Patent Application
20200292520
Not applicable.
Not applicable.
The present disclosure relates to linting of paper towels; more specifically, this disclosure relates to a method of quantitating paper towel lint; still more specifically, this disclosure relates to a method of quantitating paper towel lint that utilizes a specific wiping pattern to maximize lint deposition, a pre- and/or inter-test cleaning procedure, and/or a specific rinse water sprayer.
Pulp fibers, such as softwood fibers and hardwood fibers, are incorporated into numerous nonwoven materials. Such nonwoven materials are utilized in a variety of applications. For example, pulp fibers are used to form tissue products, including facial tissues, bath tissues, paper towels, industrial wipers, and the like. Pulp fibers are relatively inexpensive to obtain, which enables the production of relatively inexpensive products that may be disposed of after a single use.
Wiping products incorporating pulp fibers, such as paper towels, facial tissues, bath tissues and other similar products are designed to include several important properties. For example, the products are typically designed to have good bulk and a soft feel, and to be highly absorbent, while also exhibiting sufficient strength for the intended application, and tear resistance, even while wet. Unfortunately, when steps are taken to increase one desired property of the product, other characteristics of the material can be adversely affected. For example, in the manufacture of paper products, such as facial tissue, bath tissue, paper towels, dinner napkins and the like, a plethora of product properties can be imparted to the final product through the use of chemical additives applied in the wet end of the tissue making process. Two of the attributes imparted to tissue through the use of wet end chemical additives are strength and softness. Specifically for softness, a chemical debonding agent is normally utilized. Via disruption of fiber-to-fiber bonds, incorporation of such debonding agents increases the softness of the tissue sheet.
Debonding tends to increase levels of lint and slough in the product. Lint and slough can generally be defined as the tendency of the fibers in the paper sheet to be rubbed from the sheet when handled. Indeed, while softness increases, such increase is obtained at the expense of an increase in lint and slough in the product relative to an untreated control. For example, in a blended (non-layered) tissue sheet, the level of lint and slough is typically inversely proportional to the tensile strength of the tissue sheet.
As efforts to reduce slough and lint without a noticeable loss of bulk and softness have not been entirely successful, many disposable wiping products, such as paper towels and facial tissues, have an undesirable tendency to generate lint on surfaces after use. Such a tendency, which may be more noticeable, for example, when wiping a mirror or a black surface, may be viewed by a consumer or other user as undesirable or even unacceptable.
In view of the above, a need exists for a method of quantitating the amount of lint shed from a product, such as a paper towel, during a wiping motion. Such a method may be useful in producing wiping products having a reduced tendency to lint when used in a wiping motion.
Disclosed herein is a method for quantitating the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed; depositing lint from the sample onto a surface, which has been cleaned, by moving the sample thereupon in a specific pattern comprising a plurality of directional changes; collecting the lint deposited on the surface; and determining the amount of collected lint.
Also disclosed herein is a method for determining the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed; depositing lint from the sample onto a substantially lint-free surface by moving the sample thereupon in a specific pattern; collecting the lint deposited on the surface; measuring the number, the average length, and the average width of the fibers in the collected lint; and calculating the amount of collected lint as the total fiber area (mm2), by multiplying the average fiber length (mm) by the average fiber width (mm) and the fiber count and subtracting a blank therefrom, wherein the blank is calculated as the amount of lint collected from the substantially lint-free surface in the absence of the depositing step.
Further disclosed herein is a method for quantitating the amount of lint shed from a paper towel, the method comprising: cleaning a rectangular deposition surface having a short dimension and a long dimension, wherein cleaning comprises spraying the entire surface with glass cleaner, using a substantially lint-free squeegee to push the glass cleaner off one of two short sides of the surface, and using a substantially lint-free sponge to wipe the edges of the surface substantially free of lint; preparing a sample of paper towel to be analyzed; depositing lint from the sample onto the cleaned surface by moving the sample thereupon in a specific pattern; collecting the lint deposited on the surface; and determining the amount of collected lint.
Also disclosed herein is a method for quantitating the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed; depositing lint from the sample onto a substantially lint-free surface by moving the sample thereupon in a specific pattern; collecting the lint deposited on the surface, wherein collecting the lint deposited on the surface comprises, substantially immediately upon depositing lint from the sample onto the surface, washing the deposited lint from the surface into a tared, cleaned, empty vessel; and determining the amount of collected lint.
Further disclosed herein is a method for quantitating the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed, wherein preparing the sample comprises wrapping the sample around a solid support, to provide a wrapped support; depositing lint from the sample onto a surface, which has been cleaned, by moving the sample thereupon in a specific pattern comprising a plurality of directional changes; collecting the lint deposited on the surface; and determining the amount of collected lint, wherein the surface is substantially rectangular, having a long dimension and a short dimension, wherein the solid support is substantially rectangular, having a long dimension and a short dimension, and wherein wrapping the sample around the solid support further comprises placing the solid support on the sample on a side of the sample opposite a side of the sample to contact the surface during lint deposition and wrapping the sample around the solid support, with a machine direction of the sample parallel to the short dimension of the solid support.
For a more complete understanding of the present disclosure and the advantages thereof, reference is now made to the following brief description, taken in connection with the accompanying drawings and detailed description, wherein like reference numerals represent like parts.
Herein disclosed is a method for quantitating paper towel lint. The method can be utilized to determine the amount of lint shed from a paper towel during a wiping motion. ‘Lint’ as used herein means any material that originated from a fibrous structure, such as, without limitation, a paper towel or tissue product comprising the fibrous structure, that remains on a surface after the fibrous structure or product formed therefrom has come into contact therewith. The amount of lint, calculated as described hereinbelow as the total area of fiber deposited on a surface during testing, indicates the tendency of the fibers in the fibrous structure to be rubbed therefrom when utilized.
Although described hereinbelow with reference to a paper towel, a fibrous structure tested via the herein-disclosed method may be another wiping product. In general, the lint deposited during a wiping motion by any wiping product containing pulp fibers may be assessed according to the method of this disclosure. Such wiping product may comprise, for example, a paper towel, an industrial wiper, a premoistened wiper, or the like, including other nonwoven, woven or knitted wiping products. In embodiments, the wiping product comprises a tissue web, such as a paper towel, industrial wiper, and the like. Such tissue web may, for example, have a basis weight of from about 10 gsm to about 150 gsm. Bath tissues and facial tissues, for example, typically have a basis weight of from about 10 gsm to about 35 gsm, while paper towels and other wiping products may have a basis weight of from about 40 gsm to about 80 gsm.
