This application claims the benefit of Japanese Priority Patent Application JP 2015-056641 filed Mar. 19, 2015, the entire contents of each of which are incorporated herein by reference.
The present invention relates to a method for producing H-shaped steel using a slab or the like having a rectangular cross-section as a material, for example.
In the case where H-shaped steel is produced, a material, such as a slab or a bloom, extracted from a heating furnace is shaped into a raw blank (a material to be rolled with a so-called dog-bone shape) by a rough rolling mill (BD). Thicknesses of a web and flanges of the raw blank are subjected to reduction by an intermediate universal rolling mill, and moreover, flanges of a material to be rolled are subjected to width reduction and forging and shaping of end surfaces by an edger rolling mill close to the intermediate universal rolling mill. Then, an H-shaped steel product is shaped by a finishing universal rolling mill.
In such a method for producing H-shaped steel, a technology is known in which, in shaping a raw blank with a so-called dog-bone shape from a slab material having a rectangular cross-section, splits are created on slab end surfaces in a first caliber of a rough rolling step, the splits are then widened or made deeper and edging rolling is performed in a second caliber and subsequent calibers, and the splits on the slab end surfaces are erased in subsequent calibers. It is known that the depths of the splits expanded here sequentially become shallower or are approximately the same depth in the second caliber and subsequent calibers.
For example, the technology of Patent Literature 1 discloses a caliber configuration in which heights of projections of a plurality of calibers for creating splits in the rough rolling step (hereinafter also called wedge heights) are designed to be substantially the same height.
In addition, for example, the technology of Patent Literature 2 discloses a configuration in which a wedge height of a caliber for creating splits in the rough rolling step is highest in the first caliber and sequentially decreases in subsequent calibers.
Patent Literature 1: JP 2062461B
Patent Literature 2: JP 2036476B
In recent years, an increase in size of structures and the like has brought about demands for production of large-size H-shaped steel products. In particular, there have been demands for a product in which flanges, which greatly contribute to strength and rigidity of H-shaped steel, are made wider than conventional flanges. To produce an H-shaped steel product with widened flanges, it is necessary to shape a material to be rolled with a flange width larger than a conventional flange width from the stage of shaping in the rough rolling step.
However, there is a limit in widening of flanges in the technologies disclosed in Patent Literatures 1 and 2, for example, in which splits are created on end surfaces of a material such as a slab (slab end surfaces) and the end surfaces are subjected to edging, and the spread is utilized for rough rolling. That is, in order to widen flanges, conventional rough rolling methods use technologies such as wedge designing (designing of a split angle), reduction adjustment, and lubrication adjustment to improve spread, but none of the methods greatly contributes to a flange width; thus, it is known that the rate of spread, which indicates the ratio of a flange spread amount with respect to an edging amount, is approximately 0.8 even under a condition in which efficiency at the initial stage of edging is the highest, decreases as edging is repeated in the same caliber, and finally becomes approximately 0.5. It may also be possible to increase the size of the material (e.g., slab) itself to increase the edging amount, but product flanges are not sufficiently widened because there are device limits in equipment scale and an amount of reduction of rough rolling mills.
In view of such circumstances, studies have been made on employing a caliber configuration in which a wedge height is made larger to make the depth of the splits deeper than a conventional depth, for example. In such a case, however, larger wedge heights lead to left-right ununiformity in cross-sectional area of flange portions, and there is a possibility that material-passing defects occur and sufficient dimensional accuracy is not secured.
In view of the circumstances, an object of the present invention is to provide a method for producing H-shaped steel, the method enabling an improvement in material-passing property and an improvement in dimensional accuracy in the following manner: in producing H-shaped steel, when splits are created on end surfaces of a material (e.g., slab) by using projections with acute-angle tip shapes (hereinafter also called wedge portions), and flange portions formed by the splits are sequentially bent in a plurality of calibers, a wedge-portion height of each caliber is set to a height satisfying a predetermined condition.
