The present invention relates to an ultra-high vacuum creating device. To be specific, the ultra-high vacuum creating device of the present invention includes at least one ion pump. In addition, the ultra-high vacuum creating device of the present invention is configured to include another ion pump, a heating and non-evaporating getter pump and a sublimation pump arbitrarily stacked on the ion pump according to an application, and accordingly, an exhaust characteristic thereof can be optimized according to the application.
Recently, an ultra-high vacuum technique has been regarded as important along with remarkable development of a nanotechnology and an ultra-precision measurement technique. For example, a surface of a semiconductor is easily contaminated by gas molecules, and conventionally, there has been a need of maintaining the semiconductor in an ultra-high vacuum state under 10−5 Pa or lower to keep the clean semiconductor surface. In addition, a field emission type charged particle source is used in a charged particle beam device, for example, which uses a finely focused electron beam or an ion source such as a scanning electron microscope in order to improve resolution. At this time, it is necessary to maintain an internal space of the charged particle source in the ultra-high vacuum state in order to stably operate this field emission type charged particle source. Thus, conventionally, an ultra-high vacuum pump such as an ion pump has been used as a device configured for the formation of the ultra-high vacuum state.
In this manner, the ultra-high vacuum environment under 10−5 Pa or lower, particularly, a class of 10−9 Pa to 10−7 Pa provides ultimate cleanness and stability, and thus, is indispensable for nanoscale ultra-precision machining, ultra-precision measurement, and the like. Conventionally, however, it has been considered that an exhaust device such as a bulky ion pump and a cryopump is necessary for creation and maintenance of such ultra-high vacuum environment. In this manner, the exhaust device has a large-scale structure, a chamber housing the device becomes bulky, and as a result, there is a problem that the entire device scale becomes unnecessarily larger and heavier.
Thus, a light, small and highly efficient ion pump having uniaxially symmetric electrode arrangement has been developed (Patent Literature 1) in order to solve the above-described problem and a cylindrical ion pump with a larger exhaust amount has been developed (Patent Literature 2) as an evolved type thereof. In particular, the ion pump described in Patent Literature 2 is the cylindrical ion pump in which a space with little electromagnetic field modulation, configured to store a sample and a charged particle source, is secured at the center thereof, and a pump element (a permanent magnet or the like) is arranged in the form of being stuck to a casing surface of an ultra-high vacuum chamber. Thus, it is revolutionary in terms that it is possible to realize high exhaust performance and space efficiency at the same time.
Patent Literature 1: Japanese Patent No. 4831549
Patent Literature 2: Japanese Patent No. 4835756
Meanwhile, the overall shape of the cylindrical ion pump disclosed in Patent Literature 2 is formed in a shape which is long in the central-axis direction and short in the direction orthogonal to the central axis (for example, a shape like a clay pipe) in order to secure the high exhaust performance. However, there is a case where it is difficult to sufficiently secure a space for mounting of the ion pump which is long in the central-axis direction depending on a shape of the vacuum chamber as a mounting target, and there is a problem that it is difficult to mount the ion pump to a desired vacuum chamber in such a case. In particular, an electron microscope is configured by scrupulously calculating each relative arrangement of parts forming an electron gun, and thus, in the current status, a space for mounting an ion pump is hardly provided in the central-axis direction of the ion pump in the case of mounting the conventional cylindrical ion pump in a lens barrel of the electron microscope or the like.
Thus, currently, there is a demand for an ultra-high vacuum creating device which includes an ion pump whose size in the central-axis direction is further reduced while maintaining basic performances of the conventional cylindrical ion pump such as light weight, efficiency, and an exhaust property.
Thus, the inventor of the present invention has dedicatedly studied solutions to the conventional problem, and as a result, has invented a configuration in which a plate-shaped electrode group, which has a center opening and is formed by connecting a plurality of electrodes at intervals, and a pair of plate-shaped electrode and a pair of plate-shaped magnet, provided on both upper and lower sides of the electrode group, are arranged inside a casing of an ion pump. According to such a configuration, it has been found out that it is possible to realize the thin ion pump whose size in the central-axis direction is further reduced while maintaining a basic performance such as an exhaust property. Further, the present inventor has conceived that it is possible to solve the problems of the related art based on the above-described finding, and completed the present invention. To be specific, the present invention has the following configurations.
The present invention relates to an ultra-high vacuum creating device.
The ultra-high vacuum creating device of the present invention includes at least one ion pump 100.
Here, the ion pump 100 includes a casing 110, a plate-shaped electrode group 120, a pair of plate-shaped electrodes 131 and 132, and a pair of plate-shaped magnets 141 and 142.
The casing 110 includes at least one of openings 111 and 112. The plate-shaped electrode group 120 and the pair of plate-shaped electrodes 131 and 132 are at least housed inside the casing 110 such that opposite poles thereof directly oppose therebetween.
The plate-shaped electrode group 120 is arranged inside the casing 110. The electrode group 120 has a predetermined central axis (C), and a center opening 120a is formed along the central axis (C). In addition, the electrode group 120 has a structure in which electrodes 121 are connected at intervals. In addition, the electrode group 120 may have a structure in which a hollow electrode 123 having a space inside thereof is provided and the electrode 121 is housed inside the hollow electrode 123.
