Method and apparatus for an integrated laser beam scanner using a carrier substrate

Information

  • Patent Grant
  • RE38437
  • Patent Number
    RE38,437
  • Date Filed
    Thursday, December 20, 2001
    23 years ago
  • Date Issued
    Tuesday, February 24, 2004
    20 years ago
  • US Classifications
    Field of Search
    • US
    • 359 201
    • 359 202
    • 359 212
    • 359 213
    • 359 214
    • 359 220
    • 359 221
    • 359 223
    • 359 224
    • 359 225
    • 359 850
  • International Classifications
    • G02B2608
Abstract
An solid state scanning system having a single crystal silicon deflection mirror and scanning mirror is integrated with a light source. Separation of the micro-electro-mechanical systems and light emitters on separate substrates allows the use of flip-chip and solder bump bonding techniques for mounting of the light sources. The separate substrates are subsequently full wafer bonded together to create an integrated solid state scanning system.
Description




CROSS-REFERENCE TO RELATED APPLICATIONS




The present invention is related to “METHOD AND APPARATUS FOR AN INTEGRATED LASER BEAM SCANNER” by Floyd, Sun and Kubby (Attorney Docket No. D/98706). Ser. No. 09/201738, filed on the same day and assigned to the same assignee which is hereby incorporated by reference in its entirety.




BACKGROUND AND SUMMARY OF INVENTION




The present invention relates generally to the field of laser beam scanning systems, and more particularly to micro-electro-mechanical systems (MEMS) for laser beam scanning. Miniature laser beam scanning systems are important for applications such as barcode scanning, machine vision and, most importantly, xerographic printing. The use of MEMS to replace standard raster output scanning (ROS) in xerographic print engines allows simplification of printing systems by eliminating macroscopic mechanical components and replacing them with large arrays of scanning elements. Advanced computation and control algorithms are used in managing the large arrays of scanning elements. Such MEMS based printing systems are entirely solid state, reducing complexity, and allowing increased functionality, including compensation of errors or failures in the scanner elements.




An important step in constructing solid state scanning systems is integration of the semiconductor light emitter directly with MEMS actuators to gain the desired optical system simplification. Integrated scanners, which have lasers and scanning mirrors in the same structure, have been demonstrated using manual placement of laser chips onto MEMS wafers with micromachined alignment parts and adhesives by L. Y. Lin et al in Applied Physics Letters, 66, p. 2946, 1995 and by M. J. Daneman et al in Photonics Technology Letters, 8(3), p. 396, 1996. However, current techniques do not allow for wafer-scale integration of the light-emitter and MEMS device.




In accordance with the present invention a laser beam scanner consisting of a single crystal silicon deflection mirror and a torsional mirror is integrated with a laser diode in the same structure. Details of creating a torsional mirror and actuating it magnetically or electrostatically are detailed in U.S. Pat. No. 5,629,790 by Neukermans and Slater which is incorporated herein by reference in its entirety.




Using solder bump bonding methods, completed and tested laser diodes are bonded to a glass or a silicon carrier substrate. The carrier substrate is aligned and bonded to a Si or SOI wafer containing the MEMS layers. Bonding of the lasers to a carrier substrate completely partitions the bonding process from the MEMS. This complete partition eliminates possible conflicts between the conditions needed for solder bump bonding, such as the use of solder flux, and preserves the integrity of the MEMS layers.




The substrates are heated in a non-oxidizing environment to join the two substrates. High surface tension of the solder aligns the wettable metal bonding pads on each substrate with each other. The ability of the reflowed solder to self-align the substrates because of surface tension simplifies assembly.




The use of the SCS layer of a SOI wafer, rather than a polysilicon film provides for the introduction of very flat and smooth mirrors and high reliability torsion bars. The device is scalable to arrays of lasers and scanning mirrors.




Integration of the scanner and light source eliminates the need for external, manual alignment of light sources and scanning mirrors. Simplified post-processing steps such as interconnect metallization can be realized because the use of an etched recess results in nearly planar surfaces. In addition, pick and place technologies used for multi-chip module assembly can be adapted for wafer scale assembly and bonding of light sources to the carrier substrate.




Thus, the present invention allows the integration of lasers, electrical interconnects, and electrodes on a single glass or Si wafer for actuation of MEMS devices. The glass or Si wafer is aligned and bonded to the MEMS wafer, forming an integrated, three dimensional structure.











