In-line drainer enhancements

Information

  • Patent Grant
  • 6451172
  • Patent Number
    6,451,172
  • Date Filed
    Thursday, May 18, 2000
    24 years ago
  • Date Issued
    Tuesday, September 17, 2002
    21 years ago
Abstract
A drainer for a feed system for a cellulose digester has a substantially open and hollow inlet (devoid of a spiral flow imparter or a like flow restriction) and a substantially annular screen within an elongated housing having a flow direction between the housing inlet and outlet. The screen is slotted and the slots are at an angle α between 5-90° with respect to the flow direction, so as to minimize passage of cellulose material through the slots, or clogging of the slots.
Description




BACKGROUND AND SUMMARY OF THE INVENTION




U.S. Pat. Nos. 5,476,572; 5,622,598; 5,635,025; 5,766,418; and 5,968,314 disclose methods and devices for feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel that have revolutionized the art of treating comminuted cellulosic fibrous material to produce cellulose pulp. The disclosed inventions, sold under the trademark LO-LEVEL® by Ahlstrom Machinery Inc., of Glens Falls, N.Y. employ one or more slurry-type pumps for treating and transferring comminuted cellulosic material to one or more treatment vessels. Not since the initial development of the continuous cooking process in the 1940s and 1950s have such dramatic improvements been made to equipment used to transfer material to a treatment vessel, for example, a continuous or batch digester. This is confirmed by the broad acceptance of this technology by the Pulping Industry.




The present invention introduces improvements to the systems and methods described in the above patents which further simplify and enhance the effectiveness of the methods and devices disclosed therein.




The prior art systems for introducing a slurry of comminuted cellulosic fibrous material, for example, as exemplified by the system disclosed in U.S. Pat. No. 5,476,572, use a two-stage pressurization and transfer of slurry. In the first stage, the slurry is pressurized to a first pressure and transferred to a high-pressure transfer device, such as, a High Pressure feeder designed and marketed by Ahlstrom Machinery. The first stage pressurization and transfer is typically performed using a specially-designed slurry pump which handles slurries of material and liquid. In the second stage the High Pressure Feeder pressurizes the slurry to a second pressure, higher than the first pressure, by exposing the material to a high pressure liquid stream, and transports the slurry to a treatment vessel, for example, a continuous or batch cellulose pulp digester. However, according to this prior art, the amount of cellulose material, such as, wood chips, that can be transferred to the High Pressure Feeder by the slurry pump, per unit volume of liquid, is limited by the capacity of the pump to transfer solid material.




Typically, the relative amount of liquid present in slurry is indicated by a “liquid-to-solids” ratio, or, in the case of transferring slurries of wood chips, a “liquid-to-chip” ratio, or, more specifically, a “liquor-to-wood” (L/W) ratio. The liquid-to-wood ratio is a dimensionless ratio of the volume of the liquid present in the slurry to the volume of the wood present in the slurry. Conventional High Pressure Feeders can accept slurries having L/W of below 3.0:1, typically even below 2.5:1. The lower limit of the L/W ratio of a slurry being introduced to a High Pressure Feeder is about 2.0:1. Note that a reduction in L/W ratio from 3.0:1 to 2.0:1 corresponds to a 25% reduction in the volume of liquid that must be accepted by the High Pressure Feeder, or a corresponding 25% increase in the volume of chips that can be processed by the High Pressure Feeder.




Desirably the volume of liquid that is transferred to the High-pressure Feeder is reduced so that more wood chips can be introduced and processed in the digester system being fed per revolution of the High Pressure Feeder. This has the further advantage of allowing for the reduction in size of the High-pressure Feeder for a given project, or allowing for an increase in the capacity of a production-limited facility.




After introducing the slurry of chips to a high-pressure transfer device, for example, a High-Pressure Feeder sold by Ahlstrom Machinery, the slurry is displaced from the feeder by a flow of high-pressure liquid, typically at a pressure between about 5 and 15 bar gage, provided by a high-pressure pump. Typically this flushing of the slurry from the feeder by the liquid results in the slurry being propelled to a treatment vessel having a L/W ratio of between about 4.0:1 to 10.0:1, and is typically greater than 5:1, often greater than 7:1, sometimes greater than 9:1. For example, for a L/W ratio of 9:1, the volume of liquid present in the conduit transferring the slurry from the feeder to the treatment vessel, for example, to a pulping digester, the volume of liquid is 9 times the volume of the cellulose material, such as, wood chips. Typically, this volume of liquid is required in order to flush the chips from the pockets of the feeder. This relatively large volume of liquid requires a relatively large conduit in which to pass the slurry from the feeder to the digester and sufficient energy to propel the relatively large volume of liquid up to the top of the pressurized digester.




The L/W ratio of the slurry exiting the High Presser Feeder is also a function of the equipment which feeds the slurry to the feeder. In conventional, “suck through” systems typically having a pressurized chip chute the L/W ratio of the slurry introduced to the High Pressure Feeder is about 2.0-2.5:1. In “pump through” systems, such as Lo-Level Feed Systems sold by Ahlstrom Machinery, the L/W ratio of the slurry introduced to the High Pressure Feeder is about 3.0-3.5:1.




Desirably the liquid volume in the slurry transferred from the feeder to the treatment vessel is minimized by removing at least some of the liquid from the slurry after the slurry has been discharged from the feeder and before the slurry is introduced to the treatment vessel. One advantage of this embodiment of the invention is that, with reduced liquid volume, the diameter of the transfer conduit to the treatment vessel can be reduced. Reducing the size of this conduit has the further advantage of reducing the sizes, and hence the cost, of the associated valves and instruments that are located in this conduit.




The above embodiment is particularly effective in limiting the amount of heat returned to the feed system from the treatment vessel, for example, via what is known as the “Top Circulation” or “TC” line. As recognized in the art, exposing the feed system, for example, the High-pressure Feeder, to liquids having temperatures at or above 100° C. can cause flash-evaporation of this liquid (known as “flashing”) when the liquids are exposed to the atmospheric pressures present in the vicinity of the high-pressure feeder. However, when excess liquid is removed from the slurry when introducing the slurry to the treatment vessel, for example, by using of a Top Separator, heat present in the treatment vessel can migrate, for example, by convection, to the vicinity of the Top Separator and be drawn out of the vessel with the removal of liquid from the Top Separator. This heat can raise the temperature of the liquid returned to the feed system via the TC line. This increased TC line temperature can cause flashing and vibration in the feed system and interfere with the normal operation of the feed system.




One way of reducing the potential of returning undesirable heat to the feed system is by limiting the flow of liquid removed from the slurry as the slurry is introduced to the treatment vessel. That is, a liquor removal device is located in the conduit which feeds the slurry to the treatment vessel, preferably, near to or adjacent the inlet of the treatment vessel. At least some liquid is removed from the slurry using this device and returned to the feed system such that less liquid needs to be removed from the slurry as the slurry is introduced to the vessel. This reduced removal of liquid from the vessel reduces the potential for heat in the vessel to be withdrawn with the removed liquor and returned to the feed system.




One liquid separating device that is novel according to the invention, and that is particularly useful in the system and practice of the method of the present invention, is a cylindrical device having a cylindrical screen through which the slurry passes and from which liquid is removed, for example, an In-line Drainer, as sold by Ahlstrom Machinery Inc. of Glens Falls, N.Y. An In-line Drainer is typically used to isolate a stream of liquid from a stream of liquid that typically contains at least some wood chips or fine wood particles, for example, what are known as “fines” and “pins”. However, an In-line Drainer can also be used in the practice of the present invention where a liquid is preferably removed from a slurry containing a larger amount of cellulose material, in particular wood chips.




In the conventional use of an In-line drainer, the drainer is positioned in a feed system of a continuous digester, for example, in the outlet of a Sand Separator [as shown by item 37 in

FIG. 2

herein]. The liquid passed to the drainer from the Sand Separator can typically contain at least some wood particles or other material. The In-Line Drainer is typically used to remove excess liquid from the low pressure liquor circulation associated with the feed system, that is, the Chip Chute Circulation, to control the volume of liquid, for example, in the Chip Chute or Chip Tube. Conventional drainers include cylindrical screen baskets fashioned from steel bars oriented parallel to the direction of flow so that the liquid passes through vertical slots or apertures while retaining wood particles within the circulation. However, due to the low concentration of chips, pins, and fines in the liquid passing through the drainer, the flow of liquid through the basket is such that the chips, pins, and fines are oriented in the direction of flow which is also parallel to the slots in the basket. As a result, without taking appropriate measures, the chips, pins, and fines can align with and undesirably pass through the vertical slots or become lodged in the vertical slots of the drainer.




In the drainer of the conventional art, for example, as shown in

FIG. 5

herein, the potential for chips, pins, and fines to align with and pass through the vertical slots of the drainer basket is minimized by introducing a horizontal velocity component to the liquid flow as it is passes through the drainer. This is typically achieved by introducing a helical baffle, or so-called “flight”, to the inlet of the drainer in order to impart a helical flow to the liquid as it is introduced to the drainer and passes through the drainer basket. Due to this helical flow, any chips, pins, or fines that may be present are oriented in the direction of the helical flow and thus oriented obliquely to the elongation of the slots of the vertical bars. Thus, in the conventional art, the helical flight in the inlet reduces the tendency for chips, pins, and fines to pass through the drainer basket or to be lodged in the slots of the drainer basket and cause pluggage of the drainer.




