The invention relates to a method of, and an apparatus for, dispensing respectively predetermined quantities of pulverulent contents. The respective dispensing quantities are to be as constant as possible. The contents which are to be dispensed in each case are introduced into a metering chamber and transported from the latter to a container which is to be filled in each case. The contents present in the metering chamber are then emptied into such an available container.
Such dispensing devices may be designed as so-called metering tubes or as a metering roller. Whereas a metering tube, for filling purposes, is inserted from above into a stationary bed of bulk material, the metering chambers, which are distributed over the outer circumference of a metering roller, are positioned one after the other beneath the base opening of a contents-storing material store during the respective filling operation.
U.S. Pat. No. 5,826,633 discloses a metering roller with a plurality of metering chambers which are offset laterally above the base opening of a downwardly tapering, contents-accommodating material store. Terminating in the base opening of this material store is a gas line through which a gaseous medium is introduced into the material store from beneath, and the contents present in the material store can thus be fluidized. The metering chamber opening laterally into the region of the material store is bounded at the rear of its base by a filter which is permeable to gas but impermeable to contents. Depending on the rotary position of the metering roller, and thus on the position of the metering chambers of the latter, by way of a positive pressure or negative pressure being correspondingly applied through the filter, contents can be sucked into the metering chamber from the material store or the contents sucked into the metering chamber are blown out of the metering chamber into a container provided beneath the metering chamber. On account of the metering roller positioned above the base opening of the hopper-like material store, it is not possible for the contents present in the base region of the material store to be removed in their entirety from the material store; between the base opening of the material store and the metering chamber positioned thereabove, there is always an unusable residual quantity of contents remaining in the bottom hopper-like base region of the material store. Since it cannot be ensured whether, and when, this residual quantity is sucked back into the metering chambers, this residual quantity constitutes a quantity of contents which can only be used with difficulty, if at all. It is frequently also the case that it is undesirable to use this residual quantity since, in particular in the case of medicaments which are to be dispensed, timely dispensing is necessary if decomposition or some other negative change in the powdered medication as the latter resides in the material store over a relatively long period of time is to be avoided.
DE 197 13 057 discloses a powder-filling method and an apparatus for producing preferably sintered bodies. In this case, gas is introduced into a powder container through a multiplicity of holes in order that the individual powder particles in the powder container can move relative to one another. Thereafter, the powder container together with the fluidized powder present therein is positioned above a cavity which is to be filled, and the powder is displaced into the cavity, on account of its force of gravity, by suction or compressive force. The oscillating movement of the powder container is disadvantageous, this precluding a high dispensing performance. In particular, however, the arrangement of the very large number of gas-introduction tubes in the powder container proves to be disadvantageous in design terms.
The powder-filling apparatus which is known from WO 01/56726 also serves preferably for producing sintered bodies. Its material store has porous walls for the introduction of the gas which is to be used for fluidizing purposes. The porous walls prove to be particularly disadvantageous since, during the processing of contents which are to be handled very carefully, in particular pharmaceutical powders, the latter, if fine-grained enough, can settle in the porous walls. This results in it no longer being possible to guarantee hygienic dispensing.
DE 36 25 034 discloses an apparatus for automatically dispensing a free-flowing, pulverulent product into containers. This apparatus essentially comprises a vertically arranged, tubular measuring chamber which has a filter as the top boundary element. The quantity of powder which is to be dispensed is introduced in each case into the measuring chamber. The wall of the measuring chamber contains a mouth opening which is always open and is connected, by means of a connecting line, to a powder store arranged to the side of the measuring chamber. The measuring chamber comprises, in part, an elastic hose which, by virtue of being pinched, prevents powder from flowing prematurely out of the measuring tube into a container. Gas is introduced into the measuring chamber through the filter present at the top of the measuring chamber, this gas, with the hose pinched, being directed straight into the powder store and thus being capable of serving for fluidizing the contents present in the powder store. By virtue of a vacuum being applied to the filter, fluidized contents can be sucked upwards out of the powder store, through the connecting line, into the measuring chamber, as far as the region of the filter. In the case of this operation of filling the measuring chamber with powder, the measuring line is pinched beneath the connecting line. In order for the quantity of powder which is contained in the measuring chamber to be transferred to a container, the pinched hose cross section is released and a surge of compressed air into the measuring chamber is generated through the filter, this surge of compressed air forcing the quantity of powder downward out of the measuring chamber, in which case the powder present in the connecting component is sheared off laterally in relation to the quantity of powder driven out by the pressure surge. During the subsequent renewed fluidizing operation, the quantity of powder remaining in the connecting component is conveyed back into the powder store. The problem here is the unavoidable effect of the shearing operation precluding the respective quantities of powder from being separated off precisely from one another. This results in relatively large fluctuations in the quantities of powder which are to be dispensed in each case, which is undesirable, for example, in the case of dispensing medicaments. It is also possible, on account of the flexing movements of the hose wall brought about during the pinching operation and of the resulting pronounced material fatigue of the hose, for particles to be detached therefrom and then to be included in the dispensing operation; this is unacceptable in the operation of dispensing a medicament.