BRIEF DESCRIPTION OF THE DRAWINGS




A more complete appreciation of the invention and many of the attendant advantages thereof will be readily obtained and understood by referring to the following detailed description and the accompanying drawings in which like reference numerals denote like elements as between the various drawings. The drawings, briefly described below, are not to scale.





FIG. 1

is shows MEMS layers and VCSEL for a laser beam scanner in accordance with an embodiment of this invention.





FIG. 2a

shows a laser beam scanner with optical path having an electrostatically actuated torsion mirror in accordance with an embodiment of this invention.





FIG. 2b

shows a top view a laser beam scanner in accordance with an embodiment of this invention.





FIG. 3a

shows a laser beam scanner with optical path having a magnetically actuated torsion mirror in accordance with an embodiment of this invention.





FIG. 3b

shows a laser beam scanner with optical path having a magnetically actuated torsion mirror using an external magnetic field in accordance with an embodiment of this invention.





FIGS. 4a-4j

show process steps for fabricating MEMS components in accordance with an embodiment of this invention.





FIGS. 5a-5e

show steps for fabricating substrate containing laser die and mirror actuation electrodes in accordance with an embodiment of this invention





FIG. 6a

shows a completed laser beam scanner before release of deflecting mirror in accordance with an embodiment of this invention.





FIG. 6b

shows a completed integrated solid state scanner after release of deflecting mirror in accordance with an embodiment of this invention.











DETAILED DESCRIPTION




An embodiment in accordance with the present invention is shown in FIG.


1


and

FIG. 2a. A

laser beam scanner consisting of single crystal silicon (SCS) deflecting mirror


240


and torsional mirror


250


is integrated with laser diode or light emitting diode


105


. Using solder bump bonding methods, completed and tested laser diodes


105


are bonded to glass or silicon carrier substrate


101


. Carrier substrate


101


is aligned and bonded to MEMS substrate


130


containing the MEMS layers. Bonding of laser diode


105


to carrier substrate


101


completely partitions the bonding process from the MEMS layers. This complete partition eliminates possible conflicts between the conditions needed for solder bump bonding, such as the use of solder flux, and preserves the integrity of the MEMS layers. Typically, solders such as Pb/Sn, Au/Sn, or In/Sn are evaporated selectively onto wettable metal bonding pads


111


onto substrate


101


and reflowed to form hemispherical solder bumps


110


. Solder bumps


110


are contacted to wettable metal bonding pads


113


on laser substrate


106


.




Laser substrate


106


and carrier substrate


101


are heated in a non-oxidizing environment to join the respective substrates together. High surface tension of the solder aligns wettable metal bonding pads


11




1


with wettable metal bonding pads


113


on laser substrate


106


. The ability of the reflowed solder to self-align laser substrate


106


with carrier substrate


101


because of surface tension simplifies the assembly process. Additionally, very little pressure is required during the process of bonding laser substrate


106


to carrier substrate


101


.




Micromechanical elements (MEMS) are formed on MEMS substrate


130


, typically about 500 μm thick using conventional photolithography and the patterning of single crystal silicon (SCS) layer


118


, polysilicon layers


117


and insulating oxide layers


116


, which are typically PSG or thermal oxide, is performed using both dry and wet etching techniques. MEMS substrate


130


embodies SCS layer


118


, insulating oxide layer


116


and silicon substrate


115


. Typical thickness for each of layers


116


,


117


, and


118


is on the order of several μm. VCSEL (vertical cavity surface emitting laser)


105


is solder bump


110


bonded to glass or dielectric-coated (typically SiO


2


or Si


3


N


4


coated) Si substrate


101


, typically about 500 μm thick. Additionally, two actuation electrodes


220


and two interconnects


125


are formed on glass or dielectric-coated Si substrate


101


. Interconnects


125


provide current to substrate


101


to power VCSEL


105


and to electrodes


220


for control of torsional mirror


250


. After solder bonding of VCSEL


105


to glass or dielectric-coated Si substrate


101


, substrate


101


is aligned and bonded to MEMS substrate


130


.