The wiping product may be a retail or non-retail product, e.g., a retail consumer paper towel or a non-retail paper towel. The fibrous product may contain one ply or may contain multiple plies. Furthermore, although primarily described, and shown in the drawings, as being carried out manually (i.e., via human), it is to be understood that quantitating lint according to the method of this disclosure can be mechanized or automated.
The method according to this disclosure will now be described with reference to
As indicated in
A sample may be cut from a roll of paper towel which has been conditioned as noted above. A sample of a desired size is cut from the roll. In order to minimize/prevent foreign lint from contaminating the sample, cutting of the sample is effected just prior to lint testing, and is not performed well in advance of testing. For example, the sample(s) may be cut within 3, 4, or 5 minutes of lint deposition via step 30, in embodiments.
In embodiments, the sample is cut in the machine direction (MD), with a paper cutter, and the perforations are avoided. ‘Machine Direction’ or ‘MD’ as used herein means the direction parallel to the flow of the paper towel through a paper-making machine.
The sample 71 is handled as minimally as possible and is not placed on any surface that may contaminate it prior to lint testing as described herein. Any surface with which the sample comes into contact (e.g., a lab bench surface, the surface of a paper cutter, etc.) is desirably a clean, lint-free surface. Such surfaces can be cleaned, for example, via commercially available cleaner (e.g., glass cleaner such as WINDEX® in a spray bottle) and/or lint-free wipes (e.g., ACCUWIPES®, SKU 29834). The cutting blade of a paper cutter utilized to cut the sample can be cleaned with compressed air prior to cutting each sample.
Preparing the sample can further comprise wrapping a sample around a support. As the support imparts a pressure against the sample when wiped on the deposition surface, utilization of a two-sheet sample may, in embodiments, be employed to help prevent the outer sheet from tearing during the test. As depicted in
The support can comprise any solid support around which sample 71 can be wrapped, and with which the plowing motion described hereinbelow for depositing lint can be performed. In embodiments, support 70 comprises a rubberized cushion material. In embodiments, the support is rectangular, having a long dimension or length and a short dimension or width. In embodiments, the support has a length in the range of from about 4 inches to about 11 inches, from about 7 inches to about 11 inches, or from about 10 inches to about 11 inches. In embodiments, the support has a width in the range of from about 2 inches to about 5 inches, from about 3 inches to about 5 inches, or from about 4 inches to about 5 inches. In embodiments, the support has a thickness or height in the range of from about 0.25 inch to about 3 inches, from about 0.25 inch to about 1.5 inches or from 0.25 inch to 0.75 inches. By way of non-limiting example, the support may comprise a modified SWIFFER® head, having a total weight of 1500 g and providing a 35 to about 40 square inch test area. The test area is the area of sample 71 the contacts deposition surface 60 during lint deposition. The test area may be in the range of from about 8 to about 55 square inches (in2), from about 25 to about 45 in2, from about 30 to about 40 in2, or equal to about 10, 20, 25, 30, 35, 40, 45, 50, or 55 in2.
Sample 71 can be placed onto deposition surface 60 onto which lint is to be deposited, described further below, with the machine direction MD of the towel sample 71 parallel with a long dimension LD of deposition surface 60, and the side of the paper towel sample to be analyzed 51 facing the deposition surface 60, and the other side S2 of sample 71 facing the support 70. In embodiments, sample 71 can be substantially centered on deposition surface 60, whereby the midpoint MP of the towel sample along the MD is aligned with the midway point MP of the long dimension LD of deposition surface 60. Sample 71 can be wrapped around support 70 by setting support 70 on sample 71 with the short dimension of support 70 parallel to the MD of sample 71, as shown in
A method of quantitating lint according to this disclosure further comprises depositing lint from the sample onto a test or deposition surface, as indicated at 30 of the flow diagram of
As seen in the embodiment of
In embodiments, a method of quantitating lint according to this disclosure further comprises cleaning the deposition surface 60, as indicated at step 20 of the flow diagram of
A separate lint-free sponge and a stream of tap water may be utilized at this point to clean the inside of a lint collection vessel (vessel 83 in
Cleaning the test or deposition surface at step 20 can comprise spraying substantially the entire surface with cleaner, which may comprise glass cleaner. The deposition surface may be sprayed with a plurality of sprays. In embodiments, the deposition surface 60 is sprayed with 6 sprays of cleaner, which provides about 6.0 grams (±0.2 g). A spray check as described vide infra can be performed to confirm that the desired amount of cleaner or wetting agent is applied via the sprayer.
To ensure the amount of wetting agent or surface cleaner, such as glass cleaner, utilized, a spray check can be performed whenever a spray head in a spray bottle utilized to spray the cleaner is changed, and/or whenever a spray bottle or pump is replaced, to verify the initial spray weight. A spray check can comprise placing a number of (e.g., two) sheets of paper towel on a balance; taring the balance; spraying the paper towel on the tared balance with three full pumps of the spray nozzle; noting the weight. In embodiments, the desired weight provided by three full sprays is about 3.0 grams (±0.2 g). Any suitable balance may be used. The balance may have a resolution of 1 gram.
After spraying the deposition surface with the desired amount of surface cleaner, squeegee 64 can be utilized to push the cleaner off the surface. Cellulose sponges 62 may be positioned along first short side SS1 of deposition surface 60, as indicated in
As indicated in
Deposition surface 60 can be marked along the long dimension LD, as indicated in the embodiment of
In embodiments, the herein disclosed lint quantitation method is a wet testing method. Accordingly, in embodiments, wrapped support 75 is lifted (manually or mechanically) off deposition surface 60, and deposition surface 60 is sprayed with a wetting liquid in wetting liquid sprayer 63 of
Following wetting of deposition surface 60, wrapped support 75 may be placed onto the sprayed surface, centering such that the midpoint MP (along the long dimension) of wrapped support 75 is aligned with the midpoint MP (along the long dimension) of deposition surface 60. Using the marking scheme of
Lint is deposited by moving wrapped support 75 over deposition surface 60 in a specific pattern, comprising a plurality of directional changes. In embodiments, wrapped support 75 is moved back and forth along the long dimension of deposition surface 60, keeping the long dimension of wrapped support 75 perpendicular to the LD of deposition surface 60. Without wishing to be limited by theory, changing direction via the plowing back and forth wiping motion of this disclosure may enhance lint deposition. For manual (i.e., human) operation, the wrapped support may be moved by placing index fingers at the top corners and thumbs at the bottom corners thereof
When moving the wrapped support in the specific pattern to deposit lint, a plowing motion is utilized in which the wrapped support is tilted forward (e.g., in a direction of travel), whereby a leading edge of wrapped support 75 makes substantially full contact with deposition surface 60, and a trailing edge of wrapped support 75 is lifted a distance off deposition surface 60. The distance can be about 1/16, ⅛, or % inch. In embodiments, during plowing, the wrapped support is tilted forward at an angle of from about 0 to about 10 degrees, from about 0 to about 5 degrees, from about 1 to about 3 degrees, with the tilt angle of wrapped support being measured relative to the deposition surface 60. For example, for a ⅛ inch distance off deposition surface 60, the angle at which the wrapped support is tilted may be about 1.8 degrees from horizontal. Desirably, at least 50, 75 or 90 percent of the contact area of wrapped support 75 remains in contact with deposition surface 60 during plowing. Enough force is provided to the wrapped support to slide it across deposition surface 60, with no additional downward force. In embodiments, the force applied to the leading edge of wrapped support 75 is in the range of from about 0.1 to about 1 psi, from 0.1 to 0.5 psi, from 0.1 to 0.25 psi. Via the plowing motion, the wrapped support will rotate slightly forward toward the direction in which it is moving; when coming to a change in direction, the wrapped support is tilted in the opposite direction prior to moving in that opposite direction. This rotation allows the loose lint to be deposited on the surface. For manual operation, practicing of the plowing motion can be performed daily prior to testing.