Though this conventional In-line Drainer has proven to be very effective in most applications, the flight positioned in the inlet of the conventional drainer has, in some applications, been associated with an undesirable pressure drop across the drainer. That is, the helical baffle introduces an impediment to flow which causes a decrease in hydraulic pressure from the pressure of the liquid introduced to the drainer to the pressure of the liquid leaving the drainer. This pressure drop impedes the flow of liquid through the drainer and also reduces the pressure of the liquid downstream of the drainer, which can interfere with the proper operation of downstream equipment, for example, the Level Tank or Make-up Liquor Pump. This flow impediment can also reduce the velocity of the flow and thus increase the likelihood for chips, etc. to pass through or become lodged in the screen.




According to the present invention, the helical baffle present in the inlet of prior art In-line Drainers and the source of pressure drop associated with this baffle are eliminated, yet the Drainer still functions properly. To account for the loss of the baffle's function, according to the present invention, the slots or apertures of the screen basket are aligned obliquely to the direction of elongation of the drainer, and thus obliquely to the direction of flow of the liquid through the drainer. The angle of the slots relative to the direction of elongation of the screen can range from between about 5 to 90 degrees. For example, in one embodiment the slots are oriented substantially perpendicular to the direction of elongation and direction of flow. In the preferred embodiment, the slots are oriented at an angle of about 10° to 80°, preferably about 30° to 60°, most preferably about 40° to 50°.




One embodiment of the present invention consists or comprises a liquid separating device having a cylindrical housing elongated in a direction of elongation having an inlet at or adjacent a first end of the housing, an outlet at or adjacent a second end, opposite, the first end, and an inside surface; a cylindrical screen assembly centrally mounted in the housing having a plurality of elongated apertures having an angle of orientation and an outside surface; an annular cavity formed by the outside surface of the screen and the inside surface of the housing; and an outlet for separated liquid located in the housing and communicating with the annular cavity; wherein the angle of orientation of the screen assembly apertures is oblique to the direction of elongation of the housing. The angle of orientation is preferably at least 5° to the direction of elongation of the housing or screen basket, but is typically between about 10° to 80°, preferably about 30° to 60°, most preferably 40° to 50° to the direction of the elongation of the housing or screen basket. For example, the orientation of the slots relative to the elongation of the housing is about 45°.




The drainer slots may be continuous slots or they may be interrupted by unperforated “land” areas. These land areas may be uniformly located throughout the screen basket so that a uniform pattern of slots and land areas is provided or the slots and land areas may be distributed non-uniformly. The orientation of the slots may also vary, for example, the angle of orientation of the slots at one elevation in the direction of elongation of the screen basket may be different from the orientation of the slots at second or an adjacent elevation. The orientation of slots at one elevation in the direction of elongation of the screen basket may also vary, for example, producing a “herring bone”-type pattern of slots. The screen slot configuration of this device may be similar or identical to the screen designs illustrated and described in U.S. Pat. No. 6,039,841 or in co-pending application Ser. No. 09/248,005 filed on Feb. 10,1999, now U.S. Pat. No. 6,165,323 the disclosures of which are incorporated by reference herein.




The slots may be fabricated from parallel-bar-type or parallel-wire-type construction or they may be machined from plate, for example, by water-jet cutting, laser cutting, EDM machining, drilling, milling, or any other conventional method of producing apertures in plate. The housing or screen basket material is typically metallic, for example, steel, steel-based alloy, stainless steel, aluminum, titanium or any other commercially available metal, but may also be manufactured from a high-performance plastic or composite material.




The drainer according to the present invention may be used in a conventional feed system, as shown by item


37


in

FIG. 2

of this application, or for treating slurries according to the method and apparatuses of the present invention, for example, as shown as items


153


and


154


of

FIG. 3

or item


254


of FIG.


4


.




That is, the invention comprises: A drainer for draining liquid from a moving slurry, comprising: An elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; and a dimension of elongation between the inlet and outlet. The inlet substantially open and hollow. A substantially annular screen positioned between the inlet and the outlet having a plurality of slots therein. And the screen slots having an oblique inclination angle α with respect to the dimension of elongation between about 5-90° to minimize passage of solid material in the slurry through the slots, and minimizing clogging of the slots. The angle α may be substantially 90°, or between about 10-80°, e.g. between 30-60°, or between about 40-50° (e.g. about 45°).




The drainer may further comprise a plurality of land areas between regions of the slots. Also, the drainer preferably further comprises a substantially annular volume between the screen and housing, and a liquid outlet from the volume and a steam purge connected to the volume, and wherein the screen has a diameter of between about 0.5-3 feet, preferably about 8 to 24 inches.




In one embodiment the slots have a width of between about 2-4 mm, and the slots are substantially evenly spaced by about 3-4 mm. In another embodiment the slots have a width of between about 5-7 mm, and the slots are substantially evenly spaced by about 4-8 mm.




According to another aspect of the invention there is provided a pulp producing system comprising: A substantially upright digester. A feed system for feeding a slurry of comminuted cellulosic material to the digester. The feed system including a drainer which receives some liquid from a flow of slurry. And the drainer comprising: an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; a substantially annular screen positioned between the inlet and the outlet having a plurality of slots; and the screen slots having an oblique inclination angle α with respect to the dimension of elongation of between about 5-90° to minimize passage of solid material in the slurry through the slots, and minimize clogging of the slots. In one embodiment the drainer is positioned in a location in the feed system wherein the slurry has a L/W ratio of greater than about 20:1, preferably greater than about 50:1 but includes at least some pins, fines, or chips, and a pressure of from about 0-5 bar gauge; and wherein the slots are evenly spaced by about 3-4 mm and have a width of between about 2-4 mm. In another embodiment the drainer is positioned in a location in the feed system wherein the slurry has a L/W ratio of less than 15:1, preferably less than about 10:1 and a pressure of about 0-30 bar gauge; and wherein the slots have a width of between about 5-7 mm, and the slots are substantially evenly spaced by about 4-8 mm.




The feed system may include a high pressure transfer device (e.g. a high pressure feeder) or the feed system may include one or more slurry pumps as disclosed in U.S. Pat. No. 5,753,075 or co-pending applications Ser. No. 09/063,429 filed Apr. 21, 1998 now U.S. Pat. No. 6,106,668 and Ser. No. 09/568,889 filed May 11, 2000 now U.S. Pat. No. 6,325,890 the disclosures of which are incorporated by reference herein.




A method is provided for feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising or consisting of: a) slurrying the material with a slurrying liquid to produce a slurry of material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure and transferring the slurry to a high-pressure transfer device; c) introducing the slurry to the high-pressure transfer device; d) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure; e) transferring the slurry from the high-pressure transfer device to the treatment vessel; f) introducing the pressurized slurry to the treatment vessel; and g) removing at least some of the liquid from the slurry between a) and c), using the drainer described above, so that the slurry introduced to the high-pressure transfer device in c) has a second liquid-to-material ratio lower than the first ratio. In a preferred embodiment, at least some of the liquid removed during step g) is used as at least some of the slurrying liquid of step a). Preferably g) is performed immediately prior to c), but f) may be performed at any time after a).




The method also may further include h) treating the material in the treatment vessel to produce cellulose pulp, for example, by a continuous or non-continuous (that is batch) chemical pulping process. For example, those processes disclosed in U.S. Pat. Nos. 5,489,363; 5,536,366; 5,547,012; 5,575,890; 5,620,562; 5,662,775; 5,824,188; 5,849,150; and 5,849,151 and marketed by Ahlstrom Machinery under the trademark LO-SOLIDS®.




The first liquid-to-material volume ratio is used in slurrying the material in a) is typically greater than 2.75:1, preferably about 2.75 to 3.25 to 1.0. This ratio is typically required in order for the slurry pump, for example, a Hidrostal® screw-type-impeller slurry pump manufactured by Wemco of Salt Lake City, Utah, or a pump provided by Lawrence Pumps Inc. of Lawrence, Mass., to operate properly. Though for other types of slurry pumps this L/W ratio may even be lower, for example, 2.50:1 or less. The second liquid-to-material ratio (that is, the ratio for the slurry introduced to the high-pressure feeder) is preferably about 2.50:1 or less, preferably about 1.75 to 2.25:1, or even less than about 1.75:1. In a preferred embodiment of this invention the second L/W ratio is at least 0.25 less than said first liquid-to-material ratio, most preferably at least 0.50 less than said first liquid-to-material ratio.




The first pressure to which the slurry is pressurized typically is in the range of 1 to 7 bar gage; the second pressure is typically in the range of 5 to 15 bar gage.




The present invention also includes a system for feeding comminuted cellulosic fibrous material to a treatment vessel, comprising or consisting of: a first vessel containing a slurry of comminuted cellulosic fibrous material having a first liquid-to-material volume ratio; a high-pressure transfer device having a low-pressure inlet, a low-pressure outlet, a high-pressure inlet, and a high-pressure outlet connected to the treatment vessel; means for pressuring and transferring the slurry from the first vessel to the low-pressure inlet of the high-pressure transfer device; a means for removing at least some of the liquid from the slurry located between the pressurizing means and the low-pressure inlet to provide a slurry having a liquid-to-material ratio less than the first ratio, the removal means comprising the drainer described above; and a means for transferring the slurry from the high-pressure outlet to the treatment vessel.




