The present invention relates to devices providing high spatial resolution results arising from high voltage measurements of a surface.
Prior to making measurements of an STBA, the tip of the sensor must be moved close to the STBA. As the tip of the sensor moves closer to the STBA, measurement quality increases. However, in doing so, the sensor may be moved too close to the STBA such that arcing and/or contact occurs between the sensor and the STBA. Such arcing and/or contact may damage the STBA. A means that reduces the risk of arcing is needed so that the position of the sensor can be made near enough to the STBA that highly accurate measurement operations can be made.
The invention may be embodied as a method of positioning a sensor close to an STBA. Such a method may begin by providing an EFM and an STBA. The sensor tip of the EFM may be placed far enough from the STBA so that arcing and/or contact between the sensor and the STBA will not occur. With the sensor placed a distance (“D”) from the STBA, an AC bias voltage (“Vac”) may be applied to the sensor at an initial desired voltage (“Vd”). The sensor sensitivity (“G”) may be determined. G may be compared to a minimum sensor sensitivity Gmin. If G is less than Gmin, then Vac may be increased and G is again determined. If G is again less than Gmin, then the iterative process of increasing Vac and determining G is repeated until G is equal to or greater than Gmin.
If Gmin≦G<Gmax, then Vac may remain the same while the distance D is decreased. At the new D, G is determined, and if G is still less than Gmax, the iterative process of decreasing D and determining G is repeated until G is equal to or greater than Gmax.
If G÷Gmax, then Vac may be compared to a desired AC bias voltage Vd (which may be the same as the initial AC bias voltage) and if Vac is determined to be greater than Vd, Vac is decreased and G is again determined. If G is less than Gmax, then D is reduced, but if G is equal to or greater than Gmax, then Vac is again decreased. These steps are repeated (reducing D or reducing Vac) as needed to keep G close to (within a desired predetermined narrow range) Gmax until Vac is at or close to (within a desired predetermined narrow range) Vd. For example G may be considered close to Gmax if G is within 0.02×10−4 of Gmax, and Vac may be considered close to Vd if Vac is within 3 Volts of Vd. If G is approximately equal to (or close to) Gmax, and Vac is approximately equal to (or close to) Vd, then surface measurement operations with respect to the STBA using the sensor are begun.
The sensor sensitivity G may be determined by:
For a fuller understanding of the nature and objects of the invention, reference should be made to the accompanying drawings and the subsequent description. Briefly, the drawings are:
G with respect to the distance D;
We have invented a methodology for placing a sensor adjacent to an STBA, so that the sensor in a high spatial resolution/high voltage measurement apparatus can be used to accomplish voltage measurement, while simultaneously reducing the risk of arcing and/or contact between the STBA and the sensor. Generally speaking, we utilize two techniques: they are 1) providing an AC bias voltage to the sensor to nullify an electric field between the sensor and the STBA while the sensor approaches the STBA, and 2) adjusting the AC bias voltage to control the motion of the cantilevered sensor to be relatively constant even though the sensor is far from the STBA. Using these techniques, the sensor may be able to successfully approach a 500 Volt STBA without causing arcing and/or contact. In one embodiment of the invention, both the DC bias voltage system and the AC bias voltage system of the EFM may be used to position a sensor that starts at a distance that is large (for example, 1,000 μm) to bring the sensor to about 5 μm by adjusting the AC bias voltage to the sensor from a high AC bias voltage (for example, 200 Vp-p) to a lower AC bias voltage (for example, 12 Vp-p).
An EFM is highly susceptible to causing damage as a result of contact between the STBA and the sensor. The present invention may be used to bring the sensor of an EFM close to an STBA without the sensor contacting the STBA. Doing so may utilize both the DC and AC bias voltage systems of the EFM for (a) nullifying the electric field between the sensor and the STBA, and also (b) keeping the motion of the cantilevered sensor vibration nearly constant regardless of the position of the sensor relative to the STBA.
Basic Principles Of An EFM. In an EFM, the sensor is set on a cantilever of which motion is detected via an optical system.
We can measure Fω by applying a known preset DC bias voltage VDC to the sensor so that we can simply calculate the voltage on the STBA (pd0/ε) with the aforementioned equation #1. With this foundation in mind, a method of the invention will now be explained more fully.