Description of the movement utilized to deposit lint will now be provided. A plowing motion as described above is consistently utilized when moving the sample, and moving is intended to indicate ‘moving in a plowing motion’. Initial back and forth pass(es) may be utilized to wet the sample 71/absorb the wetting liquid. For example, after placement at the MP of the sprayed surface, wrapped support 75 may be moved to the first short side SS1 of deposition surface 60 (such that the leading edge of wrapped support 75 is stopped between number 2 and the edge SS1), and a complete back and forth pass across the entire long dimension LD of deposition surface 60 performed, whereby the wrapped support 75 is moved to SS2 of deposition surface 60 (such that the leading edge of wrapped support 75 is stopped between number 1 and the edge SS2), and returned to SS1 (such that the leading edge of wrapped support 75 is stopped between number 2 and the edge SS1). Wrapped support 75 may then be moved back to the second short side SS2 of deposition surface 60 (such that the leading edge of wrapped support 75 aligns with number 1). Desirably, wrapped support 75 does not extend over first short side SS1 or second short side SS2 of deposition surface 60 while moving wrapped support 75 thereupon to deposit lint thereon. Desirably, in embodiments, there is substantially no movement of wrapped support 75 in a direction parallel to the short dimension SD of deposition surface 60.
Following the initial passes, wrapped support 75 is moved over deposition surface 60 in a specific pattern, comprising a plurality of directional changes. Such a specific pattern will now be described with reference to
Positioning of wrapped support 75 refers to alignment of the leading edge thereof with a ‘position’ along the LD of deposition surface 60. In embodiments, following the initial passes, wrapped support 75 is moved over deposition surface 60 in a specific pattern comprising a plurality of directional changes that occur at a plurality of positions. For example, the specific pattern may comprise 8 direction changes, at eight direction change positions, such as numbered positions 1 through 8 in the embodiment of
In an embodiment, wrapped support 75 is brought to a first position (e.g., position 1 in the embodiment of
In embodiments, depositing lint by moving the wrapped support over the surface in a specific pattern with or without the initial passes takes from about 40 to about 45 seconds, from about 15 to about 60 seconds, from about 25 to about 60 seconds, or from 35 to about 60 seconds to complete. In embodiments, all passes performed during lint deposition, including initial wetting passes, are completed within 40, 50, or 60 seconds. The duration may depend on the friction between the surface and the particular paper towel being tested. Some samples may grab and skip on the surface, and the speed can be reduced to prevent tearing of such samples.
Once the final position has been reached (e.g., the midpoint between direction change positions 7 and 8), wrapped support 75 can be lifted off deposition surface 60, and may be set aside. Note may be made of any tears or other unusual conditions of the spent sample. The spent sample may be removed from support 70 and disposed, after lint collection as described below.
In embodiments, tests are run in duplicate. In embodiments, tests of both sides of a paper towel are performed, in duplicate. Thus, in embodiments, four samples are subjected to lint deposition and collection as described herein, the samples comprising two samples wherein the inside of the paper towel (i.e. the side facing the roll when wound on a paper towel roll) is the test side 51 of the towel to be analyzed, and two samples wherein the outside (i.e. the side facing away from the roll when wound on a paper towel roll) of the paper towel is the test side 51 of the towel to be analyzed. The four samples may be cut prior to lint deposition of any of the samples. Alternatively, each sample may be cut immediately prior to lint deposition of that sample.
The lint quantitation method of this disclosure further comprises collecting the lint deposited on the surface, as indicated at step 40 of the flow diagram of
Following lint deposition, the surface onto which lint has been deposited is placed in a raised support stand 85 comprising base 87, vertical member 86, and support attachment surface 89 (see also
Support stand 85 is positioned such that, when supported thereby at angle a, the lowermost point or corner 67 of deposition surface 60 is positioned over collection funnel 80, which may have been prepared (i.e., cleaned and allowed to dry), as described hereinabove. Collection funnel 80 may, in embodiments, have an inlet diameter of about 7, 8, or 9 inches. In embodiments, lowermost corner 67 of supported deposition surface 60 is substantially centered above collection funnel 80. Collection funnel 80 can be supported over balance 84 via a ring stand 81 comprising funnel support 82. Collection vessel 83, rinsed as described hereinabove, can be placed on balance 84, and the weight of the empty collection vessel tared.
Using a water sprayer 95, deposited lint is rinsed from deposition surface 60 through funnel 80 to collection vessel 83. Any suitable water sprayer may be utilized. In embodiments, a manual spray water bottle activated via squeezing the sides thereof is utilized. In embodiments, the water sprayer comprises a pressurized water canister and spray gun. In embodiments, water sprayer 95 comprises a pressurized water canister 92 and GUNJET® spray gun 90 number AA23L, a swivel 11990-10, enabling 360 degree operation, and a tip or nozzle TP0001 available from Spraying Systems Co.®, Wheaton, Ill. Although referred to herein as a ‘water sprayer’, in embodiments, water sprayer 95 is configured to provide water via substantially a single stream or jet of water, rather than a conventional spray or misting pattern. Water sprayer 95 may be configured to provide substantially a single stream of water having a stream diameter in the range of from about 0.01 inch to about 0.10 inch, from about 0.01 inch to about 0.05 inch, from about 0.03 inch to about 0.10 inch, or less than or equal to about 0.10 inch, 0.05 inch, or 0.03 inch. The water stream may be ejected from water sprayer 95 at a pressure in the range of from about 0.5 psi to about 10 psi, from about 0.5 psi to about 5 psi, from about 1.5 psi to about 3 psi. The water stream may be ejected from water sprayer 95 at a flow rate in the range of from about 0.5 mL/s to about 5 mL/s, from about 0.5 mL/s to about 4 mL/s, or from about 0.5 mL/s to about 3 mL/s.
