The present disclosure relates to an inspection method and an inspection apparatus for a liquid ejection head that ejects liquid from ejection ports and also to an ejection element substrate.
In a typically known ink ejection method for a print head mounted in an inkjet printing apparatus, electrothermal converters heat ink to eject droplets using the action of film boiling. A manufacturing process for such an inkjet print head needs to include a step for measuring the heat generation characteristics of the electrothermal converters and setting drive voltage to apply to the electrothermal converters.
As a method for setting ejection energy for liquid ejection, Japanese Patent Laid-Open No. 2011-224874 discloses a technique which prints inspection patterns while gradually changing at least one of the voltage value of drive voltage and the duration of time for applying the drive voltage and sets the ejection energy based on the inspection patterns thus printed.
Also, Japanese Patent Laid-Open No. 2018-153971 discloses a technique which, by utilizing the fact that a protective film protecting the electrothermal converters is sandwiched by films of different physical properties, estimates the film thickness of the protective film by measuring capacitance and calculates drive voltage based on the estimated film thickness and the electrical resistance of the electrothermal converters.
In order for the technique disclosed in Japanese Patent Laid-Open No. 2011-224874 to set the drive voltage in the manufacturing process, ink needs to be actually ejected. Thus, the manufacturing process needs to have a step for supplying ink to the ejection ports (nozzles) and a step for cleaning the ejection port surface after the ink ejection. By contrast, the technique disclosed in Japanese Patent Laid-Open No. 2018-153971 can find drive voltage needed to eject liquid without ink ejection. However, in order to be able to estimate the film thickness of the protective film through measurement of capacitance, measurement electrodes and dedicated wiring for capacitance measurement, which are not needed for actual ink ejection, need to be laid on the substrate.
The present disclosure aims to provide a technique which can inspect liquid ejection energy without having to change the electric wiring on an ejection element substrate or eject liquid.
In a first aspect of the present disclosure, there is provided an inspection method for inspecting a liquid ejection head including an ejection element substrate which has a substrate, a heat generation portion having an electrothermal converter provided on a first surface of the substrate, a protective film covering the electrothermal converter, and an organic layer covering the electrothermal converter and the protective film, the ejection element substrate being capable of ejecting liquid in a flow channel formed between the organic layer and the protective film through an ejection port formed in the organic layer by using heat generated at the heat generation portion, the inspection method comprising: acquiring, as a first measurement result, an electrical resistance value of the electrothermal converter, acquiring, as a second measurement result, a film thickness of the protective film at a film thickness measurement portion of the ejection element substrate where the protective film is exposed; and obtaining information on ejection energy needed to eject liquid through the ejection port, based on the first measurement result and the second measurement result.
In a second aspect of the present disclosure, there is provided an inspection apparatus for inspecting a liquid ejection head including an ejection element substrate which has a substrate, a heat generation portion having an electrothermal converter provided on a first surface of the substrate, a protective film covering the electrothermal converter, and an organic layer covering the electrothermal converter and the protective film, the ejection element substrate being capable of ejecting liquid in a flow channel formed between the organic layer and the protective film through an ejection port formed in the organic layer by using heat generated at the heat generation portion, the inspection apparatus comprising: a resistance value measurement unit configured to acquire, as a first measurement result, an electrical resistance value of the electrothermal converter; a film thickness measurement unit configured to acquire, as a second measurement result, a film thickness of the protective film at a film thickness measurement portion of the ejection element substrate where the protective film is exposed; and an obtainment unit configured to obtain information on ejection energy needed to eject liquid through the ejection port, based on the first measurement result and the second measurement result.
In a third aspect of the present disclosure, there is provided an ejection element substrate comprising: a substrate; a heat generation portion having an electrothermal converter provided on a first surface of the substrate; a protective film covering the electrothermal converter; and an organic layer covering the electrothermal converter and the protective film, wherein the ejection element substrate is capable of ejecting liquid in a flow channel formed between the organic layer and the protective film through an ejection port formed in the organic layer by using heat generated at the heat generation portion, and the ejection element substrate further comprises a film thickness measurement portion where the organic layer is removed to expose the protective film.
