top separator to a bottom portion of the top separator. The screen


335


is in operative engagement with the rotor


332


. A supply conduit


321


for supplying chips into the top separator is disposed between the lid


334


and the screen


335


. The supply conduit


321


extends through a side wall of the top separator. An important feature of this embodiment is that the supply conduit


321


does not extend through the lid


334


which makes the lid


334


expensive to manufacture such as by casting. Another important feature of this alternative embodiment thait is solved by this embodiment is that it is often difficult to adjust, inspect and maintain the screen and the screw member because there is only a very limited space defined between the inner wall of the vessel and the screen. This makes is particularly difficult to adjust and center the screw member relative to the screen once the installation is completed.




A top of the screen


335


of the top separator


300


is integral with a cylindrical shell


338


that has a flange


339


resting on a support member


340


of the impregnation vessel. The screen


335


has a mid-segment collar


341


that is radially and tightly fitted within a supporting ring


342


at the top separator. This is to provide additional support of the screen


335


due to the large forces that are created at the top portion of the screen


335


. A similar support device is disposed at a bottom portion of the screen


335


. An adjustment mechanism


344


is attached to a support plate


343


at the bottom of the screen


335


. The adjustment mechanism has an adjustment screw so that the position of the screen


335


relative to the wall of the top separator may be adjusted. In other words, the axial position of the bottom of the screen


335


may be adjusted with the adjustment mechanism


344


. Similarly, a second adjustment mechanism


345


is in operative engagement with the bottom of the screen. It is an important advantage to be able to made the adjustment from below the screen


335


. In fact, the adjustment can be made by standing on a platform within the vessel. The support plate


343


also ensures that the lower part of the screen


335


is lifted thanks to protruding pieces that bear against a sliding ring. Four U-beams


346


are disposed at the upper portion of the screen


335


to prevent the screen


335


from be rotated because the U-beams


346


are in operative engagement with a protruding segment


347


that is attached to the collar


341


.




The invention is not limited to that which has been shown above but can be varied within the scope of the subsequent patent claims. Thus, instead of the shown separator used with the hydraulic digester many alternatives may be used, e.g., instead of an annular supply arrangement a central pipe (as shown in WO-9615313) for supply of liquid at distance downstream of the separator device within chip pile adjacent the top of the digester.




Moreover, there are many ways of optimizing the conditions even further, e.g., new on-line measuring systems (for example using NIR-spectroscopy) provide for the possibility of exactly measuring specific contents of the fiber material and the liquids entering the digesting system, which will make it feasible to more precisely determine and control the supply/addition of specific fluids/chemicals and also their withdrawal in order to establish optimized conditions. Different kind of additives can be very beneficial to use, especially for example poly-sulphide which has a better effect in a low temperature environment than in high temperatures. Also AQ (Anthraquinone) would be very beneficial since it combines very well with high alkaline environments.




Furthermore, there are a multiplicity of alternatives for uniformly drenching the chips with white liquor at the top of the digester. For example, a centrally arranged inlet (as described in WO 95/18261) having a spreading device can be contrived, which device, provides a mushroom-like film of liquid, as can a centrally arranged showering element or an annular pipe with slots, etc.




In addition, the number of screen girdles shown is in no way limiting for the invention but, instead, the number can be varied in dependence on different requirements. The invention is in no way limited to a certain screen configuration and it is understood that bar screens can be exchanged by, for example, such as screens having slots cut out of sheet metal. Also in some installations moveable screens are preferred.




The shown system in front of the digester is in no way limiting to the invention, e.g., it is possible to exclude the steaming vessel


20


and have a direct connection between the chip bin (for example, a partly filled atmospheric vessel) and the chip chute. Furthermore, other kind of feeding systems than an high pressure feeder may be used, e.g., DISCFLO™-pumps).




While the present invention has been described in accordance with preferred compositions and embodiments, it is to be understood that certain substitutions and alterations may be made thereto without departing from the spirit and scope of the following claims.