The first vessel is preferably a Chip Chute or Chip Tube provided by Ahlstrom Machinery. The high-pressure transfer device is preferably a High-pressure Feeder as sold by Ahlstrom Machinery. The means for pressurizing and transferring the slurry to the high-pressure transfer device may be a chip pump for pumping the slurry into the high-pressure transfer device or a pump (for example, a pump known as a Chip Chute Circulation Pump) for drawing the slurry into the high-pressure transfer device, or any other suitable conventional pressurizing device. A means for transferring the slurry from the high-pressure outlet of the high-pressure transfer device preferably comprises a high-pressure pump that provides pressurized liquid to the high-pressure inlet of the high-pressure transfer device. The preferred liquid-to-material ratios and pressures are preferably as described above.




Another aspect of the invention comprises a method of feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising or consisting of: a) slurrying the material with a slurrying liquid to produce a slurry of material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure and transferring the slurry to a high-pressure transfer device; c) introducing the slurry to the high-pressure transfer device; d) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure using a pressurized liquid and to produce a slurry of liquid having a second liquid-to-material volume ratio, higher than the first ratio; e) discharging the slurry having the second volume ratio from the high-pressure transfer device; f) transferring the slurry to the treatment vessel; g) introducing the pressurized slurry to the treatment vessel; and h) removing at least some of the liquid from the slurry between e) and g) so that the slurry introduced to the treatment vessel in g) has a third liquid-to-material ratio lower than the second ratio, the liquid removal practiced using a drainer as described above.




In a preferred embodiment, at least some of the liquid removed during h) is used as the pressurized slurrying liquid for d). In another preferred embodiment at least some of the liquid removed during h) is used as the slurrying liquid in a). Also h) is preferably performed immediately after e) but h) may be performed at any time after e) but before g). The present invention also may further include i) treating the material in the treatment vessel to produce cellulose pulp, for example, by a continuous or non-continuous, that is batch, chemical pulping process. For example, those processes disclosed in U.S. Pat. Nos. 5,489,363; 5,536,366; 5,547,012; 5,575,890; 5,620,562; 5,662,775; 5,824,188; 5,849,150; and 5,849,151 and marketed by Ahlstrom Machinery under the trademark LO-SOLIDS®. Also the method is preferably practiced to, between a) and c), remove some of the liquid from the slurry before the slurry is introduced into the high pressure device so that the slurry has a fourth liquid to material ratio at least about 0.25 less than the first ratio.




In one preferred embodiment of this invention, the above method is performed such that h) is practiced prior to g) so that a slurry having a third liquid-to-material ratio is introduced to the treatment vessel. This embodiment also preferably additionally includes i) removing excess liquid from the slurry during or shortly after the process of g), that is, while introducing the slurry to the treatment vessel, or shortly thereafter, and also j) combining the liquids removed at g) and i) and using at least some of the combined liquids as the pressurizing medium in d). Furthermore, j) preferably is practiced by monitoring the temperature of the combined liquids and regulating the flow of the liquids in h) and i) so that the temperature of the combined liquid is maintained below a specified value. The specified temperature value typically ranges from about 90 to 120° C. depending upon the prevailing pressure in the feed system.




The first liquid-to-material volume ratio is used in slurrying the material in a) is typically greater than 2.75:1, that is, about 2.75 to 3.25 to 1.0. This ratio is typically required in order for the slurry pump, for example, a Hidrostal® screw-type-impeller slurry pump manufactured by Wemco, to operate properly. For other types of slurry pumps this L/W ratio may even be lower, for example, 2.50:1 or less. The second liquid-to-material ratio is typically greater than 2.50:1, for example about 5.0:1 or greater, preferably about 7.0:1 or greater, or even 9.0:1 or greater. The third liquid-to-material ratio is typically at least about 0.25 less than the second liquid-to-material ratio, most preferably at least about 0.50 less than the second liquid-to-material ratio.




The first pressure to which the slurry is pressurized typically is in the range of 1 to 7 bar gage; the second pressure is typically in the range of 5 to 15 bar gage.




According to another aspect of the invention there is provided a cellulosic fibrous material treating system comprising: A material slurry vessel. A high pressure transfer device including a low pressure inlet, low pressure outlet, high pressure inlet and high pressure outlet. The slurrying vessel operatively connected to said low pressure inlet and outlet. A treatment vessel connected to the high pressure outlet. Means for removing some liquid from slurry moving between the high pressure outlet and treatment vessel and circulating the removed liquid to the high pressure inlet, said means comprising the drainer described above. And, the system devoid of a connection from the treatment vessel to the high pressure inlet. The system may also include means for removing some liquid from the slurry between said slurrying vessel and low pressure inlet, and returning removed liquid to the slurrying vessel, said means comprising the drainer described above.




The present invention also includes a system for feeding comminuted cellulosic fibrous material to a treatment vessel having an inlet, comprising or consisting of: a first vessel containing a slurry of comminuted cellulosic fibrous material having a first liquid-to-material volume ratio; a high-pressure transfer device having an low-pressure inlet, a low-pressure outlet, a high-pressure inlet and a high-press outlet; means for pressuring and transferring the slurry from the first vessel to the low-pressure inlet of the high-pressure transfer device; means for diluting the slurry and transferring the slurry from the high-pressure outlet to the treatment vessel at a second liquid-to-material ratio, greater than the first ratio; and means for removing at least some of the liquid from the slurry located between the high-pressure outlet of the high-pressure transfer device and the treatment vessel inlet to provide a slurry having a third liquid-to-material ratio less than the second ratio to the inlet of the treatment vessel, said means comprising the drainer described above.




The first vessel is preferably a Chip Chute or Chip Tube provided by Ahlstrom Machinery. The high-pressure transfer device is preferably a High-pressure Feeder as sold by Ahlstrom Machinery. The means for pressurizing and transferring said slurry to the high-pressure transfer device may be a chip pump for pumping the slurry into the high-pressure transfer device or a pump (for example, a pump known as a Chip Chute Circulation Pump) for drawing the slurry into the high-pressure transfer device, or any other suitable conventional pressurizing device. The means for diluting the slurry and transferring the slurry from the high-pressure outlet of the high-pressure transfer device is preferably a high-pressure pump that provides pressurized liquid to the high-pressure inlet of the high-pressure transfer device. The preferred liquid-to-material ratios and pressures are as described above.




The above methods and apparatuses in which liquid is removed prior to introducing a slurry to the high pressure transfer device or liquid is removed after the slurry is discharged from the high-pressure transfer device can be used alone or in tandem. In either case, the flow of liquid from the two liquid removal devices is preferably controlled, for example, by appropriate valves, and in one embodiment the flows can be combined. The temperature of the individual liquids or of the combined liquid is preferably monitored and limited to a temperature that will prevent flashing of the liquid in the feed system. This is preferably effected by controlling the amount of liquid removed from the respective liquor separators, for example, by appropriate valves. The temperature of the liquids may also be controlled by passing one or more of the liquids through a cooling heat exchanger. This cooling heat exchanger may be used to heat other fluids, such as dilution liquids or cooking liquor, including kraft white liquor.




The present invention also includes a system for feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel, comprising or consisting of: a first vessel containing a slurry of material and liquid having a top and a bottom, with an inlet adjacent the top and an outlet adjacent the bottom; a high-pressure transfer device having a low pressure inlet, a low pressure outlet, a high-pressure inlet, and a high-pressure outlet, the high-pressure outlet operatively connected to the treatment vessel; a pump, operatively connected to the outlet of the first vessel, for pressuring and transferring the slurry to the low-pressure inlet of the high-pressure transfer device; and means for removing liquid from the slurry located between the pump and the treatment vessel. The means for removing liquid from the slurry is distinct from the high-pressure transfer device and comprises a drainer as described above. The treatment vessel is preferably one or more continuous digesters, or one or more batch digesters, for producing cellulose pulp, and comprises a drainer as described above. The drainer may be located immediately upstream or downstream of the high-pressure transfer device, or two such drainers may be used: one upstream of the transfer device and one downstream.




In a preferred embodiment, the means for removing liquid from the slurry comprises a first means located near to or adjacent the inlet of the treatment vessel while the treatment vessel also includes a second means for removing liquid from the slurry. In this embodiment, the liquid removed from the first means and second means is combined and returned to the high-pressure transfer device. The first means is preferably a drainer as described above, and the second means is preferably a Top Separator, Inverted Top separator, or “stilling well” arrangement located in the inlet of the treatment vessel, but other conventional devices may alternatively or additionally be utilized. The first and second means for removing liquid also preferably include a means for regulating the flow of liquid removed, for example, using conventional control valves. Also, the invention preferably includes means for measuring the temperature of the combined liquids, and means for regulating the flow of liquid from the first and the second means for removing liquid to maintain a specified maximum temperature of the combined liquids.