The pair of plate-shaped electrodes 131 and 132 is arranged at positions inside the casing 110 such that the electrode group 120 is sandwiched therebetween. That is, the pair of plate-shaped electrodes 131 and 132 is arranged at both sides of the electrode group 120 in the central-axis direction.
The pair of plate-shaped magnets 141 and 142 is arranged at positions such that the pair of plate-shaped electrodes 131 and 132 is sandwiched therebetween. That is, the pair of plate-shaped magnets 141 and 142 is arranged at both sides of the pair of plate-shaped electrodes 131 and 132 sandwiching the electrode group 120 in the central-axis direction. The pair of plate-shaped magnets 141 and 142 may be arranged inside the casing 110, but is preferably arranged outside the casing 110. The pair of plate-shaped magnets 141 and 142 applies a magnetic field in the vertical direction inside the casing 110, and preferably in a space between the pair of plate-shaped electrodes 131 and 132.
As the above-described configuration, the plate-shaped electrode group 120 keeping the space is arranged, and the pair of thin plate-shaped electrodes and the pair of thin plate-shaped magnets are arranged at both sides of the electrode group 120 in the central-axis direction (up-and-down direction). Accordingly, it is possible to reduce the size of the ion pump 100 in the central-axis direction while maintaining the basic performance such as the exhaust property. That is, it is possible to effectively use the internal space of the casing 110 as a gas collecting space by providing the plate-shaped electrode group 120 keeping the space to be sandwiched by the pair of plate-shaped electrodes 131 and 132, and the pair of plate-shaped magnets 141 and 142 from both the upper and lower sides. Further, the ion pump 100 maintains the exhaust performance or the likes by widening a horizontal width of the plate-shaped electrode group 120, and further, includes the thin plate-shaped electrodes 131 and 132, and the plate-shaped magnets 141 and 142 arranged at both the upper and lower sides of the electrode group 120. Thus, it is possible to reduce the length (that is, thickness) of the ion pump 100 in the central-axis direction while maintaining the exhaust performance of the ion pump 100. For example, it is possible to set the length of the ion pump 100 in the central-axis direction to be about ¼ of a length of the conventional ion pump according to the configuration of the present invention. Therefore, it is possible to mount the high-performance ion pump 100 (ultra-high vacuum creating device) without changing the basic shape or arrangement thereof even in the case of the electron microscope which has a limit regarding a mounting space, for example.
In the ultra-high vacuum creating device of the present invention, at least one of the openings 111 and 112 is preferably formed on the central axis (C) in the casing 110 of the ion pump 100.
In addition, center openings 133 and 134 are preferably formed on the central axis (C) in the pair of plate-shaped electrodes 131 and 132, respectively.
Further, center openings 143 and 144 are preferably formed on the central axis (C) in the pair of plate-shaped magnets 141 and 142, respectively.
Accordingly, a gas flow path or a space configured to house experimental equipment or cause the experimental equipment to pass therethrough is formed along the central axis (C) in the ultra-high vacuum creating device of the present invention.
As the above-described configuration, it is possible to secure the space to house the experimental equipment or cause the experimental equipment to pass therethrough by forming the columnar space along the central axis (C) of the electrode group 120. In addition, it is possible to secure a wide discharge space by, for example, forming the electrode group 120 using the plurality of ring-shaped electrodes 121 to share each central axis of the pair of plate-shaped electrodes 131 and 132 and the pair of plate-shaped magnets 141 and 142.
Further, it is possible to stack a plurality of the ion pumps 100, configured as described above by causing the openings 111 and 112 to communicate with each other. When the plurality of ion pumps 100 are stacked, the performance and service life thereof can be improved. Therefore, it is possible to mount the ultra-high vacuum creating device having the optimal configuration in terms of the device scale and the performance by adjusting the number of the ion pumps 100 to be stacked in accordance with tolerance of the mounting space. In this manner, the ultra-high vacuum creating device of the present invention has multi-stage extensibility in the central-axis direction. That is, the ultra-high vacuum creating device according to the present invention is capable of stacking the plurality of ion pumps 100 in any stages as long as the space allows it.
In the ultra-high vacuum creating device of the present invention, two or more of the ion pump 100 may be stacked along the central-axis (C) direction. In this case, it is preferable that the neighboring ion pumps 100 share one of the pair of plate-shaped magnets 141 and 142. That is, the shared plate-shaped magnet functions so as to apply the magnetic field to both the two neighboring ion pumps 100.
As the above-described configuration, it is possible to further reduce the size in the central-axis direction by causing one of the plate-shaped magnets 141 and 142 to be shared in the case of stacking the ion pumps 100, and further, it is possible to reduce the gross weight of the device as compared to the case of simply connecting the ion pumps 100 in series since it is possible to omit one plate-shaped magnet, which is a heavy object, or more.
The ultra-high vacuum creating device of the present invention may include at least one heating and non-evaporating getter pump 200 in addition to one or plurality of ion pumps 100.
The heating and non-evaporating getter pump 200 includes a casing 210, a heater 220, and a pair of getter materials 231 and 232.
The casing 210 includes at least one of openings 211 and 212. The heater 220, and the pair of getter materials 231 and 232 are arranged inside the casing 210.
The heater 220 heats the pair of getter materials 231 and 232. The heater 220 preferably has a plate shape.