MEMS substrate


130


has deep reactive ion etching (RIE) and/or wet etched hole


135


, typically 3 mm in diameter, for emitted light


299


(see

FIG. 2a

) to pass through MEMS substrate


130


and onto deflecting mirror


240


. Deflecting mirror


240


reflects emitted light


299


onto torsional mirror


250


. As shown in

FIG. 2a

, polysilicon hinge


255


attaches deflecting mirror


240


to MEMS substrate


130


. Deflecting mirror


240


is etched from SCS layer


118


. Polysilicon hinge


255


allows deflecting mirror


240


to rotate clockwise about an axis perpendicular to the plane of

FIG. 2a

, out of MEMS substrate


130


to the position above via


135


as shown in FIG.


2


a. Deflecting mirror


240


is supported by support latch


268


controlled by a spring and latch assembly (not shown) in the manner described in the paper by Lin et al. in Photonics Technology Letters, 6(12), p. 1445, 1994 which is incorporated herein in its entirety by reference. Controlling the position and length of support latch


268


allows the angle of deflecting mirror


240


to be precisely fixed. Deflection of torsional mirror


250


in both directions is accomplished by charging alternately one of two actuator electrodes


220


. Torsional mirror


250


is electrically grounded and attracted to charged one of two actuator electrodes


220


.





FIG. 2b

shows a top view of one combination deflection mirror/torsional mirror solid state element. Polysilicon hinges


255


and deflecting mirror


240


are shown along with hole


265


to receive the tab (not shown) on support latch


268


. The layout of torsional mirror


250


supported by torsion bar


270


with respect to hole


217


is also shown.




MEMS components such as deflecting mirror


240


and torsional mirror


250


can be formed in MEMS substrate


130


by using a combination of well-known surface and bulk micro-machining techniques. Polysilicon hinges


255


may be formed as described by M. C. Wu, “Micromachining for Optical and Optoelectronic Systems,” Proceedings of IEEE, Vol. 85, p. 1833, 1997 and by Pister et al., “Microfabricated Hinges,” Sensors and Actuators, A: Physical v. 33 n. 3 pp. 249-256, June 1992 which are hereby incorporated by reference in their entirety.




As seen in

FIG. 1

, bonding of VCSEL


105


to glass or SiO


2


coated Si substrate


101


completely separates the bonding process from the MEMS components. The separation eliminates possible conflicts between conditions needed for solder bump bonding, such as the use of solder flux and the integrity of the MEMS layers. Full wafer bonding of glass or dielectric-coated Si substrate


101


to MEMS substrate


130


is done at low temperature to avoid damage to VCSEL


105


. Metallization on glass or dielectric-coated Si substrate


101


is achieved by use of adhesive bonding techniques requiring temperatures of between 20° C.-100° C.




Another embodiment in accordance with the present invention is shown in FIG.


3


A. VCSEL (vertical cavity surface emitting laser)


105


is solder bump


110


bonded to glass or dielectric-coated Si substrate


101


. Glass or dielectric-coated Si substrate


101


is aligned and bonded to MEMS substrate


130


. MEMS substrate


130


has deep RIE and/or wet etched via


135


for emitted light


199


to pass through the surface of MEMS substrate


130


and onto deflecting mirror


240


which reflects emitted light


299


onto torsional mirror


250


. Torsional mirror


250


contains ferro-magnetic thin film


330


with magnetization in the plane of torsional mirror


250


. Coil


380


on glass or dielectric-coated Si substrate


101


generates magnetic field


391


perpendicular to the magnetic field created by ferromagnetic thin film


330


contained on torsional mirror


250


. Hence, actuation of coil


380


turns torsional mirror


250


. Polysilicon hinge


255


attaches deflecting mirror


240


to MEMS substrate


130


. Polysilicon hinge


255


allows deflecting mirror


240


to rotate clockwise about an axis perpendicular to the plane of

FIG. 3a

, out of MEMS substrate


130


to a position above via


135


as shown in FIG.


3


a. Deflecting mirror


240


can be supported by support latch


268


controlled by a spring and latch assembly (not shown) in the manner shown by Lin et al. in Photonics Technology Letters, 6(12), p. 1445, 1994 and incorporated herein in its entirety by reference. Fixing the position and length of support latch


268


allows the angle of deflecting mirror


240


to be precisely fixed.





FIG. 3b

shows an embodiment in accordance with this invention wherein torsional mirror


250


contains microfabricated coil


350


generating magnetic field


385


perpendicular to torsional mirror


250


but is otherwise similar to FIG.


