The present invention relates to a method for manufacturing a device for dispensing a product.
The field of the invention is more particularly that of the dispensation of products such as liquids, gels or creams, for example for the pharmaceutical or cosmetic or agri-food industry.
Devices are known for dispensing products such as, for example, that described in patent FR 3,005,459 A1. Such a device comprises:
This device, although it is good, can still be improved because it still poses some technical problems.
A first problem is that of priming, that is to say when the chamber is filled with air when the device is new, and a user is pressing on the chamber so as to pump the product from the reservoir trying to fill the chamber.
This problem is particularly real:
Thus for priming, by pressing the chamber, air can pass through the feed valve rather than through the dispensing valve. It is then difficult to raise the product from the reservoir into the chamber.
The object of the present invention is to provide a method of manufacturing a product dispensing device to solve this problem.
This object is achieved with a method of manufacturing a device for dispensing a product, comprising:
According to different embodiments:
The inside of the deformable chamber may:
The method according to the invention may further comprise, after the closing step, a priming step during which product is fed from the reservoir to the inside of the deformable chamber.
The priming step may be implemented:
The priming step may include increasing the pressure around the reservoir to the reference pressure.
The priming step may start while the inside of the deformable chamber is at a priming pressure lower than the reference pressure.
The outlet may be plugged during the priming step
During the evacuation step:
The evacuation step may create the depression in the reservoir, around the reservoir, in the deformable chamber, the deformable chamber to the outlet of the device, and/or the deformable chamber to the reservoir.
The outlet may not be plugged during the evacuation step.
Reservoir walls may be maintained apart during the evacuation step and/or during the filling step. Maintaining apart the walls of the reservoir during evacuation and/or maintaining apart the walls of the reservoir during the filling step may comprise:
In the intermediate state, the reservoir may be filled with product while, around the reservoir, from the deformable chamber to the outlet of the device, and/or from the deformable chamber to the reservoir, the pressure may be at the intermediate pressure and/or less than the reference pressure.
The outlet may be plugged during the filling step.
The closing step may be implemented while the device is in its intermediate state.
The outlet may be plugged during the closing step.
The evacuation step may precede the filling step.
The steps of evacuation, filling and closure may be performed within the same evacuation enclosure.
The steps of:
The leakage rate through the movable wall may be zero and/or the leakage rate through the dispensing valve may be zero.
According to another aspect of the invention, there is provided a system for manufacturing a device for dispensing a product, comprising:
According to different embodiments:
The inside of the deformable chamber may:
The system according to the invention may comprise priming means arranged to bring product from the reservoir to the inside of the deformable chamber.
The priming means may be arranged to bring this product:
The priming means may be arranged to bring this product by increasing the pressure around the reservoir to the reference pressure.
The priming means may be arranged to start priming while the inside of the deformable chamber is at a priming pressure lower than the reference pressure.
The priming means may be arranged to implement priming (i.e. bring this product) while the outlet is plugged.
The evacuation means may be arranged to create depression while:
The evacuation means may be arranged to create the depression in the reservoir, around the reservoir, in the deformable chamber, the deformable chamber to the outlet of the device, and/or the deformable chamber to the reservoir.
The evacuation means may be arranged so that the outlet is not plugged during the creation of the depression by the evacuation means.
The system according to the invention may comprise means for keeping apart the walls of the reservoir during the creation of the depression by the evacuation means and/or during filling by the filling means, for example:
In the intermediate state, the reservoir may be filled with product wherein around the reservoir, from the deformable chamber to the outlet of the device, and/or from the deformable chamber to the reservoir, the pressure may be at the intermediate pressure and or less than the reference pressure.
The filling means may be arranged so that the outlet is plugged during filling by the filling means.
The closure means may be arranged to seal or close the filling opening while the device is in its intermediate state.
The closure means may be arranged to seal or close the filling opening while the outlet is plugged.
The evacuation means and the filling means may be arranged so that the creation of depression by the evacuation means precedes the filling by the filling means.
The means of evacuation, filling and closure may be grouped within one evacuation enclosure.
