Wells may be drilled at various depths to access and produce oil, gas, minerals, and other naturally occurring deposits from subterranean geological formations. The drilling of a well is typically accomplished with a drill bit that is rotated within the well to advance the well by removing topsoil, sand, clay, limestone, calcites, dolomites, or other materials.
During or after drilling operations, sampling operations may be performed to collect a representative sample of formation or reservoir fluids (e.g., hydrocarbons) using a fluid sampling tool. Fluid sampling tools may be disposed on a drill string, in a bottom hole assembly, and/or deployed on a wireline. The representative sample of formation or reservoir fluid (i.e., a fluid sample) may be taken to the surface after drilling and/or logging operations. Analyses of the fluid samples may be utilized to evaluate drilling operations and production potential, or to detect the presence of certain gases or other materials in the formation that may affect well performance.
Generally, fluid sampling tools are limited in the number of fluid samples that may be taken during sampling operations. Microsamplers may be utilized to save space and may allow for a large number of fluid samples to be taken. However, each microsampler adds complexity and space to the microsampling system. This may create complex mechanical and fluid system in order to take a large number of fluid samples.
The features and advantages of certain embodiments will be more readily appreciated when considered in conjunction with the accompanying figures. The figures are not to be construed as limiting any of the preferred embodiments.
The present disclosure relates to methods and systems for a microsampler. Specifically, actuation mechanisms for acquiring a large number of microsamples in a confined amount of space. As discussed below, the methods and systems of the mechanisms described below simplify the mechanical and fluid systems needed to acquire a large number of fluid samples during a downhole sampling operation and subsequently analyze those microsamples once the microsampler has been removed to the surface.
As illustrated, a hoist 108 may be used to run fluid sampling tool 100 into wellbore 104. Hoist 108 may be disposed on a vehicle 110. Hoist 108 may be used, for example, to raise and lower conveyance 102 in wellbore 104. While hoist 108 is shown on vehicle 110, it should be understood that conveyance 102 may alternatively be disposed from a hoist 108 that is installed at surface 112 instead of being located on vehicle 110. Fluid sampling tool 100 may be suspended in wellbore 104 on conveyance 102. Other conveyance types may be used for conveying fluid sampling tool 100 into wellbore 104, including coiled tubing, drill pipe, and wired drill pipe, for example. Fluid sampling tool 100 may comprise a tool body 114, which may be elongated as shown on
In examples, fluid analysis module 118 may comprise at least one sensor that may continuously monitor a fluid such as a reservoir fluid, formation fluid, wellbore fluid, or formation nonnative fluids such as drilling fluid filtrate. Such monitoring may take place in a fluid flow line or a formation tester probe such as a pad or packer or may be able to make measurements investigating the formation including measurements into the formation. Such sensors comprise optical sensors, acoustic sensors, electromagnetic sensors, conductivity sensors, resistivity sensors, selective electrodes, density sensors, mass sensors, thermal sensors, chromatography sensors, viscosity sensors, bubble point sensors, fluid compressibility sensors, flow rate sensors, pressure sensors, nuclear magnetic resonance (NMR) sensors. Sensors may measure a contrast between drilling fluid filtrate properties and formation fluid properties. Fluid analysis module 118 may be operable to derive properties and characterize the fluid sample. By way of example, fluid analysis module 118 may measure absorption, transmittance, or reflectance spectra and translate such measurements into component concentrations of the fluid sample, which may be lumped component concentrations, as described above. The fluid analysis module 118 may also measure gas-to-oil ratio, fluid composition, water cut, live fluid density, live fluid viscosity, formation pressure, and formation temperature and fluid composition. Fluid analysis module 118 may also be operable to determine fluid contamination of the fluid sample and may comprise any instrumentality or aggregate of instrumentalities operable to compute, classify, process, transmit, receive, retrieve, originate, switch, store, display, manifest, detect, record, reproduce, handle, or utilize any form of information, intelligence, or data for business, scientific, control, or other purposes. The absorption, transmittance, or reflectance spectra absorption, transmittance, or reflectance spectra may be measured with sensors 116 by way of standard operations. For example, fluid analysis module 118 may comprise random access memory (RAM), one or more processing units, such as a central processing unit (CPU), or hardware or software control logic, ROM, and/or other types of nonvolatile memory. Fluid analysis module 118 and fluid sampling tool 100 may be communicatively coupled via communication link 120 with information handling system 122.