Claims
  • 1. A separator disposed in a hydraulic vessel having an inner wall, comprising:a screw feeder having an inlet end and an outlet end for feeding a fiber material in a downward direction from the inlet end towards the outlet end of the screw feeder; the hydraulic vessel defining an inlet opening for receiving a suspension of the fiber material and a transport liquid, and a liquid outlet opening; a rotatable shaft in operative engagement with the screw feeder; a drive unit secured to the rotatable shaft for rotating the rotatable shaft; a cylindrical screen basket enclosing the screw feeder; a liquid collecting space defined between the cylindrical screen basket and the inner wall, the liquid collecting space being in fluid communication with the liquid outlet opening of the hydraulic vessel; and the hydraulic vessel having a liquid inlet aperture defined therein, the liquid inlet aperture being disposed below the outlet end of the screw feeder.
  • 2. The separator according to claim 1 wherein the liquid inlet aperture comprises a distribution means for evenly supplying a liquid to the fiber material.
  • 3. The separator according to claim 2 wherein the distribution means is an annular distribution ring.
  • 4. The separator according to claim 1 wherein the inlet aperture of the hydraulic vessel is positioned above the liquid inlet aperture.
  • 5. The separator according to claim 1 wherein the inlet aperture is disposed above the liquid collecting space.
  • 6. The separator according to claim 1 wherein the screw feeder has a rotatable helical blade section.
  • 7. The separator according to claim 6 wherein the helical blade section is rotatable to move the fiber material through the screw feeder and the transport liquid is urged radially outwardly into the liquid collecting space by an internal pressure in the hydraulic vessel.
  • 8. The separator according to claim 1 wherein the screen basket permits the transport liquid to penetrate therethrough and prevents the fiber material from penetrating therethrough.
  • 9. The separator according to claim 1 wherein the liquid inlet aperture is positioned a sufficient distance from the screen basket to avoid any substantial back flow of liquid from the liquid inlet aperture to the screen basket.
  • 10. The separator according to claim 1 wherein the inlet aperture is positioned a sufficient distance from the screen basket to avoid any substantial heat transfer from the liquid to the screen basket.
  • 11. The separator according to claim 10 wherein a cylindrical portion of the hydraulic vessel has the liquid inlet aperture defined therein, the cylindrical portion is disposed between the screen basket and a large diameter portion of the hydraulic vessel.
  • 12. The separator according to claim 11 wherein the cylindrical portion has a conical shaped section.
  • 13. The separator according to claim 12 wherein the separator has a diameter having a value and a heat lock zone is defined between the large diameter portion of the hydraulic vessel and the screen basket, the heat lock zone has a height h that has a value that is greater than the value of the diameter of the separator.
  • 14. The separator according to claim 13 wherein the conical shaped section connects the large diameter portion of the hydraulic vessel to the separator.
  • 15. The separator according to claim 11 wherein the cylindrical portion is disposed downstream of the screen basket.
  • 16. A hydraulic vessel system having a hydraulic vessel with a top portion, comprising:the hydraulic vessel having an inlet opening and an outlet opening defined therein, the hydraulic vessel having: a hydraulic vessel wall; a separator comprising: a screw feeder having an inlet end and an outlet end for feeding a fiber material in a downward direction from the inlet end towards the outlet end of the screw feeder; a rotatable shaft in operative engagement with the screw feeder; a drive unit secured to the rotatable shaft for rotating the rotatable shaft; a cylindrical screen basket enclosing the screw feeder; a liquid collecting space defined between the cylindrical screen basket and the hydraulic vessel wall, the liquid collecting space being in fluid communication with the outlet opening of the hydraulic vessel; and the hydraulic vessel having a liquid inlet aperture defined therein adjacent the outlet end of the screw feeder for receiving a cooking liquor; and a first screen girdle section disposed immediately below the top portion of the hydraulic vessel.
  • 17. The hydraulic vessel system according to claim 16 wherein the hydraulic vessel further comprises a recirculation loop that is in fluid communication with a first screen girdle section disposed in the hydraulic vessel for recirculating the cooking liquor back to the top portion of the hydraulic vessel.
  • 18. The hydraulic vessel system according to claim 17 wherein the hydraulic vessel further comprises a connecting line that extends between an inlet portion of an impregnation zone and the first screen girdle section of the hydraulic vessel for supplying the impregnation zone with a spent liquor that is withdrawn from the first screen girdle section.
  • 19. The hydraulic vessel system according to claim 18 wherein the hydraulic vessel comprises a return line connected to a top portion of the hydraulic vessel for conveying the transport liquid from the liquid collecting space to the outlet portion of the impregnation zone.
  • 20. The hydraulic vessel system according to claim 19 wherein a recirculation line is operatively attached to the return line to recirculate a portion of the transport liquid back to a top portion of the hydraulic vessel.
  • 21. The hydraulic vessel system according to claim 20 wherein the hydraulic vessel further comprises a first flash tank, a first flash tank conduit is operatively attached to the first flash tank to conduct spent liquor back to a high pressure feeder.