Means of:
Other advantages and particularities of the invention will appear on reading the detailed description of implementations and non-limiting embodiments, and the following appended drawings:
As these embodiments are in no way limitative, it is possible in particular to consider variants of the invention comprising only a selection of characteristics described or illustrated below in isolation from the other characteristics described or illustrated (even if this selection is isolated within a sentence comprising these other characteristics), if this selection of characteristics is sufficient to confer a technical advantage or to differentiate the invention with respect to the state of the art; This selection comprises at least one preferably functional characteristic without structural details, and/or with only a part of the structural details if this part alone is sufficient to confer a technical advantage or to differentiate the invention with respect to the state of the art.
Firstly, with reference to
The various technical means described for implementing this method constitute the manufacturing system 10 according to the invention.
The initial step of this method illustrated in
The head 2 comprises a rigid frame (for example polypropylene (PP)), on which is fixed a wall 13 movable and/or deformable (for example polypropylene (PP) with a thickness much thinner than the frame) more flexible than the framework.
The head 2 comprises a deformable chamber 45.
The reservoir 3 is formed by a flexible bag, typically a multilayer polyethylene terephthalate (PET)/aluminum/cast polypropylene (PP) film, the PET layer being towards the outside of the reservoir 3.
The reservoir 3 is provided with:
During this initial step of supply, the interior of the chamber 45 is at a reference pressure.
The filling opening 8 is a direct communication between the inside of the reservoir 3 and the outside of the device 1.
The inside of the deformable chamber 45 is delimited at least in part by the wall 13, a displacement of which causes a variation of the volume of the deformable chamber 45.
During this initial step, the device 1 is “empty”.
During this initial step, the reservoir 3 does not include the product 16, and is preferably filled with only gas, preferably air and/or a neutral gas such as nitrogen.
During this initial step, the device 1 does not include the product 16, and is preferably filled with only gas, preferably air and/or a neutral gas such as nitrogen.
During this initial step, the device 1 is in an initial state called “unsealed” because the filling opening 8 exists and is not yet sealed.
The chamber 45 is separated from the reservoir 3 at least by the feed valve 4.
The feed valve 4 is flexible, typically thermoplastic elastomer (TPE) or a thermoplastic polyurethane elastomer of 80 Shore A.
The chamber 45 is arranged so that a decrease in the volume of the chamber 45 (for example by pressing on the wall 13) closes the feed valve 4, at least when the chamber 45 is filled (preferably completely) with the product 16 (which is not yet the case in this initial step).
The chamber 45 is arranged so that an increase in the volume of the chamber 45 (for example by releasing the wall 13) opens the feed valve 4, at least when the chamber 45 is filled (preferably completely) with the product 16 (which is not yet the case in this initial step).
The chamber 45 is separated from an outlet 6 of the device 1 at least by a dispensing valve 5.
The dispensing valve 5 is flexible, typically thermoplastic elastomer (TPE) or a thermoplastic polyurethane elastomer of 80 Shore A.
The chamber 45 is arranged so that a decrease in the volume of the chamber 45 (for example by pressing on the wall 13) opens the dispensing valve 5, at least when the chamber 45 is filled (preferably completely) by the product 16 (which is not yet the case in this initial step).
The chamber 45 is arranged so that an increase in the volume of the chamber 45 (e.g., by releasing the wall 13) closes the dispensing valve 5, at least when the chamber 45 is filled (preferably completely) by the product 16 (which is not yet the case in this initial step).
When open, the feed valve 4 allows a product passage, typically from the reservoir 3 to the chamber 45. When closed, the feed valve 4 does not allow such a product passage.
When opened, the dispensing valve 5 allows passage of product, typically from the chamber 45 to the outlet 6. When closed, the dispensing valve 5 does not allow such a product passage.
A feed orifice connects the chamber 45 to the feed conduit.
The feed valve 4 comprises a membrane which, in the closed state of this feed valve 4, is pressed against the feed orifice so as to close this feed orifice, and in the open state of this feed valve 4, deviates from the feed orifice so as to open this feed orifice; the feed valve 4 is an independent part of the head 2, and is housed (at least its membrane) on the side of the chamber 45.
The feed valve 4 (movable between its closed and open positions) is, in its closed state, kept pressed against a stationary part (called the feeding seat, which at least partially surrounds the periphery of the associated feed orifice), which is also a “rigid” (i.e. no flexible material) part, of an inner wall of the chamber 45. More precisely, the feed valve 4 comprises a membrane which, in the closed state of the feed valve 4, is kept pressed against the feeding seat, and away from this feeding seat in its open state.