Any suitable technique may be used for transmitting signals from the fluid sampling tool 100 to the surface 112. As illustrated, a communication link 120 (which may be wired or wireless, for example) may be provided that may transmit data from fluid sampling tool 100 to an information handling system 122 at surface 112. Information handling system 122 may comprise a processing unit 124, a monitor 126, an input device 128 (e.g., keyboard, mouse, etc.), and/or computer media 130 (e.g., optical disks, magnetic disks) that can store code representative of the methods described herein. Information handling system 122 may act as a data acquisition system and possibly a data processing system that analyzes information from fluid sampling tool 100. For example, information handling system 122 may process the information from fluid sampling tool 100 for determination of fluid contamination. The information handling system 122 may also determine additional properties of the fluid sample (or reservoir fluid), such as component concentrations, pressure-volume-temperature properties (e.g., bubble point, phase envelop prediction, etc.) based on the fluid characterization. This processing may occur at surface 112 in real-time. Alternatively, the processing may occur downhole hole or at surface 112 or another location after recovery of fluid sampling tool 100 from wellbore 104. Alternatively, the processing may be performed by an information handling system in wellbore 104, such as fluid analysis module 118. The resultant fluid contamination and fluid properties may then be transmitted to surface 112, for example, in real-time.
Referring now to
As illustrated, a drilling platform 202 may support a derrick 204 having a traveling block 206 for raising and lowering drill string 200. Drill string 200 may comprise, but is not limited to, drill pipe and coiled tubing, as generally known to those skilled in the art. A kelly 208 may support drill string 200 as it may be lowered through a rotary table 210. A drill bit 212 may be attached to the distal end of drill string 200 and may be driven either by a downhole motor and/or via rotation of drill string 200 from the surface 112. Without limitation, drill bit 212 may comprise, roller cone bits, PDC bits, natural diamond bits, any hole openers, reamers, coring bits, and the like. As drill bit 212 rotates, it may create and extend wellbore 104 that penetrates various subterranean formations 106. A pump 214 may circulate drilling fluid through a feed pipe 216 to kelly 208, downhole through interior of drill string 200, through orifices in drill bit 212, back to surface 112 via annulus 218 surrounding drill string 200, and into a retention pit 220.
Drill bit 212 may be just one piece of a downhole assembly that may comprise one or more drill collars 222 and fluid sampling tool 100. Fluid sampling tool 100, which may be built into the drill collars 222 may gather measurements and fluid samples as described herein. One or more of the drill collars 222 may form a tool body 114, which may be elongated as shown on
Fluid sampling tool 100 may further comprise one or more sensors 116 for measuring properties of the fluid sample reservoir fluid, wellbore 104, subterranean formation 106, or the like. The one or more sensors 116 may be disposed within fluid analysis module 118. In examples, more than one fluid analysis module may be disposed on drill string 200. The properties of the fluid are measured as the fluid passes from the formation through the tool and into either the wellbore or a sample container. As fluid is flushed in the near wellbore region by the mechanical pump, the fluid that passes through the tool generally reduces in drilling fluid filtrate content, and generally increases in formation fluid content. The fluid sampling tool 100 may be used to collect a fluid sample from subterranean formation 106 when the filtrate content has been determined to be sufficiently low. Sufficiently low depends on the purpose of sampling. For some laboratory testing below 10% drilling fluid contamination is sufficiently low, and for other testing below 1% drilling fluid filtrate contamination is sufficiently low. Sufficiently low also depends on the nature of the formation fluid such that lower contamination may be generally needed, the lighter the oil as designated with either a higher GOR or a higher API gravity. Sufficiently low also depends on the mechanism of property deconvolution from the effects of contamination. For instance, a single sample estimate of contamination may only allow a first order mitigation of the effects of contamination on reservoir fluid property estimation whereas multiple samples with varying degrees of contamination may allow contamination to be more effectively deconvoluted with more samples of greater variation a high accuracy contamination estimation or various combinations therein being better. Sufficiently low also depends on the rate of cleanup in a cost benefit analysis since longer pumpout times to incrementally reduce the contamination levels may have prohibitively large costs, and because samples are limited in number and multiple bulk samples across a single pumpout may be a costly way to estimate contamination. As previously described, the fluid sample may comprise a reservoir fluid, which may be contaminated with a drilling fluid or drilling fluid filtrate. Fluid sampling tool 100 may obtain and separately store different fluid samples from subterranean formation 106 with fluid analysis module 118. Fluid analysis module 118 may operate and function in the same manner as described above. However, storing of the fluid samples in the fluid sampling tool 100 may be based on the determination of the fluid contamination. For example, if the fluid contamination exceeds a tolerance, then the fluid sample may not be stored. If the fluid contamination is within a tolerance, then the fluid sample may be stored in the fluid sampling tool 100. In examples, contamination may be defined within fluid analysis module 118.
