The present invention relates to an inline concentration measurement device incorporated in a supply line of a raw material fluid of an organic metal (MO) gas or the like to a semiconductor manufacturing equipment for measuring gas concentration in the gas supply line based on a principal of an absorptiometric method.
An inline concentration measurement device to be incorporated in a raw material fluid supply line of a semiconductor manufacturing equipment is conventionally known (for example, Patent Document 1).
As shown in a detailed cross section view of
Patent Document 1: Japanese Laid-Open Patent Publication No. 2000-206045
An inline concentration measurement device having a configuration shown in
For example in a case of a window member 4, as shown in an enlarged view of
To solve the above described problem, an inline concentration measurement device according to a first aspect of the present invention includes a measurement cell main body with a gas flow path formed, a light incident part with a window member connected to the measurement cell main body, and a light receiving part with a window member connected to the measurement cell main body, and the gas flow path includes a gas flow path part for an optical path extending straight between the window member of the light incident part and the window member of the light receiving part to provide the optical path, a first communication part making a gas inlet formed in the measurement cell main body communicate with the gas flow path part for the optical path, and a second communication part making a gas outlet formed in the measurement cell main body communicate with the gas flow path part for the optical path where the first communication part obliquely extends from the gas inlet towards the window member of the light incident part.
In an inline concentration measurement device according to a second aspect of the present invention, in the first aspect, the second communication part obliquely extends from the gas outlet towards the window member of the light receiving part.
An inline concentration measurement device according to a third aspect of the present invention includes a measurement cell main body with a gas flow path formed, a light incident part with a window member connected to the measurement cell main body, and a light receiving part with a window member connected to the measurement cell main body, and the gas flow path includes a gas flow path part for an optical path extending straight between the window member of the light incident part and the window member of the light receiving part to provide the optical path, a first communication part making a gas inlet formed in the measurement cell main body communicate with the gas flow path part for the optical path, and a second communication part making a gas outlet formed in the measurement cell main body communicate with the gas flow path part for the optical path where the second communication part obliquely extends from the gas outlet towards the window member of the light receiving part.
In an inline concentration measurement device according to a fourth aspect of the present invention, in the first or third aspect, a cross section area of the flow path of the first communication part is smaller than a cross section area of the gas flow path part for the optical path.
In an inline concentration measurement device according to a fifth aspect of the present invention, in the first or third aspect, the light incident part includes a holding body for holding an optical fiber and clamping the window member between the measurement cell main body and the holding body, and a fitting recessed part is formed either on the measurement cell main body or the holding body and a fitting projected part which fits the fitting recessed part is formed on the other with the window member held between a recess bottom face of the fitting recessed part and a protruded end face of the fitting projected part.
In an inline concentration measurement device according to a sixth aspect of the present invention, in the fifth aspect, the fitting recessed part is formed as a stepped recess and the fitting projected part is formed as a stepped projection that fits the stepped recess with a sealing face formed as an abutting face by the stepped part of the fitting recessed part and the stepped part of the fitting projected part abutting each other.
In an inline concentration measurement device according to a seventh aspect of the present invention, in the first or third aspect, the light receiving part includes a holding body for holding a photo diode and clamping the window member between the measurement cell main body and the holding body, and a fitting recessed part is formed either on the measurement cell main body or the holding body and a fitting projected part which fits the fitting recessed part is formed on the other with the window member held between a recess bottom face of the fitting recessed part and a protruded end face of the fitting projected part.
In an inline concentration measurement device according to an eighth aspect of the present invention, in the seventh aspect, the fitting recessed part is formed as a stepped recess and the fitting projected part is formed as a stepped projection that fits the stepped recess with a sealing face formed as an abutting face by the stepped part of the fitting recessed part and the stepped part of the fitting projected part abutting each other.
In an inline concentration measurement device according to a ninth aspect of the present invention, in the first or third aspect, the light incident part includes a collimator lens for collimating incident light entering to the gas flog path part for the optical path.
In an inline concentration measurement device according to a tenth aspect of the present invention, in the first or third aspect, the window members are configured to obliquely cross the optical path of the gas flow path part for the optical path.