A water sprayer 95 suitable for use according to embodiments of this disclosure will now be described with reference to
Initial filling and subsequent refilling of the reservoir can introduce bubbles into line 91. Prior to use, ensure that there are no bubbles in line 91 connecting water canister 92 to spray gun 90, eliminating bubbles by activating the sprayer (i.e., depressing trigger handle 99) to bleed bubbles out of line 91.
As noted above, using water sprayer 95, deposited lint is rinsed from deposition surface 60 into through funnel 80 to collection vessel 83. Water may be sprayed with tip or nozzle 97 a desired distance away from deposition surface 60, for example, from about 1 to about 3, or about 1, 2, or 3 inches from deposition surface 60. Spraying may be directed inward (i.e., away from the edges or sides of deposition surface 60) at an angle from perpendicular with deposition surface 60, to minimize/avoid splashing and overspray. Beginning at bottom edges of deposition surface 60, a perimeter can be rinsed along both bottom-pointing sides/edges (SS2 and LS2 in the embodiment of
Collection funnel 80 can then be rinsed, primarily on the region where rinse water has dripped from deposition surface 60. Funnel rinsing may be performed until a desired total rinse water is present in collection vessel 83. The desired total rinse water may comprise 10, 20, or 30 grams more water than the desired volume of surface rinse water, such as noted hereinabove. In embodiments, the desired total rinse water may comprise from about 160 to about 230, from about 150 to about 300, or from about 50 to about 5000 grams of water. In embodiments, the desired total amount of rinse water comprises about 180, 200, 220, 230, 240, or 250 grams (±0.5 grams) of rinse water. In embodiments, the total rinse water volume is within 1.0 grams of the desired total rinse water volume.
Following rinsing of deposition surface 60 and funnel 80, collection vessel 83 may be covered, for example with plastic cling wrap, and secured, for example, with a rubber band. The vessel may be labeled with sequential numbers, for example, using painter's tape and a marker. The used towel sample 71 may be removed from support 70, and discarded. Surface cleaning, lint deposition, and lint collection may be repeated for the desired samples, e.g., duplicates of inside and outside surfaces of paper towel. In embodiments, for each product tested, four repetitions are tested in the order: outside, inside, outside, inside.
Testing may include one or more quality control (QC) sample (outside and inside of a known paper towel product), and one or more blank per tester. A blank consists of a complete sample testing as described hereinabove, without the lint deposition step. A blank may be run prior to and/or subsequent testing of a product (e.g., testing of the outside; inside; outside; inside thereof). The blank reading utilized can be an average of multiple blank runs, for example, an average of the FQA values (described further below) obtained for a blank run preformed prior to testing the sample, and a blank run performed subsequent thereto. In embodiments, the cleaning of deposition surface 60, such as described herein, provides for a blank having a total fiber area of lint, calculated as described below) in the range of from about 0.1 mm2 to about 1.0 mm2, from about 0.1 mm2 to about 0.8 mm2, or from about 0.2 mm2 to about 0.3 mm2. In embodiments, the total fiber area of lint determined for the blank is less than or equal to about 1.2 mm2, 1.0 mm2, 0.8 mm2, 0.7 mm2, 0.6 mm2, 0.5 mm2, 0.4 mm2, 0.3 mm2, or 0.2 mm2.
Samples can be retested if there is excessive tearing of the sample, if the total collected rinse water exceeds 1 gram more than the desired total rinse water volume (e.g., if the total collected rinse water is 201 grams, and the desired total rinse water is 200 grams), if the rinse water is depleted in pressurized water canister 92, or any other deviance from the procedure is encountered.
A lint quantitation method according to this disclosure further comprises determining the amount of collected lint, as indicated at step 50 of the flow diagram of
Before conducting FQA, the total volume of collected rinse water (e.g., 200 mL) is mixed, for example, by pouring back and forth a number of (e.g., 3) times to ensure adequate mixing of the sample. An aliquot (e.g., 50 mL) can then be subsampled from this beaker, transferred to an FQA test beaker, and diluted to a desired test sample volume (e.g., 600 mL (grams)) to provide an FQA test sample prior to FQA testing. Alternatively, the entirety of the collected rinse water is utilized and diluted to provide an FQA test sample, as long as the FQA is operable to count fibers up to the number of fibers therein (i.e., so long as the total number of fibers in the FQA test sample does not exceed the FQA counting capacity).
To reduce the overall run time involved in the lint analysis (in embodiments, up to 50%), the number of cycles utilized during FQA analysis testing can be reduced. For example, if utilizing 7-8 cycles results in less than 1% of the overall fiber remaining in the test beaker, while one cycle results in approximately 82% of the total fiber being counted, to save time and increase efficiency, the lint number can be reported as the first cycle lint count divided by 0.82. While not an exact number, this method can be used, in embodiments, to approximate the total lint from the aliquot while reducing the run time.
The fiber quality analyzer provides an average fiber length, average fiber width, and fiber count. As a large number or fiber count of very small fibers (e.g., microfibers) may not be perceptible visibly (for example, to a consumer), the amount of lint can be reported as a total fiber area (TFA), as differences in TFA may be meaningful visually and thus better correlate with (consumer) perception of how much lint is left behind after utilizing a product in a wiping application. Determining the amount of lint may thus further comprise calculating the amount of lint. For example, the total fiber area of the sample can be determined according to Equation (1):
Total Fiber Area (mm2)=[((Avg. Fiber Length (mm))×(Avg. Fiber Width (mm))×Fiber Count)−(TFA of Blank)] (1)
The total fiber area of the blank is determined as the average fiber length times the average fiber width times the fiber count for the blank sample, processed as described hereinabove.