The pair of getter materials 231 and 232 is arranged at positions inside the casing 210 such that the heater 220 is sandwiched therebetween from both the upper and lower sides. The getter materials 231 and 232 are heated in vacuum by a radiant heat from the heater 220 and activated by discharging a gas that has been stored therein, thereby functioning as a pump.
Further, at least one of openings 211 and 212 of the heating and non-evaporating getter pump 200 communicates with at least one of openings 111 and 112 of the ion pump 100 in the ultra-high vacuum creating device of the present invention.
As the above-described configuration, the ultra-high vacuum creating device of the present invention can be constructed by combining the ion pump 100 and the heating and non-evaporating getter pump 200.
In the ultra-high vacuum creating device of the present invention, at least one of the openings 211 and 212 is preferably formed on the central axis (C) in the casing 210 of the heating and non-evaporating getter pump 200.
In addition, a center opening 221 is preferably formed on the central axis (C) in the heater 220.
Further, center openings 233 and 234 are preferably formed on the central axis (C) in the pair of getter materials 231 and 232, respectively.
Accordingly, a gas flow path and a space configured to house experimental equipment or cause the experimental equipment to pass therethrough is formed along the central axis (C) in the ultra-high vacuum creating device which is configured to include the ion pump 100 and the heating and non-evaporating getter pump 200.
As the above-described configuration, it is possible to secure the space configured to house the experimental equipment or cause the experimental equipment to pass therethrough by forming the columnar space along the central axis (C) at the time of combining the ion pump 100 and the heating and non-evaporating getter pump 200. Thus, it is possible to efficiently use the ion pump 100 and the heating and non-evaporating getter pump 200 in combination according to the ultra-high vacuum creating device of the present invention.
The ultra-high vacuum creating device of the present invention may include a sublimation pump 300 in addition to one or plurality of ion pumps 100.
The sublimation pump 300 includes a casing 310, a sublimation filament 320, and a shield 330.
The casing 310 includes at least one of openings 311 and 312. The sublimation filament 320 is arranged inside the casing 310.
The sublimation filament 320 is a ring-shaped filament member which is sublimated when current flows.
Further, at least one of openings 311 and 312 of the sublimation pump 300 communicates with at least one of openings 111 and 112 of the ion pump 100 in the ultra-high vacuum creating device of the present invention.
As the above-described configuration, the ultra-high vacuum creating device of the present invention can be constructed by combining the ion pump 100 and the sublimation pump 300.
In the ultra-high vacuum creating device of the present invention, at least one of openings 311 and 312 is preferably formed on the central axis (C) in the casing 310 of the sublimation pump 300. Accordingly, a gas flow path or a space configured to house experimental equipment or cause the experimental equipment to pass therethrough is formed along the central axis (C) in the ultra-high vacuum creating device which is configured to include the ion pump 100 and the sublimation pump 300.
As the above-described configuration, it is possible to secure the space configured to house the experimental equipment or cause the experimental equipment to pass therethrough by forming the columnar space along the central axis (C) at the time of combining the ion pump 100 and the sublimation pump 300. Thus, various characteristics of the ion pump 100 and the sublimation pump 300 are effectively combined according to the ultra-high vacuum creating device of the present invention, and thus, can be used as an efficient pump system.
According to the present invention, it is possible to provide the ultra-high vacuum creating device which includes the ion pump whose size in the central-axis direction is further reduced while maintaining the basic performances of the conventional ion pump such as the light weight, the efficiency, and the exhaust property.
The ion pump 100 has a thin shape (preferably, a disc shape) in the present invention, and accordingly, can also be mounted in, for example, a vacuum chamber with few margin in the mounting space such as the lens barrel of the electron gun. In addition, it is also possible to mount the heating and non-evaporating getter pump 200 having an excellent gettering performance of hydrogen in an ultra-high vacuum space and the sublimation pump 300 having an excellent gettering performance in a low vacuum space as well as the ion pump 100 combinedly in the vacuum chamber with a margin in the mounting space. When a plurality of pump units are connected in tandem with each other in this manner, the exhaust amount and exhaust characteristics thereof can be enhanced and adjusted if necessary. Accordingly, the ultra-high vacuum creating device of the present invention has, for example, a start-up vacuum level of 10−4 Pa to 10−3 Pa and can improve an ultimate vacuum level up to 10−9 Pa to 10−8 Pa.
The ultra-high vacuum creating device of the present invention can be suitably applied to, for example, an ion beam processing device in which large gases are released from a sample, various processing devices, an ionized gas generation device, an ion source generation device, and the like. In addition, the ultra-high vacuum creating device of the present invention can also be suitably applied to, for example, a synchrotron radiation facility which requires more stable ultra-high vacuum environment, an ion trap, an atomic clock, and the like.
Hereinafter, embodiments of the present invention will be described with reference to the drawings. The present invention is not limited to the embodiments described below, but includes amendments thereto made appropriately by those skilled in the art to the extent obvious.
In the specification of the present application, a “plate shape” means a shape formed to have the width longer than the thickness. The plate shapes include not only a disk shape but also a polygonal plate shape such as a square plate shape.
In the specification of the present application, a “ring shape” means a shape formed to have an opening at the center thereof. The ring shapes include not only a circular ring shape but also a polygonal ring shape such as a square ring shape.