3


a. Coil


350


is a conductive loop which may be formed by vapor depositing conductive material onto torsional mirror


250


and patterning into coil


350


. External magnetic field


370


is applied parallel to the plane of torsional mirror


250


to turn torsional mirror


250


. Application of current to coil


350


results in an angular deflection of torsional mirror


250


proportional to the current introduced into coil


350


. Hence, coil


350


behaves like a galvanometer coil. Direction of current flow in coil


350


determines the direction of the angular deflection of torsional mirror


250


.




Steps for fabricating deflecting mirror, supporting latch and VCSEL in accordance with this invention are shown in

FIGS. 4a-4j

and

FIGS. 5a-5e

. The starting material is MEMS substrate


130


which comprises a silicon on insulator material (SOI). MEMS substrate


130


includes silicon substrate


115


, thermally-grown SiO


2


layer


116


bonded to wafer


113


. MEMS substrate


130


is then thinned to the required thickness. MEMS substrates


130


are commercially available from, for example, Bondtronix, Inc. of Alamo, Calif. or Ibis Technology Corporation of Danvers, Mass. Typical thickness of SCS layer


118


is 2-20 μm depending on the required stiffness of the torsional spring elements and mirror surfaces to be constructed. Other MEMS layers are deposited on top of MEMS substrate


130


by well-known methods such as low pressure chemical vapor deposition (LPCVD). These MEMS layers include mechanical layers of polycrystalline silicon (polysilicon)


117


(not shown in

FIGS. 4

) and sacrificial oxide layer


119


that is phosphorus-doped glass (PSG). The embodiment in FIG.


4


a


4


c has PSG layer


119


deposited directly on top of SCS layer


114








118



. Polysilicon layer



117


(see

FIG. 1

) is subsequently deposited on PSG layer


119


. Typical thicknesses for polysilicon layer


117


and PSG layer


119


are 1-2 μm.




Formation of MEMS elements occurs by conventional photolithography and patterning of SCS layer


114








118



, polysilicon layer



117


, and PSG layer


119


is performed using both wet and dry etching. In accordance with an embodiment of this invention, deflecting mirror


240


and deep recess


135


are required.





FIGS. 4a-4j

show steps for fabricating deflecting mirror


240


, torsional mirror


250


, supporting latch


268


, and deep recesses


135


and


217


. Latch


268


has a tab (not shown) which inserts into corresponding hole


165


in the bottom of deflecting mirror


240


. The final configuration of deflecting mirror


240


and latch


255


are shown in FIG.


6


b. Typical sizes for deflecting mirror


240


are between 0.5 mm


2


to 1 mm


2


.





FIG. 4a

has silicon nitride (SiN


x


) deposited on substrate


130


using LPCVD. SiN


x


layer (not shown) is patterned using CF


4


/O


2


RIE with a photoresist mask. Potassium hydroxide (KOH) is used to etch holes from the bottom of substrate


115


, stopping on layer


116


. Size of hole


217


is similar to torsional mirror


250


to allow free rotation. Hole


135


is simultaneously etched, for fitting VCSEL


105


which typically has dimensions of 500 μm by 500 μm. Alternatively, holes


217


and


135


may be defined by deep RIE using C


4


F


8


and SF


6


with a mask of SiN


x


or photoresist.





FIG. 4b

shows recess


135


(200-250 μm deep) etched into MEMS substrate


130


using a combination of CF


4


/O


2


RIE for etching SCS layer


114








118



and insulator layer



116


and a deep RIE of recess


135


using C


4


F


8


and SF


6


.





FIG. 4c

shows CVD deposition of PSG layer


119


.





FIG. 4d

shows the wet etch of windows


410


into PSG layer


119


down to SCS layer


114








118



.






FIG. 4e

shows deposition of aluminum film


430


(typically 0.1-0.2 μm thick) as a high reflectivity layer.





FIG. 4f

shows a wet etch (typically a mixture of phosphoric and nitric acid) of aluminum film


430


to remove aluminum in all but the mirror regions. The mirror region locations coincide with the locations of windows


410


.





FIG. 4g

shows the etch of vias


433


using CF


4


/O


2


RIE with a photoresist mask. This step also serves to open laser die window


135


.