For each sample, the fiber area may be reported as an average of the values obtained for the samples from that paper towel roll, and may include the standard deviation thereof, determined as known to those of skill in the art. For example, the average of the TFAs obtained from inside and outside, and/or replicate samples thereof may be provided. The minimum and maximum fiber areas may also be reported, as well as the number of replicates for each sample. TFAs may be reported in any desired units, for example mm2, and may be reported to the nearest tenth (e.g., the nearest 0.1 mm2). Reporting may further comprise stating any deviations from the standard procedure described herein, and any unusual features or characteristics of the sample.
The disclosure having been generally described, the following examples are given as particular embodiments of the disclosure and to demonstrate the practice and advantages thereof. It is understood that the examples are given by way of illustration and are not intended to limit the specification or the claims to follow in any manner.
A method according to this disclosure is utilized to determine the amount of lint shed from a paper towel during a wiping motion.
Paper towel samples 71 are preconditioned and conditioned according to Standard Test Method TAPPI TM-402. Specifically, a roll of paper towel is placed in an environment under a standard conditioning and testing atmosphere of 72° and 50% relative humidity, for a time of 2 hours.
Test samples are cut in the machine direction (MD) with a paper cutter, avoiding the perforation. As seen in
Cut sample using a paper cutter to avoid generation of excess lint. Do not tear sample at perforations. When cutting samples, keep testing surface (inside or outside) of towel facing up to avoid foreign lint from contaminating sample. Do not unnecessarily handle samples or lay samples on any surface that may contaminate them. Clean lab bench surface and paper cutter surface using glass cleaner in spray bottle and lint-free wipes (ACCUWIPES, SKU #29834). Clean cutting blade with compressed air prior to cutting each sample.
Set-up a water sprayer 95 comprising a pressurized water canister 92 and GUNJET® spray gun AA23L 90, swivel 11990-10, and tip TP0001 97 available from Spraying Systems Co® as shown in
Screw top 98 back on canister 92. Pressurize water sprayer 95 by opening the shutoff valve on the house compressed air, setting the mainline regulator to 10 psi and setting the spray can regulator 94 to 2.5 psi. Check the flowrate on water sprayer 95 by using a timer and (e.g., 50 mL) graduated cylinder, to ensure a flowrate of 20-22 mL per 10 sec. Check the water sprayer flowrate after adding water to reservoir, as reduced pressure, air in line 91, or a clog in spray nozzle 97 may reduce the flowrate.
Ensure that there are no air bubbles in line 91 connecting the pressurized water canister 92 to spray gun 90. Initial filling and subsequent refilling of the reservoir can introduce air bubbles in line 91. Eliminate any bubbles by activating sprayer via trigger handle 99 to bleed bubbles out of line 91.
Subsequent to testing, water sprayer 95 may be depressurized by turning off the airline ball valve, adjusting the mainline regulator 94 to 0 psi, and releasing canister pressure by pulling out relief valve by ring. Ensure that there is no pressure in water canister 92 before opening top 98.
Place 2 full sheets of extra paper towel on a balance having 1 gram resolution. Tare the balance. Check the amount of glass cleaner delivered by three full pumps of the spray nozzle. Spray 3 full sprays of glass cleaner onto paper towels and note weight. Three full sprays should equal 3.0 grams (±0.2 g). Check initial spray weight and when pump head on spray bottle is changed or a when a bottle/pump is replaced.
Before beginning testing for the day, practice spraying glass or deposition surface 60 with glass cleaner, and practice the ‘plowing’ motion with a modified SWIFFER® head support 70 having 1500 grams total weight and a 30 sq. inch test surface.
Place deposition surface 60 (e.g., black glass) in benchtop support stand with long dimension LD away from operator 65. A black glass deposition surface 60 may be an 11¼-in. X 17-in.×⅛-in. glass with custom mounting pegs and raised support stand 85, and benchtop support stand may be available from Research Dimensions, 1720 Oakridge Road, Neenah, Wis. 54956. Verify that black glass deposition surface 60 is marked along the long dimension so that the outside marks (Numbers 1 and 2 in
Rinse a lint free sponge 66 (McMaster-Carr part#7271T32) and squeegee 64 (14-in width, McMaster-Carr window squeegee part #7334T35) with tap water, then wipe the squeegee blades of squeegee 64 with the lint free sponge 66. Use a separate lint free sponge 66 and a stream of tap water to clean the inside of 500 mL beaker collection vessels 83. Rinse a funnel 80 (8-in. diameter) and 500 mL beakers with shower sprayer in the sink with tap water to thoroughly clean any fibers from the surfaces thereof, rinsing at least three times. Do not dry, but gently shake the water off and invert beakers on countertop.
Spray the entire surface of the black glass deposition surface 60 with glass cleaner (6 sprays) via liquid sprayer 63. Use the squeegee 64 to push the glass cleaner off the back (far short side SS1) of the black glass deposition surface 60, as illustrated in
As noted in ‘Sample Preparation’, cut each two-sheet sample 71 immediately before testing, in order to avoid contamination of the sample with foreign lint. Place a two-sheet sample 71 onto the center of the black glass deposition surface 60 with the machine direction (MD) of the towel parallel with the long dimension LD of the black glass deposition surface 60, and the surface to be tested 51 against the black glass deposition surface 60. Test both outside and inside surfaces for each sample 71, unless otherwise requested. Tests may be run in duplicate: outside and inside of towel for a total of four tests per sample.
Set the SWIFFER® head support 70 on the center of towel sample 71 with its short dimension parallel to the MD of towel sample 71. Wrap the edges of towel sample 71 around the SWIFFER® head support 70, securing it using the four inserts, as illustrated in
Set the wrapped support 75 comprising SWIFFER® head support 70 and towel sample 71 back onto the sprayed black glass deposition surface 60 centering the SWIFFER® head support between the numbers ‘7’ and ‘8’ markings. Grasp the wrapped SWIFFER® head support 70 by placing index fingers at the top corners and thumbs at the bottom corners thereof. When moving wrapped support 75, maintain rotation of the SWIFFER® head support 70 slightly towards the direction it is moving, referred to herein as ‘plowing’. When coming to a change in direction, roll the SWIFFER® head 70 to the opposite direction before changing direction. This rotation allows the loose lint to be deposited on black glass deposition surface 60.