The wall 13 is not mechanically connected to the feed valve 4. The feed valve 4 is a single wall that covers the feeding seat, the feed valve 4 does not fit into the feed channel.
The feeding seat is located inside the chamber 45.
A dispensing orifice connects the chamber 45 to the dispensing conduit.
The dispensing valve 5 is an independent part of the head 2 and is housed (entirely) inside the dispensing conduit.
The dispensing valve 5 comprises a membrane which, in the closed state of this dispensing valve 5, is pressed against the dispensing orifice so as to plug this dispensing orifice, and in the open state of this dispensing valve 5, deviates from the dispensing orifice so as to open this dispensing orifice.
The dispensing orifice is located on a side wall of the dispensing conduit, so that the dispensing orifice, the dispensing conduit and the dispensing valve 5 are arranged so that the product travels globally (i.e. to say on a larger scale than the vortices of the microparticles of the product 16) at a right angle or substantially a right angle, passing from the chamber 45 to the dispensing conduit, that is to say, between the direction of propagation of the product at the inlet of the dispensing valve 5 and the direction of propagation of the product at the outlet of the dispensing valve 5.
The dispensing valve 5 (movable between its closed and open positions) is, in its closed state, kept pressed (sufficiently firmly, by means of return means or a return spring of the valve 5 for example as described in the patent WO2015/155318) against an immobile part (called dispensing seat, which surrounds at least partially the periphery of the associated dispensing orifice), which is also a “rigid” (i.e. not flexible material) part, of an inner wall of the dispensing conduit. More precisely, the dispensing valve 5 comprises a diaphragm which, in the closed state of the dispensing valve, is kept pressed against the dispensing seat, and away from this seat in its open state. It is further noted that the dispensing seat is a lateral part of the dispensing conduit, that is to say that this seat is limited to a face, preferably plane, of an internal wall of the dispensing conduit and is not all around a section of the dispensing conduit that would be made in a plane perpendicular to the direction of elongation of the dispensing conduit.
The dispensing seat is located outside the chamber 45.
The feed orifice is located on a side wall of the feed conduit, so that the feed orifice, the feed conduit and the feed valve 4 are arranged so that the product travels globally at a right angle or substantially a right angle, passing from the feed conduit to the chamber 45, that is to say, between the direction of propagation of the product at the inlet of the feed valve 4 and the direction of propagation of the product at the outlet of the feed valve 4.
The feed valve 4 and the distribution valve 5 are connected by a connecting element, this feed valve 4, this dispensing valve 5 and the connecting element being integral and in one piece (manufactured for example a thermoplastic elastomer (TPE) or a thermoplastic polyurethane elastomer). This unique piece is monoblock. The junction element typically has a hardness of 70-80 Shore A. A hole creates a passage between the dispensing conduit and the feed conduit without passing through the chamber 45. The junction element plugs this hole and is maintained by tightening in this hole.
Then, with reference to
This reference pressure is equal to the atmospheric pressure, i.e. equal to 1 bar. This depression corresponds to a pressure difference of at least 0.2 or even 0.3 bar relative to the reference pressure, preferably at least 0.5 bar relative to the reference pressure, preferably from at least 0.7 bar relative to the reference pressure.
It will be noted that, in the present description, any reference to pressure or depression refers to a gas, the composition of which may possibly change during the method according to the invention.
During the evacuation step, the wall 13 is moved so as to increase the volume of the chamber 45 and/or the wall 13 is displaced so as to reduce the volume of the chamber, for example by means of a vibrating jack 25, preferably in at least one (or more) round trip(s), each round trip comprising a displacement of the wall 13 so as to increase the volume of the chamber 45 and a displacement of the wall 13 so as to reduce the volume of the chamber 45.
This opens the valve 4 and the valve 5 and thus ensures the proper realization of the depression or vacuum (which is a partial vacuum) inside the chamber 45 despite the existence of valves 4 and/or 5.
The action of the jack 25 is a useful aid, but is not mandatory especially in the case of a valve 4 and/or a valve 5 very flexible or not very tight with a possible space between the valve 4 or 5 and its seat.
During the evacuation step, the device 1 is in an enclosure 18 in which the evacuation is produced by suction carried by suction means 26 (such as a pump).
The evacuation step creates the depression:
The outlet 6 is not plugged during the evacuation step. This can help to get the air out also through the outlet 6.