As previously described, information from fluid sampling tool 100 may be transmitted to an information handling system 122, which may be located at surface 112. As illustrated, communication link 120 (which may be wired or wireless, for example) may be provided that may transmit data from fluid sampling tool 100 to an information handling system 122 at surface 112. Information handling system 122 may comprise a processing unit 124, a monitor 126, an input device 128 (e.g., keyboard, mouse, etc.), and/or computer media 130 (e.g., optical disks, magnetic disks) that may store code representative of the methods described herein. In addition to, or in place of processing at surface 112, processing may occur downhole (e.g., fluid analysis module 118). In examples, information handling system 122 may perform computations to estimate asphaltenes within a fluid sample.
Each individual component discussed above may be coupled to system bus 304, which may connect each and every individual component to each other. System bus 304 may be any of several types of bus structures including a memory bus or memory controller, a peripheral bus, and a local bus using any of a variety of bus architectures. A basic input/output (BIOS) stored in ROM 308 or the like, may provide the basic routine that helps to transfer information between elements within information handling system 122, such as during start-up. Information handling system 122 further comprises storage devices 314 or computer-readable storage media such as a hard disk drive, a magnetic disk drive, an optical disk drive, tape drive, solid-state drive, RAM drive, removable storage devices, a redundant array of inexpensive disks (RAID), hybrid storage device, or the like. Storage device 314 may comprise software modules 316, 318, and 320 for controlling processor 302. Information handling system 122 may comprise other hardware or software modules. Storage device 314 is connected to the system bus 304 by a drive interface. The drives and the associated computer-readable storage devices provide nonvolatile storage of computer-readable instructions, data structures, program modules and other data for information handling system 122. In one aspect, a hardware module that performs a particular function comprises the software component stored in a tangible computer-readable storage device in connection with the necessary hardware components, such as processor 302, system bus 304, and so forth, to carry out a particular function. In another aspect, the system may use a processor and computer-readable storage device to store instructions which, when executed by the processor, cause the processor to perform operations, a method or other specific actions. The basic components and appropriate variations may be modified depending on the type of device, such as whether information handling system 122 is a small, handheld computing device, a desktop computer, or a computer server. When processor 302 executes instructions to perform “operations”, processor 302 may perform the operations directly and/or facilitate, direct, or cooperate with another device or component to perform the operations.
As illustrated, information handling system 122 employs storage device 314, which may be a hard disk or other types of computer-readable storage devices which may store data that are accessible by a computer, such as magnetic cassettes, flash memory cards, digital versatile disks (DVDs), cartridges, random access memories (RAMs) 310, read only memory (ROM) 308, a cable containing a bit stream and the like, may also be used in the exemplary operating environment. Tangible computer-readable storage media, computer-readable storage devices, or computer-readable memory devices, expressly exclude media such as transitory waves, energy, carrier signals, electromagnetic waves, and signals per se.
To enable user interaction with information handling system 122, an input device 322 represents any number of input mechanisms, such as a microphone for speech, a touch-sensitive screen for gesture or graphical input, keyboard, mouse, motion input, speech and so forth. Additionally, input device 322 may take in data from one or more sensors 136, discussed above. An output device 324 may also be one or more of a number of output mechanisms known to those of skill in the art. In some instances, multimodal systems enable a user to provide multiple types of input to communicate with information handling system 122. Communications interface 326 generally governs and manages the user input and system output. There is no restriction on operating on any particular hardware arrangement and therefore the basic hardware depicted may easily be substituted for improved hardware or firmware arrangements as they are developed.