[1. Ion Pump]
An ultra-high vacuum creating device 1 according to the present invention is configured to include an ion pump 100.
An operation principle of an ion pump is well-known. The operation principle of the ion pump will be briefly described. First, a voltage of several kV is applied between a titanium negative electrode (cathode) and a positive electrode (anode) of the ion pump, primary electrons are released from the titanium negative electrode. The primary electrons released from the titanium negative electrode are affected by a magnetic field applied from a magnet while being attracted to the positive electrode, and thus, the primary electrons reach the positive electrode by whirling round in a long spiral motion. On the way to the positive electrode, the primary electrons collide against neutral gas molecules to generate many positive ions and secondary electrons. The positive ions are accelerated toward the titanium negative electrode by a high voltage, thereby sputtering titanium atoms. The sputtered titanium atoms adhere to the positive electrode or the like to adsorb the gas molecules (getter effect). Incidentally, the secondary electrons further perform a spiral motion and collide against the gas molecules to generate more positive ions and electrons (tertiary electrons). Accordingly, the gas molecules inside a certain space are collected in the ion pump, and the space can be set to the ultra-high vacuum state of 10−5 Pa or lower.
[1-1. Casing]
The casing 110 is a frame which forms a workspace configured to collect gas molecules or to house a sample and experimental equipment or causing the sample and the experimental equipment to pass therethrough. As illustrated in
A space formed in the periphery of the central axis of the casing 110 serves not only as a gas flow path in an exhaust operation but also as the space configured to house the sample and the experimental equipment or to cause the sample and the experimental equipment to pass therethrough. The casing 110 includes at least one opening (111 or 112). A gas flows inside or outside the casing 110 via the opening (111 or 112). In the embodiment illustrated in
As illustrated in
In addition, the upper casing member 113 includes the upper external connection flange 114, the lower casing member 115 includes the lower external connection flange 116. Further, the upper opening 111 is formed in the upper external connection flange 114, and the lower opening 112 is formed in the lower external connection flange 116. Accordingly, it is possible to connect an external device to both upper and lower sides of the ion pump 100 via the external connection flanges 114 and 116.
In addition, as illustrated in
Incidentally, a known material such as aluminum, titanium and stainless is used as a material of the casing 110. In addition, the casing 110 can also cause an inner wall of the casing 110 to directly function as an electrode. In this regard, the casing 110 is preferably made of aluminum with titanium vapor-deposited on the inner wall surface thereof. In this manner, it is possible to decrease the weight of the ion pump system, and further, it is possible to simplify and downsize the structure of the ion pump 100. In addition, a wiring (not illustrated) or the like, configured to drive an electrode, may be provided inside the casing 110.
[1-2. Electrode Group]
The electrode group 120 is a plurality of electrodes arranged inside the casing 110. A polarity of the electrode group 120 may be positive or negative as long as it is different from each polarity of the pair of plate-shaped electrodes 131 and 132 to be described later. In addition, the electrode group 120 may be configured such that the polarity thereof can be changed. However, the polarity of the electrode group 120 is preferably positive in the configuration of the ion pump 100 according to the present embodiment.
As illustrated in
In addition, a center opening 120a is formed in the electrode group 120 along the central axis (C) thereof as illustrated in
As illustrated in
In addition, the plurality of ring-shaped electrodes 121 formed in the circular ring shape are respectively arranged like concentric circles with the central axis (C) as the center thereof. That is, one the ring-shaped electrode 121 is arranged in an opening of another the ring-shaped electrode 121, and this another the ring-shaped electrode 121 is arranged in an opening of the other the ring-shaped electrode 121. In this manner, the plurality of ring-shaped electrodes 121 share the central axis. In addition, it is preferable that the intervals among the plurality of ring-shaped electrodes 121 be practically equal intervals. In addition, the number of the ring-shaped electrodes 121 forming the electrode group 120 is not particularly limited, and may be about, for example, 5 to 20 or 8 to 15.
In addition, the electrode group 120 includes a conducting wire 122 which extends in the direction orthogonal to the central-axis (C) direction in order to connect the plurality of ring-shaped electrodes 121 as illustrated in
In addition, the number of the ring-shaped electrodes 121 forming the electrode group 120 can be appropriately increased. It is possible to increase the exhaust amount of the ion pump 100 by increasing the number of the ring-shaped electrodes 121. In addition, when the number of the ring-shaped electrodes 121 is increased, the size of the ion pump 100 in the direction orthogonal to the central-axis direction (the orthogonal direction) is extended, but the size thereof in the central-axis direction does not change. Thus, it is possible to improve the exhaust amount while suppressing the size of the ion pump 100 in the central-axis direction to be small by increasing the number of the ring-shaped electrodes 121 in the configuration of the present invention. In this manner, the exhaust amount of the ion pump 100 can be adjusted by the extensibility in the orthogonal direction.
A known material can be appropriately used for the ring-shaped electrode 121 forming the electrode group 120. Examples of the material of the ring-shaped electrode 121 may include titanium, copper, graphite, and copper tungsten. In particular, the ring-shaped electrode 121 is preferably made of titanium when being configured to function as the negative electrode. In addition, the electrode group 120 may be arranged inside the casing 110 via a known fixing unit (not illustrated). For example, a protrusion may be formed in an outermost layer of the electrode group 120 so as to be fit in a groove formed in the casing 110.