Using an EFM having a comb-shaped electrode, the voltage distribution on an STBA was analyzed and the results are plotted in
We were able to measure voltages Vω up to +/−1 kV using the comb-shaped electrodes without arcing by utilizing this measurement method with a sensor located at a distance D=5 μm from the STBA. However, we realized that if the sensor was located far away from the STBA, we were not able to obtain adequate vibration of the cantilever since the sensor was too far from the STBA. In order to minimize the risk of arcing and/or contact between the STBA and the sensor by initially setting the sensor far from the STBA, a new method was needed. The method disclosed herein uses the sensor sensitivity G in conjunction with the distance D between the sensor and the STBA, and to accomplish this method, a minimum sensor sensitivity Gmin is used along with a sufficiently strong AC bias voltage signal Vac in order to guarantee adequate and accurate measurement. Even when the distance D is large, the minimum sensor sensitivity Gmin is attainable by increasing the AC bias voltage VAC. Consequently, this method performs well even though the sensor is located far away from the STBA.
EFMs typically are employed to analyze an STBA by placing the sensor close to the STBA, and often the distance D is on the order of about 5 μm. At this distance, the signal to noise ratio (“S/N Ratio”) for the system is sufficiently high to produce accurate results. But, if the distance D is large, such that the sensor is far away from the STBA, the S/N Ratio decreases accordingly and it becomes difficult to know much about the STBA, in part because the sensor is not very sensitive to the STBA conditions at such distances. Thus, we define a variable G that is an indication of the sensor sensitivity that we find useful in moving the sensor toward the STBA while minimizing the risk of arcing. We define the sensor sensitivity G with the following equation:
where VDC is the DC bias voltage applied to the sensor and Vω(VDC) is the signal obtained while applying VDC. For example, under a typical measurement condition (D=5 μm), G is in the range of 0.2×10−4 to 0.4×10−4, and G may vary depending on characteristics of each cantilevered sensor. For one such cantilevered sensor corresponding to
For a particular EFM, the dependency of G on D while D changes from 1 to 30 μm is shown in
Having provided some details about the invention, we now move to describe the invention in more detail with the goal of clarifying the invention more fully.
A resonance frequency in the form of an AC bias voltage Vac is applied to the sensor at a desired initial voltage. The desired initial AC bias voltage provided to the STBA may be selected so that the a detectable vibration on the cantilever is achieved. The initial AC bias voltage may be selected based on experience with the particular EFM and STBA being used. For example, the initial AC bias voltage may be 12 Volts peak-to-peak. With the distance D held to the initial value and the initial AC bias voltage applied to the sensor, the sensor sensitivity G of the sensor is determined. If the sensor sensitivity G is less than or equal to a minimum sensor sensitivity Gmin, the AC bias voltage is increased by an amount, and the sensor sensitivity G is again determined. The minimum sensor sensitivity Gmin may be 0.1×10−4.
If the sensor sensitivity G is still less than the minimum sensor sensitivity Gmin, the AC bias voltage is increased again, and this process is repeated until the sensor sensitivity G is equal to or greater than the minimum sensor sensitivity Gmin. When the AC bias voltage is increased as part of an effort to make the sensor sensitivity G greater than the minimum sensor sensitivity Gmin, the AC bias voltage may be increased by (for example) 5 Volts before the sensor sensitivity G is again determined and checked against Gmin.
Once the sensor sensitivity G is equal to or greater than the minimum sensor sensitivity Gmin, a comparison of the sensor sensitivity G is made to a maximum sensor sensitivity Gmax. Gmax may be selected to prevent arcing and/or contact between the sensor tip and the STBA. Also, Gmax may be selected to prevent damage to the cantilever and/or sensor caused by the vibration forces induced by the AC bias voltage signal. Typically, Gmax will be 2 to 100 times greater than Gmin. If the sensor sensitivity G is less than the maximum sensor sensitivity Gmax, then the distance D is decreased, and the sensor sensitivity G is again determined.
If the sensor sensitivity G is still greater than Gmin and less than Gmax, the distance D is decreased again, and this process is repeated until the sensor sensitivity G is equal to or greater than the maximum sensitivity Gmax. The change in the distance D may be (for example) 50 μm when G is greater than Gmin but less than Gmax. However, as G approaches Gmax, the incremental change in D may be reduced toward 1 μm.