According to the present invention in order to achieve the above-mentioned object, there is provided a method for producing H-shaped steel, the method including: a rough rolling step; an intermediate rolling step; and a finish rolling step. A slab material whose slab width/slab thickness is equal to or more than 6.0 and equal to or less than 7.7 is used as a material to be rolled. In a rolling mill that performs the rough rolling step, a plurality of calibers to shape the material to be rolled are engraved, the number of the plurality of calibers being four or more. Shaping of one or a plurality of passes is performed on the material to be rolled in the plurality of calibers. In a first caliber and a second caliber among the plurality of calibers, projections to create splits vertically with respect to a width direction of the material to be rolled are formed. The projections formed in the first caliber are designed to have a height of 100 mm or more, and the projections formed in the first caliber and the second caliber have a tip angle of 40° or less.
The slab material may have a slab width of 1800 mm or more and a slab thickness of 300 mm or more at a start of shaping in the first caliber.
The slab material may have a slab width of 1200 mm or more and a slab thickness of 250 mm or more at a start of shaping in the first caliber.
The projections formed in the first caliber and the second caliber may have a tip angle of equal to or more than 25° and equal to or less than 35°.
In the second caliber and subsequent calibers among the plurality of calibers, reduction may be performed in a state where end surfaces of the material to be rolled are in contact with caliber peripheral surfaces in shaping of at least one pass. In a third caliber and subsequent calibers among the plurality of calibers, a step of sequentially bending divided parts formed by the splits may be performed.
In the first caliber, a relief portion extending in a direction of being distanced from the material to be rolled in shaping may be formed at a material-to-be-rolled entry side of a side-wall portion that is adjacent to a side surface of the material to be rolled. The relief portion may have a curved shape in which an inner surface of the first caliber is more distanced from the material to be rolled as becoming closer to the material-to-be-rolled entry side in the side-wall portion. A curvature radius R of the curved shape may be 400 mm or less.
According to the present invention, it is possible to improve material-passing property and improve dimensional accuracy in the following manner: in producing H-shaped steel, when splits are created on end surfaces of a material (e.g., slab) by using projections with acute-angle tip shapes (hereinafter also called wedge portions), and flange portions formed by the splits are sequentially bent in a plurality of calibers, a wedge-portion height of each caliber is set to a height satisfying a predetermined condition.
1 rolling equipment
2 heating furnace
3 sizing mill
4 rough rolling mill
5 intermediate universal rolling mill
8 finishing universal rolling mill
9 edger rolling mill
11 slab
12 flange-corresponding portion
13 H-shaped raw blank
14 intermediate material
16 H-shaped steel product
20 upper caliber roll (first caliber)
21 lower caliber roll (first caliber)
25, 26 projection (first caliber)
28, 29 split (first caliber)
30 upper caliber roll (second caliber)
31 lower caliber roll (second caliber)
35, 36 projection (second caliber)
38, 39 split (second caliber)
40 upper caliber roll (third caliber)
41 lower caliber roll (third caliber)
45, 46 projection (third caliber)
48, 49 split (third caliber)
50 upper caliber roll (fourth caliber)
51 lower caliber roll (fourth caliber)
55, 56 projection (fourth caliber)
58, 59 split (fourth caliber)
80 flange portion
100 side-wall portion
102 overfill portion
110 relief portion
K1 first caliber
K2 second caliber
K3 third caliber
K4 fourth caliber
T production line
A material to be rolled
Hereinafter, (an) embodiment(s) of the present invention will be described with reference to the drawings. In this specification and the appended drawings, structural elements that have substantially the same function and structure are denoted with the same reference numerals, and repeated explanation of these structural elements is omitted.
As illustrated in
Next, description will be given on configurations and shapes of calibers that are engraved in the sizing mill 3 and the rough rolling mill 4 illustrated in
In the present embodiment, a case where four calibers are engraved is described as an example, but the number of calibers is not necessarily four, and there may be a plurality of calibers, the number of the plurality of calibers being four or more. That is, any caliber configuration suitable for shaping the H-shaped raw blank 13 may be employed. Note that
The height h1 of the projections 25 and 26 is a value satisfying a predetermined condition; specifically, in the case where slab dimensions of a material are equal to or more than a predetermined size, for example, the height h1 of the projections 25 and 26 needs to be set to 100 mm or more. The reason why the height h1 of the projections 25 and 26 needs to be a value satisfying a predetermined condition will be described later with reference to
In this first caliber K1, the projections 25 and 26 are pressed against upper and lower end portions of the material to be rolled A (slab end surfaces) to form splits 28 and 29. Here, the tip-portion angle θ1a of the projections 25 and 26 is preferably equal to or more than 25° and equal to or less than 40°, for example, further preferably equal to or more than 25° and equal to or less than 35°.