As illustrated, each individual component describe above is depicted and disclosed as individual functional blocks. The functions these blocks represent may be provided through the use of either shared or dedicated hardware, including, but not limited to, hardware capable of executing software and hardware, such as a processor 302, that is purpose-built to operate as an equivalent to software executing on a general-purpose processor. For example, the functions of one or more processors presented in
The logical operations of the various methods, described below, are implemented as: (1) a sequence of computer implemented steps, operations, or procedures running on a programmable circuit within a general use computer, (2) a sequence of computer implemented steps, operations, or procedures running on a specific-use programmable circuit; and/or (3) interconnected machine modules or program engines within the programmable circuits. Information handling system 122 may practice all or part of the recited methods, may be a part of the recited systems, and/or may operate according to instructions in the recited tangible computer-readable storage devices. Such logical operations may be implemented as modules configured to control processor 302 to perform particular functions according to the programming of software modules 316, 318, and 320.
In examples, one or more parts of the example information handling system 122, up to and including the entire information handling system 122, may be virtualized. For example, a virtual processor may be a software object that executes according to a particular instruction set, even when a physical processor of the same type as the virtual processor is unavailable. A virtualization layer or a virtual “host” may enable virtualized components of one or more different computing devices or device types by translating virtualized operations to actual operations. Ultimately however, virtualized hardware of every type is implemented or executed by some underlying physical hardware. Thus, a virtualization compute layer may operate on top of a physical compute layer. The virtualization compute layer may comprise one or more virtual machines, an overlay network, a hypervisor, virtual switching, and any other virtualization application.
Chipset 400 may also interface with one or more communication interfaces 326 that may have different physical interfaces. Such communication interfaces may comprise interfaces for wired and wireless local area networks, for broadband wireless networks, as well as personal area networks. Some applications of the methods for generating, displaying, and using the GUI disclosed herein may comprise receiving ordered datasets over the physical interface or be generated by the machine itself by processor 302 analyzing data stored in storage device 314 or RAM 310. Further, information handling system 122 receive inputs from a user via user interface components 404 and execute appropriate functions, such as browsing functions by interpreting these inputs using processor 302.
In examples, information handling system 122 may also comprise tangible and/or non-transitory computer-readable storage devices for carrying or having computer-executable instructions or data structures stored thereon. Such tangible computer-readable storage devices may be any available device that may be accessed by a general purpose or special purpose computer, including the functional design of any special purpose processor as described above. By way of example, and not limitation, such tangible computer-readable devices may comprise RAM, ROM, EEPROM, CD-ROM or other optical disk storage, magnetic disk storage or other magnetic storage devices, or any other device which may be used to carry or store desired program code in the form of computer-executable instructions, data structures, or processor chip design. When information or instructions are provided via a network, or another communications connection (either hardwired, wireless, or combination thereof), to a computer, the computer properly views the connection as a computer-readable medium. Thus, any such connection is properly termed a computer-readable medium. Combinations of the above should also be comprised within the scope of the computer-readable storage devices.
Computer-executable instructions comprise, for example, instructions and data which cause a general-purpose computer, special purpose computer, or special purpose processing device to perform a certain function or group of functions. Computer-executable instructions also comprise program modules that are executed by computers in stand-alone or network environments. Generally, program modules comprise routines, programs, components, data structures, objects, and the functions inherent in the design of special-purpose processors, etc. that perform particular tasks or implement particular abstract data types. Computer-executable instructions, associated data structures, and program modules represent examples of the program code means for executing steps of the methods disclosed herein. The particular sequence of such executable instructions or associated data structures represents examples of corresponding acts for implementing the functions described in such steps.
In additional examples, methods may be practiced in network computing environments with many types of computer system configurations, including personal computers, hand-held devices, multi-processor systems, microprocessor-based or programmable consumer electronics, network PCs, minicomputers, mainframe computers, and the like. Examples may also be practiced in distributed computing environments where tasks are performed by local and remote processing devices that are linked (either by hardwired links, wireless links, or by a combination thereof) through a communications network. In a distributed computing environment, program modules may be located in both local and remote memory storage devices. During drilling operations, information handling system 122 may process different types of the real time data which may be utilized to create an asphaltene onset pressure map (AOP).