The system of the present invention preferably also includes a pretreatment vessel, for example, a steaming vessel, having an inlet and an outlet which communicates with the inlet of the first vessel. The pretreatment vessel is preferably a DIAMONDBACK® steaming vessel as sold by Ahlstrom Machinery and described in U.S. Pat. Nos. 5,500,083; 5,617,975; 5,628,873; and 4,958,741, or a CHISELBACK™ vessel as described in co-pending application Ser. No. 09/055,408 filed on Apr. 6, 1998, now U.S. Pat. No. 6,189,288, though other more conventional screw-conveyor-type steaming vessels, or other conventional constructions, may be used. The system also preferably includes a metering device positioned between the pretreatment vessel and the first vessel. The metering device may be a star-type metering device, such as a Chip Meter as sold by Ahlstrom Machinery, or a screw-type metering device. In a preferred embodiment of the invention, the first vessel is a Chip Tube or Chip Chute as also sold by Ahlstrom Machinery.




These and other embodiments of this invention will become more apparent upon review of the following drawings and the attached claims.











BRIEF DESCRIPTION OF THE DRAWINGS





FIG. 1

is a schematic illustration of a continuous digester system employing a prior art feed system over which the present invention is an improvement.





FIG. 2

is a detailed view of the prior art feed system used in the digester system of

FIG. 1

;





FIG. 3

is a schematic illustration of one embodiment of the present invention;





FIG. 4

is a schematic illustration of another embodiment of the present invention;





FIG. 5

is a cross-sectional view of an exemplary prior art drainer that can be used in the practice of the present invention.





FIG. 6

is a cross-sectional view, similar to

FIG. 5

, of another embodiment of drainer that can be used according to the present invention.





FIG. 7

is a detailed view of the screen basket of the drainer of

FIG. 6

; and





FIG. 8

is cross-sectional view of another embodiment of the present invention.











DETAILED DESCRIPTION OF THE DRAWINGS





FIGS. 1 and 2

illustrate typical prior art systems for handling the feeding and treatment of comminuted cellulosic fibrous material to produce cellulose pulp.

FIG. 1

illustrates a cellulose treatment system


10


having a feed system


11


and a digester system


12


.

FIG. 2

illustrates a detailed view of a similar feed system


11


′ for introducing, steaming, slurrying and pressurizing comminuted cellulosic fibrous material, for example, hardwood or softwood chips, and feeding the slurry to a continuous digester system


12


. These systems are disclosed in U.S. Pat. No. 5,476,572; 5,622,598; 5,635,025; 5,766,418; and 5,968,314 and are marketed under the trademark LO-LEVEL® by Ahlstrom Machinery.




Though comminuted cellulosic fibrous material may take many forms, including sawdust; grasses, such as straw or kenaf; agricultural waste, such as bagasse; recycled paper; or sawdust, for the sake of simplicity, the term “chips” will be used when referring to comminuted cellulosic fibrous material; but any and all of the listed materials, and others not listed, may be processed by the present invention. Also, though a continuous digester in shown in

FIG. 1

, it is understood that the present invention as also applicable to feeding several continuous digesters or one or more discontinuous or batch digesters.




As shown in

FIGS. 1 and 2

, chips


13


are introduced to the system, for example, via a conveyor (not shown) from a chip storage facility, for example, a woodyard, via an isolation and metering device


14


,


14


′. For example,

FIG. 1

illustrates a star-type Airlock Feeder as sold by Ahlstrom Machinery Inc. of Glens Falls, N.Y.

FIG. 2

illustrates a screw-type isolation device


14


′ described in U.S. Pat. No. 5,766,418 and having a similar function to device


14


of FIG.


1


. The device


14


,


14


′, driven by an electric motor (not shown), introduces the chips to chip retention and streaming vessel


16


by means of a counter-weighted gate assembly


15


. Though various types of vessels are known in the art, vessel


16


is preferably a DIAMONDBACK® Steaming vessel as marketed by Ahlstrom Machinery and described in U.S. Pat. No. 5,500,083; 5,617,975; 5,628,873; and 4,958,741, or a CHISELBACK™ vessel as described in co-pending application Ser. No. 09/055,408 filed on Apr. 6, 1998 now U.S. Pat No. 6,199,299. This vessel typically includes a gamma-radiation level-detection system, a regulated vent for discharging gases which accumulate in the vessel and one or more steam introduction conduits (


16


′ in FIG.


2


), as is conventional. The pressure in the vessel


16


may be slightly below atmospheric pressure or slightly above atmospheric pressure, that is, the pressure in vessel


16


may vary from about −1 to 2 bar gage (that is, about 0 to 3 bar absolute).




During treatment with steam in vessel


16


, the air that is typically present in the chips is displaced by steam and the heating of the chips is initiated. The removal of air from the cavities within the chips permits the more efficient diffusion of cooking chemical into the chip and minimizes the buoyant forces on the chip during subsequent processing.




The steamed material is discharged from the bottom of the vessel


16


to a metering device


17


, for example, a star-type metering device or Chip Meter as sold by Ahlstrom Machinery, though any type of meeting device may be used. The metering device


17


is typically driven by an electric motor (not shown) and the speed of rotation of the metering device is typically controlled by operator input to define a set rate of introducing chips to the system. The chips discharged by the metering device


17


are introduced to a vertical conduit or pipe


18


, for example, a Chip Tube sold by Ahlstrom Machinery. Cooking chemical and other liquids are typically first introduced to the chips in conduit


18


by means of one or more conduits


19


such that a level of liquid is established in conduit


18


and a slurry of chips and liquid is present in the bottom of conduit


18


. This level of liquid is typically monitored and controlled by a level detection device, for example, a gamma-radiation level detection device or a “d-p” cell. The metering device


17


typically does not act as a pressure isolation device, though it may, and the pressure in conduit


18


typically varies from 0 to 2 bar gage (or 1 to 3 bar absolute).




Conduit


18


discharges the slurry of chips and liquid by means of a radiused section


20


to the inlet of slurry pump


21


. Though any slurry pump can be used, pump


21


is preferably a Hidrostal®) screw centrifugal pump sold by Wemco Pump of Salt Lake City, Utah or a pump provided by Lawrence Pumps Inc. of Lawrence, Mass. Slurry pump


21


, driven by electric motor


21


′ (see FIG.


2


), pressurizes and transfers the slurry in conduit


18


via conduit


22


to the low pressure inlet


23


of a high pressure transfer device


24


. This high pressure transfer device is preferably a High-pressure Feeder as sold by Ahlstrom Machinery. High-pressure Feeder


24


includes a pocketed rotor mounted in a housing typically having a low-pressure inlet


23


, a low-pressure outlet


25


, a high-pressure inlet


26


and a high-pressure outlet


27


. The low-pressure outlet


25


typically includes a screen plate (not shown) which minimizes the passage of chips out of low-pressure outlet


25


while allowing the liquid in the slurry to pass out outlet


25


to conduit


28


, though as disclosed in pending U.S. provisional application No. 60/138,280 filed on Jun. 9, 1999, the screen in the low-pressure outlet of feeder


24


may be omitted. The chips which are retained in the feeder by the screen are slurried with high-pressure liquid provided by pump


29


, preferably a Top Circulation Pump (TCP) provided by Ahlstrom Machinery, to inlet


26


via conduit


30


. The slurry is discharged out of high-pressure outlet


27


into conduit


31


and to the digester


32


of digester system


12


at a pressure of between about 5 and 15 bar gage, typically between about 7 to 12 bar gage.




Digester


32


(see

FIG. 1

) may be a single or multiple-vessel digester and may be a hydraulic or steam-phase digester. Digester


32


may also consist or comprise one or more batch digesters. The cellulose material with added cooking chemical is treated under temperature and pressure in digester


32


and essentially fully-treated chemical cellulose pulp is discharged into conduit


50


at the bottom of the digester. Digester


32


typically includes a plurality of screen assemblies


51


,


52


,


53


, and


54


; liquor circulations


55


,


56


, and


57


having pumps


58


,


59


, and


60


and heat exchangers


61


,


62


, and


63


; cooking liquor introduction conduits


64


,


65


, and


66


, supplied by pump


67


, as is conventional, in order to treat the cellulose material. Though many types of processes may be performed in digester


32


, one preferred process is the process described in U.S. Pat. Nos. 5,489,363; 5,536,366; 5,547,012; 5,575,890; 5,620,562; 5,662,775; 5,824,188; 5,849,150; and 5,849,151 and marketed by Ahlstrom Machinery under the trademark LO-SOLIDS®. According to this preferred process, one or more dilution liquid (for example, wash filtrate) introduction conduits


68


,


69


, and


70


are provided which are supplied by filtrate pump


71


, also known as a Cold Blow Pump (CBP). The liquid pressurized by pump


71


may be heated or cooled as desired by heat exchangers


72


and


73


. The process performed in digester


32


may also be one of the processes disclosed in U.S. Pat. Nos. 5,635,026 or 5,779,856 and marketed under the name EAPC™ cooking by Ahlstrom Machinery.




As shown in

FIG. 1

, excess liquor in the slurry in conduit


31


at the top of the digester


32


is separated from the slurry by a liquor separator


33


and returned to the feed system


11


by means of conduit


34


(again, also shown in FIG.


2


). The liquid in conduit


34


is pressurized by pump


29


, driven by electric motor


29


′ (FIG.


2


), and provides the pressurized slurrying liquid introduced to the high-pressure inlet


26


of feeder


24


via conduit


30


. Feeder


24


is typically driven by an electric motor (not shown), the speed of which is monitored and controlled.