Further,
To be specific, the hollow electrode 123 includes upper and lower flat surface portions 123a, and a side surface portion 123b which connects side edges of the upper and lower flat surface portions 123a in the vertical direction. The space is secured between the upper and lower flat surface portions 123a by the side surface portion 123b. In this manner, the hollow electrode 123 is formed in a hollow shape to keep the space at the internal portion thereof. In addition, a center opening 124 is formed along the central axis (C) in the hollow electrode 123. Further, the electrodes 121 connected at intervals are housed in the internal portion of the hollow electrode 123, that is, the space between the upper and lower flat surface portions 123a as illustrated in
In addition, it is preferable that the electrode 121 and the hollow electrode 123 be electrically connected to each other as illustrated in
In addition, the center opening 120a formed at the center of the electrode group 120 and the center opening 124 formed in the hollow electrode 123 communicate with each other in the vertical direction as illustrated in
[1-3. Plate-Shaped Electrode]
The plate-shaped electrodes 131 and 132 are electrodes arranged inside the casing 110 and the electrodes electrically forming a pair with the above-described electrode group 120. That is, it is necessary to form the plate-shaped electrodes 131 and 132 to have a different polarity from the electrode group 120. In addition, each polarity of the plate-shaped electrodes 131 and 132 may be appropriately changed according to the polarity of the electrode group 120. However, each polarity of the plate-shaped electrodes 131 and 132 is preferably negative in the configuration of the ion pump 100 according to the present embodiment.
As illustrated in
As illustrated in
A known material can be appropriately used for the plate-shaped electrodes 131 and 132. Titanium, copper, graphite, copper tungsten, or the like, which has supplemental performance with respect to residual gases in the vacuum may be appropriately used as the material the plate-shaped electrodes 131 and 132. In particular, the plate-shaped electrodes 131 and 132 are preferably made of titanium when being configured to function as the negative electrode. In addition, the plate-shaped electrodes 131 and 132 may be formed using a plate for enhancement of electric field application efficiency or punching metal for enhancement of permeability of the residual gas. In addition, the plate-shaped electrodes 131 and 132 may be arranged inside the casing 110 via a known fixing unit (not illustrated). For example, a protrusion may be formed in the plate-shaped electrodes 131 and 132 so as to be fit into a groove formed in the casing 110.
[1-4. Plate-Shaped Magnet]
The pair of plate-shaped magnets 141 and 142 is a magnet that applies a magnetic field inside the casing 110. Thus, the plate-shaped magnets 141 and 142 are arranged at the positions such that the pair of plate-shaped electrodes 131 and 132 is sandwiched therebetween from both the sides in the up-and-down direction (central-axis direction) as illustrated in
As illustrated in
The pair of upper and lower plate-shaped magnets 141 and 142 is formed in a thin type. That is, each of the plate-shaped magnets 141 and 142 has a shape which is formed such that a length (width) in the orthogonal direction is longer than a length (thickness) in the central-axis (C) direction. In addition, each width (length in the orthogonal direction) of the pair of plate-shaped magnets 141 and 142 is practically equal to that of the electrode group 120. That is, the plate-shaped magnets 141 and 142 are formed to have a horizontal width which enables the electrode group 120 to be entirely covered from the upper and lower sides. In addition, the plate-shaped magnets 141 and 142 preferably have a disk shape. However, the plate-shaped magnets 141 and 142 may have a triangular plate shape, a square plate shape, or other polygonal plate shapes. Each shape of the plate-shaped magnets 141 and 142 may be set in accordance with each shape of the casing 110, the electrode group 120, and the plate-shaped electrodes 131 and 132.
As illustrated in
[1-5. Magnetic Shield]
The magnetic shield 150 is a shield member that houses the casing 110 and the plate-shaped magnets 141 and 142 therein and prevents the magnetism of the plate-shaped electrodes 131 and 132 from leaking to the outside, and works to suppress the magnetic field leakage to the workspace around the central axis and suppress disturbance of a magnetic flux intruding into the electrode group 120 by forming the closed magnetic circuit together with the plate-shaped magnets 141 and 142. The magnetic shield 150 can be formed using a known material having high magnetic permeability such as mu metal and permalloy. In addition, the magnetic shield 150 is preferably conductive.
In addition, an opening is formed in a part of the magnetic shield 150 so that the external connection flanges 114 and 116 of the casing 110 protrude through the opening as illustrated in
Further, the magnetic shield 150 preferably forms the closed magnetic circuit inside the ion pump in cooperation with the pair of plate-shaped magnets 141 and 142. The concept of the closed magnetic circuit is illustrated in
With the above-described configuration, the magnetic shield 150 functions as a guide of the magnetic flux surrounding the periphery of the ion pump in cooperation with the pair of plate-shaped magnets 141 and 142. That is, when the magnetic flux vertically penetrating the ion pump is pulled into the magnetic shield 150, the closed magnetic circuit is formed. Accordingly, it is possible to align distribution of the magnetic flux intruding into the electrode group 120 and to reduce the leakage of the magnetic field into the space around the central axis.