  • 22. The hydraulic vessel system according to claim 19 wherein the hydraulic vessel further comprises a second screen girdle section disposed below the first screen girdle section, a second conduit is in fluid communication with the second screen girdle section to withdraw spent liquor from the second screen girdle section, a cooking liquor conduit has one end attached to a top portion of the hydraulic vessel to supply the top portion with a cooking liquor, a branch conduit has one end attached to the cooking liquor conduit and an opposite end attached to the second conduit to conduct a portion of the cooking liquor in the cooking liquor conduit to the second conduit.
  • 23. The hydraulic vessel system according to claim 22 wherein a conduit extends between the cooking liquor conduit and the return line to conduct the cooking liquor to the return line.
  • 24. The hydraulic vessel system according to claim 22 wherein the hydraulic vessel has a middle screen girdle section disposed between a bottom screen girdle section and the first screen girdle section, a conduit is in fluid communication with the middle screen girdle section to conduct spent liquor from the middle screen girdle section to a top portion of the hydraulic vessel.
  • 25. The hydraulic vessel system according to claim 24 wherein the hydraulic vessel system is a one vessel hydraulic digesting system and the cooking liquor conduit is in fluid communication with a recirculation line disposed adjacent the first screen girdle section, the recirculation line conducts the spent liquor withdrawn from the first screen girdle section and the cooking liquor from the cooking liquor conduit back to an impregnation zone of the hydraulic vessel.
  • 26. The hydraulic vessel system according to claim 25 wherein the recirculation line has a heat exchanger that is in operative engagement with the recirculation line and a high pressure steam line.
  • 27. The hydraulic vessel system according to claim 25 the hydraulic vessel system has an impregnation zone disposed above a concurrent cooking zone, a second screen girdle section is disposed below the first screen girdle section to conduct spent liquor via a second conduit back to the impregnation zone of the hydraulic vessel.
  • 28. The hydraulic vessel system according to claim 27 wherein the first screen girdle section conduct spent liquor back to the impregnation zone via a first conduit, a cooking liquor conduit is operatively attached to the first conduit to conduct white liquor to the first conduit.
  • 29. The hydraulic vessel system according to claim 16 wherein the hydraulic vessel system is a two hydraulic vessel system including an impregnation vessel that has a screen girdle section disposed therein, a spent liquor is withdrawn from the screen girdle section of the impregnation vessel and conducted to a recovery unit.
  • 30. The hydraulic vessel system according to claim 29 wherein a transport conduit is operatively attached to a bottom of the impregnation vessel to conduct the fiber material and the transport liquid to a liquid exchanger that exchanges a liquid in the transport conduit before the fiber material and the transport liquid are conducted to a top portion of the hydraulic vessel.
  • 31. The hydraulic vessel system according to claim 29 wherein the first screen girdle section is in fluid communication with a conduit that conducts the spent liquor withdrawn from the first screen girdle section to both the impregnation vessel and to a first flash tank, the first screen girdle section is adjacent a bottom of the hydraulic vessel.
  • 32. The hydraulic vessel system according to claim 29 wherein the impregnation vessel has a screen girdle section disposed adjacent the outlet portion of the impregnation vessel, a conduit is in fluid communication with the screen girdle section of the impregnation vessel to conduct spent liquor away from the impregnation vessel into a second flash tank.
  • 33. The hydraulic vessel system according to claim 16 wherein the hydraulic vessel has a bottom screen girdle section that is adjacent a bottom portion of the hydraulic vessel, a screen conduit is in fluid communication with the bottom screen girdle section to withdraw spent liquor from the bottom screen girdle section, a cooking liquor conduit is in fluid communication with the screen conduit for conducting cooking liquor.
  • 34. A separator disposed in a hydraulic vessel having a hydraulic vessel wall, comprising:a feeder having an inlet end and an outlet end for feeding a fiber material in a downward direction from the inlet end towards the outlet end of the feeder; the hydraulic vessel defining an inlet opening for receiving a suspension of the fiber material and a transport liquid, and an outlet opening; a screen basket enclosing the feeder; a liquid collecting space defined between the screen basket and the hydraulic vessel wall, the liquid collecting space being in fluid communication with the outlet opening of the hydraulic vessel; the hydraulic vessel having a liquid inlet aperture defined therein, the liquid inlet aperture being disposed below the outlet end of the screw feeder; and a heat zone disposed between the liquid inlet aperture and the outlet opening of the hydraulic vessel.
  • 35. The separator according to claim 34 wherein the heat zone comprises a set of level sensors to sense the level of fiber material in the hydraulic vessel.
  • 36. The separator according to claim 35 wherein the level sensors are disposed in a narrow top portion of the hydraulic vessel that has a first diameter, the hydraulic vessel has a mid-portion that has a second diameter and the second diameter is about twice as large as the first diameter.
  • 37. The separator according to claim 34 wherein the separator is attached to an impregnation vessel.
  • 38. The separator according to claim 34 wherein the separator is attached to a single hydraulic vessel.
PRIOR APPLICATION

This is a continuation-in-part application of U.S. patent application Ser. No. 08/908,285, filed Aug. 7, 1997, now U.S. Pat. No. 6,123,807.

US Referenced Citations (1)
Number Name Date Kind
5089086 Silander Feb 1992
Foreign Referenced Citations (1)
Number Date Country
9001467 Apr 1990 SE
Continuation in Parts (1)
Number Date Country
Parent 08/908285 Aug 1997 US
Child 09/024688 US