FIG. 4h

shows formation of hinges


255


for deflecting mirror


240


from polysilicon layer


117


(not shown, see

FIG. 1

) that is deposited in this step.





FIG. 4i

shows etch of PSG layer


119


and SCS layer


114








118



to pattern deflecting mirror



240


, hinges


255


and access holes


437


. A typical size for access holes


437


is 10 μm by 10 μm. Access holes


437


allow for the etchant used to release deflecting mirror


240


to reach insulating layer


116


. Deflecting mirror


240


size is typically from 1 mm


2


-2 mm


2


. Torsional mirror


250


is also defined in this step.





FIG. 4j

shows release of deflecting mirror


240


, torsional mirror


250


and hinge


255


by etching PSG layer


119


and layer


116


using an HF based etch.





FIGS. 5a-e

show the steps used to fabricate wafer


103


containing VCSEL


105


and mirror actuation electrodes


220


in accordance with an embodiment of this invention.





FIG. 5a

shows starting glass or silicon substrate


101


for fabrication of wafer


103


.





FIG. 5b

shows deposition of silicon nitride or silicon dioxide layer


502


by LPCVD or plasma-enhanced CVD process to provide electrical isolation from silicon substrate


101


.





FIG. 5c

shows deposition of electrodes


220


and solder for solder bumps


110


.





FIG. 5d

shows completed deposition of electrodes


220


for mirror actuation. Electrodes


220


are much thicker ˜200-300 μm) than solder bumps


110


(typically 50-100 μm) and are electroplated.





FIG. 5e

shows alignment and solder bump bonding of VCSEL


105


to Si substrate


101


in the GaAs bonding step. Solder bumps


110


can be defined on metal bonding pads


113


of VCSEL substrate


106


. Si substrate


101


and VCSEL substrate


106


are heated to allow solder to flow and contact wettable metal bonding pads


111


on Si substrate


101


.





FIG. 6a

shows integration of substrate


101


with MEMS substrate


130


using well-known procedures of adhesive bonding while

FIG. 6b

shows the finished assembly with raised deflecting mirror


240


locked into place with latch


168


.




Linear arrays of lasers can be bonded in a similar way; the extent of the array being perpendicular to the cross section shown in FIG.


6


a.




While the invention has been described in conjunction with specific embodiments, it is evident to those skilled in the art that many alternatives, modifications, and variations will be apparent in light of the foregoing description. Accordingly, the invention is intended to embrace all such alternatives, modifications, and variations that fall within the spirit and scope of the appended claims.



