The present invention relates to a vaporizer used for vaporizing a liquid for a variety of applications. More specifically, the present invention relates to a MEMS (Micro-electro-mechanical-systems) vaporizer and a temperature sensor both integrated in a single silicon substrate which can be used for inhaling the active ingredients of plant material, commonly cannabis, tobacco, or other herbs or blends for the purpose.
A vaporizer is a device used for vaporizing a liquid for the purpose of inhalation. It is well known that draw-over vaporizers can be used for both civilian and military anesthesia. The earliest vaporizer is an oxford miniature vaporizer which has been in service over 40 years.
Since an electronic cigarette was developed the vaporizer has become popular. The electronic cigarette is a battery-powered vaporizer which simulates tobacco smoking by producing a vapor that resembles smoke. In order to meet the needs of the electronic cigarettes many vaporizers have been designed and manufactured. Some of them can be described in the following US patents.
U.S. Pat. No. 8,742,974 discloses a vaporizer in which the heating device can be configured by fixing heater plates to cover the front, rear, left and right side surfaces and the upper and bottom surfaces of the chamber. The heater plate may be formed by, for example, incorporating a heater in a plate made of aluminum or copper, etc.
U.S. Pat. No. 8,739,786 discloses a portable hand-held vaporizer for electronic cigarette application. The heating element of the vaporizer is a tungsten-based metallic alloy in the form of a coil that is disposed at least partially within the airflow passage. In other embodiments, the heating element is made from nickel-chrome, other types of metals, or metal-based composites that have a generally low thermal resistivity and are generally safe to pass air through for human consumption. In further embodiments, the heating element may be in the form of a plate or other shape, and may be located within a piece of glass or in close proximity to the airflow passage, but yet still able to effectively transfer heat.
U.S. Pat. No. 8,757,147 discloses a personal vaporizer unit which comprises a first wick element and a second wick element having a porous ceramic. The first wick element is adapted to directly contact a liquid held in a reservoir. The reservoir may be contained by a cartridge that is removable from the personal vaporizer unit. A heating element is disposed through the second wick element. An air gap is defined between the first wick element and the second wick element with the heating element exposed to the air gap. Air enters the first wick element through a hole in a housing holding the first wick element.
U.S. Pat. No. 8,678,012 discloses a tobacco solution atomizing device for electronic cigarette which comprises a glass fiber tube, a glass fiber yarn, a heating coil, a cotton cloth layer and a synthetic fiber layer, wherein the glass fiber yarn is insert into the heating coil which is then located inside the glass fiber tube; the ends of the glass fiber silk and two wires which are used to electronically connect the heating coil to the positive and negative electrode connectors extends outward through the glass fiber tube; the cotton cloth layer enwraps the outside wall of the glass fiber tube and reveal ends of the glass fiber yarn are pressed tightly between the cotton cloth layer and the glass fiber tube; a synthetic fiber layer is filled within the annular shape space between the cotton cloth layer and the fixing sleeve for holding the tobacco solution.
It can be seen from the above described vaporizers that each vaporizer generally consists of a small heating element responsible for vaporizing e-liquid, as well as a wicking material that draws liquid in. Along with a battery, the vaporizer is the central component of every electronic cigarette. The vaporizer is assembled by putting together of all separately manufactured parts. Several disadvantages can be found with these vaporizers:
An objective of the present invention is to provide a MEMS vaporizer which can overcome the above mentioned problems with the prior art.
In order to achieve this goal a MEMS vaporizer is provided by the present invention. The MEMS vaporizer composes: a silicon substrate, a micro-channel array created in the silicon substrate, a membrane suspending over the micro-channel array and supported by the silicon substrate, a resistance heater disposed on one side portion of the membrane and laterally across one end portion of the top of the micro-channel array, a resistance temperature sensor disposed on the membrane and adjacent to the resistance heater, two cavities are recessed in the silicon substrate and connected to the two end exits of the micro-channel array respectively, which all are integrated to be a vaporizer chip, a printed circuit board for packaging the vaporizer chip, a reservoir for inserting the printed circuit board therein so as to dispose one cavity of the vaporizer on its bottom and connect its inside with one end exit of the micro-channel array, a liquid stored in the reservoir, and an air filter disposed on the top of the reservoir which allows air entering the reservoir and a same volume of the liquid in the reservoir entering the micro-channel array continually.