When the wedge angle is large, a wedge inclination angle is enlarged, which makes pressing force in the up-and-down direction due to friction force easily act on the material to be rolled A; thus, a reduction in cross-sectional area occurs at inner surface portions of flange-corresponding portions in split formation, causing a decrease in efficiency in generating flanges particularly in shaping using the second caliber K2 and subsequent calibers.
According to the above reason, the tip-portion angle θ1a of the projections 25 and 26 is preferably equal to or more than 25° and equal to or less than 40°. Similarly, a wedge angle θ1b described below is preferably equal to or more than 25° and equal to or less than 40°. From the viewpoint of achieving high efficiency in generating flanges, it is further preferable to set these wedge angles θ1a and θ1b to equal to or more than 25° and equal to or less than 35°.
Here, a caliber width of the first caliber K1 is preferably substantially equal to a thickness of the material to be rolled A (i.e., a slab thickness). Specifically, when the width of the caliber at the tip portions of the projections 25 and 26 formed in the first caliber K1 is set to be the same as the slab thickness, the property of left-right centering of the material to be rolled A is ensured suitably. Moreover, it is preferable to employ this configuration of caliber dimensions so that, in shaping using the first caliber K1, the projections 25 and 26 and part of side surfaces (side walls) of the caliber be in contact with the material to be rolled A at the upper and lower end portions of the material to be rolled A (the slab end surfaces), and active reduction not be performed by the top surface and the bottom surface of the first caliber K1 on slab upper and lower end portions, which are divided into four elements (parts) by the splits 28 and 29, as illustrated in
Here, description is given on reasons for setting the suitable numerical range of the wedge angle θ1b of the projections 35 and 36 to equal to or more than 25° and equal to or less than 40° (further preferably equal to or more than 25° and equal to or less than 35°) and a reason for accordingly setting the wedge angle θ1a of the first caliber K1 to the suitable numerical range.
A lower limit value of a wedge angle is normally decided by the strength of a roll. The material to be rolled A comes into contact with the rolls (the upper caliber roll 30 and the lower caliber roll 31 in the second caliber K2, and the upper caliber roll 20 and the lower caliber roll 21 in the first caliber K1), and the rolls are subjected to heat during the contact to swell, and when the material to be rolled A goes out of contact with the rolls, the rolls are cooled to shrink. This cycle is repeated during shaping; when the wedge angle is too small, the projections (the projections 35 and 36 in the second caliber K2, and the projections 25 and 26 in the first caliber K1) have small thicknesses, and this makes heat input from the material to be rolled A easily enter from the left and right of the projections, making the rolls have higher temperatures. When the rolls have high temperatures, thermal amplitude increases to cause a heat crack, which may break the rolls. For this reason, the wedge angles θ1a and θ1b are both preferably 25° or more.
On the other hand, when the wedge angles θ1a and θ1b are large, wedge inclination angles are enlarged, which makes pressing force in the up-and-down direction due to friction force easily act on the material to be rolled A; thus, a reduction in cross-sectional area occurs at inner surface portions of flange-corresponding portions in split formation, causing a decrease in efficiency in generating flanges particularly in shaping using the second caliber K2 and subsequent calibers. Here, the relation between the wedge angle θ1b of the second caliber K2 and a flange width of the material to be rolled A that is finally shaped is described, and a suitable upper limit value of the wedge angle θ1b is described, with reference to
As shown in
Moreover, for high inductivity and secured rolling stability, the wedge angle θ1a of the first caliber K1 is preferably the same angle as the wedge angle θ1b of the second caliber K2 subsequent to the first caliber K1.
In particular, the wedge angle θ1a of the first caliber K1 is known to greatly contribute to tip-portion thicknesses of the flange-corresponding portions (later flange portions 80); in this respect, the wedge angle θ1a is preferably as small as possible.
As shown in
As described above, in addition to setting the wedge angle θ1b of the second caliber K2 to equal to or more than 25° and equal to or less than 40°, it is preferable to set the wedge angle θ1a of the first caliber K1 to equal to or more than 25° and equal to or less than 40°, from the viewpoints of ensuring the tip-portion thicknesses of the flange-corresponding portions and securing inductivity and rolling stability. Furthermore, from the viewpoint of achieving high efficiency in generating flanges, it is preferable to set these wedge angles θ1a and θ1b to equal to or more than 25° and equal to or less than 35°.