In an inline concentration measurement device according to an eleventh aspect of the present invention, in the first or third aspect, a gas inflow path communicating with the first communication part for sending gas is provided and a cross section area of the gas inflow path is larger than a cross section area of the flow path of the first communication part.
According to the present invention, a first communication part making a gas inlet formed in a measurement cell main body to communicate with a gas flow path part for an optical path is configured to obliquely extend from the gas inlet towards a window member of a light incident part to eliminate retention of gas near the window member by causing a flow of the gas on a surface of the window member for reducing undesired accumulation of a raw material on the surface of the window member in the light incident part.
A second communication part is also configured to obliquely extend from a gas outlet towards a window member of a light receiving part for reducing undesired accumulation of the raw material on the window member of the light receiving part.
In addition, a cross section area of a flow path of the first communication part is configured to be smaller than a cross section area of the gas flow path part for the optical path to make speed of a flow in the first communication part faster than the flow in the gas flow path part for the optical path for reducing the accumulation of an organic metal material or the like in the light incident part.
Hereinafter, embodiments of an inline concentration measurement device according to the present invention are described with reference to drawings, wherein like reference numerals designate corresponding or identical elements throughout all drawings and embodiments including the background arts, and some duplicated explanations are emitted in the following description.
In the embodiment illustrated in
The gas inlet 5B1 and the gas outlet 5C1 respectively open to recessed parts 15b and 15c formed on a surface (a bottom face in the shown embodiment) of the measurement cell main body 15. Joints J1 and J2 are respectively connected to the recessed parts 15b and 15c through gaskets (see
The second communication part 5C obliquely extends from the gas outlet 5C1 towards the window member 6 of the light receiving part 8.
A cross section area of a flow path of the first communication part 5B is formed to be smaller than a cross section area of the gas flow path part 5a for the optical path and more preferably, the cross section area of the flow path of the first communication part 5B is formed to be no more than a half of the cross section area of the gas flow path part for the optical path.
The light incident part 3 includes a holding body 25 holding an optical fiber 2 and clamping the window member 4 facing to the gas flow path 5 between the measurement cell main body 15 and the holding body. A fitting recessed part 15d is formed on the measurement cell main body 15 and a fitting projected part 25a which fits the fitting recessed part 15d is formed on the holding body 25. The window member 4 is clamped between a recess bottom face of the fitting recessed part 15d and a protruded end face of the fitting projected part 25a of the holding body 25.
Sapphire glass plates may be preferably used for the window members 4 and 6. A gasket 26 intervenes between the holding body 25 and the measurement cell main body 15. The first communication part 5B opens on the window member 4 to communicate with the gas flow path part 5a for the optical path.
The fitting recessed part 15d is formed as a stepped recess with a stepped part 15e and the fitting projected part 25a is formed as a stepped projection with a stepped part 25b that fits the stepped recessed part 15d. An abutting face by the stepped part 15e of the fitting recessed part 15d and the stepped part 25b of the fitting projected part 25a abutting each other forms a sealing face.
The light receiving part 8 includes the window member 6 facing the gas flow path 5, a photo diode 7, and a holding body 30 holding the photo diode 7 and clamping the window member 6 between the measurement cell main body 15 and the holding body, and a fitting recessed part 15f is formed on the measurement cell main body 15 and a fitting projected part 30a which fits the fitting recessed part 15f is formed on the holding body 30. The window member 6 is clamped between a recess bottom face of the fitting recessed part 15f and a protruded end face of the fitting projected part 30a.
The fitting recessed part 15f is formed as a stepped recess with a stepped part 15g and the fitting projected part 30a is formed as a stepped projection with a stepped part 30b that fits the stepped recessed part 15f with the stepped part 15g. An abutting face by the stepped part 15g of the fitting recessed part 15f and the stepped part 30b of the fitting projected part 30a abutting each other forms a sealing face.