Taking this prior art as the departure point, the object of the invention is to specify a possible way of dispensing pulverulent contents which allows, as far as possible, constant quantities of pulverulent contents to be dispensed by as straightforward and compact a dispensing apparatus as possible, the intention being for this dispensing apparatus to be straightforward to handle during operation. Nevertheless, the dispensing operation using such a dispensing apparatus is to be capable of being carried out as cost-effectively as possible.
This invention is achieved, in respect of the method according to the invention, by the features of claim 1 and, in respect of an apparatus according to the invention, on which this method is to be implemented, by the features of claim 5. Expedient developments both of the method and of the apparatus form the subject matter of further claims which follow claims 1 and 5 in each case.
The invention is distinguished, in particular, in that the metering roller itself also functions as a kind of closing valve for the gas line serving for fluidizing the contents present in the material store, in that, in dependence on the respective rotary position of the metering roller, this gas line is or is not closed by the metering roller. The duration of the individual dispensing cycles thus does not depend on any actual valve arrangements for opening and closing such a gas line. Furthermore, the absence of such valve arrangements also reduces the cleaning outlay for the dispensing apparatus according to the invention.
Depending on the type of metering apparatus present, the metering roller can be rotated in the same direction of rotation, or in oscillating rotary movements, upon successive filling and emptying of its at least one metering chamber. More specific method-related details are also mentioned in conjunction with the embodiments for dispensing apparatuses according to the invention which are described more specifically hereinbelow.
A first type of dispensing apparatus according to the invention has a metering roller which contains at least one lateral line. This at least one lateral line is not line-connected to the metering chamber. Depending on the rotary position of the metering chamber, a line connection between the material store which stores the pulverulent contents and the gas line serving for fluidizing the contents stored in the material store may or may not be produced via this lateral line. It is thus possible, within a relatively long period of each dispensing cycle, for the material store to be subjected to the action of fluidizing gas. This allows very short operating cycles.
The metering roller may contain, as metering chamber, a filter piston apparatus as is described in more detail in German Utility Model Application 203 09 279.1, the priority of which is claimed. You are expressly referred to the full details of this filter piston apparatus in this respect.
Further configurations and advantages of the invention can be gathered from the features further cited in the claims and from the exemplary embodiments illustrated in the drawing.
The invention is explained and described in more detail hereinbelow with reference to the exemplary embodiments illustrated in the drawing, in which:
FIGS. 6 to 14 show illustrations, in detail form, of a third dispensing apparatus according to the invention in different rotary positions.
A first embodiment of a dispensing apparatus 10 according to the invention, which is illustrated in FIGS. 1 to 4, has a block-like housing 12. The housing 12 has a concave surface region 14. An essentially circular-cylindrical metering roller 16 fits closely, by way of its convex surface region 18, against the concave surface region 14 of the housing 12.
A first and a second through-passage channel 20, 22 project through the housing 12 and terminate in the concave surface region 14 of the housing 12.
A surface region of the metering roller 16 contains a recessed formation which constitutes a lateral line 24. In the so-called second rotary position of the metering roller 16, which. 1.i illustrated in
The first through-passage channel 20 widens into an accommodating bore 25 at its right-hand end in
The hose 26 terminates at the outlet opening 32 of a material store 34, which stores pulverulent contents 36. The hose 26 is attached to the material store 34, in the region of the outlet opening 32, in a manner which is favorable for the flow of the contents 36.
The material store 34 has a downwardly tapering hopper 38. The hopper wall is inclined such that the flow of the contents 36 out of the material store 34 produces a so-called mass flow; this means that, in all the regions of the material store 34, the contents 36 move to the same extent in the direction of the outlet opening 32, in order to avoid the contents 36 separating.
In the present example, the material store 34 is closed, for reasons of contamination, by a removable cover, which is not illustrated in the drawing. This cover allows the fluidizing gas to escape outward during the operation of fluidizing the contents 36, which is described in more detail hereinbelow. This fluidizing gas can be collected outside the material store 34.
The hose 26 which is present between the material store 34 and the first through-passage channel 20 does not have any bends or kinks which obstruct the flow of the contents 36 to any significant extent. In the present case, the hose 26 is a silicone hose.