As shown in both

FIGS. 1 and 2

, the liquid discharged from the low-pressure outlet


25


of high-pressure feeding device


24


passes via conduit


28


to a cyclone-type separator


35


which isolates undesirable material and debris, such as sand, stones, etc., from the liquid in conduit


28


. Separator


35


is preferably a Sand Separator as sold by Ahlstrom Machinery. Liquid having little or no undesirable material or debris is discharged from separator


35


and is passed through a liquor separating device


37


via conduit


36


. At least some liquid is removed from the liquid separator


35


, which is preferably an Inline Drainer as sold by Ahlstrom Machinery (preferably of the improved design seen in FIGS.


6


-


8


), via conduit


38


and sent to vessel


39


. Vessel


39


is preferably a Level Tank as sold by Ahlstrom Machinery. Liquid is discharged from vessel


39


to conduit


40


and pump


41


and is supplied to digester


32


(see

FIG. 1

) as liquor make-up as needed via conduit


42


. Pump


41


is preferably a Make-Up Liquor Pump (MLP) as sold by Ahlstrom Machinery. As also disclosed in pending application No. 60/138,280 the Sand Separator


35


, Level Tank


36


, and In-line Drainer


37


can be omitted without interfering with the ultimate function of the feed system


11


.




The liquid discharged from separator


37


into conduit


43


may be supplemented with cooking chemical, for example, kraft white, green, orange (that is, liquid containing polysulfide additives) or black liquor, introduced via conduit


44


(see

FIG. 1

) prior to being introduced to tank


45


. Tank


45


is preferably a Liquor Surge Tank as sold by Ahlstrom Machinery and described in U.S. Pat. No. 5,622,598. The cooking chemical introduced via conduit


44


may be heated or, preferably, cooled as needed by heat exchanger


46


(see FIG.


1


). Some of the liquid in conduit


43


may bypass tank


45


and be introduced via conduit


19


to conduit


18


as described above. Tank


45


communicates with conduit


18


and the inlet of pump


21


via conduits


47


and


20


. As disclosed in pending application No. 60/124,890 filed on Mar. 18,1999, tank


45


may comprise or consist of an integral vessel concentric with conduit


18


.




According to the prior art system shown in

FIGS. 1 and 2

, the amount of liquid in the slurry transferred in conduit


22


by pump


21


is governed by the capacity of the pump


21


. That is, typically screw-type-impeller slurry pumps, such as the Wemco Hidrostal® pump, are limited to pumping slurries having a minimum liquid content, that is, a minimum liquid-to-solid, or, in this case, a limited liquid-to-wood chip, ratio. Thus, in prior art systems, the amount of solid material that can be subsequently transferred by the high-pressure transfer device


24


is governed and limited by the solid transfer capacity of the pump


21


. The present invention overcomes this limitation of the prior art.





FIG. 3

illustrates one embodiment of an improved system which may effectively utilize a drainer according to the invention.

FIG. 3

illustrates a feed system


111


including many of the components found in feed system


11


of FIG.


1


and feed system


11


′ of FIG.


2


. Similar components in

FIG. 3

to those shown in

FIGS. 1 and 2

are identified by the same reference numerals shown in

FIGS. 1 and 2

but preceded by the a “1”.




Steamed chips


113


are introduced to horizontal metering-screw conveyor


117


in FIG.


3


. Conveyor


117


performs a similar function as metering device


17


in

FIGS. 1 and 2

. Chips, or other comminuted cellulosic fibrous material,


113


are typically steamed in a steaming vessel prior to being introduced to conveyor


117


, for example, the chips are steamed in a DIAMONDBACK® steaming vessel such as vessel


16


shown in FIG.


2


. The chips


113


are discharged from metering screw


117


into a vertical conduit or vessel


118


, which is preferably a Chip Tube or Chip Chute. Conduit or vessel


118


may include a radiused tramp material separation device as disclosed in copending application Ser. No. 08/905,324 filed on Aug. 4, 1997, now U.S. Pat. No. 6,024,227, the disclosure of which is included by reference herein. In a preferred embodiment, the Chip Tube includes a radiused discharge


120


which feeds a slurry pump


121


. The slurry pump


121


is preferably a Hidrostal® pump or a Lawrence pump. Slurrying liquid is introduced to conduits


118


and


120


via conduits


119


and


147


. The liquid introduced via conduits


119


and


147


typically includes some form of chip treatment liquid, for example, kraft white, green, or black liquor, weak black liquor, soda liquor, or liquor including some form of strength or yield enhancing, or metal sequestering additive, such as polysulfide, anthraquinone, chelating agents (such as EDTA and DPTA and their equivalents), surfactants, penetrants, or their equivalents or derivatives. The treatment liquid is introduced via conduit


144


. Pump


121


pressurizes and transfers the slurry via conduit


122


to a high-pressure transfer device


124


, for example, a High Pressure Feeder sold by Ahlstrom Machinery.




Slurry pumps, such as the Hidrostal pump, typically require that the slurry being pumped have a minimum content of liquid, that is, a minimum liquid-to-wood (L/W) volume ratio. For the Wemco Hidrostal slurry pump


121


shown, the L/W ratio of the slurry must be at least 2.75:1, preferably at least 3.0:1. That means that the slurry passing through conduit


122


and being introduced to feeder


124


also has approximately this same L/W ratio. In conventional systems, the pump


121


requirement limits the L/W ratio of the slurry introduced to and transferred by the feeder


124


.




However, according to the present invention, the L/W ratio of the slurry introduced to the feeder


124


is not limited by the L/W ratio that can be transferred by the slurry pump


121


. According to the present invention, some form of liquid removal device


153


is provided upstream of the feeder


124


which removes at least some of the liquid in the slurry in conduit


122


so that the slurry introduced to the feeder


124


has a lower L/W ratio, typically at least about 0.25 lower, preferably at least about 0.5 lower, than the slurry transferred by pump


121


.




The liquid removal device, or dewatering device,


153


shown schematically in

FIG. 3

may be an isolated device or it may be integral with the feeder


124


. The device


153


typically includes a liquid permeable barrier or screen


153


′, for example, a perforated cylinder, which retains the material (chips) in the flow of slurry while removing at least some of the liquid from the slurry into conduit


150


. The screen or barrier


153


′ may be made from perforated plate, for example, screen plate having circular or slotted holes, or may be made from parallel bar-type screen construction. Device


153


may include rotating, reciprocating, vibrating, or otherwise movable components which by their movement minimize or prevent the pluggage of the screen or barrier. The device


153


may also include some form of conventional back-flush mechanism (not shown) which periodically forces a flow of liquid in a direction opposite the direction that the liquid is typically removed to again minimize or prevent pluggage of the screen or barrier. One device that may be used for dewatering device


153


is an In-line Drainer as sold by Ahlstrom Machinery and shown in

FIG. 5

but preferably the device


153


is a drainer as shown in

FIGS. 6-8

.




Conduit


150


transports the liquid removed from the slurry back to conduits


118


and


120


via conduits


143


,


119


, and


147


to provide the slurrying liquid to conduits


118


,


120


. This flow of liquid is typically supplemented with treatment chemical, as described above, via conduit


144


. The flow of liquid through conduit


150


,


143


is typically regulated by a (preferably solenoid operated) flow control valve


151


. Conduit


143


may include a conventional Sand Separator (item


35


in FIG.


2


), In-line Drainer (item


37


in FIG.


2


), Level Tank (item


39


in FIG.


2


), and Liquor Surge Tank (item


45


in FIG.


2


), if desired.




The slurry having reduced liquid content is then introduced to the low-pressure inlet


123


of feeder


124


. The operation and components of feeder


124


are described in U.S. Pat. Nos. 5,236,285 and 5,236,286, the disclosures of which are included by reference herein. The pocketed rotor (not shown) of the feeder


124


accepts the slurry having reduced liquid content and, through rotation, exposes the slurry to high-pressure liquid supplied to the high-pressure inlet


126


by high pressure pump


129


via conduit


130


. This high-pressure flow flushes the chips from the rotor pocket and discharges them out of high pressure outlet


127


and into conduit


131


. The slurry, now diluted with pressurized liquid introduced by pump


129


, is then propelled to the top of a treatment vessel (item


32


shown in

FIG. 1

) via conduit


131


. Conventionally, the slurry in conduit


131


typically has a L/W ratio greater than 6.0:1, possibly even greater than 8.0:1. Again, this treatment vessel may be one or more continuous digesters or one or more batch digesters. The continuous digester may be a hydraulic or vapor-phase digester having one or more vessels, for example, the digester may include an impregnation vessel.




As is conventional, excess liquid may be removed from the slurry upon introduction to the digester, such as by using a liquid separation device, for example, a Top Separator (item


33


in FIG.


1


). This separated liquid is returned to feed system


111


via conduit


134


to supply at least some of the liquid provided by pump


129


to the high-pressure inlet


126


of feeder


124


.