In the inline concentration measurement device having the above configuration, the first communication part 5B making the gas inlet 5B1 formed in the measurement cell main body 15 communicate with the gas flow path part 5a for the optical path is configured to obliquely extend from the gas inlet 5B1 towards the window member 4 of the light incident part 3 to eliminate retention of the gas near the window member 4 by making a flow of the gas flowing from the first communication part 5B towards a surface of the window member 4 for reducing undesired accumulation of an organic metal material or the like on the surface of the window member 4.
In addition, the accumulation of the organic metal material or the like on the window member 4 of the light incident part 3 may be reduced by configuring the cross section area of the flow path of the first communication part 5B to be smaller than the cross section area of the gas flow path part 5a for the optical path to make speed of the flow in the gas flow path part 5a for the optical path faster than the flow in the first communication part 5B.
Also, the accumulation of the organic metal material or the like on the window member 4 of the light incident part 3 may be reduced by making the cross section area of the flow path of the first communication part 5B smaller than the cross section area of the gas inflow path P1 sending the gas to the first communication part 5B to increase the speed of the flow in the first communication part 5B.
The present invention is not limited to the above described embodiments but variations may be made within the scope of the invention. For example, in the previously described embodiments, the fitting recess is made on the measurement cell main body and the fitting projection is made on the holding body. On the contrary, however, the fitting projection may be made on the measurement cell main body and the fitting recess may be made on the holding body.
2 optical fiber
3 light incident part
4 window member
5 gas flow path
5
a gas flow path part for the optical path
5B first communication path
5B1 gas inlet
5C second communication path
5C1 gas outlet
6 window member
7 photo diode
8 light receiving part
15 measurement cell main body
15
d fitting recessed part
15
e stepped part
15
f fitting recessed part
15
g stepped part
25 holding body
25
a fitting projected part
25
b stepped part
30 holding body
30
a fitting projected part
30
b stepped part
P1 gas inlet path
Number | Date | Country | Kind |
---|---|---|---|
2014-154307 | Jul 2014 | JP | national |
Filing Document | Filing Date | Country | Kind |
---|---|---|---|
PCT/JP2015/003692 | 7/23/2015 | WO | 00 |
Publishing Document | Publishing Date | Country | Kind |
---|---|---|---|
WO2016/017122 | 2/4/2016 | WO | A |
Number | Name | Date | Kind |
---|---|---|---|
3727050 | Kerr | Apr 1973 | A |
4455089 | Yeung | Jun 1984 | A |
4651004 | Uno | Mar 1987 | A |
5942755 | Dreyer | Aug 1999 | A |
7547904 | Schmidt | Jun 2009 | B2 |
7649189 | Cole | Jan 2010 | B2 |
8437000 | Cole | May 2013 | B2 |
9244003 | Matsuo | Jan 2016 | B1 |
9612198 | Colman | Apr 2017 | B2 |
20020108437 | Koch | Aug 2002 | A1 |
20050063869 | Follonier | Mar 2005 | A1 |
20050286054 | Chen | Dec 2005 | A1 |
20080106737 | Weichselbaum | May 2008 | A1 |
20080151248 | Cole | Jun 2008 | A1 |
20100214556 | Mannhardt | Aug 2010 | A1 |
20130166242 | Ido | Jun 2013 | A1 |
20140063494 | Hatahori | Mar 2014 | A1 |
20140268157 | Bogoev | Sep 2014 | A1 |
20140291526 | Killich | Oct 2014 | A1 |
Number | Date | Country |
---|---|---|
2239559 | Nov 2017 | EP |
H11-183366 | Jul 1999 | JP |
2000-206045 | Jul 2000 | JP |
2004-198121 | Jul 2004 | JP |
2011-127988 | Jun 2011 | JP |
2012-137429 | Jul 2012 | JP |
2014-102152 | Jun 2014 | JP |
1999034192 | Jul 1999 | WO |
WO-2009060169 | May 2009 | WO |
Entry |
---|
AIPN English translations of Japanese applications JP 2011127988, JP 11-183366, JP 2014102152. |
International Search Report issued in PCT/JP2015/003692; dated Oct. 13, 2015. |
Number | Date | Country | |
---|---|---|---|
20170199117 A1 | Jul 2017 | US |