The second through-passage channel 22 widens into an accommodating bore 40 at its right-hand end in
In the second rotary position, which is illustrated in
Such easily fluidizable powders with adherent fines are, for example, so-called powder inhalants in which micronized active substances are bound by interparticular forces. Such interactive mixtures are inhaled for therapeutic purposes by patients as pharmaceutical preparations in the form of an air/powder mixture (aerosol) using an inhaler. During this operation, the micronized active substance, which is usually of a magnitude between 5 μm (micrometers) and 0.5 μm, separates from the carrier substance, with the result that, in a therapeutically desirable manner, only the micronized active substance passes into the human lungs for therapeutic purposes.
In addition to pharmaceutical preparations, it is also possible for other powders, for example coffee powders, to be dispensed particularly carefully by the apparatus according to the invention if an inert gas is used as the gaseous medium 46, and thus as the fluidizing medium. In the case of using an inert gas, it is not possible for any oxygen to reach the coffee powder during the dispensing operation, with the result that the coffee flavor cannot be impaired by the fluidizing medium.
The fluidizing operation in the material store 34 also has the effect of considerably reducing the dynamic viscosity of the gas/solids mixture generated by the fluidizing operation. The fluidized contents 36 thus have considerably improved flow properties, as a result of which it is possible for the first time for them to be conveyed through narrow cross sections into the metering chamber of the metering roller 16.
The metering roller 16 contains a filter piston apparatus 50, which is seated within a circular-cylindrical bore 52 of the metering roller 16. The individual parts and functioning of such a filter piston apparatus 50 are described in more detail in German patent application 203 09 279.1, the priority of which is claimed. You are expressly referred to the entire contents of this disclosure.
A hollow-cylindrical piston 56 is seated in the circular-cylindrical bore 52, which is present for the purpose of forming a metering chamber 54. In the present example, this piston is produced from a piece of tube with, in the present example, a circular cross section. The tube wall of this piston 56 is beveled conically at its right-hand end in
In the transition between the conical widening 58 and the constantly thick casing region of the piston 56, a filter 64 is inserted in a transverse slot 62 provided there, which is open on one side. The transverse slot 62, which in the present case is oriented perpendicularly to the longitudinal axis 66 of the piston 56, cuts open half of the cross section of the piston 56. The constantly thick casing of the piston 56 is thus cut open over half its circumference by the transverse slot 62. In that cross-sectional region of the piston casing which is not cut open, the transverse slot 62 extends into an inner groove 68 formed in the piston casing. The piston casing is thinner in the region of this inner groove 68 than in the respectively adjoining casing region.
The piston 56 is sealed in relation to the circular-cylindrical bore 52 by means of an O-ring 70, which is seated in an encircling groove 72.
The rear end of the piston 56—which is at the top in
In the first rotary position (
From its first rotary position, the metering roller 16 is rotated in the clockwise direction 86—in the present case through a total of 90° (degrees)—via the intermediate position, which is illustrated in
During this rotation, the lateral line 24 contained in the metering roller 16 enters into line connection with the first and second through-passage channels 20, 22.
In the second rotary position (
By virtue of this positive pressure, the quantity of powder 36.1 which is present in the metering chamber 54 is emptied out of the metering chamber from above into a container 88 provided beneath the mouth opening 80.
Axial displacement of the piston 56 in a circular-cylindrical bore 52 allows the metering chamber 54 to be rendered larger or smaller. By virtue of the piston 56 being pulled right out of the circular-cylindrical bore 52, the filter 64 can be pulled transversely out of the piston 56 and, for example, exchanged. It is then also possible, at the same time, for the piston 56 to be straightforwardly cleaned.
Following ejection of the quantity of powder 36.1 in the second rotary position of the metering roller 16, which is illustrated in
In order for the gap between the metering roller 16 and the housing 12 to be configured to be as small as possible, and in order thus to avoid inappropriate and excess air flows, the housing 12 butts against the metering roller 16 under pressure via compression springs 92.
The dispensing apparatus 10.2 illustrated in
In the region of its metering chamber 54 and of its surrounding O-ring 70, the piston 56 is seated in a sleeve 100 rather than directly in a circular-cylindrical bore of the metering roller. This sleeve 100, for its part, is seated in an accommodating bore 102 of the metering roller 16.2. This accommodating bore 102 however, does not go right through the metering roller 16.2. At its end which is opposite to the metering chamber 54, the accommodating bore 102 adjoins the circular-cylindrical bore 52 of the metering roller 16.2. This circular-cylindrical bore 52 corresponds to that of the metering roller 16.