Further features of the present invention will become apparent from the following description of exemplary embodiments with reference to the attached drawings.
Embodiments of the present disclosure are described in detail below with reference to the drawings attached hereto. Note that the embodiments below are not intended to limit the present invention according to the scope of claims, and not all the combinations of features described in the present embodiments are necessarily essential as solving unit provided by the present invention. Also, although an inkjet print head mounted in an inkjet printing apparatus as a liquid ejection apparatus is used as an example of a liquid ejection head described in the embodiments, the liquid ejection head of the present disclosure is not limited to an inkjet print head used for image formation and can also be applied to an industrial liquid ejection head used to manufacture a product by ejecting liquid other than ink.
The film thickness measurement device (film thickness measurement unit) 103 is a measurement device that optically measures the thickness of a protective film forming the surface of the wafer 401, and a spectroscopic film thickness measurement device is used in the present embodiment. Based on the substrate identification number measured by the chip number measurement device 101, the film thickness measurement device 103 selects film thickness measurement areas to measure, from a plurality of film thickness measurement areas to be described later formed on the ejection element substrate 301. A description will be given later as to the film thickness measurement areas and the protective film. The resistance value measurement device (the resistance value measurement unit) 102 is a measurement device that measures the electrical resistance value of an electrothermal converter (a heat generation portion) to be described later formed on the electrothermal conversion substrate (also referred to as an ejection element substrate) 301.
The arithmetic device (obtainment unit) 104 calculates information on the electric energy (ejection energy) needed to eject liquid, based on resistance value data indicating the electrical resistance value measured by the resistance value measurement device 102 and film thickness data indicating the film thickness value measured by the film thickness measurement device 103. For this arithmetic apparatus 104, for example, a publicly known arithmetic apparatus in the form of a computer, such as a CPU, a ROM, and a RAM, can be used. The energy information writing apparatus 105 is an apparatus that registers a calculation result on the ejection energy information calculated by the arithmetic apparatus 104 into a storage unit provided in a liquid ejection head 106.
A tape-shaped electric wiring member 303 is electrically connected to the ejection element substrate 301, and the electric wiring member 303 is provided with connection terminals 302 for supplying electric signals, power, and the like for liquid ejection. The resistance value of a heat-generating resistor (electrothermal converter) 205 (
The wafer 401 is formed of a plurality of layers for forming the ejection element substrates 301, and heat generation portions where heat is generated are covered by an insulating protective film. This protective film tends to be thicker at a center portion than at an outer peripheral portion because of its manufacturing method. Specifically, the protective film in the substrate formation regions located at the positions 402a to 402d in
The film thickness monitor portions 501 are portions where the above-described film thickness measurement device 103 measures the thickness of the protective film covering the electrothermal converters of the ejection element substrate 301, and are portions where an organic layer formed as the outermost surface of the ejection element substrate 301 is removed. In the present embodiment, film thickness monitor portions 501a to 501f are formed at six positions in an outer peripheral region 520 of the ejection element substrate 301. The film thickness monitor portions 501a to 501c are formed at three positions along one of the long sides of the rectangular ejection element substrate 301, and the film thickness monitor portions 501d to 501f are formed at three positions along the other one of the long sides of the ejection element substrate 301. Note that the x-direction and y-direction of the ejection element substrate 301 coincide with the x-direction and y-direction of the wafer 401 in
The electrothermal converter 201 is structured such that a heat-generating resistor 205 provided on a first surface 220a of a substrate 220 formed of a silicon substrate or the like, a wiring portion 204 electrically connected to the heat-generating resistor 205, and a protective film 203 covering the heat-generating resistor 205 and the wiring portion 204 are stacked sequentially. The heat-generating resistor 205 has a region 205a which is in direct contact with the protective film 203 at a notch portion formed in part of the wiring portion 204. This region 205a of the heat-generating resistor 205 which is in direct contact with the protective film 203 serves as a heat generation portion that generates heat for heating liquid. The protective film 203 of the electrothermal converter 201 is covered by an organic layer 210 forming the outermost surface of the ejection element substrate 301. A flow channel 411 supplied with liquid is formed between the organic layer 210 and the protective film 203, and an ejection port 400 is formed in the organic layer 210 to eject liquid supplied from the flow channel. The ejection port 400 is formed at a position facing the heat generation portion 205a of the heat-generating resistor 205.