The ion pump 100 configured as described above has the size which is small in the central-axis (C) direction as illustrated in
In addition, the ion pump 100 of the present invention has the small size in the central-axis direction as described above, but basic performances thereof such as the exhaust amount can be maintained as performances which are not changed from the related art. That is, it is possible to sufficiently secure the space to collect the gas by increasing the number of the ring-shaped electrodes 121 forming the electrode group 120 and extending each length (width) of the casing 110, the plate-shaped electrodes 131 and 132, and the plate-shaped magnets 141 and 142 in the orthogonal direction in accordance with the increased number. Therefore, the ion pump 100 can obtain the desired exhaust performance while suppressing the size in the central-axis direction.
[1-6. Voltage Supply Method]
For example,
In addition,
In addition,
[1-7. Multi-Stage Structure of Ion Pump]
One of the characteristics of the ion pump 100 having the above-described structure is that it is possible to stack the ion pumps 100 in a plurality of stages in the central-axis (C) direction. That is, the ion pump 100 has the extensibility in the central-axis direction.
As illustrated in
To be specific, when the ion pumps 100 are stacked, the casing 110 includes a relay casing member 117 in addition to the upper casing member 113 in which the upper external connection flange 114 is formed and the lower casing member 115 in which the lower external connection flange 116 is formed. The relay casing member 117 is arranged between the upper casing member 113 and the lower casing member 115. The relay casing member 117 is bonded to the upper casing member 113, thereby functioning as the casing 110 for the ion pump 100 at the upper stage. At the same time, the relay casing member 117 is bonded to the lower casing member 115, thereby also functioning as the casing 110 for the ion pump 100 at the lower stage. Incidentally, when the relay casing member 117 is bonded to the upper casing member 113 and the lower casing member 115, flange portions formed in the respective casing members 113, 115 and 117 can be butted and bonded to each other. In this manner, it is possible to make the overall size of the ultra-high vacuum creating device 1 in the central-axis direction compact by providing the relay casing member 117 that can be shared between the upper-stage ion pump 100 and the lower-stage ion pump 100.
In addition, a constricted portion 118 that is inwardly constricted is formed in a central portion of the relay casing member 117 in the central-axis direction as illustrated in
In addition, when the ion pumps 100 are stacked, the upper-stage ion pump 100 and the lower-stage ion pump 100 can share the plate-shaped magnet 145 (141 or 142). Originally, the ion pump 100 is provided with the pair of two plate-shaped magnets 141 and 142. However, when the ion pumps 100 are stacked in a plurality of stages, a single plate-shaped magnet can be used as the lower plate-shaped magnet 142 in the upper-stage ion pump 100 and the upper plate-shaped magnet 141 in the lower-stage ion pump 100. Thus, three plate-shaped magnets are used to realize the same function as that in the case of arranging four plate-shaped magnets in the example illustrated in
In addition,
In addition,
[2. Heating and Non-Evaporating Getter Pump]
The ultra-high vacuum creating device 1 according to the present invention may be provided with a heating and non-evaporating getter pump 200 in addition to the ion pump 100.
The ion pump 100 has an advantage that it is possible to collect an inert gas such as nitrogen, helium and argon and rapidly create the ultra-high vacuum, but has a disadvantage that exhaust efficiency regarding hydrogen as a light element molecule is poor. On the other hand, the heating and non-evaporating getter pump 200 has a disadvantage that the absolute exhaust speed and the operation in a low vacuum region are poor, but has a high exhaust performance relating to hydrogen. Thus, it is possible to complement the disadvantages of the pumps one another by combining the ion pump 100 and the heating and non-evaporating getter pump 200 like the ultra-high vacuum creating device 1 of the present invention. Therefore, it is possible to provide the ultra-high vacuum creating device 1 with the favorable usability by combining the ion pump 100 and the heating and non-evaporating getter pump 200. It is novel to provide such a uniaxially symmetric structure of the heating and non-evaporating getter pump 200 in order for series-connection with another pump.
[2-1. Casing]
The casing 210 is a frame which forms a workspace configured to collect gas molecules or to house a sample and experimental equipment or causing the sample and the experimental equipment to pass therethrough. The casing 210 of the heating and non-evaporating getter pump 200 has basically the same structure as the casing 110 of the ion pump 100 described above. Thus, the description for the casing 110 of the ion pump 100 can be appropriately incorporated to the description for the casing 210 of the heating and non-evaporating getter pump 200.
That is, the casing 210 of the heating and non-evaporating getter pump 200 includes at least one opening (211 or 212). In the embodiment illustrated in
[2-2. Heater]
The heater 220 is a heat generating source configured to heat the getter materials 231 and 232 inside the casing 210. The heater 220 may be formed using a metallic material that generates heat by electrical heating when power is applied, for example. Thus, the heater 220 is preferably connected to a power supply (not illustrated). The heater 220 is heated to a degree that can cause the getter materials 231 and 232 to be heated by the radiant heat. The heating temperature of the heater 220 is not particularly limited, and for example, is 300 to 600 degree. The heating temperature of the heater 220 may be appropriately adjusted according to each material of the getter materials 231 and 232, a positional relationship therebetween, and the like.