Rub the wrapped support 75 comprising SWIFFER® head support 70 and towel sample 71 back and forth in the long dimension LD of the black glass deposition surface 60, keeping the long dimension of the wrapped support 75 perpendicular to the long dimension LD of black glass deposition surface 60. Begin by sliding the wrapped support 75 to the top (i.e., SS1) of the black glass deposition surface 60, complete a back and forth pass across the entire surface of black glass deposition surface 60, returning to the top (i.e., SS1). Do not apply any additional downward force to the weighted wrapped support 75. The force applied is just that to slide the wrapped support 75 across the black glass deposition surface 60. Perform sliding with a ‘plowing’ motion, in which the SWIFFER® head support 70 is tilted slightly forward, with the ‘leading’ edge making full contact with the black glass deposition surface 60, and the ‘trailing’ edge lifted ⅛-inch. After the initial passes, glide the SWIFFER® head support 70 until the leading edge reaches the number 1 position. Change directions and switch the direction of the ‘plow’, sliding to number 2 at the top (i.e., SS1) of the black glass deposition surface 60. Continue a back and forth process, moving sequentially number to number until reaching number 8. Then plow to the center MP of the glass (between ‘7’ and ‘8’). The lint deposition process (as described in this paragraph) may take 40-45 seconds to complete; this will depend upon the friction between the black glass deposition surface 60 and the particular paper towel being tested. Some towel samples 71 may grab and skip on black glass deposition surface 60, and speed may then be reduced to prevent ripping of the sample 71. All passes can be completed within 50 seconds.
After the final center position (i.e., the MP, between the numbers ‘7’ and ‘8’ markings) has been reached, lift the wrapped support 75 off black glass deposition surface 60 and set aside. Note any tears or unusual conditions. (Remove and dispose of the used towel sample 71 later.)
The lint collection setup 140, as shown in
Ring stand 81 next to balance 84 supports funnel 80 over balance 84. Place a rinsed beaker collection vessel 83 on balance 84 as shown in
Carefully top off beaker collection vessel 83, while rinsing funnel 80, (especially on the region where water has dripped from black glass deposition surface 60) until there are 200 grams (±0.5 g) of rinse water in beaker collection vessel 83. Do not exceed 201 grams. Cover beaker collection vessel 83, for example, with cling wrap, and secure, for example with a rubber band. Label beaker collection vessels 83, for example, with sequential numbers using painter's tape and a marker.
Remove used towel sample 71 from the SWIFFER® head support 70 and discard. Repeat cleaning, depositing lint, and collecting lint for all samples. Record, including sample number and sample description, may be kept in a laboratory notebook. For each product (e.g., paper towel roll) tested, four reps can be tested in the following order: outside; inside; outside; inside. Each day of testing can include one QC sample (outside: inside) and one blank per operator 65. A blank consists of a complete sample testing procedure without the glass cleaner and without the towel sample 71 and SWIFFER® head steps, i.e., without the lint deposition procedure described above.
When testing is completed, ensure that the main airline of water sprayer 95 is in the off position and that the regulator 94 thereof has been closed (zero gauge pressure). Relieve pressure from water sprayer 95 and airlines by pulling open the relief valve on the spray canister 92.
Have the contents of beaker collection vessels 83 analyzed (for example, in a Fiber Lab) for FQA Fiber Counting utilizing an OPTEST® Fiber Quality Analyzer, Model FQA-360 available from: OpTest Equipment Inc., 900 Tupper Street, Hawkesbury, OT, Canada K6A 353.
Samples may be retested if there is excessive tearing of sample 71 during lint deposition, if collected rinse water during lint collection exceeds 201 grams, if DI water is depleted in pressurized spray canister 92 during lint collection, or any other change from the test method is encountered. FQA can be done no later than one day after testing/lint collection.
From the FQA results, including average fiber length, L (mm), average fiber width, W (μm), and fiber count FC (number), determine the amount of paper towel lint as the Total Fiber Area, TFA (mm2), using Equation (1) hereinabove: TFA=([L×(W/1000)×FC]−Blank), wherein Blank (mm2) is calculated using the FQA data (i.e., L×W×FC) the same way as for a sample. For each sample, report the average, standard deviation, minimum and maximum test results to the nearest 0.1 mm2 and the number of replicates for each. Clearly state any deviations from the standard procedure, and note any unusual features or characteristics of each sample 71.
The particular embodiments disclosed above are illustrative only, as the present disclosure may be modified and practiced in different but equivalent manners apparent to those skilled in the art having the benefit of the teachings herein. Furthermore, no limitations are intended to the details of construction or design herein shown, other than as described in the claims below. It is therefore evident that the particular illustrative embodiments disclosed above may be altered or modified and all such variations are considered within the scope and spirit of the present disclosure. Alternative embodiments that result from combining, integrating, and/or omitting features of the embodiment(s) are also within the scope of the disclosure. While compositions and methods are described in broader terms of “having”, “comprising,” “containing,” or “including” various components or steps, the compositions and methods can also “consist essentially of” or “consist of” the various components and steps. Use of the term “optionally” with respect to any element of a claim means that the element is required, or alternatively, the element is not required, both alternatives being within the scope of the claim.
Numbers and ranges disclosed above may vary by some amount. Whenever a numerical range with a lower limit and an upper limit is disclosed, any number and any included range falling within the range are specifically disclosed. In particular, every range of values (of the form, “from about a to about b,” or, equivalently, “from approximately a to b,” or, equivalently, “from approximately a-b”) disclosed herein is to be understood to set forth every number and range encompassed within the broader range of values. Also, the terms in the claims have their plain, ordinary meaning unless otherwise explicitly and clearly defined by the patentee. Moreover, the indefinite articles “a” or “an”, as used in the claims, are defined herein to mean one or more than one of the element that it introduces. If there is any conflict in the usages of a word or term in this specification and one or more patent or other documents, the definitions that are consistent with this specification should be adopted.
The following are nonlimiting, specific embodiments in accordance with the present disclosure:
A: A method for quantitating the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed; depositing lint from the sample onto a surface, which has been cleaned, by moving the sample thereupon in a specific pattern comprising a plurality of directional changes; collecting the lint deposited on the surface; and determining the amount of collected lint.
B: A method for determining the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed; depositing lint from the sample onto a substantially lint-free surface by moving the sample thereupon in a specific pattern; collecting the lint deposited on the surface; measuring the number, the average length, and the average width of the fibers in the collected lint; and calculating the amount of collected lint as the total fiber area (mm2), by multiplying the average fiber length (mm) by the average fiber width (mm) and the fiber count and subtracting a blank therefrom, wherein the blank is calculated as the amount of lint collected from the substantially lint-free surface in the absence of the depositing step.
C: A method for quantitating the amount of lint shed from a paper towel, the method comprising: cleaning a rectangular deposition surface having a short dimension and a long dimension, wherein cleaning comprises spraying the entire surface with glass cleaner, using a substantially lint-free squeegee to push the glass cleaner off one of two short sides of the surface, and using a substantially lint-free sponge to wipe the edges of the surface substantially free of lint; preparing a sample of paper towel to be analyzed; depositing lint from the sample onto the cleaned surface by moving the sample thereupon in a specific pattern; collecting the lint deposited on the surface; and determining the amount of collected lint.