To ensure the tip-portion thicknesses of the flange-corresponding portions, increase inductivity, and secure rolling stability, it is preferable to set the wedge angle θ1a of the first caliber K1 to the same angle as the wedge angle θ1b of the second caliber K2 subsequent to the first caliber K1.
A height (protrusion length) h2 of the projections 35 and 36 is configured to be larger than the height h1 of the projections 25 and 26 of the first caliber K1; h2>h1 is satisfied.
As described above, the height h2 of the projections 35 and 36 formed in the second caliber K2 is larger than the height h1 of the projections 25 and 26 formed in the first caliber K1, and similarly, an intrusion length into the upper and lower end portions of the material to be rolled A (the slab end surfaces) is larger for the second caliber K2. Here, an intrusion depth of the projections 35 and 36 into the material to be rolled A in the second caliber K2 is the same as the height h2 of the projections 35 and 36. That is, an intrusion depth h1′ of the projections 25 and 26 into the material to be rolled A in the first caliber K1 and an intrusion depth h2 of the projections 35 and 36 into the material to be rolled A in the second caliber K2 satisfy a relation of h1′<h2.
As illustrated in
Shaping using the second caliber K2 illustrated in
On the other hand, in other passes, the caliber is not in contact with the material to be rolled A, besides the projections 35 and 36, at the upper and lower end portions of the material to be rolled A (the slab end surfaces), and active reduction is not performed on the material to be rolled A in these passes. This is because reduction causes stretch of the material to be rolled A in the longitudinal direction, which decreases efficiency in generating the flange-corresponding portions (corresponding to the flange portions 80 described later).
That is, in multi-pass shaping using the second caliber K2, it is preferable to set a pass schedule in which reduction is performed by bringing the upper and lower end portions of the material to be rolled A (the slab end surfaces) into contact with the inside of the caliber in minimum necessary passes (e.g., only the final pass), and active reduction is not performed in other passes. Also in this second caliber K2, as with the first caliber K1, an amount of reduction at the projections 35 and 36 (amount of reduction ΔT at wedge tips) is set to be sufficiently larger than an amount of reduction at the slab upper and lower end portions (amount of reduction ΔE at slab end surfaces); thus, the splits 38 and 39 are formed.
A tip-portion angle θ2 of the projections 45 and 46 is configured to be wider than the angle θ1b, and an intrusion depth h3 of the projections 45 and 46 into the material to be rolled A is shorter than the intrusion depth h2 of the projections 35 and 36 (i.e. h3<h2).
As illustrated in
Shaping using the third caliber K3 illustrated in
On the other hand, in other passes, the caliber is not in contact with the material to be rolled A, besides the projections 45 and 46, at the upper and lower end portions of the material to be rolled A (the slab end surfaces), and active reduction is not performed on the material to be rolled A in these passes. This is because reduction causes stretch of the material to be rolled A in the longitudinal direction, which decreases efficiency in generating the flange-corresponding portions (corresponding to the flange portions 80 described later).
A tip-portion angle θ3 of the projections 55 and 56 is configured to be wider than the angle θ2, and an intrusion depth h4 of the projections 55 and 56 into the material to be rolled A is shorter than the intrusion depth h3 of the projections 45 and 46 (i.e. h4<h3).
In the fourth caliber K4, the material to be rolled A that has passed through the third caliber K3 is shaped in the following manner: the projections 55 and 56 are pressed against the splits 48 and 49 formed in the third caliber K3, at the upper and lower end portions of the material to be rolled A (the slab end surfaces); thus, the splits 48 and 49 are expanded to become splits 58 and 59. That is, in a final pass in shaping using the fourth caliber K4, a deepest-portion angle of the splits 58 and 59 (hereinafter also called a split angle) becomes θ3. In other words, shaping is performed in a manner that the divided parts (parts corresponding to the flange portions 80 described later) shaped together with the formation of the splits 48 and 49 in the third caliber K3 are further bent outwardly. The parts at the upper and lower end portions of the material to be rolled A shaped in this manner are parts corresponding to flanges of a later H-shaped steel product, and are called flange portions 80 here. Note that the split angle θ3 of the fourth caliber K4 is preferably set to an angle somewhat smaller than 180°. This is because if the split angle θ3 is 180°, spread occurs at the outer side of the flange portions 80 when web thickness is decreased in a web thinning caliber in the next step, and overfill is likely to occur in rolling using the web thinning caliber. That is, since the amount of spread at the outer side of the flange portions 80 is decided by the shape of the web thinning caliber in the next step and an amount of reduction of the web thickness, the split angle θ3 here is preferably determined suitably with the shape of the web thinning caliber and the amount of reduction of the web thickness taken into consideration.