To cause liquid supplied into the flow channel 411 to be ejected from the ejection port 400, the heat-generating resistor 205 is energized via the wiring portion 204 so that the heat generation portion 205a raises the temperature of the surface of the protective film 203. As a result, an air bubble is generated by film boiling inside the liquid (ink) in contact with the surface of the protective film 203, and the pressure produced by the bubble generation causes the liquid to be ejected from the ejection port 400.
Electric energy needed to eject liquid (ejection energy) greatly depends on the resistance value of the heat-generating resistor 205 and the film thickness of the protective film 203. In other words, with a constant voltage supplied from the printing apparatus, the larger the resistance value of the heat-generating resistor 205, the smaller the current value. Thus, in a case where the resistance value of the heat-generating resistor 205 is large, it is necessary for the printing apparatus to either apply voltage to the heat-generating resistor 205 for a longer duration of time or increase the voltage applied to the heat-generating resistor 205.
Also, in a case where the protective film 203 is thick, the distance from the heat-generating resistor 205 to the ink to be ejected is long, which means that larger ejection energy is needed in order to eject liquid. Strictly speaking, other fluctuations which may occur in the manufacturing process also affect fluctuations in the ejection energy, but the influences by such fluctuations are negligible compared to the resistance value of the heat-generating resistor 205 and the thickness of the protective film 203. Thus, information on ejection energy for generating heat needed to eject liquid can be found by measurement of the resistance value of the heat-generating resistor and the thickness of the protective film 203. In the present embodiment, in order to measure the thickness of the protective film 203 with high accuracy, the film thickness measurement device 103 of the inspection apparatus 100 measures the film thickness of the protective film 203 at the film thickness monitor portions (film thickness measurement portions) 501 illustrated in
It is desirable that the thickness of the protective film 203 to be measured for estimation of ink ejection energy be measured immediately under the ejection port 400. However, the spot diameter of a spectroscopic film thickness gauge as a film thickness measurement device is larger than the ink ejection port, and thus, measurement using the ejection port 400 is difficult. For this reason, the monitor portions for performing film thickness measurement need to be at positions where the electrothermal converter 201, the wiring portion 204, the flow channel 411 formed for liquid ejection, and the like are not affected and where the protective film 203 appears as the uppermost portion. Thus, in the ejection element substrate 301 of the present embodiment, the film thickness monitor portions 501 are formed in the outer peripheral region 520 where there are no electrothermal converter 201 or wiring portion 204. The protective film 203 is exposed and measured at these film thickness monitor portions 501. The region of the organic layer 210 removed to form the film thickness monitor portion 501 needs to be equal to or larger than the spot diameter of the spectral film thickness measurement device. Thus, in the present embodiment, the film thickness monitor portion 501 is a rectangle whose short side is approximately 15 μm.