D: A method for quantitating the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed; depositing lint from the sample onto a substantially lint-free surface by moving the sample thereupon in a specific pattern; collecting the lint deposited on the surface, wherein collecting the lint deposited on the surface comprises, substantially immediately upon depositing lint from the sample onto the surface, washing the deposited lint from the surface into a tared, cleaned, empty vessel; and determining the amount of collected lint.
E: A method for quantitating the amount of lint shed from a paper towel, the method comprising: preparing a sample of paper towel to be analyzed, wherein preparing the sample comprises wrapping the sample around a solid support, to provide a wrapped support; depositing lint from the sample onto a surface, which has been cleaned, by moving the sample thereupon in a specific pattern comprising a plurality of directional changes; collecting the lint deposited on the surface; and determining the amount of collected lint, wherein the surface is substantially rectangular, having a long dimension and a short dimension, wherein the solid support is substantially rectangular, having a long dimension and a short dimension, and wherein wrapping the sample around the solid support further comprises placing the solid support on the sample on a side of the sample opposite a side of the sample to contact the surface during lint deposition and wrapping the sample around the solid support, with a machine direction of the sample parallel to the short dimension of the solid support.
Each of embodiments A, B, C, D, and E may have one or more of the following additional elements: Element 1: wherein the surface is glass. Element 2: wherein the surface is black glass. Element 3: wherein preparing the sample further comprises wrapping the sample around a solid support, to provide a wrapped support, and wherein depositing lint from the sample onto the surface further comprises placing the wrapped support on the surface and moving the sample using a plowing motion in which the wrapped support is tilted forward, whereby a leading edge of the wrapped support makes substantially full contact with the surface, and a trailing edge of the wrapped support is lifted a distance off the surface. Element 4: wherein the distance is about ⅛ inch. Element 5: wherein the wrapped support is tilted forward at an angle of from about 5 to about 10 degrees from horizontal. Element 6: wherein the surface is substantially rectangular, having a long dimension and a short dimension. Element 7: wherein the solid support is substantially rectangular, having a long dimension and a short dimension, and wherein wrapping the sample around the solid support further comprises placing the solid support on the sample on a side of the sample opposite a side of the sample to contact the surface during lint deposition and wrapping the sample around the solid support, with a machine direction of the sample parallel to the short dimension of the solid support. Element 8: further comprising securing the sample to the solid support. Element 9: wherein placing the wrapped support on the surface provides an area of sample that contacts the surface during moving that is in the range of from about 8 to about 55 square inches. Element 10: wherein moving the sample on the support in a specific pattern comprising a plurality of directional changes further comprises moving the wrapped support back and forth along the long dimension of the surface, with the short dimension of the solid support parallel to the long dimension of the surface during the moving. Element 11: wherein moving the wrapped support back and forth along the long dimension of the surface further comprises positioning the wrapped support at a first position along the long dimension of the surface, moving the wrapped support in a plowing motion past a midway point along the long dimension to a second position along the long dimension of the surface, changing direction and moving the wrapped support in a plowing motion past the midway point along the long dimension to a third position along the long dimension of the surface, wherein the third position is closer to the midway point than the first position, wherein parallel alignment of the short dimension of the wrapped support with the long dimension of the surface is maintained during the moving, wherein movement of the wrapped support in a direction parallel to the short dimension of the surface is minimized, and wherein positioning of the wrapped support at a position along the long dimension of the surface comprises aligning the leading edge thereof with that position. Element 12: further comprising changing direction and moving the wrapped support in a plowing motion past the midway point along the long dimension to a subsequent position along the long dimension of the surface, wherein the subsequent position is closer to the midway point than the previous position on that side of the midway point. Element 13: further comprising changing direction and moving the wrapped support in a plowing motion past the midway point along the long dimension to a fourth position along the long dimension of the surface, wherein the fourth position is closer to the midway point than the second position; changing direction and moving the wrapped support in a plowing motion past the midway point along the long dimension to a fifth position along the long dimension of the surface, wherein the fifth position is closer to the midway point than the third position; changing direction and moving the wrapped support in a plowing motion past the midway point along the long dimension to a sixth position along the long dimension of the surface, wherein the sixth position is closer to the midway point than the fourth position; changing direction and moving the wrapped support in a plowing motion past the midway point along the long dimension to a seventh position along the long dimension of the surface, wherein the seventh position is closer to the midway point than the fifth position; and changing direction and moving the wrapped support in a plowing motion past the midway point along the long dimension to an eighth position along the long dimension of the surface, wherein the eighth position is closer to the midway point than the sixth position. Element 14: wherein the first and third positions are from about 5-10 inches from the midway point along the long dimension of the surface, the third and fourth positions are 1-2 inches closer to the midway point along the long dimension than the first and second positions, respectively, the fifth and sixth positions are 1-2 inches closer to the midway point along the long dimension than the third and fourth positions, respectively, and the seventh and eighth positions are 0.5-1.5 inches closer to the midway point along the long dimension than the fifth and sixth positions, respectively. Element 15: wherein the first and third positions are about seven inches from the midway point along the long dimension of the surface, the third and fourth positions are about 1.5 inches closer to the midway point along the long dimension than the first and second positions, respectively, the fifth and sixth positions are about 1.5 inches closer to the midway point along the long dimension than the third and fourth positions, respectively, and the seventh and eighth positions are about 1 inch closer to the midway point along the long dimension than the fifth and sixth positions, respectively. Element 16: wherein placing the wrapped support on the surface and moving the sample using a plowing motion begins by spraying the surface with an amount of glass cleaner prior to placing the wrapped support on the sprayed surface. Element 17: wherein the amount of glass cleaner comprises about 3 grams. Element 18: wherein spraying the glass surface with glass cleaner comprises wetting substantially the entire width of the surface near a midway point along the long dimension thereof, with the extent of the concentrated spray falling within about the center two thirds of the surface in the long dimension. Element 19: wherein placing the wrapped support on the sprayed surface comprises placing the wrapped support on the sprayed surface with a midway point along a short dimension thereof aligned with about the midway point of the surface in the long dimension. Element 20: further comprising, subsequent to placing the