A data agent 502 may be a desktop application, website application, or any software-based application that is run on information handling system 122. As illustrated, information handling system 122 may be disposed at any rig site (e.g., referring to
Secondary storage computing device 504 may operate and function to create secondary copies of primary data objects (or some components thereof) in various cloud storage sites 506A-N. Additionally, secondary storage computing device 504 may run determinative algorithms on data uploaded from one or more information handling systems 122, discussed further below.
Communications between the secondary storage computing devices 504 and cloud storage sites 506A-N may utilize REST protocols (Representational state transfer interfaces) that satisfy basic C/R/U/D semantics (Create/Read/Update/Delete semantics), or other hypertext transfer protocol (“HTTP”)-based or file-transfer protocol (“FTP”)-based protocols (e.g., Simple Object Access Protocol).
In conjunction with creating secondary copies in cloud storage sites 506A-N, the secondary storage computing device 504 may also perform local content indexing and/or local object-level, sub-object-level or block-level deduplication when performing storage operations involving various cloud storage sites 506A-N. Cloud storage sites 506A-N may further record and maintain DTC code logs for each downhole operation or run, map DTC codes, store repair and maintenance data, store operational data, and/or provide outputs from determinative algorithms that are fun at cloud storage sites 506A-N.
During operations, inputs 608 data are given to neurons 612 in input layer 604. Neurons 612, 614, and 616 are defined as individual or multiple information handling systems 122 connected in a network, which may compute information to make drilling, completion or production decisions such as but not limited how to drill the well, where to drill the well, how to complete a well, or where to complete a well, or how to produce a well, or where to produce a well. Any of computations may be from the current well being evaluated or analogue wells which may be in the field, in the basis, or not so if other characteristics such as but not limited to formation type or formation fluid provide a basis for analogy. The output from neurons 612 may be transferred to one or more neurons 614 within one or more hidden layers 602. Hidden layers 602 comprises one or more neurons 614 connected in a network that further process information from neurons 612. The number of hidden layers 602 and neurons 612 in hidden layer 602 may be determined by personnel that designs NN 600. Hidden layers 602 is defined as a set of information handling system 122 assigned to specific processing. Hidden layers 602 spread computation to neurons 614, which may allow for faster computing, processing, training, and learning by NN 600.
Information from fluid sampling tool 100 may be gathered and/or processed by the information handling system 122 (e.g., referring to
In examples, fluid sampling tool 100 may comprise one or more enhanced probe sections 704 and stabilizers 724. A probe may be a pad of multiple designs or packer of multiple designs or combinations therein. Each enhanced probe section may comprise a dual probe section 706 or a focus sampling probe section 708. Both of which may extract fluid from the reservoir and deliver said fluid to a channel 710 that extends from one end of fluid sampling tool 100 to the other. Without limitation, dual probe section 706 comprises two probes 712, 714 which may extend from fluid sampling tool 100 and press against the inner wall of wellbore 104 (e.g., referring to
In examples, channel 710 may connect other parts and sections of fluid sampling tool 100 to each other. Additionally, fluid sampling tool 100 may comprise a second high-volume bidirectional pump 730 for pumping fluid through channel 710 to one or more multi-chamber sections 732, one or more microsampling device 734, and/or one or more fluid analysis modules 736. Multiple multichambered sampling sections may be disposed within and may form fluid sampling tool 100.
Moreover, body 902 may have a concave cylinder shape. That is, an exterior surface 916 of body 902 between top end 912 and bottom end 914 may be recessed inward about body 902 such that body 902 has a concave cylinder shape. The concave shape may at least partially define a cavity 904 in which a microsample may be stored. Alternatively, exterior surface 916 may comprise other suitable profiles for at least partially defining cavity 904. For example, body 902 may have a substantially cylindrical shape with an annulus recess formed in exterior surface 916, which may at least partially define cavity 904. In another example, cavity 904 may be formed in an interior portion of body 902.