Shaping using the fourth caliber K4 illustrated in
On the other hand, in other passes, the caliber is not in contact with the material to be rolled A, besides the projections 55 and 56, at the upper and lower end portions of the material to be rolled A (the slab end surfaces), and active reduction is not performed on the material to be rolled A in these passes. This is because reduction causes stretch of the material to be rolled A in the longitudinal direction, which decreases efficiency in generating the flange portions 80.
The material to be rolled A shaped by the first to fourth calibers K1 to K4 described above is further subjected to reduction and shaping using a known caliber; thus, the H-shaped raw blank 13 with a so-called dog-bone shape is shaped. Normally, web thickness is then decreased in a web thinning caliber for thinning a portion corresponding to slab thickness. After that, reverse rolling of a plurality of passes is performed using a rolling mill train composed of two rolling mills of the intermediate universal rolling mill 5 and the edger rolling mill 9, which is illustrated in
In producing the H-shaped steel product 16 described above, the formation of the splits 28 and 29 using the projections 25 and 26 in the first caliber K1 illustrated in
In split formation according to a conventional method, in the intermediate pass in split formation using the second caliber K2, the slab end surface and the slab thickness are ununiform between left and right (see dotted-line portions in the drawing), and the actual shape differs from the desired shape of the material to be rolled, as illustrated in
In view of such problems illustrated in
Here, in a conventional technology, the slab end surface and the slab thickness are already ununiform between the left and right in the intermediate pass of the second caliber K2, as illustrated in
The present inventors carried out studies on a case where shaping of H-shaped steel is performed by using three types of slabs having a slab thickness of 300 mm and a slab width of 2300 mm, a slab thickness of 300 mm and a slab width of 1800 mm, a slab thickness of 250 mm and a slab width of 1200 mm, as a material slab serving as the material to be rolled A. Specifically, in a shaping process using the four calibers described with reference to
Thickness variations of left and right flange-corresponding portions are preferably suppressed to 5% or less. According to JIS standard (JIS G 3192), an allowance of shape dimensions of large-size H-shaped steel is as follows: in the case where a flange thickness exceeds 40 mm, tolerance of the flange thickness is 4 mm (i.e., ±2 mm), which corresponds to 10% of a flange thickness of a product. In the case where flange dimensions of a product are out of the tolerance, correction by working is difficult, and the product is not recognized as a product with predetermined quality, which is problematic in terms of production efficiency and cost. Accordingly, it is necessary to ensure sufficient process capability in each shaping step and suppress thickness variations of left and right flange-corresponding portions in producing an H-shaped steel product. Normally, it is preferable to set tolerance of a flange thickness to 6σ to ensure sufficient process capability in each shaping step. To match 10% of a flange thickness of an H-shaped steel product with 6σ on the basis of the HS standard, it is preferable to set the target value of thickness variations 3σ of left and right flange-corresponding portions to 5% or less.
As shown by the above finding, in the case where shaping of H-shaped steel according to the present embodiment is performed with a slab with predetermined dimensions used as a material, setting the wedge height of the first caliber K1 to a predetermined height or more decreases flange thickness variations in subsequent shaping, making thickness variations of left and right flange-corresponding portions after rolling using the third caliber K3 equal to or less than 5%, for example.
According to studies by the present inventors, it has been found that a ratio between width and thickness of a material slab (=slab width/slab thickness) is related to flange thickness variations in shaping. That is, the ratio of slab width/slab thickness of the material slab has been found to be associated with ease of rotation of the material to be rolled in the caliber; for example, larger slab width/slab thickness makes rotation easier and smaller slab width/slab thickness makes rotation more difficult. Values of slab width/slab thickness in the cases shown in
In the case where slab width/slab thickness is small as shown in
On the other hand, in the case where slab width/slab thickness is large as shown in
As shown in
These facts show that when slab width/slab thickness of the material slab is equal to or more than 6.0 and equal to or less than 7.7, setting the wedge height of the first caliber K1 to 100 mm or more decreases flange thickness variations in subsequent shaping, making thickness variations of left and right flange-corresponding portions after rolling using the third caliber K3 equal to or less than 5%, for example.