wrapped support on the sprayed surface, moving the wrapped support in a plowing motion to a first of two short sides along the short dimension of the surface, changing direction and moving the wrapped support in a plowing direction to a second of the two short sides of the surface, changing direction and moving the wrapped support in a plowing direction to the first of the two short sides of the surface, and changing direction and moving the wrapped support in a plowing direction back to the second of the two short sides of the surface. Element 21: wherein preparing the sample further comprises cutting the sample from a roll of paper towels. Element 22: wherein cutting the sample further comprises cutting the sample in the machine direction, avoiding any perforations. Element 23: wherein cutting the sample further comprises cutting the sample from a full sheet roll of paper towels, about ⅛ inch to the left of perforations thereof, or cutting the sample from a select-a-size roll of paper towels such that perforations thereof are positioned a maximum possible distance from a center of the sample in the machine direction. Element 24: wherein cutting the sample is performed with the side of the sample to be analyzed facing up. Element 25: wherein cutting the sample is performed just prior to depositing lint from the sample on the surface. Element 26: wherein preparing the sample further comprises conditioning the sample. Element 27: wherein conditioning the sample further comprises allowing the sample, the paper towel from which the sample is taken, a roll of paper towels from which is taken the paper towel from which the sample is taken, or a combination thereof, to acclimate in an area having a temperature of 72 degrees and a relative humidity of 50%. Element 28: wherein depositing lint from the sample onto the surface terminates by moving the wrapped support in a plowing motion to a position in which a midway point along a short dimension of the support is aligned with a midway point along a long dimension of the surface, and raising the wrapped support off the surface. Element 29: wherein collecting the lint deposited on the surface further comprises, substantially immediately upon depositing lint from the sample onto the surface, washing the deposited lint from the surface into a tared, cleaned, empty vessel. Element 30: wherein washing the deposited lint from the surface further comprises placing the surface in a raised support stand above a funnel, wherein the funnel is centered above the tared, cleaned, empty vessel. Element 31: wherein placing the surface in a raised support stand further comprises tipping the long dimension of the support to an angle from vertical, with a corner of the surface being the lowest point of the supported surface and pointing into the funnel. Element 32: wherein washing further comprises spraying the surface on which the lint has been deposited with rinse water via a water sprayer. Element 33: wherein washing with the water sprayer further comprises rinsing a 1-3 inch perimeter along two bottommost edges of the surface, such that the sprayed rinse water flows into the vessel. Element 34: wherein washing with the water sprayer further comprises wetting the innermost portions of the surface from a top to a bottom thereof, until substantially the entirety of the surface is wet. Element 35: wherein washing with the water sprayer further comprises rinsing two uppermost edges of the surface inward, and rinsing in a back and forth motion across the entire width of the surface, spraying across and down until there is a desired surface wash volume of rinse water in the vessel. Element 36: wherein the desired surface wash volume comprises about 180 grams of water. Element 37: wherein the rinse water is substantially lint-free prior to being sprayed. Element 38: wherein the water comprises de-ionized water, distilled water, or a combination thereof. Element 39: further comprising rinsing the funnel with rinse water, until there is a desired total wash volume of rinse water in the vessel. Element 40: wherein the total wash volume of rinse water is about 200 (±0.5) grams. Element 41: wherein the water sprayer provides water at a pressure in the range of from about 0.5 psi to about 10 psi, a flow rate in the range of from about 0.5 mL/s to about 5 mL/s, in substantially a single jet of water, or a combination thereof. Element 42: wherein determining the amount of collected lint further comprises measuring the number, the average length, and the average width of the fibers in the collected lint. Element 43: wherein determining the amount of collected lint comprises calculating the total fiber area (mm2) of deposited lint from the sample, by multiplying the average fiber length (mm) by the average fiber width (mm) and the fiber count. Element 44: wherein determining the amount of collected lint further comprises measuring the number, the average length, and the average width of the fibers in an amount of collected lint in a blank, wherein the blank is obtained by collecting lint on the surface without the lint depositing step, calculating the total fiber area (mm2) of deposited lint from the blank, by multiplying the average fiber length (mm) by the average fiber width (mm) and the fiber count, and subtracting the total fiber area of the blank from the total fiber area of deposited lint from the sample to obtain the amount of collected lint. Element 45: further comprising cleaning the surface prior to depositing the lint thereupon. Element 46: wherein cleaning the surface further comprises spraying the entire surface with glass cleaner, using a substantially lint-free squeegee to push the glass cleaner off one of two short sides of the surface, and using a substantially lint-free sponge to wipe the edges of the surface substantially free of lint. Element 47: wherein the paper towel is a retail paper towel. Element 48: wherein the specific pattern comprises a plurality of directional changes. Element 49: wherein washing further comprises spraying the surface on which the lint has been deposited with water via a spray gun. Element 50: wherein the spray gun provides water at a pressure in the range of from about 0.5 psi to about 10 psi, a flow rate in the range of from about 0.5 mL/s to about 5 mL/s, in substantially a single jet of water, or a combination thereof. Element 51: wherein the method is manual or automated.
While preferred embodiments of the invention have been shown and described, modifications thereof can be made by one skilled in the art without departing from the teachings of this disclosure. The embodiments described herein are exemplary only, and are not intended to be limiting. Many variations and modifications of the invention disclosed herein are possible and are within the scope of the invention.
Numerous other modifications, equivalents, and alternatives, will become apparent to those skilled in the art once the above disclosure is fully appreciated. It is intended that the following claims be interpreted to embrace all such modifications, equivalents, and alternatives where applicable. Accordingly, the scope of protection is not limited by the description set out above but is only limited by the claims which follow, that scope including all equivalents of the subject matter of the claims. Each and every claim is incorporated into the specification as an embodiment of the present invention. Thus, the claims are a further description and are an addition to the detailed description of the present invention. The disclosures of all patents, patent applications, and publications cited herein are hereby incorporated by reference, to the extent that they provide exemplary, procedural or other details supplementary to those set forth herein.
The present application is a divisional of and claims priority under 35 U.S.C. § 119(e) to U.S. patent application Ser. No. 15/946,313 filed on Apr. 5, 2018, published as U.S. Patent Application Publication No. US 2019/0004025 A1, which is a non-provisional application claiming priority to U.S. Provisional Patent Application No. 62/527,677 filed on Jun. 30, 2017, and both entitled “Method for Quantitating Retail Paper Towel Lint,” the disclosure of each of which is hereby incorporated by reference in its entirety.
| Number | Date | Country | |
|---|---|---|---|
| 62527677 | Jun 2017 | US |
| Number | Date | Country | |
|---|---|---|---|
| Parent | 15946313 | Apr 2018 | US |
| Child | 16890261 | US |