According to the present invention the MEMS vaporizer is installed in an electronic cigarette. The electronic cigarette usually comprises: a housing, a battery; a reservoir, an air flow sensor, a microcontroller, a MEMS vaporizer, a temperature sensor, a small cloud of smoke, an air inlet, a light emitting diode, and a mouthpiece.
In the electronic cigarette the vaporizer is electrically heated for vaporizing the active ingredients of plant materials including cannabis, tobacco, or other herbs or blends for the purpose of inhalation. However, they also can be used with pure chemicals when mixed with plant material (e.g. tobacco-free nicotine).
According to the present invention the vaporizer is fabricated using a Micro-Electro-Mechanical Systems technology. The MEMS technology in its most general form can be defined as miniaturized mechanical and electro-mechanical elements that are made using the techniques of micro-fabrication. The most significant advantage of MEMS is their ability to communicate easily with electrical elements in semiconductor chips. Other advantages include small size, compact structure, lower power consumption, lower cost, increased reliability and higher precision.
The vaporizer is operated by filling a liquid in the reservoir, which automatically flows into the micro-channel array due to the surface tension of the liquid in the micro-channel array, and by heating the liquid using an electrical current passing through the resistive heater so that a certain amount of the liquid in the micro-channel array can be vaporized and a cloud of vapor can come out from the outlet of the micro-channel array.
According to the present invention, a method of manufacturing the MEMS vaporizer comprises steps of:
Looking at the vaporizer design and its fabrication method provided by the present invention their advantages can be summarized as the follows:
An advantage of the present invention is that the MEMS vaporizer is fabricated using the techniques of micro-fabrication, which provides with lower cost, increased reliability and higher precision.
Another advantage of the present invention is that the heater of the vaporizer is disposed on a membrane that helps to achieve thermal isolation of the heater from its supporting substrate.
Another advantage of the present invention is that the heater of the vaporizer allows for contacting the heated liquid directly which can result in very high heating efficiency.
Still another advantage of the present invention is that the temperature sensor of the vaporizer allows for measuring the vaporization temperature of the liquid precisely, which is necessary for controlling the heater of the vaporizer.
Still another advantage of the present invention is that the vaporizer allows to be combined with an air flow sensor which can make its applications such as electronic cigarettes digital and intelligent.
Still another advantage of the present invention is that the vaporizer is a silicon-based integrated actuator which provides advantages including small size, lower power consumption, lower cost, increased reliability, higher precision, and environmentally friend.
The various features of the present invention are shown in the drawings in which like numerals indicate similar elements.
The following detailed description of the invention is merely exemplary in nature and is not intended to limit the invention or the application and uses of the invention. Furthermore, there is no intention to be bound by any theory presented in the preceding background of the invention or the following detailed description of the invention.
As shown in
It is noted that the MEMS vaporizer provided by the present invention is a phase change actuator by which a liquid can be changed to a vapor. This change is governed by the conservation equations of mass, momentum, and energy. Since the change takes place in the micro-channels which have a large surface-to-volume ratio, the capillary force can provide sufficient pressure to push liquid flow in the micro-channels.
Reference to
The first term, the thermal power transferred into the vaporizer by dissipating electrical power in the resistance heater 105, is determined by measuring the voltage drop across the resistance heater 105 and the voltage drop across a power resistor in series with the resistance heater 105. The voltage drop across the power resistor is used to calculate the current through the resistance heater 105 using Ohm's Law. The power Pin dissipated in the resistance heater 105 is then:
Pin=VI (1)
where V and I are the voltage and current applied to the resistance heater 105 respectively.
The second term, the sensible heat is conducted out of the vaporizer by the micro-channel array 103, membrane 104 and liquid 112 and 116, which can be determined from the temperatures measured by the temperature sensor 106 positioned on the membrane 104.
The third term in the energy balance, the latent heat carried away by the vaporization of the liquid 112, can be determined by measuring the mass transfer rate from the micro-channel array 103, Jm. The latent heat transfer rate from the micro-channels, Ql, is then:
Ql=JmHfg (2)
where Hfg is the latent heat of vaporization of the liquid 112.