As the slurry is introduced to feeder


124


via conduit


122


at least some of the liquid in the slurry passes through the rotor pocket (again, not shown) and is discharged from the feeder


124


via low-pressure outlet


125


. The outlet


125


may include a conventional screen element to prevent the passage of chips out of outlet


125


or no screen element may be present. As in conventional operation, the liquid moving through outlet


125


, which is under pressure supplied by pump


121


, is passed via conduit


128


to conduits


119


and


147


to provide the source of slurrying liquid in conduits


118


and


120


. However, in the embodiment of the present invention shown in

FIG. 3

, the slurrying liquid is also provided to conduits


118


,


120


via conduits


119


,


147


,


150


and


143


from dewatering device


153


. Since the liquid in line


128


may be hotter than 100° C. and the pressure in conduits


143


,


147


,


118


,


119


, or


120


may be lower than 1 atm, to prevent flash evaporation, the liquid in line


128


may be cooled by heat exchanger


156


prior to introducing the liquor to line


143


.




Another advantage of the present invention is that by removing liquid from the slurry in conduit


122


via separator


153


, prior to exposing this liquid to the hotter temperature liquid in feeder


124


(for example, the hot liquid returned from the treatment vessel via conduits


134


and


130


), the temperature of the liquid returned to the typically unpressurized conduits


118


and


120


may be cooler. Therefore, the liquid in conduits


150


,


143


,


147


and


119


typically will not have to be cooled to prevent flash evaporation in these conduits or in conduits


118


and


120


.




In another embodiment of the invention, a liquor separator


154


may also be introduced adjacent to the high-pressure outlet


127


of feeder


124


. This separator


154


typically is similar to separator


153


described above and typically includes a barrier or screen


154


′ and, again, may be integral with the feeder


124


or separate from feeder


124


. The separator


154


may be used in place of separator


153


or in conjunction with separator


153


to remove additional liquid from the slurry prior to passing the slurry via conduit


131


to the treatment vessel. The liquid removed using the separator


154


, since it is pressurized and typically hotter than 100° C., is preferably passed via conduit


157


to conduit


134


, which is also typically pressurized and hotter. The flow of liquid out of separator


154


and through conduit


157


is typically regulated by control valve


158


, which is desirably automatically operated.




The liquid removed by means of separator


154


may also be returned to conduits


118


and


120


directly or via conduit


150


via conduit


159


, shown in phantom. Since the liquid in conduit


159


may be hotter than 100° C., the liquid in conduit


159


will typically require some form of cooling prior to introducing it to conduit


150


, for example, by passing it through heat exchanger


160


. The flow of liquid through conduit


159


is typically regulated by valve


161


.




In one mode of operation, the liquid removed from the slurry by separators


153


or


154


is of sufficient volume so that little or no excess liquor is introduced to the treatment vessel via conduit


131


, so that in turn little or no liquid need be returned to the feed system via conduit


134


, and conduit


134


may be eliminated. In such a case, the liquor separation device (item


33


in

FIG. 1

) is unnecessary and this device may be eliminated along with its associated cost and maintenance. Furthermore, by eliminating this return of liquid to the feed system from the treatment vessel, little or no heat that is typically returned with this liquid is introduced to the feed system. As a result, the impact of this heat upon the operation of the feed system, for example, undesirable liquid flashing, and upon the treatment of the material is reduced or substantially eliminated. For example, by employing this mode of operation, the cooler impregnation processes disclosed in U.S. Pat. Nos. 5,736,006 and 5,958,181 are more readily implemented.




Furthermore, should sluicing liquid be desired and the top separator (


33


in

FIG. 1

) and the return line


134


from the top separator have been eliminated, sluicing liquor may also be obtained from one or more of the liquor circulations associated with digester


32


(see

FIG. 1

) which are closer in proximity than separator


33


. In conventional pulp mill installations, pump


29


is physically located in an area adjacent to the pumps associated with the liquor circulations of digester


32


, for example, pumps


50


,


59


, or


60


in FIG.


1


. By using the liquors in these circulations, for example, the liquor extracted from the upper cooking circulation screens


51


and pressurized by pump


50


, a more accessible source of sluicing liquor is obtained. For example, only a short pipe run need be required from the piping associated with pump


50


to the inlet of pump


29


, instead of the long pipe run from the Top Separator


33


(in

FIG. 1

) at the top of the digester to pump


29


adjacent the feeder


24


. In addition, the active cooking chemical, that is, the alkali, present in the circulations associated with the digester may offset the alkali typically needed in the feed system. The sluicing liquors obtained from these cooking circulations may also contain at least some sulfide which, as is known in the art, is beneficial to have in the treatment liquors used early in the cooking process, for example, in the sluicing liquor in conduit


34


,


134


.




Another embodiment of the present invention is shown in FIG.


4


.

FIG. 4

partially illustrates a feed system


211


similar to feed systems


11


,


11


′, and


111


described above, which feeds a continuous digester


232


, similar to digester


32


in FIG.


1


. Components in

FIG. 4

comparable to those in

FIGS. 1-3

are shown by the same two digit reference numeral but preceded by a “2”.




In feed system


211


, a slurry of comminuted cellulosic fibrous material


222


is introduced to a high-pressure transfer device


224


, similar to devices


24


and


124


above. This slurry


222


may be pressurized by a slurry pump, such as pumps


21


and


121


in

FIGS. 1

,


2


, and


3


, or may simply be provided by a conventional Chip Chute from a horizontal screw-type steaming vessel. The feeder


224


pressurizes and transfers the slurry to digester


232


via conduit


231


. Though not shown in

FIG. 4

, liquid removal devices


153


and


154


may also be present adjacent the feeder


224


as shown in FIG.


3


.




The inlet of the digester


232


includes a conventional liquor removal device


233


, a Top Separator, such as item


33


in

FIG. 1

, having a screw conveyor


261


, driven by electric motor


274


, and a perforated cylindrical screen


262


. The conveyor transfers the chips to the vessel in the direction of arrow


263


while removing liquid from the slurry as shown by arrow


264


and returning the liquid via conduits


265


and


234


, the TC line, to pump


229


and to feeder


224


via conduit


230


, as is conventional. The lower section of the separator housing


266


is preferably non-permeable so that little or no heated liquor can migrate from the exothermic reactions that are occurring in the chip column


267


in the vessel


232


.




According to this embodiment of the invention, a liquor removal device


254


is located in conduit


231


. This liquid removal device is preferably similar to devices


153


and


154


discussed above, and is preferably an In-line Drainer-type device as also discussed above, preferably of the improved design of

FIGS. 6-8

. According to this invention, at least some liquid is removed from the slurry via device


254


via conduit


257


, such that less liquid is introduced to the vessel


232


via conduit


260


. As a result, less liquid need be removed from the slurry by separator device


233


and less heat is withdrawn from the vessel and returned to the feed system where the heat can cause operational problems. In addition, by reducing the temperature of the liquid returned to the feed system, cooler, more beneficial treatments of the cellulose can be performed in the feed system, for example, those methods disclosed in U.S. Pat. Nos. 5,736,006 and 5,958,181.




As shown in

FIG. 4

, the temperature of the liquid in line


234


is preferably monitored by temperature sensor


270


. The temperature measured by sensor


270


can be used to regulate the flow of liquid from liquid separators


254


and


233


, for example, control signals


275


and


276


and automatic flow control valves


271


and


272


. Should the temperature of the liquid in line


234


exceed a specified value, for example, 100° C., the flow of hotter liquid through valve


271


can be reduced and the flow of cooler liquid through valve


272


can be increased. Also, the pressure drop across the inlet of the vessel, from conduit


260


to the outlet of the liquid separator at conduit


265


, can be monitored by pressure difference sensor


273


. This pressure difference can be limited to a specified value by controlling the speed of the screw of separator


233


. The speed of this screw can be varied by varying the speed of the motor


274


driving the screw.




The invention particularly contemplates all specific narrow ranges within a broad range. For example a L/W ratio of between about 4.0:1 and 10:0:1 means 8.5:1 to 10.0:1, 4.5:1 to 6.5:1, 5.0:1 to 9.0:1, and all other narrower ranges within that broad range.




One example of a liquor separating device that can be used in the practice of the present invention or as item


37


of

FIG. 2

is shown in FIG.


5


.

FIG. 5

illustrates a conventional In-line Drainer


300


as sold by Ahlstrom Machinery having an inlet


301


for a particulate-bearing liquid to be strained, an outlet


302


for liquid that has been strained, and an outlet


303


for the strained liquid. Drainer


300


includes a cylindrical housing


304


, having a cover plate


305


at a first or inlet end having the inlet opening


301


and a second or outlet end having end cover plate


306


. The cover plate


306


typically includes a lifting eye


307


and appropriate mounting hardware


308


, for example, threaded studs and nuts. The drainer


300


includes a cylindrical screen basket


309


positioned in the housing


304


. The upper end the screen basket


309


is mounted to the housing


304


by means of a annular mounting flange


310


on the housing and appropriate mounting hardware


311


, for example, threaded screws. The lower end of the screen basket


309


is snugly fit into a machined surface in the inlet


301


. The screen basket


309


is positioned in the housing


304


so that an annular cavity


312


is created between the outside surface of the screen basket


309


and the inside surface of the housing


304


. The screen basket


309


may also include a lifting eye


313


for removing the basked for replacement or servicing. The housing


304


also typically includes a gusseted mounting flange


314


for installing the drainer in the desired location and a steam purge inlet


315


for introducing steam for periodic steam cleaning of the drainer.