The walls 31, 32 of the reservoir 3 are kept apart from each other during the evacuation step.
Maintaining the space between the walls 31, 32 of the reservoir 3 during the evacuation comprises maintaining the space between the walls 31, 32 of the reservoir 3 by a filling nozzle 11 inserted in the reservoir 3 through the filling opening 8.
Then, with reference to
Product 16 is a liquid, a cream, a paste, a gel or a mixture thereof.
The walls 31, 32 of the reservoir 3 are kept apart between them during the filling step.
Maintaining, spaced apart, the walls 31, 32 of the reservoir during the filling step comprises:
Each spacer 12 is a suction cup.
In the first embodiment of the method according to the invention illustrated, the evacuation step precedes the filling step. This allows:
The order of the evacuation and filling steps may be reversed.
The steps of evacuation and filling are combined or succeeded so as to obtain a so-called “intermediate” state of the device 1 in which:
This intermediate pressure is equal to the pressure obtained by the evacuation created during the evacuation step.
This intermediate pressure is less than 0.7 bar, preferably less than 0.5 bar, preferably less than 0.3 bar or even 0.2 bar.
The intermediate pressure is at least 0.2 or even 0.3 bar lower than the reference pressure, preferably at least 0.5 bar with respect to the reference pressure, preferably at least 0.7 bar relative to the reference pressure.
In the intermediate state corresponding to the end of the step illustrated in
Then, with reference to
The closing step is implemented while the device 1 is in its intermediate state.
Closing is performed for example by means of a pliers 9 of ultrasonic welding or hot welding.
The outlet 6 is plugged during the closing step.
There is a means (not shown) arranged to bring the edges of the bag (i.e. the edges of the walls 31, 32 delimiting the opening 8) closer together before welding or closing the opening 8, and implements a step of bringing closer together the edges of the bag (i.e. edges of the walls 31, 32 delimiting the opening 8) before welding or closing the opening 8.
Next, with reference to
The priming step starts while the inside of the deformable chamber 45 is at a priming pressure (equal to the intermediate pressure) lower than the reference pressure, which greatly helps this priming.
This priming pressure is less than 0.7 bar, preferably less than 0.5 bar, preferably less than 0.3 bar or even 0.2 bar.
The priming pressure is respectively at least 0.2 or even 0.3 bar lower than the reference pressure, preferably at least 0.5 bar with respect to the reference pressure, preferably at least 0.7 bar with relative to the reference pressure.
The priming step is implemented:
Outlet 6 is plugged during the priming step. This prevents the entry of air or gas into the device 1 through the outlet 6 when opening the enclosure.
After priming, the device 1 is then in its “final” state, ready to be used by a user.
In the first embodiment of the method according to the invention, the steps of evacuation, filling, closing and priming are performed within the same enclosure 18 for evacuation.
In this first embodiment:
In the first embodiment of the method according to the invention, when the outlet 6 is plugged, it is typically plugged by a plug 19 (for example rubber or polymer) which is pressed against the outlet 6. However, in variants:
Note that, in the first embodiment of the method according to the invention, the opening 8 is always located higher than the orifice 7 (the height increases with distance from the earth parallel to the earth's gravity field, or increases in the direction opposite to the direction in which the product 16 flows from the nozzle 11 to the reservoir 3 during the filling step)
A second embodiment of the method according to the invention for manufacturing a product dispensing device 1 will now be described with reference to
This second embodiment will only be described for its differences with respect to the first method embodiment of the invention, and all the numerical references already described above will therefore not necessarily be described again.
In this second embodiment, the reservoir 3 is not formed by a flexible bag but by a tube.
In this second embodiment, the outlet 6 is plugged during the evacuation step, the method being compatible with the manufacture of a device 1 carrying a plug 22. It is also plugged during the filling step, the closing step and the priming step.
In this second embodiment, when the outlet 6 is plugged, it is plugged by a removable plug 22, preferably connected to the head 2 by a hinge 23.
The hinge 23 and the plug 22 are ideally in the same material as the frame of the head 2.
In this second embodiment, the walls 31, 32 do not need to be kept apart.
The filling step by the nozzle 11 is not illustrated.
We will now describe, with reference to
The evacuation step is carried out in a first enclosure 181, so as not to trap an air bubble between the product 16 and the reservoir 3 and to create the depression in the chamber 45, particularly if the product 16 is viscous.