Micro-channel vaporization efficiency, ηvap, is defined to be the ratio of latent heat transfer rate by vaporization over the power into the vaporizer:
ηvap=Ql/Pin (3)
The driving force for liquid flow along the micro-channel array 103 is the capillary pressure Pc, given by the equation:
Pc=2γ cos θ/r (4)
where γ is the surface tension between the liquid 112 and air, θ is the contact angle between the liquid 112 and the wall of the micro-channel array 103, r is the smallest dimension of the micro-channel array 103.
The liquid flow rate can then be found using force balance, by equating capillary pressure forces driving flow with liquid viscous force retarding flow. With assumptions: steady fluid flow in the micro-channel array 103; neglecting temperature variation in liquid properties; and fully developed laminar flow. The following expression can be obtained:
u=(r2/8μι)/(2γ cos θ/r) (5)
where u is the liquid velocity, μ is the liquid viscosity, ι is the distance over which liquid has traveled.
The mass flow rate of liquid 112 in the micro-channel array 103 is then:
Jm=uAρ (6)
where ρ is the density of the liquid 112, A is the cross-sectional area of the micro-channel array 103.
Knowing the mass flow rate the vapor generating rate in the micro-channel array 103 can be found:
Vvap=Jm/MRuTsPa (7)
where M is the molecular weight of the average liquid 112, Ru is the universal gas constant, Pa is the atmospheric pressures and Ts is the saturation temperatures of the liquid 112.
Several factors have been identified as having a significant impact on the vaporizer performance, which include: the compliance and thermal isolation of the membrane 104; the electrical and thermal properties of the resistance heater 105 and temperature sensor 106; and the length and size of the micro-channel 103.
In order to optimize all these factors the flowing requirements applied to the vaporizer design are appropriate and necessary:
The vaporizer further composes: an electrically insulating layer such as a silicon nitride layer or the like disposed on the top 108 and bottom 109 of the membrane 104, and a passivation layer 110 such as a double layer consisting of a silicon nitride layer and a silicon carbide layer, which covers the top of the resistance heater 105 and the resistance temperature sensor 106.
The micro-channel array 103 of the vaporizer is configured to consist of 1 to 30 micro-channels in which each micro-channel having a length ranging from 50 to 500 micron, a width ranging from 20 to 200 micron, and a height ranging from 10 to 50 micron and two adjacent micro-channels are separated by a trapezium-shape side wall with a top width ranging from 2 to 20 micron;
The membrane 104 of the vaporizer is made of polysilicon layer, or amorphous silicon, or amorphous silicon carbide layer with a thickness ranging from 2 to 5 micron;
The resistance heater 105 of the vaporizer is made of Ta—Al or Ni—Cr alloy thin film, or the like with a resistance ranging from 1 to 100 ohm; The resistance temperature sensor 106 of the vaporizer is made of Ni metal thin film or the like with a resistance ranging from 100 to 1000 ohm.
The MEMS vaporizer provided by the present invention has several applications. A main application is for electronic cigarettes.
As shown in
The operation of the MEMS vaporizer in an electronic cigarette provided by the present invention can be run as shown in
A signal produced by the air flow sensor 303 is amplified by a pre-amplifier 304 and then send to a microcontroller 305 for digital processing. The temperature of the vaporizer 306 is measured by a temperature sensor 306. A signal produced by the temperature sensor 306 is amplified by a pre-amplifier 307 and then send to the microcontroller 305 for digital processing. After digital processing the microcontroller 305 send a pulse-width modulation (PWM) to the gate of the power field-effect transistor 302 which allows the voltage 308 being applied to the vaporizer 306 according to both the air flow rate signal and the heating temperature signal of the vaporizer 306.
It is noted that the MEMS vaporizer has been getting more and more attention due to its compact structure and high heat transfer efficiency. Compared with a conventional vaporizer, the MEMS vaporizer offers higher heat and mass transfer rate. Therefore MEMS vaporizer has been applied in many other fields, such as chemical industry, medical instrument, mechanical engineering and electric chip cooling.