Claims
  • 1. An integrated laser beam scanning structure comprising:a first wafer having a first surface and a second surface, said wafer having a recess piercing said first surface and said second surface; a layer having a first region and a second region, said layer being attached to said first surface; a deflecting mirror fashioned from said first region of said layer; a torsional mirror fashioned from said second region of said layer; a second wafer having a first side; and a light source mounted on said first side of said second wafer, said first side of said second wafer being attached to said second surface of said first wafer such that said light source occupies said recess whereby a light beam emitted from said light source is deflected by said deflecting mirror onto said torsional mirror.
  • 2. The structure of claim 1 wherein said first wafer is a silicon on oxide wafer.
  • 3. The structure of claim 1 wherein said layer is a single crystal silicon layer.
  • 4. The structure of claim 1 wherein said light source is a semiconductor light emitter.
  • 5. The structure of claim 4 wherein said semiconductor light emitter is mounted on said first side of said second wafer using solder bumps.
  • 6. The structure of claim 4 wherein said semiconductor light emitter is a VCSEL chip.
  • 7. The structure of claim 1 wherein said recess is deep reactive ion etched.
  • 8. The structure of claim 1 wherein said torsional mirror is actuated by a pair of electrodes.
  • 9. The structure of claim 1 wherein said torsional mirror is actuated by a thin film coil.
  • 10. The structure of claim 1 wherein a ferromagnetic thin film coil is attached to said torsional mirror.
  • 11. The structure of claim 1 wherein a thin film coil is attached to said torsional mirror.
  • 12. A method for making an integrated laser beam scanner comprising the steps of:providing a first wafer having a first surface and a second surface, said wafer having a recess piercing said first surface and said second surface; attaching a layer having a first region and a second region to said first surface of said first wafer; fashioning a deflecting mirror from said first region of said layer; fashioning a torsional mirror from said second region of said layer; providing a second wafer having a first side, said second wafer having a light source mounted on said first side; and attaching said first side of said second wafer to said second surface of said first wafer such that said light source occupies said recess whereby a light beam emitted from said light source is deflected by said deflecting mirror onto said torsional mirror.
  • 13. The method of claim 12 wherein said layer is a single crystalline silicon layer.
  • 14. The method of claim 12 wherein said light source is a semiconductor light emitter.
  • 15. The method of claim 14 wherein said semiconductor light emitter is a VCSEL chip.
  • 16. The method of claim 14 wherein said semiconductor light emitter is mounted using solder bumps.
  • 17. The method of claim 12 wherein said torsional mirror is actuated by a pair of electrodes.
  • 18. The method of claim 12 wherein said torsional mirror is actuated by a thin film coil and an external magnetic field.
  • 19. The method of claim 12 wherein a ferromagnetic thin film coil is attached to said torsional mirror.
  • 20. The method of claim 12 wherein a thin film coil is attached to said torsional mirror.
  • 21. A MEMS formation method including:providing a single crystal silicon layer; forming at least one first MEMS component by patterning the single crystal silicon layer; depositing at least one layer of polysilicon on the patterned single crystal silicon; and forming at least one second MEMS component by patterning the polysilicon.
  • 22. The method of claim 21 wherein the single crystal silicon layer is bonded to an insulator layer in a SOI wafer and providing a single crystal silicon layer comprises providing a SOI wafer.
  • 23. The method of claim 21 wherein the at least one second MEMS component is a hinge.
  • 24. The method of claim 23 wherein the at least one first MEMS component is a mirror retained by the hinge.
  • 25. The method of claim 21 wherein depositing at least one layer of polysilicon includes chemical vapor deposition.
  • 26. The method of claim 21 wherein forming at least one first MEMS component includes forming a deflecting mirror.
  • 27. A MEMS formation method including:providing a single crystal silicon layer; forming at least one first MEMS component by patterning the single crystal silicon layer; depositing at least one layer of polysilicon on the patterned single crystal silicon; and forming at least one second MEMS component by patterning the polysilicon, the at least one second MEMS component including a hinge retaining a deflecting mirror.
  • 28. The method of claim 27 wherein forming at least one first MEMS component further includes forming a torsional mirror, and the method further comprises forming a recess in the single crystal silicon layer and directing a light beam through the recess at the deflecting mirror so that the deflecting mirror deflects light to the torsional mirror.
  • 29. A MEMS device comprising:at least one single crystal silicon component; and a hinge derived from a layer of polysilicon applied over the at least one single crystal silicon component.
  • 30. The MEMS device of claim 29 wherein the at least one single crystal silicon component is bonded to an insulator that rests on a handle wafer as a result of being formed from a single crystal silicon layer of a SOI wafer.
  • 31. The MEMS device of claim 29 wherein the at least one single crystal silicon component comprises a deflecting mirror.
  • 32. The MEMS device of claim 31 wherein the hinge retains the deflecting mirror.
  • 33. The MEMS device of claim 29 wherein the at least one single crystal silicon component comprises a torsional mirror.
  • 34. A MEMS device comprising:at least one single crystal silicon component; at least one polysilicon component derived from a layer of polysilicon applied over the at least one single crystalline silicon component; and a semiconductor light emitter mounted on a substrate bonded to a supporting structure of the at least one single crystal silicon component and oriented to emit a light beam at the at least one single crystal silicon component.
  • 35. The MEMS device of claim 34 wherein the at least one single crystal silicon component is bonded to an insulator as a result of having been formed from a single crystal silicon layer of an SOI wafer to which the semiconductor light emitter substrate is bonded.
  • 36. The MEMS device of claim 35 wherein the SOI wafer includes a recess into which the semiconductor light emitter projects.
  • 37. The MEMS device of claim 34 wherein the at least one single crystal silicon component comprises a deflecting mirror at which the light beam is directed and a torsional mirror to which the deflecting mirror deflects the light beam, and the at least one polysilicon component comprises a hinge retaining the deflecting mirror.
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Entry
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Divisions (1)
Number Date Country
Parent 09/203442 Dec 1998 US
Child 10/022917 US
Reissues (1)
Number Date Country
Parent 09/203442 Dec 1998 US
Child 10/022917 US