Though the centerline of the outlet


302


shown in

FIG. 5

is positioned at a right angle to the centerline of the housing


304


, the outlet


302


may also positioned in the top plate


306


so that its centerline is essentially collinear with the centerline of the housing. An outlet collinear with the centerline of the housing, and thus with the direction of flow, may be more desirable when the invention is used in the systems shown in

FIGS. 3 and 4

, that is, where the concentration of cellulose material is greater and abrupt changes in flow direction can cause undesirable flow restrictions and stagnation. The right-angled outlet orientation shown in

FIG. 5

is preferred when the drainer


300


is used as shown by item


37


in FIG.


2


.




In the conventional drainer


300


shown in

FIG. 5

, the screen basket


309


is fabricated from a series of evenly-spaced vertical bars


316


supported by a series of external annular rings


317


so that a straining surface is provided having a series of vertical slots


318


between the bars


316


. The bars


316


are typically welded to the rings


317


and to support rings


319


and


320


located at either end of the basket. The screen basket


309


also typically includes unperforated cylindrical sections


321


and


322


at each end of the screen basket


309


.




According to the prior art shown in

FIG. 5

, the lower cylindrical section


322


of the basket


309


includes a helical baffle


323


, which is typically referred to as the “flight”. As discussed above, this flight


323


induces a helical flow to the liquid introduced under pressure to inlet


301


so that the orientation of any chips, pins or fines that may be present in the slurry is less likely to be aligned with the vertical slots of the screen basket


309


.




The device shown in

FIG. 5

operates as follows. A pressurized flow of liquid, typically containing at least some wood chips, pins, or fines, or a slurry of liquid and chips, is introduced to the inlet


301


of the drainer


300


. When used as item


37


in

FIG. 2

, the liquid typically has a pressure ranging from about 0 to about 5 bar gage. When used as item


153


or


154


of

FIG. 3

or item


254


of

FIG. 4

, the pressure of the slurry introduced to the inlet


301


typically ranges from about 0 to about 30 bar gage. The design of the housing


304


and basket


309


will vary depending, among other things, upon this pressure. The helical baffle


323


imparts a tangential velocity component to this liquid flow so that the flow through the screen basket


309


is somewhat helical. As the liquid passes through the cylindrical screen basket


309


at least some liquid passes through the apertures, that is, the slots


318


, of the screen


309


, collects in substantially annular cavity or volume


312


, and is discharged out of the liquid outlet


303


. The liquid from outlet


303


can be forwarded to any appropriate location but is typically forwarded to Level Tank


39


when used in a feed system, as in

FIG. 2

, or can be recirculated as shown in

FIGS. 3 and 4

. The liquid and chips, fines, and pins and other material which do not pass through the screen basket


309


continue to and are discharged from the outlet


302


. When used as item


37


in

FIG. 2

, the liquid discharged from outlet


302


is typically passed to a conduit leading to the inlet of a High-pressure Feeder, such as a Chip Tube (item


18


in FIG.


2


), Chip Chute, or Liquor Surge Tank (item


45


in FIG.


2


). When used as item


153


or


154


of

FIG. 3

or item


254


of

FIG. 4

, the liquid discharged from outlet


302


is typically passed to a High-pressure Feeder (item


126


in FIG.


3


), or to a digester (via conduit


131


in

FIG. 3

or via conduit


260


in FIG.


4


).




The slot width and slot spacing will typically be a function of the content of the slurry passing through the drainer


300


and the desired pressure drop across the slots


318


. In the conventional use of the device


300


, for example, as used to treat a low-solid concentration slurry with smaller particles, as in as item


37


in

FIG. 2

, the slot


318


width may vary from between about 1 to 4 mm and the slots


318


are typically evenly spaced by about 2 to 6 mm. In the application of the present invention, for example, shown by item


153


or


154


in

FIG. 4

, when treating a slurry having a higher solid concentration with larger particles, the slot


318


width will typically vary between about 4 and 8 mm and typically be uniformly spaced by about 3 to 7 mm.




In the prior art device


300


shown in

FIG. 5

, the helical baffle


323


which induces a helical flow to the slurry or liquid passing through the drainer, in some instances, can produce an undesirable pressure drop across the drainer. According to the present invention, this baffle or flight


323


and the restriction to flow, or pressure drop, it can create are eliminated. Though this baffle or flight


323


may be used in conjunction with the obliquely oriented slots


318


of the present invention, it is preferred that this baffle or flight


323


be eliminated.




Two embodiments of the present invention are shown in

FIGS. 6

,


7


and


8


. The items in

FIGS. 6

,


7


, and


8


that are essentially identical to those found in

FIG. 5

are identified by the same reference numbers. The distinctions between the prior art and the present invention are identified by the same two digit reference numerals but are prefaced by the numerals “4” and “5”, respectively, instead of by the numeral “3” as shown in FIG.


5


.





FIG. 6

illustrates one embodiment of the present invention in which the screen basket slots are oriented obliquely to the direction of elongation of the housing. First, note that the “flight”, item


323


in

FIG. 5

, has been eliminated in FIG.


6


. That is, the inlet


301


is substantially devoid of any flow director or impediment, i.e., is substantially open and hollow. In addition, according to the present invention, in the substantially annular screen basket


409


of

FIG. 6

, the slots


418


formed by bars


416


and supported by annular rings


417


, are oriented at an oblique angle α to the direction of elongation of the screen basket


409


and the direction of elongation of the cylindrical housing


404


so that slots


418


are also oriented at an angle α to the direction of flow of liquid through the screen basket


409


. This is more clearly shown in the detail schematic of FIG.


7


.





FIG. 7

illustrates a detailed cross-section of a partial view of the screen basket


409


. Though the angle α shown in

FIG. 7

is illustrated at a preferred orientation of the slots


418


of approximately 45°, it is to be understood that according to this invention the angle α may range from plus or minus 5° to plus or minus 90 ° from the direction of elongation of the housing


404


. For example, in the embodiment of

FIG. 8

, the angle α is approximately plus 90°, that is, if the housing


404


is vertically elongated, the slots


518


are essentially horizontal. Again, in

FIG. 8

, the helical baffle


323


shown in

FIG. 5

is eliminated. All other features of

FIGS. 6 and 8

are essentially the same as FIG.


5


.




Though the embodiments shown in

FIGS. 6

,


7


, and


8


, illustrate parallel bar type construction, the present invention also includes machined-plate type construction. For example, the slots


418


,


518


, either continuous or discontinuous, may be fabricated from metal plate by any appropriate machining means including, but not limited to, water-jet cutting, laser cutting, EDM machining, drilling, milling, or any other conventional method of producing apertures in plate.




Also, the slots


418


,


518


may be continuous slots or they may be discontinuous slots interrupted by unperforated “land” areas. These land areas may be uniformly distributed throughout the screen basket


409


,


509


so that a uniform pattern of slots and land areas is established or the slots and land areas may be distributed non-uniformly. The orientation of the slots may also vary, for example, the angle of orientation of the slots


418


,


518


at one elevation in the direction of elongation of the screen basket may be different from the orientation of the slots at a second or an adjacent elevation. The orientation of slots at one elevation in the direction of elongation of the screen basket may also vary, for example, producing a “herring bone”-type pattern of slots. The angle α of the slots may also vary from one elevation to another or adjacent elevation or the angle α of the slots may vary within a given elevation.




The slots


418


,


518


of the screen basket


409


,


509


are preferably uniformly spaced and have a width of between about 1 to 20 mm and a distance between slots


418


,


518


that may vary from about 1 to 20 mm, depending upon the slurry treated by the drainer


400


,


500


and the desired pressure drop across the slots


418


,


518


. When used as item


37


in

FIG. 2

, the slurry being treated will typically have a relatively lower concentration of cellulose material and the slots


418


,


518


will have a width of about 0.5 to 10 mm, typically about 1 to 6 mm, preferably about 2 to 4 mm, and a distance between slots will be about 1 to 10 mm, typically about 1 to 6 mm, preferably about 3 to 4 mm. When used as item


153


or


154


of

FIG. 3

or item


254


of

FIG. 4

, the slurry being treated typically will have a relatively higher concentration of cellulose material and the slots


418


,


518


will have a width of about 0.5 to 15 mm, typically about 3 to 9 mm, preferably about 5 to 7 mm and a distance between slots of about 1 to 10, typically about 2 to 8 mm, preferably about 4 to 6 mm.




The invention shown in

FIGS. 6

,


7


, and


8


can be used in any desired location where liquid separation from a slurry of liquid and cellulose material is desired. The invention shown in

FIGS. 6

,


7


, and


8


may be used in a feed system for a digester, for example, as the device


37


in the feed system shown in

FIG. 2

herein. The invention shown in

FIGS. 6

,


7


, and


8


may also be used for treating slurries being handled by a High-pressure Feeder or being fed to a digester, either continuous or batch, as shown as item


153


or


154


of

FIG. 3

or item


254


of FIG.


4


.




The present invention provides a more effective system and method of introducing a slurry of comminuted cellulosic fibrous material to a treatment vessel. Unlike the prior art, the present invention is not limited to the solids transfer capacity of the pumping device. The present invention can transfer more material and less liquid so that more material can be introduced and treated per unit time than as in prior art systems, or the size and cost of the feed system reduced. As described above, the present invention also has various other benefits compared to the prior art.




While the invention has been described in connection with what is presently considered to be the most practical and preferred embodiment, it is to be understood that the invention is not to be limited to the disclosed embodiment, but on the contrary, is intended to cover various modifications and equivalent arrangements, structures, systems, and methods included within the spirit and scope of the appended claims.