Then, with the sensor sensitivity at or above Gmax, the AC bias voltage is compared to a desired AC bias voltage Vac, which may be the initial desired AC bias voltage Vd. If the AC bias voltage Vac is greater than the desired AC bias voltage, the AC bias voltage is decreased and the sensor sensitivity G is determined. If the sensor sensitivity G is at or above Gmax, then the AC bias voltage is again reduced, but if the sensor sensitivity is less than Gmax, then the distance D is decreased. When G is close to (within a desired predetermined narrow range) or above Gmax, the increments of Vac may be 5 Volts or less and the increments of D may be about 1 μm. Following either a reduction in AC bias voltage or a decrease in distance D, the sensor sensitivity is determined and this process continues until the sensor sensitivity G is equal to (or approximately equal to) Gmax and the AC bias voltage is equal to (or approximately equal to) the desired AC bias voltage Vd.
Once the sensor sensitivity equals (or is approximately equal to) Gmax and the AC bias voltage equals (or is approximately equal to) the desired AC bias voltage Vd, the sensor may be used to make measurements of the STBA. For example, the sensor may be caused to reside over different areas of the STBA, and the charge detected by the sensor may be recorded for each area of the STBA that is of interest. The measured charge for each area may be used to determine information about the STBA, such as the surface voltage distribution of the STBA.
The sensor sensitivity G may be determined by setting the DC bias voltage to the sensor at a desired voltage (“Vp”) that is greater than 0 Volts. For example, Vn may be +3 Volts. Using the sensor, the voltage Vω is detected and recorded as V1. Then the DC bias voltage to the sensor is set at a desired voltage (“Vn”) that is less than 0 Volts. For example, Vp may be −3 Volts. Using the sensor, the voltage is detected and recorded as V2. The order in which V1 and V2 are determined may be reversed—that is to say that V2 may be determined after V1. Having determined V1 and V2 at DC bias voltages Vp and Vn respectively, the sensor sensitivity may be determined using the following equation:
G=(V1−V2)—(Vp−Vn)
It will now be realized that the chance of arcing and/or contact between the sensor tip and the STBA is reduced during the positioning of the EFM sensor tip near the STBA by a method and device that:
Once the sensor tip is placed near the STBA such that the AC bias voltage Vac is at a desired level Vd and the sensor sensitivity G is close to (within a desired predetermined narrow range) Gmax, measurement operations by the EFM are then undertaken with respect to the STBA.
Ideally, there is a location of the sensor that will allow both (i) Vac to be equal to the desired AC bias voltage Vd, and (ii) G to be equal to Gmax. However, there may be a situation in which the ability of the EFM to increment D and the ability to increment Vac are not precise enough to achieve both Vd and Gmax. In that situation, that position of the sensor which achieves either Vd or Gmax may be selected, and the other variable may be allowed to be close to (within a desired predetermined narrow range) but not exactly at the desired value. For example, the distance D may be selected such that Vac is at the desired voltage Vd, even though G is not at Gmax. Or, the distance D may be selected such that G is at Gmax, even though Vac is not at the desired voltage Vd.
It should be noted that a computer may be used to store information needed to calculate G, and ultimately to calculate G. Also, the computer may be used to store information needed to execute the processes described herein. For example, the computer may be used to store information such as Gmin, Gmax, V1, V2, Vd, various Vω readings, Vp and Vn. The computer may be programmed to execute a method according to the invention, and to that end the program may provide instructions to the computer to make comparisons and provide instructions to the EFM that result in the adjusting of Vac and/or D accordingly. The computer may, or may not, be packaged with (or part of) the EFM.
As such, the computer may be programmed to carry out the following method:
The computer may be part of a system for positioning a cantilevered sensor of an EFM relative to a surface. Such a system may have an EFM having (i) a cantilever, (ii) a sensor, (iii) a DC bias voltage generator, (iv) an AC bias voltage generator, and (v) a computer programmed to accept information from the sensor, and to provide control signals to the EFM.
The computer may be programmed to determine the sensor sensitivity G by:
U.S. provisional patent application No. 61/593,837 filed on Feb. 1, 2012, discloses additional details about the invention. The disclosure of that patent application is incorporated herein by this reference. To the extent that incorporation by reference is not permitted, Exhibit A hereto is made part of this patent application.
Although the present invention has been described with respect to one or more particular embodiments, it will be understood that other embodiments of the present invention may be made without departing from the spirit and scope of the present invention. Hence, the present invention is deemed limited only by the appended claims and the reasonable interpretation thereof.
This application claims the benefit of priority to U.S. provisional patent application Ser. No. 61/542,648, filed on Oct. 3, 2011, and to U.S. provisional patent application Ser. No. 61/593,837 filed on Feb. 1, 2012.
Number | Date | Country | |
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61542648 | Oct 2011 | US | |
61593837 | Feb 2012 | US |