Referring back to
As noted above, there may be a plurality of microsamplers 804 disposed within microsampling tube 800. Each microsampler 804 may be separated by a spacer 806. In examples, spacer 806 may have a volume to capture a fluid sample should a microsampler 804 leak. For examples, spacer 806 may from a liquid/pressure tight seal. Further, spacer 806 may be made of a material that may absorb a fluid that may leak out of a microsampler 804, which may prevent contamination between each microsampler 804. As illustrated, microsamplers 804 and spacers 806 may be connected to each other. In examples, microsampler 804 may attach to spacer 806 through, a press fitting, nuts and bold, hooks and loops, glue, and/or the like. Like microsampler 804, spacer 806 may be threaded, which may allow for spacer 806 to rotate with and/or connect to microsampler 804 via a threaded rod 814.
Referring to
Additionally, seals 908, 910 may apply enough force to microsampling tube 800 to maintain a seal between seals 908, 910 and an inner surface of the structural wall of microsampling tube 800 as microsampler 804 moves along or through microsampling tube 800. Seals 908, 910 may comprise one or more polymeric O-rings (not shown) that may be compressed with and/or by microsampler 804 positioned in the microsampling tube 800 such that elastic forces of the O-rings apply sufficient force to maintain the seal. Alternatively, or in combination, the polymeric O-ring may swell in contact with oil or water and create a leak-free seal 900. Further, the polymeric O-ring may be oleophilic or oleophobic. The polymeric O-ring may be hydrophobic or hydrophilic. Utilizing a plurality of polymeric O-rings, a “sandwich” of polymeric O-rings may be used to increase the seal between microsamplers 804, wherein an oleophobic polymeric O-ring is in between two oleophilic polymeric O-rings to seal a fluid sample, such as oil, in cavity 904 within microsampler 804. In another example, a hydrophobic polymeric O-ring is in between two hydrophilic polymeric O-rings to seal a fluid sample, such as brine, in cavity 904 within microsampler 804. It should be noted that any number of stacking or “sandwiching” between different polymeric O-rings may be created. Referring back to
In
Referring back to
After sampling operations, microsampling tube 800 may be sealed. For example, the topmost and or bottom most microsamplers 804 (e.g., referring to
In current technology, bulk samples generally collect many milliliters of fluid and up to one or more liters of fluid. This restricts how many fluid samples may be collected in a downhole sampling tool from a few fluid samples a tens of fluid samples per single run. The microsampling tool provides the ability to collect many tens to many hundreds of samples per run and in some embodiments even up to a thousand or so. With the capability to collect a large number of microsamples new possibilities in reservoir characterization and sample characterization are possible. For instance, many locations along a wellbore may be sampled in order to provide a dense characterization of the wellbore. Multiple analytical equipment may make use of microsamples including but not limited to gas chromatography, liquid chromatography, other chromatographic methods, mass spectroscopic methods, and some bulk physical properties including PVT and phase behavior properties from devices such as MEMS devices and microfluidic devices. Multiple samples may be taken along a single pumpout such as three to ten fluid samples (or more) allowing clean fluid properties of the reservoir fluid to be more easily deconvoluted from the mud properties. Therein samples may be of higher contamination than 1% or 10% contamination and still provide reliable deconvoluted reservoir properties. This analysis may be done in conjunction with bulk samples, and microsamples are used to extrapolate properties derived from the bulk sample. Multiple samples from a single station at near time such that the samples have similar contamination levels may be used to determine the repeatability of the microsample and provide statistical assessment of fluid properties.
The systems and methods for a microsampling device discussed above, may comprise any of the various features of the systems and methods disclosed herein, comprising one or more of the following statements.
Statement 1: A microsampling device for taking fluid samples in a wellbore. The microsampling device may comprise a microsampling tube in which one or more microsamplers disposed in the microsampling tube. Additionally, the microsampling device may comprise a fluid flow line connected to the microsampling tube in which a fluid sample traverses and a secondary fluid flow line in which at least a part of the fluid sample may traverse from the microsampling tube through the secondary fluid flow line and into a wellbore.
Statement 2: The microsampling device of statement 1, wherein the one or more microsamplers comprise a body and a top seal disposed at one end of the body and a bottom seal disposed at an opposite end of the top seal.
Statement 3: The microsampling device of statement 2, wherein the body is a concave shape and forms an annulus around the body.
Statement 4: The microsampling device of statement 2, wherein the body comprises a threaded corridor that traverses the body along a longitudinal axis.
Statement 5: The microsampling device of statement 4, wherein the threaded corridor may mate to a threaded rod, wherein the threaded rod is connected to at least one motor.