The filling step is then performed in the first enclosures 181.
The device 1 is then transported from the first enclosures 181 to a second enclosures 182 with the outlet 6 plugged by the means 19, 20 or 21, so as to be able to maintain the depression in the chamber 45.
Then, the “evacuation” is made at the priming pressure around the reservoir 3 in the second enclosures 182 in anticipation of priming.
The step of closing the reservoir 3 is then performed by welding in the second enclosures 182.
A first part of the priming step (by increasing the pressure) is then performed during the opening of the enclosures 182 and the gas inlet 17 in the volume 15.
A second part of the priming step is performed outside the enclosures 181, 182 by the mechanical means 14 crushing the reservoir 3.
The separation of the steps of the method according to the invention in different “stations” or different enclosures allows to increase the production rate.
We will now describe, with reference to
This third embodiment will only be described for its differences with respect to the first embodiment of the method according to the invention, and all the numerical references already described above will not necessarily be described again.
In this third embodiment:
This third embodiment is implemented on a continuous vertical filling machine.
The reservoir 3 is formed by two flexible films which are assembled.
Each of these two films is for example a multilayer polyethylene terephthalate (PET)/aluminum/polypropylene (PP) film.
These two assembled flexible films form several devices 1 connected in series and which move in a direction 24 from one station to another of the filling machine.
The initial step of supplying a device 1 is implemented by assembling these two films between which is inserted the head 2 of this device 1, as illustrated in the part 101 at the top of
Then the device 1 moves in the direction 24 and takes place the step of filling the reservoir 3 of the device 1 by the nozzle 11 with the product 16, as shown in the part 102 at the middle of
Then the device 1 moves in direction 24 and takes place:
Of course, the invention is not limited to the examples which have just been described and many adjustments can be made to these examples without departing from the scope of the invention.
Note that in the embodiments described the filling step precedes the closing step.
Note that in the embodiments described the closing step precedes the priming step.
Note that in the embodiments described the evacuation step precedes the priming step.
Note that, in the embodiments described, the evacuation step may take place:
In addition, in the embodiments described, the priming step is not mandatory and this priming can be performed later manually by a user, although this is much less advantageous (in case of leakage, the inside of the chamber 45 can gradually return to atmospheric pressure).
In addition, in a variant of the embodiments described, maintaining the space between the wads 31, 32 of the reservoir 3:
In addition, in a variant of the embodiments described, the priming step may be implemented:
Furthermore, in a variant of the described embodiments, the deformable mobile wall 13 may be replaced by a movable wall such as a rigid piston connected to an actuating button arranged to move the piston so as to vary the volume of the chamber 45.
In addition, in a variant of the embodiments described, the priming may comprise (preferably at the end of the cycle after the various other steps previously described of the priming) the exertion of a force on the chamber 45, typically on the wall 13. This may for example allow a little more product 16 to enter the chamber 45 to ensure that the device 1 does not become useless later.
A fourth embodiment of the method according to the invention for manufacturing a product dispensing device 1 will now be described with reference to
This fourth embodiment will only be described for its differences with respect to the first method embodiment of the invention, and all the numerical references already described above will therefore not necessarily be described again.
With reference to
The evacuation step creates the depression:
Next, with reference to
After this assembly, the previous steps of evacuation and filling are combined or succeeded so as to obtain a so-called “intermediate” state of the device 1 in which:
Then, with reference to
The amount of product that rises depends on the airtightness of the chamber 45 and the level of depression in the chamber 45.
The priming step starts while the inside of the deformable chamber 45 is at the starting pressure (equal to the intermediate pressure) lower than the reference pressure, which greatly helps this priming.
The reservoir 3 is delimited at least in part by a movable wall 46 in contact with the space 15.
The priming step is carried out by increasing the gas pressure in the space around the reservoir 3 from the priming pressure and at least up to the reference pressure (up to reference pressure or above the reference pressure); this increase is implemented by opening the enclosures 18 in which the device 1 is located so as to introduce gas 17 (for example air) into the space 15 around the reservoir 3.
This increase causes aspiration by the chamber 45 and a thrust of the wall 46 so as to reduce the volume of the reservoir 3. This facilitates the priming.
This has the advantage of being very simple and very quick to implement.
The dispensing valve 5 is more firmly sealed than the feed valve 4.