In the ejection element substrate 301 of the liquid ejection head 106 configured as described above, the ejection energy for ejecting liquid from the ejection port 400 can be set using the inspection apparatus 100 illustrated in
First, the inspection apparatus 100 determines from which position on the wafer 401 illustrated in
For example, the ejection element substrate 301 formed by cutting and separating the substrate formation region 402a of the wafer 401 illustrated in
Meanwhile, the ejection element substrates 301 formed by cutting and separating the substrate formation regions 402b, 402d illustrated in
The film thickness data obtained as described above and the resistance value of the heat generation portion 205a (a first measurement result) are inputted to the arithmetic apparatus 104. Based on the film thickness data and the resistance value data inputted thereto, the arithmetic apparatus 104 calculates information on ejection energy needed to eject liquid and sends the calculated ejection energy information to the ejection energy information writing apparatus 105. The ejection energy information writing apparatus 105 writes the ejection energy information calculated by the arithmetic apparatus 104 into non-volatile memory provided in the liquid ejection head 106 to be inspected. The ejection energy information written into the non-volatile memory serves as individual information on the liquid ejection head 106. Once the liquid ejection head 106 is mounted in a liquid ejection apparatus (an inkjet printing apparatus), the liquid ejection apparatus reads ejection energy information written into the non-volatile memory in the liquid ejection head 106. Then, in a case where the ejection energy thus read is smaller than a currently set ejection energy, the liquid ejection apparatus controls at least one of the drive voltage and the drive voltage application duration to generate the ejection energy read from the liquid ejection head 106. As a result, droplets can be ejected properly from the liquid ejection head 106.
As thus described, by directly measuring the resistance value of the electrothermal converter and the thickness of the protective film, the present embodiment can measure accurate ejection energy in a short period of time without having to actually eject liquid. In other words, because actual liquid ejection is not needed, a step of supplying liquid to the ejection ports and a step of cleaning the nozzle surface after the liquid ejection are unnecessary, which makes it possible to measure the ejection energy in a short period of time. Also, because the manufacturing process for the liquid ejection head is simplified, the facility and apparatus for manufacturing the liquid ejection head can be small in size. Further, because the ejection element substrate 301 in the present embodiment does not need dedicated wiring and measurement electrodes for film thickness measurement, costs for manufacturing the ejection element substrate 301 is not increased.
Next, a second embodiment of the present invention is described with reference to
The ejection element substrate 301A of the present embodiment illustrated in
In such an ejection element substrate 301A including the dummy ejection ports 400A, the film thickness monitor portions 601 (601a to 601d) are disposed in the ejection port formation regions of the ejection element substrate 301A, at positions close to the dummy ejection ports 400A. Note that the film thickness monitor portions 601 need to be disposed at positions not affecting, e.g., the other ejection ports and the flow channel that are used for liquid ejection. Note that, as illustrated in
As thus described, according to the present embodiment, the film thickness monitor portions 601 are set at portions having the same layer structure as the layer structure at the positions facing the ejection ports 400 and the dummy ejection ports 400A, and the film thickness of the protective film 203 is measured by the inspection apparatus 100 formed of a spectroscopic film thickness measurement device. Thus, the film thickness of the protective film 203 that closely approximates the true value can be expected to be obtained. Further, because the film thickness monitor portions 601 are disposed at positions close to the dummy ejection ports 400A not used for ejection, the formation of the film thickness monitor portions 601 does not affect the ejection ports 400 that actually eject liquid.
Although the film thickness monitor portions formed in the above embodiments are rectangular as an example, the film thickness monitor portions may be in a shape other than a rectangle. For example, the film thickness monitor portions may be a square whose sides are each approximately 15 μm or a circle whose diameter is approximately 15 μm.
The present disclosure can inspect liquid ejection energy without having to change the electric wiring on the ejection element substrate or to eject liquid.
While the present invention has been described with reference to exemplary embodiments, it is to be understood that the invention is not limited to the disclosed exemplary embodiments. The scope of the following claims is to be accorded the broadest interpretation so as to encompass all such modifications and equivalent structures and functions.
This application claims the benefit of Japanese Patent Application No. 2022-124639, filed Aug. 4, 2022, which is hereby incorporated by reference wherein in its entirety.
Number | Date | Country | Kind |
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2022-124639 | Aug 2022 | JP | national |