As illustrated in
In addition, the center opening 221 is formed at the central portion of the heater 220. A size of the center opening 221 may be set to the same level as the openings 211 and 212 formed in the casing 210, for example. Further, heater 220 is arranged such that the center opening 221 is positioned on the central axis (C) as illustrated in
[2-3. Getter Material]
The getter materials 231 and 232 are members each of which are activated when being heated by the heater 220 in the vacuum and causes gas molecules such as hydrogen to be continuously stored through the chain reactions. A known material having a getter effect and a hydrogen storage effect can be used as the getter materials 231 and 232. For example, the getter materials 231 and 232 may be made of an alloy including, for example, Ti, V, Fe and the like.
As illustrated in
As illustrated in
In addition, a plurality of concave portions 235 and a plurality of convex portions 236 are alternately formed on each face of the getter materials 231 and 232 on each side opposing the heater 220 as illustrated in
[2-4. Heat Shield]
The heat shield 240 is a shield member which is configured to house the casing 210 therein and to prevent heat generated by the heater 220 from leaking outside. The heat shield 240 is a member that is arbitrarily provided, but is preferably provided in order to prevent an external device from being affected by the heat. The heat shield 240 can be formed using a known material. In addition, an opening is formed in a part of the heat shield 240 so that the external connection flanges 214 and 216 of the casing 210 protrude through the opening as illustrated in
[2-5. Combination of Ion Pump and Heating and Non-Evaporating Getter Pump]
The heating and non-evaporating getter pump 200 having the above-described configuration can be combined with the ion pump 100 in a stacked manner. That is, the ultra-high vacuum creating device 1 of the present invention can be constructed by combining one or a plurality of ion pumps 100 and one or a plurality of heating and non-evaporating getter pumps 200.
To be specific, the relay casing member 117 is provided when the ion pump 100 and the heating and non-evaporating getter pump 200 are stacked. The relay casing member 117 is arranged between the upper casing member 213 of the heating and non-evaporating getter pump 200 and the lower casing member 115 of the ion pump 100. The relay casing member 117 is bonded to the upper casing member 213 of the heating and non-evaporating getter pump 200, thereby functioning as the casing 210 for the heating and non-evaporating getter pump 200. At the same time, the relay casing member 117 is bonded to the lower casing member 115 of the ion pump 100, thereby also functioning as the casing 110 for the ion pump 100. Incidentally, when the relay casing member 117 is bonded to the upper casing member 213 of the heating and non-evaporating getter pump 200 and the lower casing member 115 of the ion pump 100, flange portions formed in the respective casing members 213, 115 and 117 can be butted and bonded to each other. In this manner, it is possible to make the overall size of the ultra-high vacuum creating device 1 in the central-axis direction compact by providing the relay casing member 117 that can be shared between the heating and non-evaporating getter pump 200 and the ion pump 100.
In addition, the constricted portion 118 that is inwardly constricted is formed in the central portion of the relay casing member 117 in the central-axis direction. The plate-shaped magnets 141 and 142 of the ion pump 100 are arranged in the constricted portion 118 of the relay casing member 117.
In addition,
In addition,
[2-6. Multi-Stage Structure of Heating and Non-Evaporating Getter Pump]
To be specific, when the heating and non-evaporating getter pumps 200 are stacked, the casing 210 includes a relay casing member 217 in addition to the upper casing member 213 in which the upper external connection flange 214 is formed and the lower casing member 215 in which the lower external connection flange 216 is formed. The relay casing member 217 is arranged between the upper casing member 213 and the lower casing member 215. The relay casing member 217 is bonded to the upper casing member 213, thereby functioning as the casing 210 for the heating and non-evaporating getter pump 200 at the upper stage. At the same time, the relay casing member 217 is bonded to the lower casing member 215, thereby also functioning as the casing 210 for the heating and non-evaporating getter pump 200 at the lower stage. Incidentally, when the relay casing member 217 is bonded to the upper casing member 213 and the lower casing member 215, flange portions formed in the respective casing members 213, 215 and 217 can be butted and bonded to each other. In this manner, it is possible to make the overall size of the ultra-high vacuum creating device 1 in the central-axis direction compact by providing the relay casing member 217 that can be shared between the upper-stage heating and non-evaporating getter pump 200 and the lower-stage heating and non-evaporating getter pump 200.
In addition, when the heating and non-evaporating getter pumps 200 are stacked as illustrated in
[3. Sublimation Pump]
The ultra-high vacuum creating device 1 according to the present invention may be provided with a sublimation pump 300 in addition to the ion pump 100. In addition, the above-described heating and non-evaporating getter pump 200 can be further combined.
The ion pump 100 has an advantage that it is possible to collect an inert gas such as nitrogen, helium, and argon, but has a disadvantage that rough adsorption using another vacuum device in advance is required in order to use the ion pump 100 because an operating range thereof is the ultra-high vacuum (0.1 to 10−5 Pa) or lower. On the other hand, the sublimation pump 300 can operate in the low vacuum (100 Pa or higher) or the medium vacuum (100 to 0.1 Pa) and has an advantage that the operating range is relatively wide, but has a disadvantage that a vacuum level inside a vacuum bath temporarily deteriorates during the sublimation operation because the operating time of the formed active film is short and it is necessary to perform the sublimation work every two to four hours. Thus, it is possible to complement the disadvantages of the pumps one another by combining the ion pump 100 and the sublimation pump 300 like the ultra-high vacuum creating device 1 of the present invention. Therefore, it is possible to provide the ultra-high vacuum creating device 1 with the favorable usability by combining the ion pump 100 and the sublimation pump 300. It is novel to provide such a uniaxially symmetric structure of the sublimation pump 300 in order for series-connection with another pump.