Statement 6: The microsampling device of statement 5, wherein the at least one motor rotates the threaded rod which moves the one or more microsamplers within the microsampling tube.
Statement 7: The microsampling device of statements 2 or 3, further comprising a plunger connected to at least one motor through a rod.
Statement 8: The microsampling device of claim 7, wherein the plunger is in contact with one of the one or more microsamplers.
Statement 9: The microsampling device of claim 8, wherein the at least one motor pushes the one or more microsamplers with the plunger through the microsampling tube.
Statement 10: The microsampling device of statements 2, 3, or 7, further comprising a wire connected to at least one of the one or more microsamplers and at least one motor.
Statement 11: The microsampling device of claim 10, wherein each of the one or more microsamplers are connected to each other.
Statements 12: The microsampling device of statement 10, wherein the at least one motor pulls the wire which pulls the one or more microsamplers through the microsampling tube.
Statement 13: The microsampling device of statements 1 or 2, wherein the one or more microsamplers are separated by at least one spacer.
Statement 14: The microsampling device of statements 1, 2, or 13, further comprising one or more capillary ports disposed in the microsampling tube.
Statement 15: The microsampling device of statement 14, further comprising at least one syringe pump connect to one of the one or more capillary ports.
Statement 16: The microsampling device of statement 15, further comprising an analytical instrument connected to a second of the capillary one or more ports.
Statement 17: The microsampling device of statement 14, further comprising a housing in which the microsampling tube is disposed.
Statement 18: The microsampling device of statement 17, further comprising an analytical instrument connected to a first capillary port of the capillary one or more ports.
Statement 19: The microsampling device of statement 18, wherein the housing further comprising a ballast that applies pressure to the fluid sample disposed in the microsampling tube to force the fluid sample into the analytical instrument through the first capillary port.
Statement 20: The microsampling device of statements 1, 2, 13, or 14, wherein the secondary fluid flow line comprises a first check valve and a second check valve.
The preceding description provides various embodiments of the systems and methods of use disclosed herein which may contain different method steps and alternative combinations of components. It should be understood that, although individual embodiments may be discussed herein, the present disclosure covers all combinations of the disclosed embodiments, including, without limitation, the different component combinations, method step combinations, and properties of the system. It should be understood that the compositions and methods are described in terms of “including,” “containing,” or “including” various components or steps, the compositions and methods can also “consist essentially of” or “consist of” the various components and steps. Moreover, the indefinite articles “a” or “an,” as used in the claims, are defined herein to mean one or more than one of the element that it introduces.
For the sake of brevity, only certain ranges are explicitly disclosed herein. However, ranges from any lower limit may be combined with any upper limit to recite a range not explicitly recited, as well as, ranges from any lower limit may be combined with any other lower limit to recite a range not explicitly recited, in the same way, ranges from any upper limit may be combined with any other upper limit to recite a range not explicitly recited. Additionally, whenever a numerical range with a lower limit and an upper limit is disclosed, any number and any comprised range falling within the range are specifically disclosed. In particular, every range of values (of the form, “from about a to about b,” or, equivalently, “from approximately a to b,” or, equivalently, “from approximately a-b”) disclosed herein is to be understood to set forth every number and range encompassed within the broader range of values even if not explicitly recited. Thus, every point or individual value may serve as its own lower or upper limit combined with any other point or individual value or any other lower or upper limit, to recite a range not explicitly recited.
Therefore, the present embodiments are well adapted to attain the ends and advantages mentioned as well as those that are inherent therein. The particular embodiments disclosed above are illustrative only, and may be modified and practiced in different but equivalent manners apparent to those skilled in the art having the benefit of the teachings herein. Although individual embodiments are discussed, the disclosure covers all combinations of all of the embodiments. Furthermore, no limitations are intended to the details of construction or design herein shown, other than as described in the claims below. Also, the terms in the claims have their plain, ordinary meaning unless otherwise explicitly and clearly defined by the patentee. It is therefore evident that the particular illustrative embodiments disclosed above may be altered or modified and all such variations are considered within the scope and spirit of those embodiments. If there is any conflict in the usages of a word or term in this specification and one or more patent(s) or other documents that may be incorporated herein by reference, the definitions that are consistent with this specification should be adopted.
Number | Date | Country | |
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63388787 | Jul 2022 | US |