Information
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Patent Application
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20230295484
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Publication Number
20230295484
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Date Filed
February 18, 20222 years ago
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Date Published
September 21, 2023a year ago
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Inventors
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Original Assignees
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CPC
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International Classifications
- C09K8/512
- C09K23/00
- C09K8/516
Abstract
Lost circulation material (LCM) compositions may include a resin; an emulsifier selected from the group consisting of ethoxylated phenol, sodium salt of modified tall oil fatty amide, carboxylic acid terminated fatty polyamide, modified amidoamine, tall oil fatty acid, oxidized tall oil fatty amidoamine, ether carboxylic acid, and combinations thereof; a crosslinker; a cementitious and/or weighting agent; a retarder; a dispersant; and a silicon-based defoamer. The LCM compositions may have a thickening time of from about 3 hours than about 6 hours by reaching a Bearden consistency of 100 Bc. Methods of eliminating or reducing lost circulation in a lost circulation zone from a well may include introducing these LCM compositions into the well.
Claims
- 1. A lost circulation material (LCM) composition comprising:
from about 1% to about 15% bwoc of a resin;from about 0.01% to about 5% bwoc of an emulsifier selected from the group consisting of ethoxylated phenol, sodium salt of modified tall oil fatty amide, carboxylic acid terminated fatty polyamide, modified amidoamine, tall oil fatty acid, oxidized tall oil fatty amidoamine, ether carboxylic acid, and combinations thereof;from about 0.01% to about 5% bwoc of a crosslinker to crosslink the resin, where the crosslinker comprises at least one amine group;a cementitious and/or weighting agent;from about 0.01% to about 0.5% bwoc of a retarder, where the retarder is selected from the group consisting of lignosulfonates, organic acids, phosphonic acid derivatives, copolymers of 2-acrylamido-2-methylpropane sulfonic acid (“AMPS”) and unsaturated carboxylic acids, inorganic borate salts, and combinations thereof;from about 0.1% to about 2.0% bwoc of a dispersant; andfrom about 0.001% to about 0.5% bwoc of a silicon-based defoamer,wherein the LCM composition has a thickening time of from about 3 hours than about 6 hours by reaching a Bearden consistency of 100 Bc.
- 2. The LCM composition of claim 1, where the LCM composition has a thickening time of from about 3 hours than about 5 hours by reaching a Bearden consistency of 70 Bc.
- 3. The LCM composition of claim 1, where the resin comprises at least one of bisphenol-A-epichlorohydrin resin, C12-C14 alkyl glycidyl ether derivatives, 2,3-epoxypropyl o-tolyl ether, 1,6-hexanediol diglycidyl ether, butyl glycidyl ether, cyclohexanedimethanol diglycidyl ether, or combinations of these.
- 4. The LCM composition of claim 1, where the resin comprises bisphenol-A-epichlorohydrin resin and C12-C14 alkyl glycidyl ether.
- 5. The LCM composition of claim 1, where the crosslinker comprises at least one of diethylenetriamine (DETA), diethyltoluenediamine (DETDA), polyoxypropylene diamine, or combinations of these.
- 6. The LCM composition of claim 1, where the LCM composition comprises from about 0.10 weight percent to about 0.20 weight percent of crosslinker.
- 7. The LCM composition of claim 1, where the cementitious and/or weighting agent comprises class G cement and/or silica sand.
- 8. The LCM composition of claim 7, where the cementitious and/or weighting agent further comprises barite and/or manganese tetraoxide.
- 9. The LCM composition of claim 1, where the LCM composition has a density of from about 115 pounds per cubic foot (pcf) to about 150 pcf.
- 10. (canceled)
- 11. A method of eliminating or reducing lost circulation in a lost circulation zone from a well, the method comprising:
introducing a lost circulation material (LCM) composition into the well, the LCM composition comprising:
from about 1% to about 15% bwoc of a resin;from about 0.01% to about 5% bwoc of an emulsifier selected from the group consisting of ethoxylated phenol, sodium salt of modified tall oil fatty amide, carboxylic acid terminated fatty polyamide, modified amidoamine, tall oil fatty acid, oxidized tall oil fatty amidoamine, ether carboxylic acid, and combinations thereof;from about 0.01% to about 5% bwoc of a crosslinker to crosslink the resin,where the crosslinker comprises at least one amine group;
a cementitious and/or weighting agent;from about 0.01% to about 0.5% bwoc of a retarder, where the retarder is selected from the group consisting of lignosulfonates, organic acids, phosphonic acid derivatives, copolymers of 2-acrylamido-2-methylpropane sulfonic acid (“AMPS”) and unsaturated carboxylic acids, inorganic borate salts, and combinations thereof;from about 0.1% to about 2.0% bwoc of a dispersant; andfrom about 0.001% to about 0.5% bwoc of a silicon-based defoamer, wherein the LCM composition has a thickening time of from about 3 hours than about 6 hours by reaching a Bearden consistency of 100 Bc.
- 12. The method of claim 11, further comprising thickening the LCM composition in the well.
- 13. The method of claim 12, where the LCM composition has a thickening time of from about 3 hours than about 5 hours by reaching a Bearden consistency of 70 Bc.
- 14. The method of claim 12, where the LCM composition has a density of from about 115 pounds per cubic foot (pcf) to about 150 pcf.
- 15. The method of claim 11, where the lost circulation zone is located at a depth of up to 15,000 feet.