[3-1. Casing]
The casing 310 is a frame which forms a workspace configured to collect gas molecules or to house a sample and experimental equipment or causing the sample and the experimental equipment to pass therethrough. The casing 310 of the sublimation pump 300 has basically the same structure as the casing 110 of the ion pump 100 described above. Thus, the description for the casing 110 of the ion pump 100 can be appropriately incorporated to the description for the casing 310 of the sublimation pump 300.
That is, the casing 310 of the sublimation pump 300 includes at least one opening (311 or 312). In the embodiment illustrated in
[3-2. Sublimation Filament]
The sublimation filament 320 is a member that is sublimated when being heated by electrical heating to form the active film having the getter effect inside the casing 310. Thus, the sublimation filament 320 is connected to a power supply (not illustrated). A known material having the getter effect can be used as the sublimation filament 320. For example, the sublimation filament 320 may be a simple metal substance made of titanium, samarium, titanium, ytterbium, gadolinium, or erbium or may be made of an alloy including these metals.
As illustrated in
The sublimation filament 320 and the casing 310 share the central axis (C). Thus, the opening of the sublimation filament 320 communicates with the two openings 311 and 312 of the casing 310 along the central axis (C).
[3-3. Shield Member]
The shield member 330 is a member configured to form the active film by causing metal atoms generated from the sublimation filament 320 and having the getter effect to adhere thereto. When the shield member 330 is provided, a surface area of the active film is improved. As illustrated in
The shield member 330 has preferably a ring shape as illustrated in
The shield member 330 and the casing 310 and the sublimation filament 320 share the central axis (C). Thus, the opening of the shield member 330 communicates with the two openings 311 and 312 of the casing 310 and the opening of the sublimation filament 320 along the central axis (C). Accordingly, a linear flow path is formed in the sublimation pump 300 along the central axis (C).
[3-4. Heat Shield]
The heat shield 340 is a shield member which is configured to house the casing 310 therein and to prevent heat generated by the sublimation filament 320 from leaking to the outside. The heat shield 3400 is a member that is arbitrarily provided, but is preferably provided in order to prevent an external device from being affected by the heat. The heat shield 340 can be formed using a known material. In addition, an opening is formed in a part of the heat shield 340 so that the external connection flanges 314 and 316 of the casing 310 protrude through the opening as illustrated in
[2-5. Combination of Ion Pump, Sublimation Pump and Heating and Non-Evaporating Getter Pump]
The sublimation pump 300 having the above-described configuration can be combined with the ion pump 100 and the heating and non-evaporating getter pump 200 in a stacked manner. That is, the ultra-high vacuum creating device 1 of the present invention can be constructed by combining one or a plurality of ion pumps 100 with one or a plurality of heating and non-evaporating getter pumps 200 and one or a plurality of sublimation pumps 300.
To be specific, the two relay casing members 117 are provided when the heating and non-evaporating getter pump 200 and the sublimation pump 300 are stacked on the ion pump 100. In such a three-stage structure, the casing 110 of the ion pump 100 positioned at the middle stage is formed by bonding the two relay casing members 117 to each other. In addition, the upper relay casing member 117 is bonded to the lower casing member 215 of the heating and non-evaporating getter pump 200. Thus, the upper relay casing member 117 functions as both the casing 110 of the ion pump 100 and the casing 210 of the heating and non-evaporating getter pump 200. In addition, the lower relay casing member 117 is bonded to the upper casing member 313 of the sublimation pump 300. Thus, the lower relay casing member 117 functions as both the casing 110 of the ion pump 100 and the casing 310 of the sublimation pump 300. In this manner, it is possible to make the overall size of the ultra-high vacuum creating device 1 in the central-axis direction compact by providing the relay casing member 117 that can be shared among the respective vacuum pumps 100, 200 and 300.
In addition, the constricted portion 118 that is inwardly constricted is formed in the central portion of the relay casing member 117 in the central-axis direction. The plate-shaped magnets 141 and 142 of the ion pump 100 are arranged in the constricted portion 118 of the relay casing member 117.
The embodiment of the present invention has been described as above with reference to drawings in the specifications of the present application in order to express the content of the present invention. However, the present invention is not limited to the embodiment described hereinbefore, and encompasses obvious modifications and improvements made by those skilled in the art based on the matters described in the specifications of the present application.
The present invention relates to the ultra-high vacuum creating device including the ion pump. The ultra-high vacuum creating device of the present invention can be suitably applied to, for example, an ion beam processing device, various processing devices, an ionized gas generation device, an ion source generation device, and the like. In addition, the ultra-high vacuum creating device of the present invention can also be suitably applied to, for example, a synchrotron radiation facility, an ion trap, an atomic clock, and the like.
Number | Date | Country | Kind |
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2014-134301 | Jun 2014 | JP | national |
Filing Document | Filing Date | Country | Kind |
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PCT/JP2015/062082 | 4/21/2015 | WO | 00 |