For the same depression (typically at least 0.2 or even 0.3 bar or at least 0.5 bar or at least 0.7 bar or between 0.7 and 0.95 bar, corresponding to the depression in the chamber created during the evacuation step or corresponding to the difference between the reference pressure and the “intermediate pressure” or the difference between the reference pressure and the “priming pressure”):
For the same depression (typically at least 0.2 or even 0.3 bar or at least 0.5 bar or at least 0.7 bar or between 0.7 and 0.95 bar, corresponding to the depression in the chamber created during the evacuation step or corresponding to the difference between the reference pressure and the “intermediate pressure” or the difference between the reference pressure and the “priming pressure”):
The leakage rate of the feed valve 4 is greater than 1 cm3/minute (typically for air at 20° C. and the depression in the chamber 45 corresponding to the priming pressure, i.e. say at the start of the priming step).
The leak rate (typically for air at 20° C.) through the wall 13 is zero or almost zero.
The leak rate (typically for air at 20° C.) through the valve 5 is zero or almost zero.
These zero or almost zero leakage rates of the wall 13 and/or of the valve 5 are measured with a pressure difference (in the chamber 45 and the reservoir 3 with respect to the outlet 6 or the space 15) of 0.9 bar for 1 hour having removed the feed valve 4 for measurements, the sum of the chamber 45 and the reservoir 3 having a total volume of one liter.
The outlet 6 is preferably plugged during the priming step, to prevent any air entering through the outlet 6 to the chamber 45.
It is further noted that the chamber 45 is completely sealed, apart from the valves 4 and/or 5 which can open. In other words, the chamber 45 (apart from the valve 4 and/or 5):
Each junction is for example maintained by clamping (for example between two clamping rings respectively 50 and 51 or 150 and 151) or by welding (for example by ultrasonic welding or overmoulding or bi-injection).
In the present case, there are only two junctions:
This makes it possible to prevent the entry of air or gas into the device 1 via the outlet 6 during the opening of the enclosures 18, and makes it possible to keep the vacuum in the chamber 45 until it is primed.
The final state is shown in
We will now describe, with reference to
In these variants, the enclosure (typically 18) in which the evacuation is carried out is provided with a vibrating support 49 on which the device(s) 1 rest(s).
During the evacuation step, the dispensing valve 5 is opened. Typically, during the evacuation step:
During the priming step, or opens the feed valve 4. For example:
In these variants, the enclosure (typically 18), in which the evacuation is made, is located along a conveyor and bordered by two removable doors 47 and 48.
If the dispensers 80 according to the invention have the head 2 down in the enclosure (the dispensing valve 5 to the ground) as shown in
With reference to
Of course, the various features, shapes, variants and embodiments of the invention can be associated with each other in various combinations to the extent that they are not incompatible or exclusive of each other. In particular all the variants and embodiments described above are combinable with each other.
Note that in all the embodiments of
This facilitates the creation of depression in the pocket 45.
The case of
Note that in all the embodiments of
This prevents air from entering the chamber 45 through the outlet 6 during priming.
The case of
It will be noted that, in all the embodiments of
This facilitates priming.
Number | Date | Country | Kind |
---|---|---|---|
1750598 | Jan 2017 | FR | national |
1800015 | Jan 2018 | FR | national |
Filing Document | Filing Date | Country | Kind |
---|---|---|---|
PCT/EP2018/051898 | 1/25/2018 | WO | 00 |
Publishing Document | Publishing Date | Country | Kind |
---|---|---|---|
WO2018/138230 | 8/2/2018 | WO | A |
Number | Name | Date | Kind |
---|---|---|---|
5144788 | Varlet | Sep 1992 | A |
5237797 | Varlet | Aug 1993 | A |
20010040175 | Bailly | Nov 2001 | A1 |
20170021375 | Boulais | Jan 2017 | A1 |
Number | Date | Country |
---|---|---|
0349396 | Jan 1990 | EP |
0509179 | Oct 1992 | EP |
0928635 | Jul 1999 | EP |
3005459 | Nov 2014 | FR |
2015155318 | Oct 2015 | WO |
Entry |
---|
International Search Report for corresponding Application No. PCT/EP2018/051898, dated Mar. 26, 2018. |
Written Opinion for corresponding Application No. PCT/EP2018/051898, dated Mar. 26, 2018. |
Number | Date | Country | |
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20190389606 A1 | Dec 2019 | US |