Claims
- 1. A method for producing a crystalline inorganic builder having the following composition in its anhydrous form:
- xM.sub.2 O.ySiO.sub.2.zMeO,
- wherein x, y and z are numerical values satisfying the following relationships: y/x is 1.0 to 4.0, z/y is not more than 1.0, M stands for Na and K, K/Na is 0.01 to 2.0, and Me stands for Ca and/or Mg, the method comprising the steps of:
- (a) adding water, a Na-containing compound, a K-containing compound, and at least one member of Ca-containing compounds and Mg-containing compounds to silica sand, to give a mixture;
- (b) subjecting the resulting mixture to a hydrothermal treatment, wherein said hydrothermal treatment is carried out under the condition of from 5 to 15 kg/cm.sup.2 G, thereby dissolving the silica sand in the mixture; and thereafter
- (c) baking the resulting treated mixture.
- 2. The method according to claim 1, wherein the Na-containing compound and the K-containing compound are selected from the group consisting of NaOH, KOH, Na.sub.2 CO.sub.3, K.sub.2 CO.sub.3, NaNO.sub.3, KNO.sub.3, Na.sub.2 SO.sub.4, and K.sub.2 SO.sub.4.
- 3. The method according to claim 1, wherein the Na-containing compound and the K-containing compound are each supplied as an aqueous solution of the Na-containing compound and an aqueous solution of the K-containing compound, and wherein a concentration of each of the aqueous solution of an Na-containing compound and the aqueous solution of a K-containing compound is from 20 to 70% by weight.
- 4. The method according to claim 1, wherein the mixture obtained in step (a) has a water content of from 24 to 50% by weight.
- 5. A method for producing a crystalline inorganic builder having the following composition in its anhydrous form:
- xM.sub.2 O.ySiO.sub.2,
- wherein x and y are numerical values satisfying the following relationship: y/x is 1.0 to 4.0, M stands for Na and K, and K/Na is 0.01 to 2.0, the method comprising the steps of:
- (a) adding water, a Na-containing compound, and a K-containing compound to silica sand, to give a mixture;
- (b) subjecting the resulting mixture to a hydrothermal treatment, wherein said hydrothermal treatment is carried out under the condition of from 5 to 15 kg/cm.sup.2 G, thereby dissolving the silica sand in the mixture; and thereafter
- (c) baking the resulting treated mixture.
- 6. The method according to claim 5, wherein the Na-containing compound and the K-containing compound are selected from the group consisting of NaOH, KOH, Na.sub.2 CO.sub.3, K.sub.2 CO.sub.3, NaNO.sub.3, KNO.sub.3, Na.sub.2 SO.sub.4, and K.sub.2 SO.sub.4.
- 7. The method according to claim 5, wherein the Na-containing compound and the K-containing compound are each supplied as an aqueous solution of the Na-containing compound and an aqueous solution of the K-containing compound, and wherein a concentration of each of the aqueous solution of an Na-containing compound and the aqueous solution of a K-containing compound is from 20 to 70% by weight.
- 8. The method according to claim 5, wherein the mixture obtained in step (a) has a water content of from 24 to 50% by weight.
Priority Claims (1)
Number |
Date |
Country |
Kind |
9-19892 |
Jan 1997 |
JPX |
|
Parent Case Info
This application is the national phase under 35 U.S.C. .sctn.371 of prior PCT International Application No. PCT/JP98/00147 which has an International filing date of Jan. 14, 1998 which designated the United States of America, the entire contents of which are hereby incorporated by reference.
PCT Information
Filing Document |
Filing Date |
Country |
Kind |
102e Date |
371c Date |
PCT/JP98/00147 |
1/14/1998 |
|
|
8/26/1998 |
8/26/1998 |
Publishing Document |
Publishing Date |
Country |
Kind |
WO98/31631 |
7/23/1998 |
|
|
US Referenced Citations (5)
Foreign Referenced Citations (2)
Number |
Date |
Country |
49-21240 |
May 1974 |
JPX |
8-290913 |
Nov 1996 |
JPX |