Claims
  • 1. A drainer for draining liquid from a slurry moving in an axial flow direction, comprising:an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; and a dimension of elongation between said inlet and outlet and which is aligned with said axial flow direction; said inlet substantially open and hollow; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots therein; and said screen slots having an oblique inclination angle α with respect to said dimension of elongation between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots as said slurry moves in said axial flow direction along said dimension of elongation relative to said screen slots.
  • 2. A drainer as recited in claim 1 further comprising a plurality of land areas between regions of said slots.
  • 3. A drainer as recited in claim 1 further comprising a substantially annular volume between said screen and housing, and a steam purge connected to said volume.
  • 4. A drainer as recited in claim 1 further comprising a substantially annular volume between said screen and housing, and a liquid outlet from said volume.
  • 5. A drainer as recited in claim 1 wherein said screen comprises a plurality of spaced bars or wires.
  • 6. A drainer as recited in claim 1 wherein said screen comprises a milled plate.
  • 7. A method of feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel comprising;a) slurrying the material with a slurrying liquid to produce a slurry of material and liquid having a first liquid-to-material volume ratio; b) pressurizing the slurry to a first pressure and transferring the slurry to a high-pressure transfer device; c) introducing the slurry to the high-pressure transfer device; d) in the high-pressure transfer device, pressurizing the slurry to a second pressure, higher than the first pressure; e) transferring the slurry from the high-pressure transfer device to the treatment vessel; f) introducing the pressurized slurry to the treatment vessel; and g) removing at least some of the liquid from the slurry between a) and c) so that the slurry introduced to the high-pressure transfer device in c) has a second liquid-to-material ratio lower than the first ratio, wherein (g) is practiced using the drainer of claim 1.
  • 8. A drainer for draining liquid from a moving slurry, comprising:an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; and a dimension of elongation between said inlet and outlet; said inlet substantially open and hollow; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots therein; and said screen slots having an oblique inclination angle α with respect to said dimension of elongation between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots, a substantially annular volume between said screen and housing, and a liquid outlet from said volume, and a steam purge connected to said volume, and wherein said screen has a diameter of between about 0.5-3 feet.
  • 9. A drainer as recited in claim 8 wherein said angle α is substantially 90°.
  • 10. A drainer as recited in claim 8 wherein said angle α is between about 30-60°.
  • 11. A drainer as recited in claim 8 wherein said slots have a width of between about 2-4 mm, and said slots are substantially evenly spaced by about 3-4 mm.
  • 12. A drainer as recited in claim 8 wherein said slots have a width of between about 5-7 mm, and said slots are substantially evenly spaced by about 4-8 mm.
  • 13. A drainer for draining liquid from a moving slurry, comprising:an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; and a dimension of elongation between said inlet and outlet; said inlet substantially open and hollow; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots therein; and said screen slots having an oblique inclination angle α with respect to said dimension of elongation between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots, wherein said angle α is between about 10-80°, and said screen has a diameter of between about 0.5-3 feet.
  • 14. A pulp producing system comprising:a substantially upright digester; a feed system for feeding a slurry of comminuted cellulosic material to said digester; said feed system including a drainer which receives some liquid from a flow of slurry; and said drainer comprising: an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots; and said screen slots having an oblique inclination angle α with respect to said dimension of elongation of between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots; wherein said drainer inlet is substantially open and hollow and is positioned in a location in said feed system wherein the slurry has a L/W ratio of greater than about 20:1 but includes at least some pins, fines, or chips, and a pressure of from about 0-5 bar gauge; and wherein said slots are evenly spaced by about 3-4 mm and have a width of between about 2-4 mm.
  • 15. A pulp producing system comprising:a substantially upright digester; a feed system for feeding a slurry of comminuted cellulosic material to said digester; said feed system including a drainer which receives some liquid from a flow of slurry; and said drainer comprising: an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots; and said screen slots having an oblique inclination α with respect to said dimension of elongation of between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots; wherein said drainer inlet is substantially open and hollow; and is positioned in a location in said feed system wherein the slurry has a L/W ratio of less than about 15:1 and a pressure of about 0-30 bar gauge; and wherein said slots have a width of between about 5-7 mm, and wherein said slots are substantially evenly spaced by about 4-8 mm.
  • 16. A system for feeding comminuted cellulosic fibrous material to a treatment vessel having an inlet, comprising:a first vessel containing a slurry of comminuted cellulosic fibrous material having a first liquid-to-material volume ratio; a high-pressure transfer device having an low-pressure inlet, a low-pressure outlet, a high-pressure inlet and a high-pressure outlet; means for pressuring and transferring the slurry from said first vessel to said low-pressure inlet of said high-pressure transfer device; means for diluting said slurry and transferring the slurry from said high-pressure outlet to said treatment vessel at a second liquid-to-material ratio, greater than the first ratio; and means for removing at least some of the liquid from the slurry located between said high-pressure outlet of said high-pressure transfer device and said treatment vessel inlet to provide a slurry having a third liquid-to-material ratio, less than the second ratio, so as to feed slurry with the third ratio to the inlet of said treatment vessel; said liquid removal means comprising a drainer comprising: an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots; and said screen slots having an oblique inclination α with respect to said dimension of elongation of between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots.
  • 17. A system as recited in claim 16 wherein said drainer inlet is substantially open and hollow.
  • 18. A system as recited in claim 16 wherein α is between about 30-60°.
  • 19. A system as recited in claim 16 wherein α is substantially 90°.
  • 20. A cellulosic fibrous material treating system comprising:a material slurrying vessel; a high pressure transfer device including a low pressure inlet, low pressure outlet, high pressure inlet and high pressure outlet; said slurrying vessel operatively connected to said low pressure inlet and outlet; a treatment vessel connected to said high pressure outlet; means for removing some liquid from slurry moving between said high pressure outlet and treatment vessel and circulating the removed liquid to said high pressure inlet; means for removing some liquid from the slurry between said slurrying vessel and low pressure inlet, and returning removed liquid to said slurrying vessel, said means comprising a drainer comprising: an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots; and said screen slots having an oblique inclination angle α with respect to said dimension of elongation of between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots.
  • 21. A system as recited in claim 20 wherein said drainer inlet is substantially open and hollow.
  • 22. A system as recited in claim 20 wherein α is between about 30-60°.
  • 23. A system as recited in claim 20 wherein α is substantially 90°.
  • 24. A system for feeding a slurry of comminuted cellulosic fibrous material to a treatment vessel, comprising:a first vessel containing a slurry of material and liquid having a top and a bottom, with an inlet adjacent said top and an outlet adjacent said bottom; a high-pressure transfer device having a low pressure inlet, a low pressure outlet, a high-pressure inlet, and a high-pressure outlet, said high-pressure outlet operatively connected to said treatment vessel; a pump, operatively connected to said outlet of said first vessel and said low-pressure inlet of said high-pressure transfer device; and means located between said pump and said treatment vessel for removing liquid from the slurry, said means comprising a drainer comprising: an elongated housing having an inlet and an outlet at or adjacent opposite ends thereof; a substantially annular screen positioned between said inlet and said outlet having a plurality of slots; and said screen slots having an oblique inclination α with respect to said dimension of elongation of between about 5-90° to minimize passage of solid material in the slurry through said slots, and minimize clogging of said slots.
  • 25. A system as recited in claim 24 wherein said drainer inlet is substantially open and hollow.
  • 26. A system as recited in claim 24 wherein α is between about 30-60°.
  • 27. A system as recited in claim 24 wherein α is substantially 90°.
US Referenced Citations (32)
Number Name Date Kind
3713541 Nelson Jan 1973 A
4259150 Prough Mar 1981 A
4309284 Morimoto et al. Jan 1982 A
4885090 Chupka et al. Dec 1989 A
4958741 Johanson Sep 1990 A
4961844 Ekholm et al. Oct 1990 A
5236285 Prough Aug 1993 A
5236286 Prough Aug 1993 A
5401361 Prough et al. Mar 1995 A
5476572 Prough Dec 1995 A
5489363 Marcoccia et al. Feb 1996 A
5500083 Johanson Mar 1996 A
5536366 Marcoccia et al. Jul 1996 A
5547012 Marcoccia et al. Aug 1996 A
5575890 Prough et al. Nov 1996 A
5617975 Johanson et al. Apr 1997 A
5620562 Marcoccia et al. Apr 1997 A
5622598 Prough Apr 1997 A
5628873 Johanson et al. May 1997 A
5635025 Bilodeau Jun 1997 A
5635026 Kettunen et al. Jun 1997 A
5662775 Marcoccia et al. Sep 1997 A
5736006 Prough Apr 1998 A
5753075 Stromberg et al. May 1998 A
5766418 Prough Jun 1998 A
5779856 Kettunen Jul 1998 A
5824188 Prough et al. Oct 1998 A
5849150 Marcoccia et al. Dec 1998 A
5849151 Marcoccia et al. Dec 1998 A
5958181 Stromberg et al. Sep 1999 A
5968314 Prough Oct 1999 A
6039841 Hernesniemi Mar 2000 A
Foreign Referenced Citations (2)
Number Date Country
WO 9626315 Aug 1996 WO
WO 0006282 Feb 2000 WO