As described above, when a slab with predetermined dimensions is used as a material and the wedge height of the first caliber K1 is set to a height larger than a conventional height to fall within a suitable range, in shaping of the material to be rolled A using subsequent calibers (e.g., the second caliber K2 and the third caliber K3), a difference in cross-sectional area between left and right flange-corresponding portions can be decreased, leading to a decrease in thickness variations, and material-passing property can be improved. This improves dimensional accuracy of an H-shaped steel product after shaping.
The embodiment(s) of the present invention has/have been described above, whilst the present invention is not limited to the illustrated examples. A person skilled in the art may find various alterations and modifications within the scope of the appended claims, and it should be understood that they will naturally come under the technical scope of the present invention.
For example, the above embodiment describes that for shaping of the material to be rolled A using the first caliber K1 described with reference to
In view of such circumstances, the present inventors found that providing relief portions for releasing metal at the material-to-be-rolled entry side of the side-wall portions 100 in the first caliber K1 prevents formation of the overfill portions 102. These relief portions will be described with reference to
The relief portions 110 may be provided in any shapes that prevent occurrence of overfill of metal in the caliber as described above, and preferably have curved shapes with a curvature radius R of 400 mm or less, for example. As described above with reference to
Providing the relief portions 110 in the first caliber K1 in this manner prevents occurrence of overfill of metal in the side-wall portions 100 in shaping, and thus can prevent occurrence of shape defects due to overfill in flanges of an H-shaped steel product that is finally shaped.
In addition, the above embodiment describes a step in which, in shaping of H-shaped steel using the second to fourth calibers K2 to K4, shaping is performed in a manner that splits are formed on slab end surfaces (upper and lower end portions of the material to be rolled A), and left and right flange-corresponding portions are bent outwardly together with the formation of the splits, as illustrated in
For example, in the above embodiment, description is given assuming that the four calibers of the first to fourth calibers K1 to K4 are engraved to perform shaping of the material to be rolled A, but the number of calibers for performing the rough rolling step is not limited to this. That is, the number of calibers engraved in the sizing mill 3 and the rough rolling mill 4 can be changed arbitrarily, and is changed as appropriate to the extent that the rough rolling step can be performed suitably.
The above embodiment describes that shaping of bending the flange-corresponding portions (later flange portions 80) is performed by using the third caliber K3 and the fourth caliber K4. This is because it is preferable to assign a plurality of calibers (the third caliber K3 and the fourth caliber K4 in the above embodiment) to bending shaping, because if bending shaping is performed with the bending angle (i.e., the wedge angle in each caliber) rapidly increased, friction force between the projections and the material to be rolled A is likely to cause a reduction in cross-sectional area, and bending power increases, which may impair uniformity in cross-sectional area between the four flange-corresponding portions (later flange portions 80). According to experimental results by the present inventors, it is preferable to perform bending shaping in two calibers of the third caliber K3 and the fourth caliber K4 described in the above embodiment.
As Examples of the present invention, H-shaped steel was shaped by the method described in the above embodiment by using a slab with a thickness of 300 mm and a width of 2300 mm as a material. In Comparative Example 1, the wedge height in the first caliber K1 was set to 80 mm, which is the same as a conventional wedge height, and in Example 1, the wedge height in the first caliber K1 was set to 160 mm, which is larger than a conventional wedge height. Then, for each of Example 1 and Comparative Example 1, a difference between thicknesses of left and right flange-corresponding portions (flange thicknesses) at the end of shaping using the third caliber K3 was measured as a flange center-portion thickness difference. Table 1 below shows a pass schedule; G1, G2, and G3 in the table indicate, respectively, the first caliber K1, the second caliber K2, and the third caliber K3.
The present invention can be applied to a method for producing H-shaped steel using a slab or the like having a rectangular cross-section as a material, for example.
Number | Date | Country | Kind |
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2015-056641 | Mar 2015 | JP | national |
Filing Document | Filing Date | Country | Kind |
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PCT/JP2016/057654 | 3/10/2016 | WO | 00 |