The sleeve 100 has an end surface 104 which is shaped convexly to correspond to the mouth opening 80. This end surface 104 serves as a doctor blade by means of which, when the metering roller 16.2 is rotated out of its first rotary position, which is comparable to
Positioned between the left-hand end of the sleeve 100 in
When the O-ring 106, the sliding plate 108 and the sleeve 100 are installed in the metering roller 16.2, the sleeve 100 projects slightly beyond the right-hand end of the metering roller in
Terminating in the metering roller 16.2 is an air channel 110 by way of which the sleeve 100 is mounted, as it were, in a manner assisted by air pressure. The air-pressure assistance means that pulverulent contents 36 which have penetrated into the annular gap 112, which encloses the sleeve 100 on the outside, and into the further annular gap 114, which is formed between the sleeve 100 and the piston 56, are blown out of the metering chamber 54 and thus out of the filter piston apparatus 50.2. Such powder cannot be blown out of the filter piston apparatus 50.2 in the opposite direction—to the left in relation to
The dispensing apparatus 10.3 illustrated in
Located approximately opposite one another on the outside of the metering roller 16.3 are two trough-like or groove-like recessed formations which constitute a first and a second lateral line 124, 124.1, as is basically the case with the lateral line 24 of the dispensing apparatus 10. Opening out into the left-hand lateral line 124 in
The two gas lines 126, 126.1 are not connected to one another. At one end, the two lateral lines 124, 124.1 are separated from one another by a tube region 130 of the metering chamber 54.3. The metering chamber 54.3 is located at the other end of the two lateral lines 124, 124.1. The tube region 132, which encloses the metering chamber 54.3, does not just form the sleeve-like body for the metering chamber 54.3; it also separates the two lateral lines 124, 124.1 from one another in this region of the metering chamber 54.3.
In the case of the rotary position which is illustrated in
It is thus possible, in the same way as with the dispensing apparatus illustrated in
Whereas, in the case of the apparatuses 10 and 10.2, the metering roller 16, 16.2 is rotated back and forth in an oscillating manner, the metering roller 16.3 of the apparatus 10.3 illustrated in
Following its emptying position, which is illustrated in
Through this second gas line 126.1, it would be possible to introduce into the region of the second lateral line 124.1 gas which would pass out of this lateral line at the bottom from the region of the metering chamber 54.3. If this were undesirable, it would also be possible to interrupt the gas throughflow into the second gas line 126.1 and thus into the region of the second lateral line 124.1.
With continued rotation of the metering roller 16.3, the latter passes into its rotary position which is illustrated in
With continued rotation of the metering roller 16.3 into the position which is illustrated in
With continued rotation of the metering roller 16.3 into its rotary position which is illustrated in
The pulverulent contents 36 which are present in the material store 34.3, as before, can be fluidized via the second gas line 126.1 and the now first lateral line 124.
In that rotary position of the metering roller 16.3 which is illustrated in
With continued rotation of the metering roller 16.3 into its rotary position which is illustrated in
In the following rotary position, which is illustrated in
With continued rotation of the metering roller 16.3 into its position which is illustrated in
The metering roller 16.3 is then rotated further again into its position which is illustrated in
The opening periphery 134 of the material store 34.3 (
It is clear from the above that the contents 36 which are present in the material store can be subjected to the action of gas from one or two gas lines 126, 126.1. In order to achieve uniform fluidization, it may be recommendable to provide a gas-volume-flow regulating device, by means of which the gas is introduced into the two gas lines 126, 126.1 such that always the same quantity of gas flows into the material store 34.3. A uniform quantity of gas results in a uniform fluidized bed of contents 36 in the material store 34.3, which, in turn, ensures identical pressure and flow conditions for the contents which are present in the material store 34.3. In this context, it is further recommended to combine the two gas lines 126, 126.1 in a common line, for example, outside the housing 12.3, in which case only a single volume-flow regulating means would have to be provided.
In the case of the abovedescribed fluidizing operation, it is possible to fluidize all the contents which are present in the material store 34.3. The fluidization takes place in parallel with other operating sequences. It is thus possible to ensure a high dispensing performance along with low fluctuation of the quantity dispensed.
Instead of one metering chamber, it is also possible to provide a plurality of metering chambers with, correspondingly, a plurality of lateral lines and gas lines.
In the present examples, the filter piston apparatuses each have circular cross-sectional shapes. Filter piston apparatuses could also have non-circular cross-sectional shapes. In this case, the circular bore 52 would have to be replaced by a channel with a cross-sectional shape which is adapted to the respective piston.
Number | Date | Country | Kind |
---|---|---|---|
203 09 279.1 | Jun 2003 | DE | national |
103 30 771.0 | Jul 2003 | DE | national |