At the start of the process, a silicon substrate 401 with one side polished is provided which has a resistivity ranging from 0.1 to 0.001 ohm-cm and a (100) crystal orientation.
In step 1, as shown in
In step 2, as shown in
Each porous silicon rectangular region of the porous silicon array 403 has a length ranging from 50 to 500 micron and a width ranging from 20 to 200 micron. The thickness of the porous silicon layer depends upon the anodic current intensity and the process timing. The resulted thickness of the porous silicon layer is ranging from 10 to 50 micron. Two adjacent porous silicon rectangular regions are separated by a trapezium side wall with a top width ranging from 2 to 20 micron.
In step 3, as shown in
In step 4, as shown in
The thickness of the polysilicon layer, or amorphous silicon layer, or amorphous silicon carbide layer 405 is ranging from 2 to 5 micron. It is noted that the polysilicon layer, or amorphous silicon layer, or amorphous silicon carbide layer 405 functions as the basic structure material for the membrane of the vaporizer which will be formed.
In step 4, as shown in
Reference to
Then a Ni metal thin film resistance temperature sensor 408 is created on the top of the porous silicon array 403 and adjacent to the resistance heater 407. Since there is no etchant available for wet etching Ni metal a lift-off process is needed. Using a photo-resist pattern as mask a Ni metal thin film deposition is performed by sputtering. In order to increase the thickness of the Ni metal thin film an additional chemical plating process may be performed hereafter. After removing the photo-resist pattern in a micro-strip a Ni metal thin film sensor 408 is left on the top of the porous silicon array 403. The resistance of the temperature sensor 408 is ranging from 100 to 1000 ohm. The Ni metal is chosen for the temperature sensor 408 because it has a higher temperature coefficient of bulk resistance of 6.8×10−3/° C., compared to the 3.9×10−3/° C. of bulk platinum. It is noted that in this step a Ni metal thin film interconnection line and four Ni metal bonding pads are also created, which not only connect the Ni metal thin film resistance temperature sensor 408 but also the Ta—Al or Ni—Cr alloy thin film, or the like resistance heater 407.
Reference to
Reference to
Reference to
It is noted that step 8 results in a completed vaporizer chip which is marked by 101 in
Back to
Still reference to
As shown in
The embodiments and examples set forth herein were presented in order to best explain the present invention and its particular application and to thereby enable those skilled in the art to make and use the invention. However, those skilled in the art will recognize that the foregoing description and examples have been presented for the purposes of illustration and example only. The description as set forth is not intended to be exhaustive or to limit the invention to the precise form disclosed. Many modifications and variations are possible in light of the above teaching without departing from the spirit of the forthcoming claims.
Number | Name | Date | Kind |
---|---|---|---|
4808009 | Sittler | Feb 1989 | A |
5644676 | Blomberg | Jul 1997 | A |
6136212 | Mastrangelo | Oct 2000 | A |
6748164 | Kuzyk | Jun 2004 | B1 |
6821819 | Benavides | Nov 2004 | B1 |
7088914 | Whittle | Aug 2006 | B2 |
7171975 | Moon | Feb 2007 | B2 |
8678012 | Li et al. | Mar 2014 | B2 |
8739786 | Postma et al. | Jun 2014 | B2 |
8742974 | Sishtla et al. | Jun 2014 | B1 |
8757147 | Terry et al. | Jun 2014 | B2 |
20020084510 | Jun | Jul 2002 | A1 |
20030106551 | Sprinkel, Jr. | Jun 2003 | A1 |
20040056016 | Tian | Mar 2004 | A1 |
20050155615 | Rohdewald | Jul 2005 | A1 |
20070095507 | Henderson | May 2007 | A1 |
20080087629 | Shimomura | Apr 2008 | A1 |
20080248613 | Chen | Oct 2008 | A1 |
20080257367 | Paterno | Oct 2008 | A1 |
Entry |
---|
Innovative Sensor Technology; published Mar. 31 2014 www.ist-ag.com/eh/ist-ag/en/home.nsf/contentview/EB0D258CF05CA816C12578930071FD43. |
Number | Date | Country | |
---|---|---|---|
20160007653 A1 | Jan 2016 | US |